CN111449271A - Smoke release particle material containing biomass fibers and preparation method thereof - Google Patents
Smoke release particle material containing biomass fibers and preparation method thereof Download PDFInfo
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- CN111449271A CN111449271A CN202010273707.5A CN202010273707A CN111449271A CN 111449271 A CN111449271 A CN 111449271A CN 202010273707 A CN202010273707 A CN 202010273707A CN 111449271 A CN111449271 A CN 111449271A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
Abstract
The invention discloses a smoke-releasing granular material containing biomass fibers and a preparation method thereof, belonging to the technical field of novel tobacco products, wherein the smoke-releasing granular material comprises the following raw materials in percentage by mass: 40-70% of tobacco powder, 5-30% of other biomass fiber powder, 10-20% of atomizing agent, 0-5% of binder and 1-5% of essence and spice for cigarettes. The particle size of the smoke release particle material containing the biomass fiber is uniform, the released smoke is stable, the smoke can be endowed with unique aroma and taste by adding the biomass fiber, the 'sweet aroma' smell is increased, the smoke is coordinated with the tobacco aroma, the moisture absorption of the tobacco particles is reduced, the smoke release amount is increased, and the dry feeling of the throat during smoking is improved.
Description
Technical Field
The invention relates to a smoke-releasing granular material containing biomass fibers, belonging to the technical field of novel tobacco products.
Background
In recent years, with the enhancement of global smoking control and the improvement of health consciousness of people, the research and development of novel tobacco products are greatly accelerated by various international big tobacco plants. Since 1988, tobacco in various countries has been controversial to propose various types of non-combustible heating tobacco products such as carbon heating, electric heating, chemical reaction heating and the like, and reynolds has proposed various products such as "premier", "eclipse", "REVO" and the like in sequence, but the smoking taste is greatly different from that of the traditional cigarettes, so that the tobacco products are difficult to accept by the public. Until the beginning of 2015, the international tobacco major Femo company raised a wave of heated cigarettes with "iQOS", which is popular to date.
The heating cigarette is a novel tobacco product which precisely heats tobacco to release smoke containing fragrant substances and nicotine by a temperature control technology. Different from the traditional cigarette, the tobacco substrate in the heated cigarette is in a non-combustion state, so that harmful substances generated by high-temperature combustion and pyrolysis of tobacco can be reduced, and because the heating temperature is low (below 500 ℃), an atomizing agent can be added in the production process to increase the smoke quantity, which is an important index influencing the smoking experience of the heated cigarette.
The type of the smoke-releasing material of the heated cigarette is an important factor influencing the smoking taste, and the current international smoke-releasing materials of the heated cigarette mainly comprise: the tobacco sheet cannot avoid the miscellaneous gas of added paper pulp fibers in the heating process, and the granular heating cigarette serving as a novel special product can release the cigarette fragrance to the maximum degree during heating.
The tobacco leaves have a porous capillary structure, so that a physical space is provided for moisture adsorption, and meanwhile, polysaccharide, pectin and inorganic ions in the components of the tobacco leaves also have hydrophilicity. Moisture can affect the taste, smoking temperature and smoke yield of a heated cigarette. Because the tobacco particles are prepared from pure tobacco leaf raw materials, and a certain amount of paper pulp fibers are added into the tobacco sheets, the tobacco particles with the same glycerin content have stronger moisture absorption and higher raw material cost than the tobacco sheets. In addition, the phenomenon that the throat generates dry feeling when smoking is generally existed in the heating cigarette. How to reduce the moisture absorption of tobacco particles while ensuring the taste of the particle-type heated cigarette so as to generate larger, uniform and stable smoke quantity and improve the dry sensation of the throat during smoking is a problem which is difficult to solve by the prior art.
