CN108936782A - The method for heating cigarette sucked material of not burning using dry granulation preparation - Google Patents

The method for heating cigarette sucked material of not burning using dry granulation preparation Download PDF

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Publication number
CN108936782A
CN108936782A CN201811082539.0A CN201811082539A CN108936782A CN 108936782 A CN108936782 A CN 108936782A CN 201811082539 A CN201811082539 A CN 201811082539A CN 108936782 A CN108936782 A CN 108936782A
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China
Prior art keywords
burning
cigarette
tobacco
atomized liquid
dry granulation
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Granted
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CN201811082539.0A
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Chinese (zh)
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CN108936782B (en
Inventor
李锐
周桂园
张文军
魏明文
周潇
李潇逸
尚珂超
周俊
刘王
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China Tobacco Shi Weice (yunnan) Reconstituted Tobacco Co Ltd
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China Tobacco Shi Weice (yunnan) Reconstituted Tobacco Co Ltd
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Publication of CN108936782A publication Critical patent/CN108936782A/en
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/12Steaming, curing, or flavouring tobacco
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/24Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
    • A24B15/26Use of organic solvents for extraction
    • A24F47/004

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)

Abstract

The invention discloses a kind of methods for heating cigarette sucked material of not burning using dry granulation preparation, comprising the following steps: S1: tobacco material being carried out pulverization process using Ultra-Micro Grinding Equipment, ultra micro tobacco powder is prepared;S2: the ultra micro tobacco powder that will be prepared in S1 step is added excipient and stirs to obtain solid base;S3: taking adhesive, smoke agent, the uniform atomized liquid of essence spice for cigarette mixture are adjusted, mixture uniformly, obtains clear atomized liquid after standing filtering under room temperature using density of the distilled water to atomized liquid;S4: by the solid base being prepared in S2 step and S3 step to atomized liquid dry granulating machine is added feed bin in be granulated, the graininess heating that the particle after granulation goes moisture removal and sieving to obtain different grain size size after drying is not burnt cigarette sucked material.The present invention provides a kind of completely newly suction experience of consumer, further promotes the suction safety for heating the tobacco product that do not burn.

