CN111466613B - Flavoring particle for filter stick, preparation method thereof and filter stick - Google Patents
Flavoring particle for filter stick, preparation method thereof and filter stick Download PDFInfo
- Publication number
- CN111466613B CN111466613B CN202010272668.7A CN202010272668A CN111466613B CN 111466613 B CN111466613 B CN 111466613B CN 202010272668 A CN202010272668 A CN 202010272668A CN 111466613 B CN111466613 B CN 111466613B
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- parts
- filter stick
- filter
- disintegrating agent
- combination
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D39/00—Filtering material for liquid or gaseous fluids
- B01D39/02—Loose filtering material, e.g. loose fibres
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The flavoring particles for the filter stick comprise 137-174 parts by weight of disintegrating agent A, 80-100 parts by weight of disintegrating agent B, 300-700 parts by weight of filler, 5-25 parts by weight of functional additive and 5-15 parts by weight of adhesive with the concentration of dissolving 95% ethanol solution being 10-15%, wherein the disintegrating agent A is one or more than two selected from citric acid, tartaric acid and malic acid, the disintegrating agent B is one or more than two selected from sodium bicarbonate, potassium bicarbonate and sodium carbonate, the filler is one or more than two selected from water-soluble starch, cane sugar, mannitol, lactose and glucose, the functional additive is one or more than two selected from solid powder essence, lactose and glucose, One or more of solid powder lyophilized powder, solid powder tobacco extract, and sweetener.
Description
Technical Field
The invention relates to the field of functional particles of a cigarette material, in particular to an aroma-enhancing particle for a filter stick, a preparation method thereof and the filter stick.
Background
In recent years, as tobacco flavoring materials are gradually applied to auxiliary materials for cigarettes, the direct addition of some particle additives with the effects of flavoring, sweetening and the like in filter sticks not only becomes a common means in the field of tobacco manufacturing, but also is a positive response to the idea of non-combustion flavoring in the industry. The non-combustion flavoring is generally to add the flavoring substance directly into the cigarette auxiliary material, because it does not participate in combustion, so the damage to the effective component is small, and the introduction of impurity components with negative effects is avoided.
The added effect particles directly act on smoke, the components are known and controllable, and the effect particles are more direct and targeted to curing cigarette style characteristics and strengthening product characteristics. Relevant researches show that the aroma-enhancing and quality-improving or aroma-enhancing plant material is directly added into the filter stick, the temperature of the filter stick is about 40-50 ℃ during suction, a certain negative pressure exists, the smoke aerosol has a certain elution capability on components in the particle additive, and the aroma of the particle additive can be transferred into mainstream smoke, so that the style characteristic positioning and the quality characteristic of the cigarette are obviously influenced.
Therefore, by using the idea of blending the cigarette, the blending technology is applied to the design of cigarette auxiliary materials, functional additives with specific effects are selected for compounding, and through the release characteristics of the functional particles for the cigarette, fragrant substances are introduced during smoking of the cigarette, so that the cigarette can be flavored and supplemented without participating in combustion. At present, related researches on perfuming by taking a filter stick as a carrier exist: for example, the active release type cigarette flavor-supplementing granules disclosed in CN102533445B preparation method of active release type cigarette flavor-supplementing granules, CN103045362B preparation method of lac coated granules for cigarette filter tip, obtained product and application, and CN103060093B preparation method of flavor-supplementing moisture-preserving granules for cigarette, obtained product and application use, release base material, organic acid and organic polymer skeleton are used as main raw materials. Active release type cigarette fragrance supplementing particles are formed through processes of fragrance supplementing, granulation, solidification and the like, and fragrance materials are actively released after encountering mainstream smoke, so that the style and smoking quality of cigarettes can be enhanced.
The patent technology or the patent product has respective advantages, but the patent technology or the patent product has various defects of more production process steps, higher manufacturing cost, poor health and environmental protection and the like. Can not be applied to the production practice of cigarette filter sticks in a large scale.
Disclosure of Invention
An object of the present invention is to provide a flavoring particle for filter rods, which can increase the flavor of cigarette smoke when the cigarette material smoke releases the smoke, a method for preparing the same, and a filter rod.