China has abundant biomass resources as a big agricultural country, a large amount of agricultural waste biomass fibers exist, corn is one of main crops of China, byproducts of corn comprise corncobs, cornhusks and cornstalks, and the corncobs are commonly used for preparing furfural in industry. Research shows that the corncob can generate fragrant substances with 'sweet-burnt fragrance' smell, such as furfural and 5-methylfurfural, when the corncob is pyrolyzed at 350 ℃. The bamboo leaves and reed leaves have unique faint scent, and the effective components of the bamboo leaves comprise flavone, phenolic ketone, anthraquinone, lactone, polysaccharide, amino acid, trace elements and the like, so the bamboo leaves have excellent effects of resisting free radicals, oxidation, aging, fatigue, blood fat, cardiovascular and cerebrovascular diseases and the like. Therefore, the biomass fiber has better application prospect in heating cigarettes.
Disclosure of Invention
In order to solve the problems of the prior art, the invention aims to develop a smoke-releasing granular material containing biomass fibers so as to improve the smoke-releasing amount of the smoke-releasing granular material, reduce the moisture absorption and improve the dry sensation of the throat during smoking.
In order to achieve the purpose, the invention adopts the following technical scheme:
the invention relates to a smoke-releasing granular material containing biomass fibers, which comprises the following raw materials in percentage by mass: 40-70% of tobacco powder, 5-30% of other biomass fiber powder, 10-20% of atomizing agent, 0-5% of binder and 1-5% of essence and spice for cigarettes.
Preferably, the tobacco powder is selected from at least one of flue-cured tobacco, burley tobacco, aromatic tobacco, expanded tobacco and tobacco stem powder.
Preferably, the particle size of the tobacco powder is less than or equal to 100 μm, and more preferably less than or equal to 80 μm.
Preferably, the other biomass fiber powder is at least one selected from corncob, cornhusk, cornstalk, sugar cane, bamboo leaves and reed leaf powder.
Preferably, the particle size of the other biomass fiber powder is less than or equal to 100 mu m.
Preferably, the atomizing agent is selected from at least one of 1, 2-propylene glycol and glycerol.
Preferably, the binder is selected from at least one of starch, xanthan gum, carrageenan, gum arabic, gelatin, guar gum, maltodextrin, lactose, hydroxypropylmethylcellulose, and sodium carboxymethylcellulose.
Preferably, the tobacco flavor is at least one selected from the group consisting of tobacco dry distillation flavor, tobacco extract, Maillard reaction product, natural plant extract and baking flavor.
The preparation method of the smoke-releasing granular material containing the biomass fibers comprises the following steps:
and 4, screening the smoke release particles with the moisture removed in the step 3 to obtain the smoke release particle material containing the biomass fibers.
In step 3, the drying conditions are as follows: the temperature is 80-100 ℃; the time is 20min-60 min.
In step 4, the screening conditions are as follows: sieving with 20-80 mesh standard sieve.
The smoke-releasing granular material containing the biomass fibers is uniform spherical granules with the diameter of 0.3-0.6 mm.
Compared with the prior art, the invention has the beneficial effects that:
the smoke-releasing granular material containing the biomass fibers has uniform granularity, and the smoke released during heating is stable. The addition of the biomass fiber can endow the smoke with unique aroma and taste, increase the aroma of 'sweet burnt aroma', coordinate with the smoke aroma, increase the richness of the smoke, reduce the moisture absorption of tobacco particles, improve the smoke release amount, improve the dry feeling of the throat during smoking, and simultaneously effectively reduce the cost.
Drawings
FIG. 1 is a graph comparing the moisture content of the smoke-releasing granule obtained in example 2 with that of the comparative example with time at 22 ℃ and 60% RH, and it can be seen from FIG. 1 that the moisture absorption of the smoke-releasing granule in example 2 is significantly reduced compared with that of the pure tobacco granule, and the moisture content of 6h is reduced from 16% to 14%.
FIG. 2 is a graph showing the comparison between the total smoke generation amount of the smoke-releasing granule obtained in example 2 and that of the smoke-releasing granule obtained in the comparative example in a heat non-combustible state (350 ℃ C.) with time, and it can be seen from FIG. 2 that the smoke release amount of the smoke-releasing granule material in example 2 is superior to that of a pure tobacco granule, and the smoke release amount of the smoke-releasing granule material to which biomass fibers are added is larger in a heat non-combustible state under the same conditions.
