CN108936781A - The method for heating cigarette sucked material of not burning using wet granulation preparation - Google Patents
The method for heating cigarette sucked material of not burning using wet granulation preparation Download PDFInfo
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- CN108936781A CN108936781A CN201811082538.6A CN201811082538A CN108936781A CN 108936781 A CN108936781 A CN 108936781A CN 201811082538 A CN201811082538 A CN 201811082538A CN 108936781 A CN108936781 A CN 108936781A
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- cigarette
- tobacco
- burning
- wet granulation
- atomized liquid
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
-
- A24F47/004—
Abstract
The invention discloses a kind of methods for heating cigarette sucked material of not burning using wet granulation preparation, comprising the following steps: (1) tobacco material is carried out pulverization process using Ultra-Micro Grinding Equipment and ultra micro tobacco powder is prepared；(2) excipient is added into ultra micro tobacco powder to stir to obtain solid base；(3) taking adhesive, smoke agent, the uniform atomized liquid of essence spice for cigarette mixture, are adjusted, mixture uniformly, obtains clear atomized liquid after standing filtering under room temperature using density of the distilled water to atomized liquid；(4) solid base and atomized liquid are added in the feed bin of wet granulator and are granulated, the graininess heating that the particle after granulation goes moisture removal and sieving to obtain different grain size size after drying is not burnt cigarette sucked material.The present invention provides a kind of completely newly suction experience of consumer, further promotes the suction safety for heating the tobacco product that do not burn.
Description
Technical field
The present invention relates to tobacco product technical fields, and in particular to a kind of to heat the cigarette that do not burn using wet granulation preparation
With the method for sucked material.
Background technique
Under the increasingly severe background of tobacco control environment, the sales volume of conventional tobacco products is in some developed countries and developing country
Stagnating, which occurs, in market even to be declined, and quick with the generally raising of people's health consciousness and intelligent microelectronic technology
Development, the exploitation of new tobacco products are in eruptive growth.Representative non-traditional tobacco product mainly has heating not in the market
Several classes such as burning type tobacco product, smoke-free tobacco product.Heating does not burn cigarette as one kind master in new tobacco products
Product is wanted, research and development generally receive the attention of tobacco enterprise.
Current heating does not burn cigarette product due to the limitation of preparation method and the limitation of raw material, in aspiration procedure
There is the release of a large amount of harmful substances, be easy to causeing tobacco product suction, there are a large amount of healthy hidden dangers.
Summary of the invention
The purpose of the present invention is to provide a kind of sides that cigarette sucked material of not burning is heated using wet granulation preparation
Method, solve current heating do not burn cigarette product suction experience poor, the low problem of flue gas mass.
In order to solve the above technical problems, the invention adopts the following technical scheme:
A method of cigarette sucked material of not burning is heated using wet granulation preparation, comprising the following steps:
1) tobacco material is subjected to pulverization process using Ultra-Micro Grinding Equipment and ultra micro tobacco powder is prepared；
2) the ultra micro tobacco powder that will be prepared in step 1) is added excipient and stirs to obtain solid base；This
Excipient is added in step can make the granular sucked material finally produced and the graininess that excipient is produced is not added
Sucked material different microstructures is presented；It can make molecule gap in granular sucked material more after excipient is added
Add uniformly so that the cigarette sucked material it is final smoke effect it is more uniform, suction effect is more preferable.