Another object of the present invention is to provide a flavoring particle for filter stick, a preparation method thereof and a filter stick, wherein the preparation process of the flavoring particle for filter stick is simple and suitable for mass production.
To achieve at least one of the above objects of the present invention, the present invention provides a preparation of flavored particles for filter rods, comprising:
(S1): uniformly mixing 137-174 parts (weight parts) of a disintegrant A, 80-100 parts (weight parts) of a disintegrant B, 300-700 parts (weight parts) of a filler and 5-25 parts (weight parts) of a functional additive, wherein the disintegrant A is one or a combination of more than two selected from citric acid, tartaric acid and malic acid, the disintegrant B is one or a combination of more than two selected from sodium bicarbonate, potassium bicarbonate and sodium carbonate, the filler is one or a combination of more than two selected from water-soluble starch, sucrose, mannitol, lactose and glucose, and the functional additive is one or a combination of more than two selected from solid powder essence, solid powder freeze-dried powder, solid powder tobacco extract and sweetener;
(S2): weighing adhesive dissolved in 95% ethanol solution with concentration of 10% -15%;
(S3): mixing (S1) the formed material with 5-15 parts (by weight) (S2) of the formed material;
(S4): granulating the material formed in (S3); and
(S5) drying and sieving the formed granules.
According to an embodiment of the invention, the particle size after sieving ranges from 16 mesh to 80 mesh, and the moisture content is less than 8%.
According to an embodiment of the invention, the binder is implemented as a material selected from polyvinylpyrrolidone.
According to an embodiment of the present invention, the granulation technology is selected from the group consisting of extrusion granulation equipment, fluidized bed granulation equipment, and dry granulation equipment, wherein the drying technology employs equipment such as boiling drying equipment and spray drying equipment, and the screening technology employs a vibrating screen.
According to another aspect of the invention, the invention provides that the flavoring particles for filter sticks are prepared by the preparation method of the flavoring particles for filter sticks.
According to another aspect of the invention, there is provided a flavoured granule for filter rods, characterised in that it comprises:
137-174 parts (by weight) of a disintegrating agent A, wherein the disintegrating agent A is implemented by one or a combination of more than two of citric acid, tartaric acid and malic acid;
80-100 parts (by weight) of a disintegrant B, wherein the disintegrant B is one or a combination of more than two selected from sodium bicarbonate, potassium bicarbonate and sodium carbonate;
300-700 parts (by weight) of filler, wherein the filler is selected from one or a combination of more than two of water-soluble starch, sucrose, mannitol, lactose and glucose;
5-25 parts (by weight) of a functional additive, wherein the functional additive is one or a combination of more than two of solid powder essence, solid powder freeze-dried powder, solid powder tobacco extract and sweetener; and
5-15 parts (by weight) of adhesive with the concentration of 10% -15% dissolved in 95% ethanol solution.
According to another aspect of the invention, there is provided a filter rod comprising flavouring granules as described above for a filter rod.
According to an embodiment of the invention, when the filter stick is a binary filter stick, the adding proportion of the aroma-enhancing particles for the filter stick in a cigarette filter stick tow is 1-3 mg/mm.
According to an embodiment of the invention, the adding proportion of the flavoring particles for the filter stick is 5-20 mg/mm.
Further objects and advantages of the invention will be fully apparent from the ensuing description and understanding.
These and other objects, features and advantages of the present invention will become more fully apparent from the following detailed description, the appended claims and the accompanying drawings.
Detailed Description
The preferred embodiments in the following description are given by way of example only, and other obvious variations will occur to those skilled in the art. The basic principles of the invention, as defined in the following description, may be applied to other embodiments, variations, modifications, equivalents, and other technical solutions without departing from the spirit and scope of the invention.
It will be understood by those skilled in the art that in the present disclosure, the terms "longitudinal," "lateral," "upper," "lower," "front," "rear," "left," "right," "vertical," "horizontal," "top," "bottom," "inner," "outer," and the like are used in an orientation or positional relationship indicated based on the orientation or positional relationship shown, which is for convenience in describing and simplifying the description, and do not indicate or imply that the device or element being referred to must have a particular orientation, be constructed and operated in a particular orientation, and thus the terms should not be construed as limiting the invention.
