CN107802032A - A kind of discontinuous temperature causes production method and the application of the fragrant filter stick of phase change gel load - Google Patents
A kind of discontinuous temperature causes production method and the application of the fragrant filter stick of phase change gel load Download PDFInfo
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- CN107802032A CN107802032A CN201711105526.6A CN201711105526A CN107802032A CN 107802032 A CN107802032 A CN 107802032A CN 201711105526 A CN201711105526 A CN 201711105526A CN 107802032 A CN107802032 A CN 107802032A
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- filter stick
- gel
- phase change
- fragrant
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/022—Applying additives to filter materials with liquid additives, e.g. application of plasticisers
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/04—Tobacco smoke filters characterised by their shape or structure
- A24D3/048—Tobacco smoke filters characterised by their shape or structure containing additives
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/08—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
- A24D3/10—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent of cellulose or cellulose derivatives
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The present invention relates to production method and the application that a kind of discontinuous temperature causes the fragrant filter stick of phase change gel load, the production method includes the production that temperature causes the preparation of phase change gel colloid and discontinuous temperature causes the fragrant filter stick of phase change gel load.It is big that the discontinuous temperature of the present invention causes phase change gel to carry the fragrant fragrant amount of filter stick load, perfuming amount is stable, aroma-keeping time is grown, fragrance matter volatilization is few, in cigarette smoking, the heat effect of flue gas heat makes solid gel be transformed into liquid, and the fragrance component loaded in gel slowly releases, fragrance release is uniform, and section taste is consistent before and after cigarette.Cigarette made of the discontinuous gel filter stick of the present invention, consumer will not directly contact gel in oral cavity in suction, sense of discomfort and psychological dislike mood when avoiding consumer's oral contact gel, and front and rear section flavor concentration and flavor-stable when aspirating, effectively increase cigarette smoking quality.
Description
Technical field
The present invention relates to a kind of production method of filter stick, and in particular to a kind of discontinuous temperature causes phase change gel to carry fragrant filter stick
Production method, further relate to its application, belong to technical field of tobacco processing.
Background technology
With the continuous progress and development of social science, the philosophy of life of people also occurs to change gradually.Consumer
Requirement to cigarette is also constantly lifted.It is low that thin slice, stem etc. are added with the propulsion of Tar, in cigarette tobacco leaf formulation
The increase of tar content component and the application of filter stick aeration technology, effectively reduce tar content and harmful substance in cigarette smoke
Content, but while good reducing tar and reducing harm effect is obtained, also reduce tobacco aroma and bring the satisfaction of consumer and enjoy
Felt.Cigarette, which mends fragrant traditional approach, to be realized by way of adding fragrance matter in tobacco leaf formulation, the flavor of addition
It is upright to connect the combustion process for participating in cigarette, the fragrance material of costliness had both been wasted, while because the product of burning generation is uncontrollable, meeting
Some unknown materials are produced, do not meet the requirement of reducing tar and reducing harm.By way of fragrance deficiency being supplemented the direct perfuming of filter tip, because
The fragrance matter added in filter tip does not participate in the high-temp combustion of cigarette directly, and safely controllable and qualitative, quantitative is convenient, can be fine
Targetedly addition fragrance matter, directly make up the deficiency of fragrance in cigarette, increase fragrance rich harmony cigarette perfume and
Flue gas.
Filter stick perfuming is mainly realized by several method at present, first, in plasticizer triacetic acid during filter stick formation
The good essence and flavoring agent of dissolubility is added in glyceride, this method is simple and convenient, but is that essence and flavoring agent will be with three the problem of exist
The compatibility of acetin is good, limits the application of most of soluble perfume spices, and essence and flavoring agent is stored in filter stick in addition
During it is readily volatilized scatter and disappear.Second, realizing that filter stick is mended fragrant by way of perfuming cored wire, perfuming cored wire filter stick is by add
Fragrant line is carrier, and the main material of cored wire is cotton thread or cellulose, and one or more immersion fragrant plant is added in filter stick
Perfuming line, to realize that flavouring mends fragrant purpose.The problem of perfuming cored wire filter stick is present be, with the extension of filter stick resting period,
The fragrance matter adsorbed on cored wire is volatile, and the resting period is short, and fragrance matter adsorbance is few, front and rear section fragrance during cigarette smoking
Discharge uneven.Another filter stick perfuming mode is to load fragrance matter by papery scented tea, then will during filter stick formation
The papery scented tea of load fragrance matter is added in filter stick, realizes the purpose that can reach filter stick perfuming, has novel appearance again
The advantages of, however, papery scented tea loads fragrance filter stick there is also fragrance matter adsorbance is few, fragrance matter is volatile, Er Qiehui
Extra band carrys out the problem of papery peculiar smell.Still an alternative is that cored wire and scented tea are combined, such as it is made by two cored wires
With the smiling face filter stick of scented tea composition, this method is also to have that fragrance matter adsorbance is few, and the fragrance matter of absorption is volatile,
And the shortcomings that easily entraining papery peculiar smell.