Detailed Description
The following examples are given for the detailed implementation and specific operation of the present invention, but the scope of the present invention is not limited to the following examples.
Example 1
The embodiment provides a smoke-releasing particle material containing biomass fibers, and the preparation method comprises the following steps:
And 2, mixing and granulating the main material and the auxiliary material in the step 1 by adopting a wet granulation process to obtain the smoke release granules.
And 3, drying the smoke-releasing particles obtained in the step 2 in an oven at 100 ℃ for 30 min.
And 4, screening the dried smoke-releasing particles obtained in the step 3 by using a standard sieve with a size of 20-80 meshes to obtain the smoke-releasing particle material with the particle size of 0.3-0.6mm and containing the biomass fibers.
Example 2
The embodiment provides a smoke-releasing particle material containing biomass fibers, and the preparation method comprises the following steps:
step 1: pulverizing flue-cured tobacco, burley tobacco leaf, corncob, cornstalk and bamboo leaf, and sieving with 80 μm sieve; 350g of flue-cured tobacco powder, 130g of burley tobacco powder, 60g of corncob powder, 30g of cornstalk powder and 30g of bamboo leaf powder are respectively weighed as main materials, and 100g of glycerol, 30g of 1, 2-propylene glycol, 10g of guar gum, 10g of maltodextrin, 10g of tobacco dry distillation spice, 10g of tobacco extract and 10g of baking essence are respectively weighed as auxiliary materials.
And 2, mixing and granulating the main material and the auxiliary material in the step 1 by adopting a wet granulation process to obtain the smoke release granules.
And 3, drying the smoke-releasing particles obtained in the step 2 in an oven at 100 ℃ for 30 min.
And 4, screening the dried smoke-releasing particles obtained in the step 3 by using a standard sieve with a size of 20-80 meshes to obtain the smoke-releasing particle material with the particle size of 0.3-0.6mm and containing the biomass fibers.
Example 3
The embodiment provides a smoke-releasing particle material containing biomass fibers, and the preparation method comprises the following steps:
And 2, mixing and granulating the main material and the auxiliary material in the step 1 by adopting a wet granulation process to obtain the smoke release granules.
And 3, drying the smoke-releasing particles obtained in the step 2 in an oven at 100 ℃ for 30 min.
And 4, screening the dried smoke-releasing particles obtained in the step 3 by using a standard sieve with a size of 20-80 meshes to obtain the smoke-releasing particle material with the particle size of 0.3-0.6mm and containing the biomass fibers.
Comparative example
The embodiment provides a smoke-releasing granular material without biomass fibers, and the preparation method comprises the following steps:
And 2, mixing and granulating the main material and the auxiliary material in the step 1 by adopting a wet granulation process to obtain the smoke release granules.
And 3, drying the smoke-releasing particles obtained in the step 2 in an oven at 100 ℃ for 30 min.
And 4, screening the dried smoke-releasing particles obtained in the step 3 by using a standard sieve with a size of 20-80 meshes to obtain smoke-releasing particle materials with the particle size of 0.3-0.6 mm.
The smoke-releasing particulate materials prepared in example 1, example 2, example 3 and comparative example were packed in cigarettes, and sensory evaluation was performed using a matched electrically heated smoking set, and the evaluation results are shown in table 1.
TABLE 1 sensory evaluation results of heated cigarettes
As can be seen from Table 1: the comparative example had a lower smoke content, a strong throat dryness and a lower sensory quality. The smoke release particle material added with a small amount (about 7-15%) of biomass fiber in the embodiment 1 and the embodiment 2 can effectively improve the smoke amount and the mouth-to-mouth stability, reduce the dry feeling of the throat, increase the sweet smell of the coke, coordinate with the smoke smell, enrich the fragrance and improve the aftertaste. However, when the addition ratio of example 3 is too high (about 30%), the stiffness may be weakened and the satisfaction may be lowered. In summary, the sensory evaluation results of example 2 in the present invention were the best.