Description

The method for heating cigarette sucked material of not burning using dry granulation preparation
Technical field
The present invention relates to tobacco product technical fields, and in particular to a kind of to heat the cigarette that do not burn using dry granulation preparation With the method for sucked material.
Background technique
Under the increasingly severe background of tobacco control environment, the sales volume of conventional tobacco products is in some developed countries and developing country Stagnating, which occurs, in market even to be declined, and quick with the generally raising of people's health consciousness and intelligent microelectronic technology Development, the exploitation of new tobacco products are in eruptive growth.Representative non-traditional tobacco product mainly has heating not in the market Several classes such as burning type tobacco product, smoke-free tobacco product.Heating does not burn cigarette as one kind master in new tobacco products Product is wanted, research and development generally receive the attention of tobacco enterprise.
Current heating does not burn cigarette product due to the limitation of preparation method and the limitation of raw material, in aspiration procedure There is the release of a large amount of harmful substances, be easy to causeing tobacco product suction, there are a large amount of healthy hidden dangers.
Summary of the invention
The purpose of the present invention is to provide a kind of sides that cigarette sucked material of not burning is heated using dry granulation preparation Method, solve current heating do not burn cigarette product suction experience poor, the low problem of flue gas mass.
In order to solve the above technical problems, the invention adopts the following technical scheme:
A method of cigarette sucked material of not burning is heated using dry granulation preparation, comprising the following steps:
S1: 50~100 parts by weight tobacco materials are subjected to pulverization process using Ultra-Micro Grinding Equipment, ultra micro tobacco powder is prepared End;
S2: the ultra micro tobacco powder that will be prepared in S1 step is added 2~50 parts by weight excipient and stirs to obtain Solid base;Excipient is added in this step can make the granular sucked material finally produced and excipient production is not added Different microstructures is presented in granular sucked material out;It can make in granular sucked material after excipient is added Molecule gap is more uniform so that the cigarette sucked material it is final smoke effect it is more uniform, suction effect is more preferable.
S3: 2~10 parts by weight of binder, 5~40 parts by weight smoke agents, 2~10 parts by weight essence spice for cigarette mixtures are taken Uniform atomized liquid, is adjusted using density of the distilled water to atomized liquid, and mixture uniformly, obtains after standing filtering under room temperature Clear atomized liquid;It is more equal in order to enable the raw materials such as adhesive, smoke agent and essence spice for cigarette to mix with solid base It is even, facilitate granulation, therefore mix to above-mentioned raw materials being prepared into atomized liquid being added in dry granulating machine together with solid base Close granulation;The density of atomized liquid should control in a certain range, too it is dense will affect it is uniformly mixed, it is too dilute to will affect subsequent drying The control of process;
S4: the atomized liquid arrived in the solid base being prepared in S2 step and S3 step is added to the feed bin of dry granulating machine In be granulated, the particle after granulation go after drying moisture removal and sieve obtain different grain size size graininess heating it is non-ignitable Burn cigarette sucked material.
Preferably, tobacco material in the S1 step be natural tobacco, cigarette leaf group raw material, offal, tobacco leaf fragment, One of offal, cigarette ash, cigarette ash stick or a variety of combinations.
Preferably, the mesh number of the ultra micro tobacco powder is 50~2000 mesh.
Preferably, the excipient in the S2 step is one or more groups of calcium carbonate, bentonite, diatomite It closes, the excipient is crushed into 100~2000 mesh powders using disintegrating apparatus.
Preferably, the adhesive in the S3 step is water, ethyl alcohol, guar gum, amylan, chitosan, carboxymethyl fibre Tie up one or more of element, pectin, Arabic gum, sodium alginate, gelatin, glucose, POLYPROPYLENE GLYCOL, fructose, honey etc. Combination.
Preferably, smoke agent in the S3 step be one of propylene glycol, glycerine, butanediol and triethylene glycol or A variety of combinations.
Preferably, the density of atomized liquid is 1.1~1.25 g/mL in the S3 step.
Preferably, the obtained solid base in the S2 step further includes 50~100 parts by weight natural plant raw materials, It is mixed that ultra micro tobacco powder obtained in S1 step is added after Ultra-Micro Grinding Equipment carries out pulverization process in the natural plant raw material It closes uniform.
Preferably, the natural plant raw material is wild chrysanthemum, dandelion, pueraria lobata, lily, dried orange peel, Jasmine, rose Combination.
Compared with prior art, the beneficial effects of the present invention are:
The method for heating cigarette sucked material of not burning using dry granulation preparation of the invention, has preparation method simple, Feature at low cost;The graininess heating for preparing formation simultaneously does not burn cigarette sucked material with flue gas concentration, fragrance, wind Controllable advantage that lattice feature, taste, puff number are adjustable, with currently on the market used in the heating cigarette that do not burn aspirate material Material is compared, and has entirely different mode of appearance, provides a kind of completely new suction experience of consumer.
