CN111759001A - Cigarette flavoring slow-release gel particles and preparation method thereof - Google Patents
Cigarette flavoring slow-release gel particles and preparation method thereof Download PDFInfo
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- CN111759001A CN111759001A CN202010665552.XA CN202010665552A CN111759001A CN 111759001 A CN111759001 A CN 111759001A CN 202010665552 A CN202010665552 A CN 202010665552A CN 111759001 A CN111759001 A CN 111759001A
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- cigarette
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- gel
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0225—Applying additives to filter materials with solid additives, e.g. incorporation of a granular product
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0275—Manufacture of tobacco smoke filters for filters with special features
- A24D3/0287—Manufacture of tobacco smoke filters for filters with special features for composite filters
Abstract
The invention discloses cigarette perfuming slow-release gel particles and a preparation method thereof. The particle is prepared by uniformly mixing, melting, drying, crushing and screening 5-30 parts of polyethylene glycol-1000, 5-40 parts of polyethylene glycol-4000, 10-40 parts of lauric acid, 5-40 parts of octenyl succinate starch, 10-50 parts of cassava starch, 1-10 parts of humectant, 5-20 parts of adhesive and tobacco essence accounting for 10-30% of the total weight of the raw materials. The invention combines the excellent slow release performance of the gel and the high stability of the particles, and has the advantages of excellent fragrance adding effect, lasting fragrance storage, strong fragrance releasing capability and high-efficiency and uniform fragrance release; and the problem that the existing gel perfuming material is easy to produce gel powder falling after being dried can be improved to a certain extent, and the gel perfuming material is safe and environment-friendly. The preparation method is simple in preparation process, easy in quality control, low in production cost, convenient for realizing large-scale production and good in application prospect.
Description
Technical Field
The invention belongs to the technical field of cigarette flavoring, and particularly relates to a slow-release gel particle for flavoring a cigarette filter stick; meanwhile, the invention also relates to a preparation method of the sustained-release gel particles.
Background
In order to improve the smoking quality of cigarettes, make up for the deficiency of the original fragrance of tobacco and achieve the aims of increasing fragrance and keeping moisture, the cigarettes are usually required to be flavored. At present, cigarette flavoring mainly adopts two modes: tobacco shred perfuming and filter stick perfuming. The tobacco shred flavoring is to add a flavoring substance into a tobacco leaf rolling formula to directly participate in cigarette combustion, which easily causes the waste of expensive essence substances; meanwhile, the added aroma substances can generate uncontrollable products due to high temperature during smoking of the cigarettes, so that the sensory quality of the cigarettes is influenced. And in the mode of flavoring the filter stick, because the flavor substances added in the filter tip do not directly participate in the cigarette combustion, the cigarette filter stick is safe, controllable, convenient to qualitatively and quantitatively add the flavor substances, more beneficial to adding the flavor substances in a targeted manner, increasing the richness of the flavor, and harmonizing the cigarette flavor and the smoke. In recent years, the addition of materials with adsorption and flavor-blending effects in filter sticks has become an important subject of research in the tobacco industry.
At present, the perfuming of the cigarette filter stick mainly comprises the following modes: the fragrant thread is fragrant, the core thread is mainly made of cotton thread or cellulose, and one or more core threads soaked with plant perfume are added into the filter stick, so that the purposes of fragrance enhancement and fragrance supplement are achieved. However, there is a problem that the flavor substance adsorbed on the core thread is volatile and the flavor is not uniformly released from the front and rear stages when the cigarette is smoked. The particles are added into the cigarette filter stick, and when main stream smoke of the cigarette passes through, the fragrant substances are released, so that the purpose of flavoring is achieved. The perfuming of the particles has the advantages of simple equipment and process, low requirement on the character of the fragrant substance and the like, but has the defects of less attachment of the fragrant substance, low transmission efficiency and the like. The flavoring of the puffed bead is to wrap the essence in the soft capsule, place the soft capsule in the cigarette filter, and pinch the soft capsule with the help of external force to release the essence therein during smoking. However, the problems that the exploded beads are not easy to store at high humidity temperature, are easy to absorb moisture and deteriorate, and the oil-soluble essence is easy to pollute the filter stick forming paper after the exploded beads are extruded are solved. Gel perfuming is generally realized by adding gel perfume threads in the filter stick forming process, but the problems of complex production process, low efficiency, easy powder falling after drying and the like exist. In addition, Chinese patent CN2016107640493 discloses a compound gel flavor sustained-release granule, which also has the disadvantages of complex preparation process, difficult control of granule particle size, difficult flavor-loading release, etc. Therefore, there is a need to develop an aroma-carrying material which can better realize the flavoring of cigarette filter sticks.