Also there is a kind of solidifying perfume (or spice) and release slow filter stick in prior art, however, because gel section is discontinuous, consumer is aspirating
Oral cavity will not directly contact gel during cigarette, the sense of discomfort in oral cavity and psychological when avoiding consumer's oral contact gel
, can effectively save gel use cost while disliking mood, and can meet to compensate fragrance again.
Therefore, it is badly in need of filter stick and the preparation that a kind of fragrance matter load capacity is big, fragrance release is uniform, protects fragrant time length at present
Method.
The content of the invention
The purpose of the present invention is directed to the deficiency of existing filter stick perfuming technology, there is provided a kind of discontinuous temperature causes phase change gel to carry
Fragrant filter stick and its production method, essence or spices are loaded with plural gel, plural gel is in a heated condition in liquid form
It is injected into vinegar fibre filter stick by way of discontinuous addition, is transformed into admittedly after condensation after gelling temp drops to normal temperature
State.In cigarette smoking by the heat effect of flue gas, the fragrance matter for making to load in gel evaporates, to realize that filter stick adds
Fragrant purpose.Concrete scheme is as follows：
A kind of discontinuous temperature causes the production method of the fragrant filter stick of phase change gel load, it is characterised in that：Comprise the following steps：
Step（1）：The preparation of Wen Zhixiang variable load perfume (or spice) gels
Prepare raw material by following mass percent：Carry perfumery 10-75%, water 15-25%, additive 1-30%, emulsifying agent 0.1-5% and
Colouring agent 0-15%；
The load perfumery prepared in proportion is poured into water, heating stirring 0.3-0.5h fills it under 45-70 DEG C of temperature conditionss
Divide fusing, be well mixed, the temperature cause phase transformation composite colloid that fusing point is 40-60 DEG C is obtained, by additive, emulsifying agent and colouring agent point
It is not added in the composite colloid melted, stirs, the Wen Zhixiang variable load perfume (or spice) gels prepared；
Step（2）：The preparation of Wen Zhixiang variable load perfume (or spice) gel filter sticks
During conventional vinegar fibre filter stick formation, by step（1）The Wen Zhixiang variable load perfume (or spice) gels of middle preparation inject in liquid form
Into vinegar fibre filter stick, form temperature and cause phase change gel cored wire, be applied for discontinuous of the gel in filter stick adds, described discontinuous
Formula is added in filter stick apply the first length after, be spaced a distance, then again continue to the second length, and so on, directly
To obtain it is discontinuous addition gel filter stick.
Further, the colouring agent of addition can be that lycopene, maize, safflower, Gardenia Yellow, cape jasmine be green, capsicum
The natural colorants such as red, pumpkin is yellow, sea-buckthorn is yellow, citrus is yellow, matrimony vine, balsam pear, dandelion, these are all in the market on sale
Product.
Further, the length of the filter stick of discontinuous addition gel is 120mm, and the first length is 50mm, and the second length is
50mm, spacing distance 10mm, cut off, obtain by 5mm spacers, 50mm among the 10mm spacing distances of both ends when filter stick produces
The filter that first length section, 10mm spacers, the overall length of 5 length section compositions of the length sections of 50mm second and 5mm spacers are 120mm
Rod.In discontinuous temperature causes phase change gel to carry fragrant filter stick production process, apply the length of gel segment length and spacer, can be with
Needs are designed according to cigarette brand and do orientation adjustment.
Further, the load perfumery is polyethylene glycol, hydroxymethyl cellulose, sodium carboxymethylcellulose, pectin, Guar
One or more in glue, carragheen, agar, chitosan, sodium alginate, modified starch and beta-schardinger dextrin.
Further, Studies of The Aromatic Substances is carried by polyethylene glycol, chitosan, sodium carboxymethylcellulose, modified starch, pectin, marine alga
Sour sodium and beta-schardinger dextrin composition, the mass ratio of said components are：2.5~28.5:0.5:1:0.2:0.1:0.4:0.5.