3) taking adhesive, smoke agent, the uniform atomized liquid of essence spice for cigarette mixture, using distilled water to atomized liquid
Density is adjusted and adjusts density to 1.1~1.25g/mL, and mixture uniformly, obtains clear atomization after standing filtering under room temperature
Liquid；It is more uniform in order to enable the raw materials such as adhesive, smoke agent and essence spice for cigarette to mix with solid base, facilitate system
Grain, therefore mixing granulation is carried out to above-mentioned raw materials being prepared into atomized liquid being added in wet granulator together with solid base；Mist
The density for changing liquid should control in a certain range, too dense to will affect uniformly mixed, too dilute control that will affect subsequent drying process
System；
4) atomized liquid obtained in the solid base being prepared in step 2 and step 3) is added to the feed bin of wet granulator
In be granulated, the particle after granulation go after drying moisture removal and sieve obtain different grain size size graininess heating it is non-ignitable
Burn cigarette sucked material；
Wherein, in parts by weight, the tobacco material is 50~100 parts, and the excipient is 2~50 parts, described adhesive
It is 2~10 parts, the smoke agent is 5~40 parts, and the essence spice for cigarette is 2~10 parts.
Preferably, tobacco material in the step 1) be natural tobacco, cigarette leaf group raw material, offal, tobacco leaf fragment,
One of offal, cigarette ash, cigarette ash stick or a variety of combinations.
Preferably, the mesh number of the ultra micro tobacco powder is 50~2000 mesh.
Preferably, the excipient in the step 2 is one or more groups of calcium carbonate, bentonite, diatomite
It closes, the excipient is crushed into 100~2000 mesh powders using disintegrating apparatus.
Preferably, the adhesive in the step 3) is water, ethyl alcohol, guar gum, amylan, chitosan, carboxymethyl fibre
Tie up one or more of element, pectin, Arabic gum, sodium alginate, gelatin, glucose, POLYPROPYLENE GLYCOL, fructose, honey etc.
Combination.
Preferably, smoke agent in the step 3) be one of propylene glycol, glycerine, butanediol and triethylene glycol or
A variety of combinations.
Preferably, the obtained solid base in the step 2 further includes 50~100 parts by weight natural plant raw materials,
It is mixed that ultra micro tobacco powder obtained in step 1) is added after Ultra-Micro Grinding Equipment carries out pulverization process in the natural plant raw material
It closes uniform.
Preferably, the natural plant raw material is wild chrysanthemum, dandelion, pueraria lobata, lily, dried orange peel, Jasmine, rose
Combination.
Compared with prior art, the beneficial effects of the present invention are:
The method for heating cigarette sucked material of not burning using wet granulation preparation of the invention, has preparation method simple,
Feature at low cost；The graininess heating for preparing formation simultaneously does not burn cigarette sucked material with flue gas concentration, fragrance, wind
Controllable advantage that lattice feature, taste, puff number are adjustable, with currently on the market used in the heating cigarette that do not burn aspirate material
Material is compared, and has entirely different mode of appearance, provides a kind of completely new suction experience of consumer.
The present invention can reduce the release of harmful substance in aspiration procedure simultaneously, promote the pumping for heating the tobacco product that do not burn
Inhale safety.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention.
Embodiment 1:
A method of cigarette sucked material of not burning is heated using wet granulation preparation, comprising the following steps:
S1: 500g tobacco material is subjected to pulverization process using Ultra-Micro Grinding Equipment, the ultra micro tobacco that granularity is 50 mesh is prepared
Powder；Tobacco material is natural tobacco, cigarette leaf group raw material and combinations thereof；
S2: the ultra micro tobacco powder that will be prepared in S1 step is added the excipient that 20g granularity is 100 mesh and is sufficiently stirred
It is even to obtain solid base；Excipient is one or more combinations of calcium carbonate, bentonite, diatomite,
S3: 20g adhesive, 50g smoke agent, 50g essence spice for cigarette mixture uniformly atomized liquid are taken, is placed in agitator tank and fills
Divide and be uniformly mixed, adds distilled water to adjust density and atomized liquid is prepared to 1.1g/mL, atomized liquid is filtered using 200 mesh filter screens
Obtain clear atomized liquid；Adhesive be water, ethyl alcohol, guar gum, amylan, chitosan, carboxymethyl cellulose, pectin, I
The combination of one or more of primary glue, sodium alginate, gelatin, glucose, POLYPROPYLENE GLYCOL, fructose, honey etc.；Smoke agent is
One of propylene glycol, glycerine, butanediol and triethylene glycol or a variety of combinations；
S4: by the solid base being prepared in S2 step and S3 step to atomized liquid be sufficiently mixed after be added to wet process
It in the feed bin of granulator, is pelletized using wet granulator, particle is passed through through 100 DEG C of dryings, adjusting moisture to 5%~15%
Different meshes sieve is prepared the graininess that partial size is 5~200 mesh and heats cigarette sucked material of not burning after being sieved.