Disclosure of Invention
The invention aims to provide slow-release gel particles for perfuming a cigarette filter stick aiming at the defects of the prior art, so as to solve the problems of poor perfuming effect, weak perfume releasing capability and uneven perfume release of the conventional cigarette filter stick perfuming particles.
The present invention also aims to provide a method for preparing the sustained-release gel particles.
The purpose of the invention is realized by the following technical scheme.
All percentages used herein are by weight unless otherwise indicated.
The cigarette flavoring slow-release gel particles are prepared from the following raw materials in parts by weight: 5-30 parts of polyethylene glycol-1000, 5-40 parts of polyethylene glycol-4000, 10-40 parts of lauric acid, 5-40 parts of octenyl succinate starch, 10-50 parts of cassava starch, 1-10 parts of humectant, 5-20 parts of adhesive and tobacco essence accounting for 10-30% of the total weight of the raw materials.
The humectant is one of glycerol, propylene glycol and sorbitol.
The adhesive is one of sodium carboxymethylcellulose, casein acrylic acid copolymer, soybean protein, chitosan or carboxymethyl cellulose.
The method for preparing the cigarette flavoring slow-release gel particles comprises the following steps:
(1) weighing polyethylene glycol-1000, polyethylene glycol-4000, lauric acid, starch octenyl succinate, tapioca starch, humectant and adhesive according to the weight parts, placing the materials in a water bath kettle at the temperature of 50-70 ℃, uniformly mixing and stirring the materials, and melting the materials to obtain a gel solution;
(2) adding tobacco essence with the weight of 10-30% of the gel solution, and uniformly stirring to obtain a fragrant gel solution;
(3) and (3) drying the fragrant gel solution in low-temperature freeze drying equipment, crushing and screening the dried material to obtain particles with the particle size of 20-50 meshes, namely the required cigarette perfuming slow-release gel particles.
The use method of the cigarette flavoring slow-release gel particles comprises the following steps: adding the sustained-release gel particles into the cigarette filter stick according to the amount of 80-130 mg of each cigarette.
Compared with the prior art, the invention has the following beneficial effects:
(1) the cigarette flavoring slow-release gel particles provided by the invention combine the excellent slow-release performance of gel and the high stability of the particles, and have the advantages of excellent flavor attaching effect, lasting flavor storage, strong flavor release capacity and efficient and uniform flavor release when being applied to cigarette filter sticks.
(2) The preparation method has the advantages of simple preparation process, easy quality control, low production cost and convenient realization of large-scale production.
(3) The invention can improve the problem that the existing gel perfuming material is easy to produce gel powder falling after being dried to a certain extent, and is safe and environment-friendly.
Detailed Description
The present invention is further described in detail by the following examples, which are not intended to limit the technical scope of the present invention, and all changes and equivalents made based on the teaching of the present invention shall fall within the scope of the present invention.
Example 1: preparation of Green tea flavored sustained-release gel particles
1. Weighing 30 parts of polyethylene glycol-1000, 05 parts of polyethylene glycol-40005 parts of lauric acid, 8 parts of octenyl succinate starch, 50 parts of cassava starch, 2 parts of propylene glycol and 5 parts of sodium carboxymethylcellulose according to parts by weight, and uniformly stirring and melting in a water bath kettle at 50-70 ℃ to obtain a gel solution. Weighing green tea essence with the weight of 20% of the gel solution, adding into the gel solution, and stirring to obtain green tea-flavored gel solution. Drying the green tea flavor gel solution by adopting low-temperature freeze drying equipment, and crushing and screening by adopting a crusher after drying to obtain green tea flavor slow-release gel particles with the particle size of 20-50 meshes.