Further, the additive is included in natural essence, synthetic fragrance, natural plant extracts and humectant
One or more.Preferably functional additive of the invention have selected blue berry flavor, strawberry flavor, mint flavored, durian taste, cocktail
The essence of the fragrance such as taste, radix scrophulariae taste, pseudo-ginseng taste, sealwort taste, winter wheat taste, honey flavour, rose taste, tobacco flavor, Yunnan olive taste, these
Product is all product on sale in the market.
Further, the emulsifying agent is glycerine monofatty ester, sucrose ester, sorbitol ester, granulesten, laurate
One or more in monoglyceride and methyl glycol fatty acid ester.
Further, every filter stick includes 1-4 bar discontinuous temperature cause phase change gel cored wire, and described temperature causes phase change gel
The diameter of cored wire is 0.4-2.0mm.The position of every cored wire can be adjusted with the position that syringe needle is placed, and every filter stick is transversal
The section of face gel cored wire can be able to be circle, star, pentagon, heart, square by designing the alteration of form of pin hole
Deng.Fragrance per core branch linear load can change fragrance according to the difference of the fragrant gel essence of load of application, and cored wire color also may be used
To be changed according to the change for carrying fragrant gel colouring agent.
According to the present invention, described discontinuous temperature causes a diameter of 0.4-2.0mm of the fragrant filter stick cored wire of phase change gel load, core
Line can be by the big minor adjustment that applies the needle aperture of gel.If the diameter of gel cored wire is less than 0.4mm, gel is in the process of application
In easily block syringe needle, cause resin added unstable, influence manufacturing schedule；If the diameter of cored wire is more than 2.0mm, can cause to coagulate
Glue applied amount is too high, is unfavorable for transformation of the gel by solid-state to liquid, while can also influence the stabilization of filtering rod, also results in
Production cost is too high.Therefore, the diameter of the gel cored wire is suitable, preferably 0.7- in the range of 0.4-2.0mm
1.7mm, more preferably 0.9-1.5mm.
Further, the addition of Wen Zhixiang variable loads perfume (or spice) gel is 0.2-8.0mg/mm.
The discontinuous temperature that preparation method of the present invention obtains causes phase change gel to carry fragrant filter stick in cigarette is produced
Using.
Obtained discontinuous temperature causes phase change gel to carry fragrant filter stick when rolling cigarette, is not applying the 10mm filter sticks of gel
Centre cut-out, is mounted connected to nearly pipe tobacco end by one section that is applied with gel, using the one end for not applying gel as lip end, that is, obtains non-
Continuous warm-natured cause phase variable load perfume (or spice) gel cored wire filter stick.On the one hand consumer causes the load of phase change gel in cigarette smoking by temperature
Perfume effect obtains fragrance component and the improvement of overall organoleptic qualities, while turn avoid because gel directly contacts what lip end was brought
Oral cavity sense of discomfort and psychological resentment.In discontinuous Wen Zhixiang variable load perfume (or spice) gel cored wire filter stick production processes, apply
Gel segment length and the length for not applying gel section, needs can be designed according to cigarette brand and do orientation adjustment；Can also whole branch
Filter stick all applies gel, then will carry fragrant gel filter stick and vinegar fibre filter stick and is combined binary compound filter candle, carries fragrant gel filter
Rod section is placed in nearly pipe tobacco end.
Temperature causes the load Studies of The Aromatic Substances of phase transformation composite colloid good for absorption property, is at ambient temperature solid-state and load flavor
The not volatile material of matter, liquid can be transformed from the solidified state into after 45 DEG C of temperatures above are heated, its fragrance matter energy loaded
Slowly release.
Compared with prior art, beneficial effects of the present invention are as follows：
The present invention does not need the carrier of traditional cotton thread or papery scented tea as fragrance matter, and the plural gel generation of phase transformation is caused with temperature
For the fragrant line of tradition or scented tea, fragrance matter load capacity is big, and in cigarette smoking, temperature causes the gel of phase transformation to be transformed from the solidified state into liquid
State, fragrance component release uniformly, stably, protect fragrant time length, and front and rear section taste and style are consistent, the compatibility with cigarette brand
Property is good.
The present invention loads essence with plural gel or spices, plural gel are added in filter stick in liquid, taken out in cigarette
By the heating of flue gas during suction, the fragrance matter loaded in gel is evaporated.It is food grade materials using material, peace
Entirely, nontoxic, fragrance matter load capacity is big, and fragrance is not volatile, and fragrance matter release is uniform, resting period length, and gel is with non-
The mode of continous way is added, and the nearly lip section of cigarette filter rod is not added with gel, is avoided consumer and is visually seen the nearly lip end of filter stick
Psychological inadaptability sense added with gel.