A method of preparing flavored particles for filter rods according to a preferred embodiment of the present invention will be described in detail below. Specifically, the preparation method of the flavoring particles for the filter stick comprises the following steps:
(S1): uniformly mixing 137-174 parts (by weight) of a disintegrating agent A, 80-100 parts (by weight) of a disintegrating agent B, 300-700 parts (by weight) of a filler and 5-25 parts (by weight) of a functional additive;
(S2): weighing adhesive dissolved in 95% ethanol solution with concentration of 10% -15%;
(S3): mixing (S1) the formed material with 5-15 parts (by weight) (S2) of the formed material;
(S4): granulating the material formed in (S3); and
(S5) drying and sieving the formed granules.
It is worth integrating, said disintegrating agent A is implemented as one or more than two combinations selected from citric acid, tartaric acid, malic acid. The disintegrant B is one or more of sodium bicarbonate, potassium bicarbonate and sodium carbonate, and the filler is one or more of water soluble starch, sucrose, mannitol, lactose and glucose. The functional additive is one or more selected from solid powder essence, solid powder lyophilized powder, solid powder tobacco extract, and sweetener.
The binder is selected from polyvinylpyrrolidone.
The granulation technology can adopt extrusion granulation equipment, fluidized bed granulation equipment and dry granulation equipment; the drying equipment can be boiling drying equipment or spray drying equipment; the screening technical department adopts a vibrating screen.
Preferably, the particle size after sieving ranges from 16 mesh to 80 mesh with moisture < 8%.
Further, according to another aspect of the invention, a filter rod is disclosed. The filter stick comprises the flavoring particles for the filter stick, which are prepared according to the preparation method of the flavoring particles for the filter stick.
Preferably, when the filter stick is a binary or ternary composite filter stick, the adding proportion of the aroma-enhancing particles for the filter stick in a cigarette filter stick tow is 1-3 mg/mm; when the filter stick is a cavity filter stick, the adding proportion of the aroma-enhancing particles for the filter stick is 5-20 mg/mm.
In the first embodiment of the invention, 174 parts of citric acid as a raw material of a disintegrating agent A, 100 parts of sodium bicarbonate as a raw material of a disintegrating agent B, 300 parts of lactose as a filler and 5 parts of orange powder essence as a functional additive are weighed and mixed uniformly for later use. Preparing 95% ethanol solution containing 10% of polyvinylpyrrolidone, weighing 5 parts, adding the 5 parts into 100 parts of standby materials, uniformly mixing, preparing a granular soft material by planetary extrusion granulation, placing the granular soft material into boiling drying equipment, drying at the equipment drying temperature of 45 ℃, drying until the moisture of the granules is less than 8%, taking out, placing the granular soft material into a double-layer vibrating screen with 16-40 meshes for screening to obtain functional granules for cigarettes with the particle size of 16-40 meshes and the moisture of less than 8%, and preparing a binary composite according to the adding proportion of 1mg/mm in cigarette filter stick tows to be applied to the cigarettes to play roles of increasing orange flavor, improving smoke moistening and the like.
In the second embodiment of the invention, 174 parts of tartaric acid as a raw material of a disintegrating agent A, 100 parts of potassium bicarbonate as a raw material of a disintegrating agent B, 700 parts of lactose as a filler and 25 parts of mint powder essence as a functional additive are weighed and mixed uniformly for later use. Preparing 95% ethanol solution containing 10% of polyvinylpyrrolidone, weighing 15 parts, adding the 15 parts into 100 parts of standby materials, uniformly mixing, preparing a granular soft material by swing extrusion granulation, placing the granular soft material into fluidized bed drying equipment, drying at the equipment drying temperature of 45 ℃, drying until the moisture of the granules is less than 8%, taking out, placing the granular soft material into a 40-60-mesh double-layer vibrating screen for screening to obtain functional granules for cigarettes with the particle size of 40-60 meshes and the moisture of less than 8%, and preparing the functional granules for cigarettes into a binary composite filter stick according to the adding proportion of 3mg/mm in the cigarette filter stick tow to be applied to the cigarettes to play roles of increasing cool feeling, improving smoke moistening feeling and the like.