The prepared green tea flavor sustained-release gel particles are added into a cigarette filter stick according to 110mg of each cigarette, and the adding mode is ternary cavity compounding.
2. Preparation of control samples: 10g of green tea essence is uniformly sprayed on 50g of starch granules by adopting a rolling atomization perfuming mode. Finally, the particles are added into the cigarette filter stick according to 110mg of each cigarette, and the adding mode is ternary cavity compounding. Namely, the three-element hollow granular filter stick is added into the cavity of the filter stick during the formation of the three-element hollow filter stick, and the three-element hollow granular filter stick is prepared.
3. Comparison and evaluation experiment: the prepared cigarettes are immediately smoked, 4 groups of cigarettes are simultaneously manufactured and stored in a constant temperature and humidity box for 4 weeks, and the conditions of the constant temperature and humidity box are as follows: the temperature is 22 ℃, the humidity is 60%, and a group of cigarettes are taken out every week for smoking evaluation. The evaluation was carried out by a group of 7 evaluation experts according to the standard GB5606.4-2005 "cigarette sensory technical requirements", and the evaluation results are shown in Table 1.
TABLE 1 cigarette sensory evaluation results
Example 2: preparation of mint flavored sustained release gel particles
1. Weighing polyethylene glycol-100015 parts, polyethylene glycol-400010 parts, 10 parts of lauric acid, 40 parts of octenyl succinate starch, 10 parts of cassava starch, 2 parts of glycerol and 15 parts of carboxymethyl cellulose according to parts by weight, and uniformly stirring and melting in a water bath kettle at 50-70 ℃ to obtain a gel solution. And weighing mint essence accounting for 10% of the weight of the gel solution, adding the mint essence into the gel solution, and uniformly stirring to obtain the mint-flavored gel solution. Drying the mint-flavored gel solution by using low-temperature freeze drying equipment, and crushing and screening by using a crusher after drying to obtain the mint-flavored slow-release gel particles with the particle size of 20-50 meshes.
The prepared mint-flavored slow-release gel particles are added into a cigarette filter stick according to 80mg of each cigarette, and the adding mode is ternary cavity compounding.
2. Preparation of control samples: 5g of mint essence is uniformly sprayed on 50g of starch granules by adopting a rolling atomization perfuming mode. Finally, adding the particles into the cigarette filter stick according to 80mg of each cigarette, wherein the adding mode is ternary cavity compounding.
3. Comparative aspiration experiments were carried out as described in example 1, and the results are shown in Table 2.
TABLE 2 sensory evaluation results of cigarettes
Example 3: preparation of orange-flavored sustained-release gel particles
1. Weighing 20 parts of polyethylene glycol-1000, 400040 parts of polyethylene glycol-400040 parts, 10 parts of lauric acid, 20 parts of octenyl succinate starch, 25 parts of cassava starch, 8 parts of sorbitol and 14 parts of casein acrylic acid copolymer according to parts by weight, and uniformly stirring and melting in a water bath kettle at 50-70 ℃ to obtain a gel solution. And weighing orange essence accounting for 30% of the weight of the gel solution, adding the orange essence into the gel solution, and uniformly stirring to obtain the orange-flavored gel solution. Drying the orange-flavor gel solution by adopting low-temperature freeze drying equipment, and crushing and screening by adopting a crusher after drying to obtain the orange-flavor slow-release gel particles with the particle size of 20-50 meshes.
Adding the prepared orange-flavor sustained-release gel particles into a cigarette filter stick according to 130mg of each cigarette, wherein the adding mode is ternary cavity compounding.
2. Preparation of control samples: 15g of orange essence is uniformly sprayed on 50g of starch granules by adopting a rolling atomization perfuming mode. And finally, adding the particles into the cigarette filter stick according to 130mg of each cigarette, wherein the adding mode is ternary cavity compounding.