The concentration of the fragrance of the present invention can be adjusted as needed, and the fragrance species of carrying can be one or more, fragrant
Tolerance is sufficient, and Type of aroma enriches, and can meet the needs of different crowd and taste.
Brief description of the drawings
Fig. 1 is the cigarette filter rod cross-sectional view of the present invention；
Fig. 2 is the end view of cigarette filter rod of the present invention；
Fig. 3 is the end view of the second embodiment of cigarette filter rod of the present invention；
Fig. 4 is the end view of the 3rd embodiment of cigarette filter rod of the present invention；
Fig. 5 is the end view of the fourth embodiment of cigarette filter rod of the present invention；
Fig. 6 is the end view of the 5th embodiment of cigarette filter rod of the present invention；
Wherein：1- filter sticks, 2- temperature cause phase change gel cored wire.
Embodiment
With reference to embodiment, the present invention is described in further detail, but embodiment is not to the technology of the present invention side
The restriction of case.Any one skilled in the art can be used for reference in the present invention in the technical scope of present disclosure
Hold, the link such as appropriate feed change, process conditions realizes corresponding other purposes, and its correlation changes all without departing from the present invention
Content, all similar replacements and change are it will become apparent to those skilled in the art that be considered as being included in
Within the scope of the present invention.
Preferably to be annotated to technical scheme, spy provides following specific embodiment, but the present invention is simultaneously
It is not restricted by the embodiments.
In the present invention, for illustrating that " percentage " or " % " of concentration is mass percent, " part " is mass parts.
Embodiment 1：The single discontinuous temperature of strawberry taste causes the preparation of the fragrant filter stick of phase change gel load
Step（1）, Wen Zhixiang variable load perfume (or spice) composite colloids preparation
The load Studies of The Aromatic Substances prepared in proportion is poured into water, carries Studies of The Aromatic Substances by polyethylene glycol, chitosan, carboxymethyl cellulose
7 kinds of component compositions such as sodium, starch, pectin, sodium alginate and beta-schardinger dextrin, each component ratio are：16:0.5:1:0.2:0.1:
0.4:0.5.The weight ratio for carrying perfumery and water is 4:1, heating stirring 0.5h makes it fully melt at 55 DEG C of temperature, and mixing is equal
It is even, obtain the temperature that fusing point is 45 DEG C and cause phase transformation composite colloid, then strawberry essence, methyl glycol fatty acid ester, lycopene are added
Into the composite colloid prepared, stir, the strawberry essence of addition, methyl glycol fatty acid ester, the weight point of lycopene
15%, 1% and the 1.5% of composite colloid weight is not accounted for, obtains carrying fragrant plural gel finished product.
Step（2）, Wen Zhixiang variable load perfume (or spice) gel filter sticks preparation
During conventional vinegar fibre filter stick formation, by step（1）The Wen Zhixiang variable load perfume (or spice) gels of middle preparation are poured into gel addition
In equipment charging basket, fragrant gel will be carried by the pulsed screw pump of gel addition equipment loading and be injected into the fine filter of vinegar in liquid form
In rod, gel is applied for discontinuous addition in filter stick, i.e., after applying 50mm in filter stick, in subsequent 10mm length
Stop applying gel, then continue to 50mm again, stop applying again in subsequent 10mm filter rod segments, and so on, be made
Filter lengths are that the gel of 120mm discontinuous application gel carries fragrant filter stick, as shown in Figure 1.
The gel of injection is single gel cored wire, and a diameter of 1.2mm of cored wire, the cross section character of cored wire is circle, such as
Shown in Fig. 2, cored wire position is placed in the middle, and the addition for applying gel section gel is 1.5mg/mm.
Embodiment 2：Sweet orange taste discontinuous temperature causes the preparation of the fragrant filter stick of phase change gel load
The sweet orange taste discontinuous temperature of the present embodiment causes the preparation of the fragrant filter stick of phase change gel load, as follows：
Step（1）In, carry Studies of The Aromatic Substances by polyethylene glycol, chitosan, sodium carboxymethylcellulose, starch, pectin, sodium alginate and β-
7 kinds of component compositions such as cyclodextrin, each component ratio is 16:0.6:1:0.1:0.2:0.4:0.4, the weight ratio for carrying perfumery and water is
3:1, heating stirring 0.5h makes it fully melt under temperature 60 C, is well mixed, and obtains the temperature that fusing point is 50 DEG C and causes phase transformation to answer
Rubber alloy body, then orange flavor, methyl glycol fatty acid ester, curcumin are added in the composite colloid prepared, stir, add
The orange flavor that enters, methyl glycol fatty acid ester, the weight of curcumin account for 13%, 1.3% and the 1.6% of composite colloid weight respectively, obtain
To the fragrant plural gel finished product of load.