Embodiment 2:
A method of cigarette sucked material of not burning is heated using wet granulation preparation, comprising the following steps:
S1: 1000g tobacco material is subjected to pulverization process using Ultra-Micro Grinding Equipment, the ultra micro that granularity is 2000 mesh is prepared
Tobacco powder；Tobacco material is offal, tobacco leaf fragment and combinations thereof；
S2: the ultra micro tobacco powder that will be prepared in S1 step is added the excipient that 500g granularity is 2000 mesh and is sufficiently stirred
Uniformly obtain solid base；Excipient is one or more combinations of calcium carbonate, bentonite, diatomite；Smoke agent is the third two
One of alcohol, glycerine, butanediol and triethylene glycol or a variety of combinations；
S3: 100g adhesive, 400g smoke agent, 100g essence spice for cigarette mixture uniformly atomized liquid are taken, agitator tank is placed in
In be sufficiently mixed uniformly, add distilled water to adjust density and atomized liquid be prepared to 1.25g/mL, atomized liquid is used into 200 mesh filter screens
Clear atomized liquid is obtained by filtration；Adhesive be water, ethyl alcohol, guar gum, amylan, chitosan, carboxymethyl cellulose, pectin,
The combination of one or more of Arabic gum, sodium alginate, gelatin, glucose, POLYPROPYLENE GLYCOL, fructose, honey etc.；
S4: by the solid base being prepared in S2 step and S3 step to atomized liquid be sufficiently mixed after be added to wet process
It in the feed bin of granulator, is pelletized using wet granulator, particle is passed through through 100 DEG C of dryings, adjusting moisture to 5%~15%
Different meshes sieve is prepared the graininess that partial size is 5~200 mesh and heats cigarette sucked material of not burning after being sieved.
Embodiment 3:
A method of cigarette sucked material of not burning is heated using wet granulation preparation, comprising the following steps:
S1: 750g tobacco material is subjected to pulverization process using Ultra-Micro Grinding Equipment, the ultra micro cigarette that granularity is 1000 mesh is prepared
Grass meal end；Tobacco material is offal, cigarette ash, cigarette ash stick and combinations thereof；
S2: the ultra micro tobacco powder that will be prepared in S1 step is added the excipient that 250g granularity is 1000 mesh and is sufficiently stirred
Uniformly obtain solid base；Excipient is one or more combinations of calcium carbonate, bentonite, diatomite；Smoke agent is the third two
One of alcohol, glycerine, butanediol and triethylene glycol or a variety of combinations；
S3: 80g adhesive, 200g smoke agent, 80g essence spice for cigarette mixture uniformly atomized liquid are taken, is placed in agitator tank
It is sufficiently mixed uniformly, adds distilled water to adjust density and atomized liquid is prepared to 1.2g/mL, atomized liquid is used into 200 mesh filter screen mistakes
Filter obtains clear atomized liquid；Adhesive be water, ethyl alcohol, guar gum, amylan, chitosan, carboxymethyl cellulose, pectin, Ah
Draw the combination of one or more of primary glue, sodium alginate, gelatin, glucose, POLYPROPYLENE GLYCOL, fructose, honey etc.；
S4: by the solid base being prepared in S2 step and S3 step to atomized liquid be sufficiently mixed after be added to wet process
It in the feed bin of granulator, is pelletized using wet granulator, particle is passed through through 100 DEG C of dryings, adjusting moisture to 5%~15%
Different meshes sieve is prepared the graininess that partial size is 5~200 mesh and heats cigarette sucked material of not burning after being sieved.