3. Comparative aspiration tests were carried out according to the method shown in example 1, and the results are shown in Table 3
TABLE 3 sensory evaluation results of cigarettes
The comparative experiments show that the sustained-release gel particles have the advantages of high stability, excellent fragrance-attaching effect, lasting fragrance, strong fragrance-releasing capability and high-efficiency and uniform fragrance release, and can effectively solve the problems of poor fragrance-attaching effect, low fragrance-attaching persistence and non-uniform fragrance release in the prior art.
Claims (5)
1. A cigarette perfuming slow-release gel particle is characterized in that: the feed is prepared from the following raw materials in parts by weight: 5-30 parts of polyethylene glycol-1000, 5-40 parts of polyethylene glycol-4000, 10-40 parts of lauric acid, 5-40 parts of octenyl succinate starch, 10-50 parts of cassava starch, 1-10 parts of humectant, 5-20 parts of adhesive and tobacco essence accounting for 10-30% of the total weight of the raw materials.
2. The cigarette flavoring sustained-release gel particles according to claim 1, wherein: the humectant is one of glycerol, propylene glycol and sorbitol.
3. The cigarette flavoring sustained-release gel particles according to claim 1, wherein: the adhesive is one of sodium carboxymethylcellulose, casein acrylic acid copolymer, soybean protein, chitosan or carboxymethyl cellulose.
4. The method for preparing the cigarette flavoring slow-release gel particles as claimed in claim 1, which comprises the following steps:
(1) weighing polyethylene glycol-1000, polyethylene glycol-4000, lauric acid, starch octenyl succinate, tapioca starch, humectant and adhesive according to the weight parts, placing the materials in a water bath kettle at the temperature of 50-70 ℃, uniformly mixing and stirring the materials, and melting the materials to obtain a gel solution;
(2) adding tobacco essence with the weight of 10-30% of the gel solution, and uniformly stirring to obtain a fragrant gel solution;
(3) and (3) drying the fragrant gel solution in low-temperature freeze drying equipment, crushing and screening the dried material to obtain particles with the particle size of 20-50 meshes, namely the required cigarette perfuming slow-release gel particles.
5. The use method of the cigarette perfuming slow-release gel particles as claimed in claim 1, is characterized in that: adding the sustained-release gel particles into the cigarette filter stick according to the amount of 80-130 mg of each cigarette.
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Cited By (4)
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| CN114621818A (en) * | 2022-03-09 | 2022-06-14 | 山东省食品发酵工业研究设计院 | Nano essence particles for cigarette filter stick and preparation method thereof |
| CN114762533A (en) * | 2021-01-12 | 2022-07-19 | 云南恩典科技产业发展有限公司 | Low-temperature slow-release flavoring particles for cigarette filter stick and preparation method and application thereof |
| CN114762534A (en) * | 2021-01-12 | 2022-07-19 | 云南恩典科技产业发展有限公司 | Low-temperature slow-release microcrystalline granules and preparation method and application thereof |
| CN115886314A (en) * | 2023-01-17 | 2023-04-04 | 云南养瑞科技集团有限公司 | Preparation method of waxy phase-change slow-release aroma-carrying particles, particles obtained by method and application of particles |
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| CN114762533A (en) * | 2021-01-12 | 2022-07-19 | 云南恩典科技产业发展有限公司 | Low-temperature slow-release flavoring particles for cigarette filter stick and preparation method and application thereof |
| CN114762534A (en) * | 2021-01-12 | 2022-07-19 | 云南恩典科技产业发展有限公司 | Low-temperature slow-release microcrystalline granules and preparation method and application thereof |
| CN114621818A (en) * | 2022-03-09 | 2022-06-14 | 山东省食品发酵工业研究设计院 | Nano essence particles for cigarette filter stick and preparation method thereof |
| CN115886314A (en) * | 2023-01-17 | 2023-04-04 | 云南养瑞科技集团有限公司 | Preparation method of waxy phase-change slow-release aroma-carrying particles, particles obtained by method and application of particles |
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