Step（2）In, gel in filter stick be applied for discontinuous addition, be in filter stick apply 36mm after, with
Stop applying gel in 12mm length afterwards, then continue to 36mm again, stop applying again in subsequent 12mm filter rod segments,
And so on, the gel that the discontinuous application gel that filter lengths are 144mm is made carries fragrant filter stick.The cross section character of cored wire is
Star, as shown in figure 3, cored wire position is placed in the middle, the addition for applying gel section gel is 1.6mg/mm.Remaining and the phase of embodiment 1
Together.
Embodiment 3：Coffee taste discontinuous temperature causes the preparation of the fragrant filter stick of phase change gel load
The coffee taste discontinuous temperature of the present embodiment causes the preparation of the fragrant filter stick of phase change gel load, as follows：
Step（1）In, carry Studies of The Aromatic Substances by polyethylene glycol, chitosan, sodium carboxymethylcellulose, starch, pectin, sodium alginate and β-
Cyclodextrin forms, and each component ratio is：16:0.4:1.1:0.05:0.2:0.45:0.5, heating stirring 1h makes under temperature 60 C
It fully melts, and is well mixed, and obtains the temperature that fusing point is 55 DEG C and causes phase transformation composite colloid, then by coffee aroma, propylene glycol fatty
Acid esters, cacao color are added in the composite colloid prepared, are stirred, the coffee aroma of addition, methyl glycol fatty acid ester,
The weight of cacao color accounts for 10%, 1.5% and the 1% of composite colloid weight respectively, obtains carrying fragrant plural gel finished product.
Step（2）In, gel in filter stick be applied for discontinuous addition, be in filter stick apply 50mm after, with
Stop applying gel in 10mm length afterwards, then continue to 10mm again, stop applying again in subsequent 10mm filter rod segments,
And so on, the gel that the discontinuous application gel that filter lengths are 120mm is made carries fragrant filter stick.The cross section character of cored wire is
Heart, as shown in figure 4, cored wire position is placed in the middle, the addition for applying gel section gel is 1.5mg/mm.Remaining and the phase of embodiment 1
Together.
Embodiment 4：Durian taste discontinuous temperature causes the preparation of the fragrant filter stick of phase change gel load
The durian taste discontinuous temperature of the present embodiment causes the preparation of the fragrant filter stick of phase change gel load, as follows：
Step（1）In, carry Studies of The Aromatic Substances by polyethylene glycol, chitosan, sodium carboxymethylcellulose, starch, pectin, sodium alginate and β-
7 kinds of components such as cyclodextrin, each component ratio are 16:0.4:1:0.1:0.2:0.35:0.4, the weight ratio for carrying perfumery and water is 4:
1, heating stirring 1h makes it fully melt at 65 DEG C of temperature, is well mixed, and obtains the temperature that fusing point is 55 DEG C and causes phase transformation compound adhesive
Body, then durian essence, methyl glycol fatty acid ester, lutein are added in the composite colloid prepared, stir, addition
Durian essence, methyl glycol fatty acid ester, the weight of lutein account for 5%, 1.5% and the 0.5% of composite colloid weight respectively, are carried
Fragrant plural gel finished product.
Step（2）In, gel in filter stick be applied for discontinuous addition, be in filter stick apply 36mm after, with
Stop applying gel in 12mm length afterwards, then continue to 36mm again, stop applying again in subsequent 12mm filter rod segments,
And so on, the gel that the discontinuous application gel that filter lengths are 144mm is made carries fragrant filter stick.The cross section character of cored wire is
Hexagon, as shown in figure 5, cored wire position is placed in the middle, the addition for applying gel section gel is 1.25mg/mm.Remaining and embodiment 1
It is identical.
Embodiment 5：Olive taste discontinuous more temperature in Yunnan cause the preparation of the fragrant filter stick of phase change gel load
The Yunnan olive taste discontinuous temperature of the present embodiment causes the preparation of the fragrant filter stick of phase change gel load, as follows：
Step（1）In, carry Studies of The Aromatic Substances by polyethylene glycol, chitosan, sodium carboxymethylcellulose, starch, pectin, sodium alginate and β-
7 kinds of component compositions such as cyclodextrin, each component ratio is 16:0.4:1:0.05:0.1:0.55:0.5, carry the weight ratio of perfumery and water
For 4:1, heating stirring 1h makes it fully melt at 58 DEG C of temperature, is well mixed, and obtains the temperature that fusing point is 48 DEG C and causes phase transformation to answer
Rubber alloy body, then Yunnan olive essence, methyl glycol fatty acid ester, chlorophyll copper sodium are added in the composite colloid prepared, stir
Uniformly, the Yunnan olive essence of addition, methyl glycol fatty acid ester, the weight of chlorophyll copper sodium account for respectively composite colloid weight 10%,
1.5% and 1%, obtain carrying fragrant plural gel finished product.