Embodiment 4:
On the basis of embodiment 1, the natural plants that 500g partial size is 50 mesh be joined when solid base mixes in S2 step
Raw material, the natural plant raw material include the combination of wild chrysanthemum, dandelion, pueraria lobata, lily, dried orange peel, Jasmine, rose.
Embodiment 5:
On the basis of embodiment 2, joined 1000g partial size when solid base mixes in S2 step is that 2000 purposes are naturally planted
Raw material, the natural plant raw material include the combination of wild chrysanthemum, dandelion, pueraria lobata, lily, dried orange peel, Jasmine, rose.
Embodiment 6:
On the basis of embodiment 3, joined 750g partial size when solid base mixes in S2 step is that 1000 purposes are naturally planted
Raw material, the natural plant raw material include the combination of wild chrysanthemum, dandelion, pueraria lobata, lily, dried orange peel, Jasmine, rose.
Embodiment 1,2,3 be using method of the invention and its cigarette that any natural plant raw material is fabricated is not added
With sucked material, embodiment 4,5,6 is respectively that natural plant raw material is added on the basis of embodiment 1,2,3 to use to make cigarette
Sucked material；By in each embodiment carry out Experimental comparison's discovery,
Natural tobacco and cigarette leaf group raw material are used in embodiment 1, taste is purer when suction, has and more preferably takes out
Experience is inhaled, while joined excipient to make sucked material that there is entirely different microstructure, is prepared after joined excipient
It is more uniform into the microscopic particles gap of graininess sucked material, while there is appropriate pore size, finally to aspirate
Flue gas release in material is more uniform, gentle, and suction experience is more preferably；Offal and tobacco leaf fragment are used in embodiment 2 to make
Standby sucked material, suction taste are poor compared with natural tobacco and cigarette leaf group raw material；Offal, cigarette ash, cigarette ash stick are used in embodiment 3
Equal raw materials preparation, suction taste are worst.
But natural plant raw material is increased on the basis of embodiment 4,5,6 is respectively in embodiment 1,2,3, it increases
After natural plant raw material, the smoke smell in sucked material is improved to the maximum extent, makes suction experience more preferably；Such as embodiment
5, although using offal and tobacco leaf fragment, natural plant raw material is increased, the various aromatics objects in natural plant raw material
Matter can change the smoke smell that original offal and tobacco leaf fragment generate, and finally make the smoke smell generated in sucked material more
Excellent, suction is more enjoyed, and experience is more；In embodiment 6, using raw materials such as worst offal, cigarette ash, cigarette ash sticks, add
Suction experience is no different with embodiment 4,5 after having entered natural plant raw material, more save the cost.
On the other hand, the substance in the natural plant raw material in embodiment 4,5,6 is wild chrysanthemum, dandelion, pueraria lobata, hundred
The effect of conjunction, the combination of dried orange peel, Jasmine, rose, wherein wild chrysanthemum has clearing heat and detoxicating, wind-dispelling heat-dissipating；Dandelion has
Diuresis, laxative, removing jaundice subcutaneous ulcer, cholagogue and other effects；Control acute mastitis, adenolymphitis, scrofula, boil poisonous soreness, acute conjunctivitis, sense
Emit fever, acute tonsillitis, acute bronchitis, gastritis, hepatitis, cholecystitis, urinary tract infections and other effects；Pueraria lobata, which has, to be promoted
Liver detoxification function is reinforced in metabolism；Lily has the effect of Yin nourishing and lung moistening, clearing away the heart fire and tranquillizing；Dried orange peel is used for damp retention in middle-jiao, gastral cavity
The diseases such as abdomen swollen ruffian, loose stool diarrhea and many coughs of phlegm；Jasmine has clearing heat and detoxicating, dampness removing effect；Rose not only has spy
Some rose fragrance, additionally it is possible to stomachache due to emotional depression and the hyperactive liver-qi attacking the stomach is cured mainly, new long wandering arthritis, hemoptysis of spitting blood；
By the complex role in above-mentioned raw materials, there can be better cigarette by wild chrysanthemum, dandelion, pueraria lobata, lily compounding
The effect of gas removing toxic substances, can greatly reduce the toxin in sucked material flue gas, substantially reduce smoking bring healthy hidden danger, simultaneously
It is acted on by the fragrance of Jasmine and rose, improves the suction experience in flue gas, improve the flue gas mass in different material.