The present invention can reduce the release of harmful substance in aspiration procedure simultaneously, promote the pumping for heating the tobacco product that do not burn Inhale safety.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to embodiments, to the present invention It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to Limit the present invention.
Embodiment 1:
A method of cigarette sucked material of not burning is heated using dry granulation preparation, comprising the following steps:
S1: 500g tobacco material is subjected to pulverization process using Ultra-Micro Grinding Equipment, the ultra micro tobacco that granularity is 50 mesh is prepared Powder;Tobacco material is natural tobacco, cigarette leaf group raw material and combinations thereof;
S2: the ultra micro tobacco powder that will be prepared in S1 step is added the excipient that 20g granularity is 100 mesh and is sufficiently stirred It is even to obtain solid base;Excipient is one or more combinations of calcium carbonate, bentonite, diatomite,
S3: 20g adhesive, 50g smoke agent, 50g essence spice for cigarette mixture uniformly atomized liquid are taken, is placed in agitator tank and fills Divide and be uniformly mixed, adds distilled water to adjust density and atomized liquid is prepared to 1.1g/mL, atomized liquid is filtered using 200 mesh filter screens Obtain clear atomized liquid;Adhesive be water, ethyl alcohol, guar gum, amylan, chitosan, carboxymethyl cellulose, pectin, I The combination of one or more of primary glue, sodium alginate, gelatin, glucose, POLYPROPYLENE GLYCOL, fructose, honey etc.;Smoke agent is One of propylene glycol, glycerine, butanediol and triethylene glycol or a variety of combinations;
S4: by the solid base being prepared in S2 step and S3 step to atomized liquid be sufficiently mixed after be added to dry method It in the feed bin of granulator, is pelletized using dry granulating machine, particle is passed through through 100 DEG C of dryings, adjusting moisture to 5%~15% Different meshes sieve is prepared the graininess that partial size is 5~200 mesh and heats cigarette sucked material of not burning after being sieved.
Embodiment 2:
A method of cigarette sucked material of not burning is heated using dry granulation preparation, comprising the following steps:
S1: 1000g tobacco material is subjected to pulverization process using Ultra-Micro Grinding Equipment, the ultra micro that granularity is 2000 mesh is prepared Tobacco powder;Tobacco material is offal, tobacco leaf fragment and combinations thereof;
S2: the ultra micro tobacco powder that will be prepared in S1 step is added the excipient that 500g granularity is 2000 mesh and is sufficiently stirred Uniformly obtain solid base;Excipient is one or more combinations of calcium carbonate, bentonite, diatomite;Smoke agent is the third two One of alcohol, glycerine, butanediol and triethylene glycol or a variety of combinations;
S3: 100g adhesive, 400g smoke agent, 100g essence spice for cigarette mixture uniformly atomized liquid are taken, agitator tank is placed in In be sufficiently mixed uniformly, add distilled water to adjust density and atomized liquid be prepared to 1.25g/mL, atomized liquid is used into 200 mesh filter screens Clear atomized liquid is obtained by filtration;Adhesive be water, ethyl alcohol, guar gum, amylan, chitosan, carboxymethyl cellulose, pectin, The combination of one or more of Arabic gum, sodium alginate, gelatin, glucose, POLYPROPYLENE GLYCOL, fructose, honey etc.;
S4: by the solid base being prepared in S2 step and S3 step to atomized liquid be sufficiently mixed after be added to dry method It in the feed bin of granulator, is pelletized using dry granulating machine, particle is passed through through 100 DEG C of dryings, adjusting moisture to 5%~15% Different meshes sieve is prepared the graininess that partial size is 5~200 mesh and heats cigarette sucked material of not burning after being sieved.
Embodiment 3:
A method of cigarette sucked material of not burning is heated using dry granulation preparation, comprising the following steps:
S1: 750g tobacco material is subjected to pulverization process using Ultra-Micro Grinding Equipment, the ultra micro cigarette that granularity is 1000 mesh is prepared Grass meal end;Tobacco material is offal, cigarette ash, cigarette ash stick and combinations thereof;
S2: the ultra micro tobacco powder that will be prepared in S1 step is added the excipient that 250g granularity is 1000 mesh and is sufficiently stirred Uniformly obtain solid base;Excipient is one or more combinations of calcium carbonate, bentonite, diatomite;Smoke agent is the third two One of alcohol, glycerine, butanediol and triethylene glycol or a variety of combinations;
S3: 80g adhesive, 200g smoke agent, 80g essence spice for cigarette mixture uniformly atomized liquid are taken, is placed in agitator tank It is sufficiently mixed uniformly, adds distilled water to adjust density and atomized liquid is prepared to 1.2g/mL, atomized liquid is used into 200 mesh filter screen mistakes Filter obtains clear atomized liquid;Adhesive be water, ethyl alcohol, guar gum, amylan, chitosan, carboxymethyl cellulose, pectin, Ah Draw the combination of one or more of primary glue, sodium alginate, gelatin, glucose, POLYPROPYLENE GLYCOL, fructose, honey etc.;
S4: by the solid base being prepared in S2 step and S3 step to atomized liquid be sufficiently mixed after be added to dry method It in the feed bin of granulator, is pelletized using dry granulating machine, particle is passed through through 100 DEG C of dryings, adjusting moisture to 5%~15% Different meshes sieve is prepared the graininess that partial size is 5~200 mesh and heats cigarette sucked material of not burning after being sieved.