Step（2）In, gel in filter stick be applied for discontinuous addition, be in filter stick apply 50mm after, with
Stop applying gel in 10mm length afterwards, then continue to 10mm again, stop applying again in subsequent 10mm filter rod segments,
And so on, the gel that the discontinuous application gel that filter lengths are 120mm is made carries fragrant filter stick.The cross section character of cored wire is
3 stars, as shown in fig. 6, the applied amount of every gel cored wire is 0.6mg/mm, the total addition level of 3 gel cored wires is
1.5mg/mm.Remaining is same as Example 1.
Embodiment 6：The measure of aroma component reserved
Producing strawberry taste discontinuous temperature according to embodiment 1 causes phase change gel to carry fragrant filter stick, and measure the present embodiment produces solidifying
Glue carries the residual quantity for the aroma component that fragrant filter stick compares with traditional single rod.Its measurement result is as shown in table 1 below：
The measurement result of the aroma component reserved of table 1
Wherein, all detection samples are the filter stick prepared, and the detection method of aroma component is laboratory method, specific point
Analysis method is：After causing fragrant composition extract addition internal standard, carried out using gas/matter combined instrument Agilent GC 6890N/MS 5975
Analysis, is as a result calculated using internal standard method（It is Internal standard correction methods peak area relative amount to cause fragrant component content, is not considering instrument signal
In the case of response difference, i.e., when relative correction factor is 1, the unit of numerical value is μ g/g）.Chromatographic mass spectrometry condition is：Hair
Capillary column：HP-5MS（30m×0.25mm×0.25μm）, injector temperature：260 DEG C, carrier gas：He, flow velocity：1ml/min, stove
Temperature：50℃（Keep 1min）—8℃/min—160℃（Keep 2min） —8℃/min--280℃（Keep 15min）, GC-MS
Interface temperature：280 DEG C, ion gun：EI sources, electron energy：70eV, scanning range：35-455amu.
After the closed storage four weeks of filter stick sample it can be seen from the testing result of table 1, the discontinuous of the present embodiment production
Temperature causes the reserved of the aroma component of the fragrant filter stick of phase change gel load to be compareed apparently higher than traditional single rod, and the cause of gel cored wire filter stick is fragrant
Composition reserved is 3.7 times of traditional filter stick；Compared with the sample detected immediately after adding essence gel, climatic chamber is closed
After depositing four weeks, the aroma component content of gel cored wire filter stick reduces 9.77%, and simulates and perfume is caused in the filter stick sample of cored wire injection
The content of composition then significantly reduces 73.68%, and this directly represent discontinuous temperature made of plural gel and causes phase change gel filter
Rod, which has, significantly to be carried fragrant effect and permanent holds fragrant ability.
Embodiment 7：The measure of filter stick safety indexes
Producing strawberry taste discontinuous temperature according to embodiment 1 causes phase change gel to carry fragrant filter stick, determines filter stick safety indexes.
The measurement result of the filter stick safety indexes of table 2
Detect foundation：Lead, arsenic use YC/T 294《Arsenic, lead, cadmium, chromium, nickel-silicon nitride sampling Graphite Furnace Atomic in flavouring essence for tobacco and feed liquid
Absorption spectrometry》Method detected；Total plate count uses GB 4789.2-2010《National food safety standard food is micro-
Biological test total plate count determines》Method be measured, testing result is as shown in table 2.From the safety indexes of filter stick
The security that testing result can be seen that the fragrant filter stick of gel load meets requirement.
Embodiment 8：The aesthetic quality comparative evaluation of cigarette sample
The filter stick of cigarette finished product is taken out with tip tweezers, the simulation cored wire prepared respectively with embodiment 6 and embodiment 1 is injected
Perfuming filter stick and gel carry fragrant filter stick and filled in cigarette, and unnecessary filter stick is cut off with blade, roll into simulation cored wire injection respectively
Perfuming filter stick and gel carry fragrant filter stick cigarette sample.