Although reference be made herein to invention has been described for multiple explanatory embodiments of the invention, however, it is to be understood that
Those skilled in the art can be designed that a lot of other modification and implementations, these modifications and implementations will fall in this Shen
It please be within disclosed scope and spirit.It more specifically, within the scope of the present disclosure and claims, can be to master
The building block and/or layout for inscribing composite configuration carry out a variety of variations and modifications.In addition to what is carried out to building block and/or layout
Outside modification and improvement, to those skilled in the art, other purposes also be will be apparent.
Claims (8)
1. a kind of method for heating cigarette sucked material of not burning using wet granulation preparation, it is characterised in that: including following
Step:
1) tobacco material is subjected to pulverization process using Ultra-Micro Grinding Equipment and ultra micro tobacco powder is prepared；
2) the ultra micro tobacco powder that will be prepared in step 1) is added excipient and stirs to obtain solid base；
3) taking adhesive, smoke agent, the uniform atomized liquid of essence spice for cigarette mixture, using distilled water to the density of atomized liquid
It is adjusted and adjusts density to 1.1~1.25g/mL, mixture uniformly, obtains clear atomized liquid after standing filtering under room temperature；
4) atomized liquid obtained in the solid base being prepared in step 2 and step 3) is added to the feed bin of wet granulator
In be granulated, the particle after granulation go after drying moisture removal and sieve obtain different grain size size graininess heating it is non-ignitable
Burn cigarette sucked material；
Wherein, in parts by weight, the tobacco material is 50~100 parts, and the excipient is 2~50 parts, described adhesive
It is 2~10 parts, the smoke agent is 5~40 parts, and the essence spice for cigarette is 2~10 parts.
2. the method according to claim 1 for heating cigarette sucked material of not burning using wet granulation preparation, special
Sign is: tobacco material in the step 1) be natural tobacco, cigarette leaf group raw material, offal, tobacco leaf fragment, offal, cigarette ash,
One of cigarette ash stick or a variety of combinations.
3. heating cigarette sucked material of not burning using wet granulation preparation described in any one according to claim 1~2
Method, it is characterised in that: the mesh number of the ultra micro tobacco powder be 50~2000 mesh.
4. the method according to claim 1 for heating cigarette sucked material of not burning using wet granulation preparation, special
Sign is: the excipient in the step 2 is one or more combinations of calcium carbonate, bentonite, diatomite, the figuration
Agent is crushed into 100~2000 mesh powders using disintegrating apparatus.
5. the method according to claim 1 for heating cigarette sucked material of not burning using wet granulation preparation, special
Sign is: adhesive in the step 3) be water, ethyl alcohol, guar gum, amylan, chitosan, carboxymethyl cellulose, pectin,
The combination of one or more of Arabic gum, sodium alginate, gelatin, glucose, POLYPROPYLENE GLYCOL, fructose, honey etc..
6. the method according to claim 1 for heating cigarette sucked material of not burning using wet granulation preparation, special
Sign is: the smoke agent in the step 3) is one of propylene glycol, glycerine, butanediol and triethylene glycol or a variety of groups
It closes.