The smoke release particle materials prepared in the example 2 and the comparative example are placed in a constant temperature and humidity box with the temperature of 22 ℃ and the relative humidity of 60%, the mass is weighed once every 0.5-1 h, a moisture absorption experiment is carried out for 6h, and a time-dependent change graph of the moisture content of the smoke release particles is drawn after the moisture content is calculated, as shown in fig. 1. As can be seen from the figure, compared with pure tobacco particles, the moisture absorption of the tobacco particles is effectively improved after the biomass fibers are added, and the moisture content of 6h is reduced from 16% to 14%.
The smoke-releasing particulate materials prepared in example 2 and comparative example were compared in terms of total smoke release in a heat non-combustible state (350 ℃) using a cone calorimeter, as shown in fig. 2. As can be seen from fig. 2, the smoke releasing amount of the smoke releasing granule of example 2 is superior to that of the pure tobacco granule, and the smoke releasing amount of the smoke releasing granule material to which the biomass fiber is added is larger in the state of not burning under heating under the same condition.
The above description is only exemplary of the present invention and should not be taken as limiting the invention, and any modifications, equivalents, improvements, etc. made within the spirit and principle of the present invention should be included in the scope of the present invention.
Claims (9)
1. The smoke-releasing granular material containing biomass fibers is characterized by comprising the following raw materials in percentage by mass: 40-70% of tobacco powder, 5-30% of other biomass fiber powder, 10-20% of atomizing agent, 0-5% of binder and 1-5% of essence and spice for cigarettes.
2. A smoke releasing particulate material containing biomass fibres as claimed in claim 1 wherein: the tobacco powder is selected from at least one of flue-cured tobacco, burley tobacco, aromatic tobacco, expanded tobacco and tobacco stem powder; the particle size of the tobacco powder is less than or equal to 100 mu m.
3. A smoke releasing particulate material containing biomass fibres as claimed in claim 1 wherein: the other biomass fiber powder is selected from at least one of corncob, cornhusk, cornstalk, sugarcane, bamboo leaf and reed leaf powder; the particle size of the other biomass fiber powder is less than or equal to 100 mu m.
4. A smoke releasing particulate material containing biomass fibres as claimed in claim 1 wherein: the atomizing agent is at least one of 1, 2-propylene glycol and glycerol.
5. A smoke releasing particulate material containing biomass fibres as claimed in claim 1 wherein: the binder is selected from at least one of starch, xanthan gum, carrageenan, arabic gum, gelatin, guar gum, maltodextrin, lactose, hydroxypropyl methylcellulose and sodium carboxymethylcellulose.
6. A smoke releasing particulate material containing biomass fibres as claimed in claim 1 wherein: the tobacco essence perfume is at least one of tobacco dry distillation perfume, tobacco extract, Maillard reaction product, natural plant extract and baking essence.
7. A method of preparing a smoke releasing particulate material containing biomass fibres as claimed in any one of claims 1 to 6 comprising the steps of:
step 1, mixing tobacco powder and other biomass fiber powder according to a proportion to serve as a main material, and mixing an atomizing agent, a binder and tobacco essence and flavor according to a proportion to serve as an auxiliary material;
step 2, mixing and granulating the auxiliary materials and the main materials in the step 1 by adopting a wet granulation process to obtain smoke release particles;
step 3, drying the smoke release particles obtained in the step 2 to remove moisture;
and 4, screening the smoke release particles with the moisture removed in the step 3 to obtain the smoke release particle material containing the biomass fibers.
8. The method of claim 7, wherein: in step 3, the drying conditions are as follows: the temperature is 80-100 ℃; the time is 20min-60 min.
9. The method of claim 7, wherein: in step 4, the screening conditions are as follows: sieving with 20-80 mesh standard sieve.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202010273707.5A CN111449271A (en) | 2020-04-09 | 2020-04-09 | Smoke release particle material containing biomass fibers and preparation method thereof |
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| CN202010273707.5A CN111449271A (en) | 2020-04-09 | 2020-04-09 | Smoke release particle material containing biomass fibers and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN114027545A (en) * | 2021-10-27 | 2022-02-11 | 深圳市真味生物科技有限公司 | Heating non-combustible fuming particle and preparation method thereof |
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