The storage and sensory evaluation of sample：
The simulation cored wire prepared is injected into cigarette sample and gel carry fragrant filter stick cigarette sample and be placed on 20 DEG C of temperature, relatively wet
In the climatic chamber of degree 60%, deposit 4 weeks, carrying out aesthetic quality's contrast at interval of sampling in one week smokes panel test.Group of smokeing panel test is by 7 volumes
Cigarette aesthetic quality smoke panel test expert composition, according to GB 5606.4-2005《Cigarette sense organ technical requirements》Method carry out marking and comment
Valency, and evaluation opinion is provided, smoking result is summarized in table 3.
Aesthetic quality's comparative evaluation's result of the cigarette sample of table 3
It can be seen from the smoking result of the cigarette sample of table 3 with traditional direct method that fragrance matter is added into filter stick
Compare, discontinuous temperature of the invention cause phase change gel carry time that fragrance level is denseer, fragrance matter retains of fragrant filter stick compared with
Long, fragrance release is uniform, and section is protected substantially before and after the fragrance level and style and features of cigarette sample made of filter stick sample of the present invention
Hold consistent.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
God any modification, equivalent substitution and improvements made etc., should be included in the scope of the protection with principle.
Claims (10)
1. a kind of discontinuous temperature causes the production method of the fragrant filter stick of phase change gel load, it is characterised in that：Comprise the following steps：
Step（1）：The preparation of Wen Zhixiang variable load perfume (or spice) gels
Prepare raw material by following mass percent：Carry perfumery 10-75%, water 15-25%, additive 1-30%, emulsifying agent 0.1-5% and
Colouring agent 0-15%；
The load perfumery prepared in proportion is poured into water, heating stirring 0.3-0.5h fills it under 45-70 DEG C of temperature conditionss
Divide fusing, be well mixed, the temperature cause phase transformation composite colloid that fusing point is 40-60 DEG C is obtained, by additive, emulsifying agent and colouring agent point
It is not added in the composite colloid melted, stirs, the Wen Zhixiang variable load perfume (or spice) gels prepared；
Step（2）：The preparation of Wen Zhixiang variable load perfume (or spice) gel filter sticks
During conventional vinegar fibre filter stick formation, by step（1）The Wen Zhixiang variable load perfume (or spice) gels of middle preparation inject in liquid form
Into vinegar fibre filter stick, form temperature and cause phase change gel cored wire, be applied for discontinuous of the gel in filter stick adds, described discontinuous
Formula is added in filter stick apply the first length after, be spaced a distance, then again continue to the second length, and so on, directly
To obtain it is discontinuous addition gel filter stick.
2. discontinuous temperature according to claim 1 causes the production method of the fragrant filter stick of phase change gel load, it is characterised in that：It is non-
The length of the filter stick of continuous addition gel is 120mm, and the first length is 50mm, and the second length is 50mm, spacing distance 10mm,
When filter stick produces, cut off, obtained by 5mm spacers, the length sections of 50mm first, 10mm intervals from both ends 10mm spacing distances centre
The filter stick that section, the overall length of 5 length section compositions of the length sections of 50mm second and 5mm spacers are 120mm.
3. discontinuous temperature according to claim 1 causes the production method of the fragrant filter stick of phase change gel load, it is characterised in that：Institute
Load perfumery is stated for polyethylene glycol, hydroxymethyl cellulose, sodium carboxymethylcellulose, pectin, guar gum, carragheen, agar, shell to gather
One or more in sugar, sodium alginate, modified starch and beta-schardinger dextrin.
4. discontinuous temperature according to claim 3 causes the production method of the fragrant filter stick of phase change gel load, it is characterised in that：Carry
Studies of The Aromatic Substances is made up of polyethylene glycol, chitosan, sodium carboxymethylcellulose, modified starch, pectin, sodium alginate and beta-schardinger dextrin,
The mass ratio of said components is：2.5~28.5:0.5:1:0.2:0.1:0.4:0.5.
5. discontinuous temperature according to claim 1 causes the production method of the fragrant filter stick of phase change gel load, it is characterised in that：Institute
Stating additive includes the one or more in natural essence, synthetic fragrance, natural plant extracts and humectant.
6. discontinuous temperature according to claim 1 causes the production method of the fragrant filter stick of phase change gel load, it is characterised in that：Institute
It is glycerine monofatty ester, sucrose ester, sorbitol ester, granulesten, lauric monoglyceride and propane diols fat to state emulsifying agent
One or more in fat acid esters.
7. discontinuous temperature according to claim 1 causes the production method of the fragrant filter stick of phase change gel load, it is characterised in that：Often
Branch filter stick includes 1-4 bar discontinuous temperature and causes phase change gel cored wire, and it is 0.4- that described temperature, which causes the diameter of phase change gel cored wire,
2.0mm, the position that the position of every cored wire is placed with syringe needle are adjusted, and the section of every filter stick cross section gel cored wire passes through
Design the alteration of form of pin hole.