In the third embodiment of the invention, 174 parts of malic acid as a raw material of a disintegrating agent A, 100 parts of sodium carbonate as a raw material of a disintegrating agent B, 300 parts of mannitol as a filling agent and 5 parts of dried orange peel powder essence as a functional additive are weighed and mixed uniformly for later use. Preparing 95% ethanol solution containing 10% of polyvinylpyrrolidone, weighing 5 parts, adding the 5 parts into 100 parts of standby materials, uniformly mixing, preparing a soft particle material through dry granulation, placing the soft particle material into spray drying equipment, drying at the equipment drying temperature of 45 ℃, drying until the moisture content of the particles is less than 8%, taking out, placing the soft particle material into a 60-80-mesh double-layer vibrating screen for screening to obtain functional particles for cigarettes with the particle size of 60-80 meshes and the moisture content of less than 8%, and preparing a binary composite filter stick according to the adding proportion of 2mg/mm in a cigarette filter stick tow to be applied to the cigarettes to play roles of increasing the fragrance of dried orange peel, improving the smoke moistening feeling and the like.
In the fourth embodiment of the invention, 137 parts of citric acid as a raw material of a disintegrating agent A, 80 parts of sodium bicarbonate as a raw material of a disintegrating agent B, 300 parts of water-soluble starch as a filling agent and 5 parts of Zimbabwe extract as a functional additive are weighed and mixed uniformly for later use. Preparing 95% ethanol solution containing 10% of polyvinylpyrrolidone, weighing 10 parts of the solution, adding the solution into 100 parts of standby materials through fluidized bed granulation equipment to prepare a soft particle material, placing the soft particle material into spray drying and drying equipment, drying at the equipment drying temperature of 45 ℃, drying until the moisture content of the particles is less than 8%, taking out the soft particle material, placing the soft particle material into a 16-40-mesh double-layer vibrating screen for screening to obtain functional particles for cigarettes with the particle size of 16-40 meshes and the moisture content of less than 8%, and preparing a ternary cavity composite filter stick according to the adding proportion of 5mg/mm in cigarette filter stick tows to be applied to the cigarettes to play roles of increasing the original fragrance concentration of the cigarettes, improving the smoke moistening feeling and the like.
In the fifth embodiment of the invention, 137 parts of tartaric acid as a raw material of a disintegrating agent A, 80 parts of potassium bicarbonate as a raw material of a disintegrating agent B, 300 parts of cane sugar as a filler and 5 parts of stevioside as a functional additive are weighed and uniformly mixed for later use. Preparing 95% ethanol solution containing 10% of polyvinylpyrrolidone, weighing 15 parts, adding the 15 parts into 100 parts of standby materials, uniformly mixing, preparing a granular soft material through a planetary granulating device, placing the granular soft material into a spray drying and drying device, drying at the device drying temperature of 45 ℃, taking out after drying until the moisture of the granules is less than 8%, placing the granular soft material into a 40-60-mesh double-layer vibrating screen for screening to obtain functional granules for cigarettes with the particle size of 40-60 meshes and the moisture of less than 8%, and preparing a ternary composite cavity filter stick according to the adding proportion of 20mg/mm in a cigarette filter stick tow to be applied to the cigarettes to play roles of increasing the sweet feeling, improving the smoking quality and the like.
In the sixth embodiment of the invention, 100 parts of citric acid as a disintegrating agent A raw material, 37 parts of malic acid, 60 parts of sodium carbonate as a disintegrating agent B raw material, 20 parts of sodium bicarbonate, 200 parts of lactose as a filling agent, 100 parts of glucose and 5 parts of jasmine pollen essence as a functional additive are weighed and mixed uniformly for later use. Preparing 95% ethanol solution containing 10% of polyvinylpyrrolidone, weighing 5 parts, adding the 5 parts into 100 parts of standby materials, uniformly mixing, preparing a granular soft material through dry granulation, placing the granular soft material into spray drying equipment, drying at the equipment drying temperature of 45 ℃, drying until the moisture content of the granules is less than 8%, taking out, placing the granular soft material into a 60-80-mesh double-layer vibrating screen for screening to obtain functional granules for cigarettes with the particle size of 60-80 meshes and the moisture content of less than 8%, and preparing a binary composite filter stick according to the adding proportion of 1.5mg/mm in a cigarette filter stick tow to be applied to the cigarettes to play roles of increasing the fragrance of jasmine flowers, improving the moist feeling of smoke and the like.