7. the method according to claim 1 for heating cigarette sucked material of not burning using wet granulation preparation, special
Sign is: the obtained solid base in the step 2 further includes 50~100 parts by weight natural plant raw materials, the natural plants
Raw material is added ultra micro tobacco powder obtained in step 1) after Ultra-Micro Grinding Equipment carries out pulverization process and is uniformly mixed.
8. the method according to claim 7 for heating cigarette sucked material of not burning using wet granulation preparation, special
Sign is: the natural plant raw material is the combination of wild chrysanthemum, dandelion, pueraria lobata, lily, dried orange peel, Jasmine, rose.
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| CN201811082538.6A CN108936781B (en) | 2018-09-17 | 2018-09-17 | Method for preparing smoking material for heating non-combustible cigarettes by wet granulation |
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| CN201811082538.6A CN108936781B (en) | 2018-09-17 | 2018-09-17 | Method for preparing smoking material for heating non-combustible cigarettes by wet granulation |
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| CN108936781B CN108936781B (en) | 2021-07-23 |
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Cited By (7)
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| CN110477437A (en) * | 2019-09-25 | 2019-11-22 | 湖北中烟工业有限责任公司 | A kind of electronic cigarette Chinese style flue-cured tobacco odor type solid particle and preparation method thereof |
| CN111329120A (en) * | 2020-04-09 | 2020-06-26 | 上海华宝生物科技有限公司 | Low-temperature heating non-combustible fuming particle and preparation method thereof |
| CN111449271A (en) * | 2020-04-09 | 2020-07-28 | 安徽中烟工业有限责任公司 | Smoke release particle material containing biomass fibers and preparation method thereof |
| CN112890270A (en) * | 2021-03-31 | 2021-06-04 | 云南巴菰生物科技有限公司 | Sweetening granule for heating non-burning cigarette and preparation method thereof |
| CN114027541A (en) * | 2021-11-02 | 2022-02-11 | 江苏大亚滤嘴材料有限公司 | Preparation method of tobacco fragrant granules |
| CN114271534A (en) * | 2021-12-29 | 2022-04-05 | 深圳波顿香料有限公司 | Functional stopper for cigarette without burning under heating and preparation method thereof |
| CN115445578A (en) * | 2022-08-30 | 2022-12-09 | 南京植创生物技术研究院有限公司 | Composite montmorillonite particles for cigarette filter tip and preparation method and application thereof |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110477437A (en) * | 2019-09-25 | 2019-11-22 | 湖北中烟工业有限责任公司 | A kind of electronic cigarette Chinese style flue-cured tobacco odor type solid particle and preparation method thereof |
| CN111329120A (en) * | 2020-04-09 | 2020-06-26 | 上海华宝生物科技有限公司 | Low-temperature heating non-combustible fuming particle and preparation method thereof |
| CN111449271A (en) * | 2020-04-09 | 2020-07-28 | 安徽中烟工业有限责任公司 | Smoke release particle material containing biomass fibers and preparation method thereof |
| CN112890270A (en) * | 2021-03-31 | 2021-06-04 | 云南巴菰生物科技有限公司 | Sweetening granule for heating non-burning cigarette and preparation method thereof |
| CN114027541A (en) * | 2021-11-02 | 2022-02-11 | 江苏大亚滤嘴材料有限公司 | Preparation method of tobacco fragrant granules |
| CN114271534A (en) * | 2021-12-29 | 2022-04-05 | 深圳波顿香料有限公司 | Functional stopper for cigarette without burning under heating and preparation method thereof |
| CN115445578A (en) * | 2022-08-30 | 2022-12-09 | 南京植创生物技术研究院有限公司 | Composite montmorillonite particles for cigarette filter tip and preparation method and application thereof |
| CN115445578B (en) * | 2022-08-30 | 2024-03-01 | 南京植创生物技术研究院有限公司 | Composite montmorillonite particle for cigarette filter tip and preparation method and application thereof |
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| CN108936781B (en) | 2021-07-23 |
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