Embodiment 4:
On the basis of embodiment 1, the natural plants that 500g partial size is 50 mesh be joined when solid base mixes in S2 step Raw material, the natural plant raw material include the combination of wild chrysanthemum, dandelion, pueraria lobata, lily, dried orange peel, Jasmine, rose.
Embodiment 5:
On the basis of embodiment 2, joined 1000g partial size when solid base mixes in S2 step is that 2000 purposes are naturally planted Raw material, the natural plant raw material include the combination of wild chrysanthemum, dandelion, pueraria lobata, lily, dried orange peel, Jasmine, rose.
Embodiment 6:
On the basis of embodiment 3, joined 750g partial size when solid base mixes in S2 step is that 1000 purposes are naturally planted Raw material, the natural plant raw material include the combination of wild chrysanthemum, dandelion, pueraria lobata, lily, dried orange peel, Jasmine, rose.
Embodiment 1,2,3 be using method of the invention and its cigarette that any natural plant raw material is fabricated is not added With sucked material, embodiment 4,5,6 is respectively that natural plant raw material is added on the basis of embodiment 1,2,3 to use to make cigarette Sucked material;By in each embodiment carry out Experimental comparison's discovery,
Natural tobacco and cigarette leaf group raw material are used in embodiment 1, taste is purer when suction, has and more preferably takes out Experience is inhaled, while joined excipient to make sucked material that there is entirely different microstructure, is prepared after joined excipient It is more uniform into the microscopic particles gap of graininess sucked material, while there is appropriate pore size, finally to aspirate Flue gas release in material is more uniform, gentle, and suction experience is more preferably;Offal and tobacco leaf fragment are used in embodiment 2 to make Standby sucked material, suction taste are poor compared with natural tobacco and cigarette leaf group raw material;Offal, cigarette ash, cigarette ash stick are used in embodiment 3 Equal raw materials preparation, suction taste are worst.
But natural plant raw material is increased on the basis of embodiment 4,5,6 is respectively in embodiment 1,2,3, it increases After natural plant raw material, the smoke smell in sucked material is improved to the maximum extent, makes suction experience more preferably;Such as embodiment 5, although using offal and tobacco leaf fragment, natural plant raw material is increased, the various aromatics objects in natural plant raw material Matter can change the smoke smell that original offal and tobacco leaf fragment generate, and finally make the smoke smell generated in sucked material more Excellent, suction is more enjoyed, and experience is more;In embodiment 6, using raw materials such as worst offal, cigarette ash, cigarette ash sticks, add Suction experience is no different with embodiment 4,5 after having entered natural plant raw material, more save the cost.
On the other hand, the substance in the natural plant raw material in embodiment 4,5,6 is wild chrysanthemum, dandelion, pueraria lobata, hundred The effect of conjunction, the combination of dried orange peel, Jasmine, rose, wherein wild chrysanthemum has clearing heat and detoxicating, wind-dispelling heat-dissipating;Dandelion has Diuresis, laxative, removing jaundice subcutaneous ulcer, cholagogue and other effects;Control acute mastitis, adenolymphitis, scrofula, boil poisonous soreness, acute conjunctivitis, sense Emit fever, acute tonsillitis, acute bronchitis, gastritis, hepatitis, cholecystitis, urinary tract infections and other effects;Pueraria lobata, which has, to be promoted Liver detoxification function is reinforced in metabolism;Lily has the effect of Yin nourishing and lung moistening, clearing away the heart fire and tranquillizing;Dried orange peel is used for damp retention in middle-jiao, gastral cavity The diseases such as abdomen swollen ruffian, loose stool diarrhea and many coughs of phlegm;Jasmine has clearing heat and detoxicating, dampness removing effect;Rose not only has spy Some rose fragrance, additionally it is possible to stomachache due to emotional depression and the hyperactive liver-qi attacking the stomach is cured mainly, new long wandering arthritis, hemoptysis of spitting blood;
By the complex role in above-mentioned raw materials, there can be better cigarette by wild chrysanthemum, dandelion, pueraria lobata, lily compounding The effect of gas removing toxic substances, can greatly reduce the toxin in sucked material flue gas, substantially reduce smoking bring healthy hidden danger, simultaneously It is acted on by the fragrance of Jasmine and rose, improves the suction experience in flue gas, improve the flue gas mass in different material.
Although reference be made herein to invention has been described for multiple explanatory embodiments of the invention, however, it is to be understood that Those skilled in the art can be designed that a lot of other modification and implementations, these modifications and implementations will fall in this Shen It please be within disclosed scope and spirit.It more specifically, within the scope of the present disclosure and claims, can be to master The building block and/or layout for inscribing composite configuration carry out a variety of variations and modifications.In addition to what is carried out to building block and/or layout Outside modification and improvement, to those skilled in the art, other purposes also be will be apparent.