8. discontinuous temperature according to claim 7 causes the production method of the fragrant filter stick of phase change gel load, it is characterised in that：Temperature
The addition for causing phase variable load perfume (or spice) gel is 0.5-8.0mg/mm.
9. discontinuous temperature according to claim 1 causes the production method of the fragrant filter stick of phase change gel load, it is characterised in that：Institute
State that colouring agent is green lycopene, maize, safflower, Gardenia Yellow, cape jasmine, capsanthin, pumpkin is yellow, sea-buckthorn is yellow, citrus is yellow, Chinese holly
Qi, balsam pear or dandelion.
10. the discontinuous temperature that the preparation method according to claim 1-9 any claims obtains causes phase change gel to carry
Application of the fragrant filter stick in cigarette is produced.
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Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2723554A1 (en) * | 1977-05-25 | 1978-11-30 | Wolfgang Dipl Phys Seeger | Cigarette with reduced harmful effects - has tube down centre divided into compartments by spheres or discs, with tube possibly corrugated |
| US5622190A (en) * | 1990-08-24 | 1997-04-22 | Philip Morris Incorporated | Concentric smoking filter having cellulose acetate tow periphery and carbon-particle-loaded web filter core |
| CN101083916A (en) * | 2004-12-22 | 2007-12-05 | 菲利普莫里斯生产公司 | Compound filter rod making apparatus and process |
| CN103271442A (en) * | 2013-06-07 | 2013-09-04 | 安徽中烟工业有限责任公司 | Linear polyethylene glycol fragrance slow-release cigarette filter rod and production method thereof |
| CN105595417A (en) * | 2016-01-29 | 2016-05-25 | 云南芯韵科技开发有限公司 | Linear composite gel fragrance controlled-release filter stick and preparation method and application thereof |
| CN105996121A (en) * | 2016-06-28 | 2016-10-12 | 云南瑞升烟草技术（集团）有限公司 | Filter stick additive capable of releasing functional substance through phase change and preparation method and application thereof |
| CN105876852B (en) * | 2016-06-13 | 2017-04-12 | 四川三联卷烟材料有限公司 | Production method of thermal-induced fragrance-holding filter rod |
| CN106723341A (en) * | 2017-03-16 | 2017-05-31 | 云南巴菰生物科技有限公司 | Fragrance slow-release material composition and sustained release spices colloid and application thereof |
| CN107173848A (en) * | 2017-06-30 | 2017-09-19 | 云南恩典科技产业发展有限公司 | A kind of temperature becomes sustained release gel complex material and its application in cigarette filter rod |
-
2017
- 2017-11-10 CN CN201711105526.6A patent/CN107802032B/en active Active
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2723554A1 (en) * | 1977-05-25 | 1978-11-30 | Wolfgang Dipl Phys Seeger | Cigarette with reduced harmful effects - has tube down centre divided into compartments by spheres or discs, with tube possibly corrugated |
| US5622190A (en) * | 1990-08-24 | 1997-04-22 | Philip Morris Incorporated | Concentric smoking filter having cellulose acetate tow periphery and carbon-particle-loaded web filter core |
| CN101083916A (en) * | 2004-12-22 | 2007-12-05 | 菲利普莫里斯生产公司 | Compound filter rod making apparatus and process |
| CN103271442A (en) * | 2013-06-07 | 2013-09-04 | 安徽中烟工业有限责任公司 | Linear polyethylene glycol fragrance slow-release cigarette filter rod and production method thereof |
| CN105595417A (en) * | 2016-01-29 | 2016-05-25 | 云南芯韵科技开发有限公司 | Linear composite gel fragrance controlled-release filter stick and preparation method and application thereof |
| CN105876852B (en) * | 2016-06-13 | 2017-04-12 | 四川三联卷烟材料有限公司 | Production method of thermal-induced fragrance-holding filter rod |
| CN105996121A (en) * | 2016-06-28 | 2016-10-12 | 云南瑞升烟草技术（集团）有限公司 | Filter stick additive capable of releasing functional substance through phase change and preparation method and application thereof |
| CN106723341A (en) * | 2017-03-16 | 2017-05-31 | 云南巴菰生物科技有限公司 | Fragrance slow-release material composition and sustained release spices colloid and application thereof |
| CN107173848A (en) * | 2017-06-30 | 2017-09-19 | 云南恩典科技产业发展有限公司 | A kind of temperature becomes sustained release gel complex material and its application in cigarette filter rod |
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