It will be appreciated by persons skilled in the art that the embodiments of the invention described above and shown in the drawings are given by way of example only and are not limiting of the invention. The objects of the invention have been fully and effectively accomplished. The functional and structural principles of the present invention have been shown and described in the examples, and any variations or modifications of the embodiments of the present invention may be made without departing from the principles.
Claims (9)
1. The preparation method of the flavoring particles for the filter stick is characterized by comprising the following steps:
(S1): uniformly mixing 137-174 parts of a disintegrating agent A, 80-100 parts of a disintegrating agent B, 300-700 parts of a filling agent and 5-25 parts of a functional additive according to parts by weight, wherein the disintegrating agent A is one or a combination of more than two of citric acid, tartaric acid and malic acid, the disintegrating agent B is one or a combination of more than two of sodium bicarbonate, potassium bicarbonate and sodium carbonate, the filling agent is one or a combination of more than two of water-soluble starch, sucrose, mannitol, lactose and glucose, and the functional additive is one or a combination of more than two of solid powder essence, solid powder freeze-dried powder, solid powder tobacco extract and sweetener;
(S2): weighing polyvinylpyrrolidone with concentration of 10% -15% dissolved in 95% ethanol solution;
(S3): mixing (S1) the formed material with 5-15 parts (S2) by weight of the formed material;
(S4): granulating the material formed in (S3); and
(S5) drying and sieving the formed granules.
2. The method for preparing flavor-enhancing granules for filter sticks according to claim 1, wherein the granules after sieving have a particle size ranging from 16 meshes to 80 meshes and a moisture content of less than 8%.
3. The method for preparing flavor-enhancing granules for filter rods according to claim 1, wherein the granulation is selected from extrusion granulation equipment, fluidized bed granulation equipment and dry granulation equipment, wherein the drying technology is selected from boiling drying equipment and spray drying equipment, and wherein the screening technology is selected from vibrating screen.
4. Flavoring granule for filter rods, wherein the flavoring granule for filter rods is produced by the method for producing flavoring granule for filter rods according to any one of claims 1 to 3.
5. The flavoring particle for the filter stick is characterized by comprising the following components in parts by weight:
137-174 parts of a disintegrating agent A, wherein the disintegrating agent A is implemented by one or a combination of more than two of citric acid, tartaric acid and malic acid;
80-100 parts of a disintegrating agent B, wherein the disintegrating agent B is implemented by one or a combination of more than two of sodium bicarbonate, potassium bicarbonate and sodium carbonate;
300-700 parts of a filler, wherein the filler is selected from one or a combination of more than two of water-soluble starch, sucrose, mannitol, lactose and glucose;
5-25 parts of a functional additive, wherein the functional additive is one or a combination of more than two of solid powder essence, solid powder freeze-dried powder, solid powder tobacco extract and sweetener; and
5-15 parts of adhesive with the concentration of 10-15% dissolved in 95% ethanol solution.
6. Flavored granules for filter rods according to claim 5, wherein the binder is chosen from polyvinylpyrrolidone.
7. The filter stick is characterized by comprising:
flavouring granules for filter rods as claimed in claim 5 or 6.
8. The filter stick according to claim 7, wherein when the filter stick is a binary filter stick, the proportion of the flavor-enhancing particles for the filter stick added to the filter tow of the cigarette filter stick is 1-3 mg/mm.
9. The filter stick according to claim 8, wherein when the filter stick is a hollow filter stick, the adding proportion of the flavor-enhancing particles for the filter stick is 5-20 mg/mm.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202010272668.7A CN111466613B (en) | 2020-04-09 | 2020-04-09 | Flavoring particle for filter stick, preparation method thereof and filter stick |
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| CN202010272668.7A CN111466613B (en) | 2020-04-09 | 2020-04-09 | Flavoring particle for filter stick, preparation method thereof and filter stick |
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| CN111466613A CN111466613A (en) | 2020-07-31 |
| CN111466613B true CN111466613B (en) | 2022-04-08 |
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| CN111466613A (en) | 2020-07-31 |
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