Claims (9)

1. a kind of method for heating cigarette sucked material of not burning using dry granulation preparation, it is characterised in that: including following Step:
S1: 50~100 parts by weight tobacco materials are subjected to pulverization process using Ultra-Micro Grinding Equipment, ultra micro tobacco powder is prepared End;
S2: the ultra micro tobacco powder that will be prepared in S1 step is added 2~50 parts by weight excipient and stirs to obtain Solid base;
S3: 2~10 parts by weight of binder, 5~40 parts by weight smoke agents, 2~10 parts by weight essence spice for cigarette mixtures are taken uniformly Atomized liquid is adjusted using density of the distilled water to atomized liquid, and mixture uniformly, is clarified after standing filtering under room temperature Atomized liquid;
S4: atomized liquid obtained in the solid base being prepared in S2 step and S3 step is added to the feed bin of dry granulating machine In be granulated, the particle after granulation go after drying moisture removal and sieve obtain different grain size size graininess heating it is non-ignitable Burn cigarette sucked material.
2. the method according to claim 1 for heating cigarette sucked material of not burning using dry granulation preparation, special Sign is: tobacco material in the S1 step be natural tobacco, cigarette leaf group raw material, offal, tobacco leaf fragment, offal, cigarette ash, One of cigarette ash stick or a variety of combinations.
3. heating cigarette sucked material of not burning using dry granulation preparation described in any one according to claim 1~2 Method, it is characterised in that: the mesh number of the ultra micro tobacco powder be 50~2000 mesh.
4. the method according to claim 1 for heating cigarette sucked material of not burning using dry granulation preparation, special Sign is: the excipient in the S2 step is one or more combinations of calcium carbonate, bentonite, diatomite, the figuration Agent is crushed into 100~2000 mesh powders using disintegrating apparatus.
5. the method according to claim 1 for heating cigarette sucked material of not burning using dry granulation preparation, special Sign is: adhesive in the S3 step be water, ethyl alcohol, guar gum, amylan, chitosan, carboxymethyl cellulose, pectin, The combination of one or more of Arabic gum, sodium alginate, gelatin, glucose, POLYPROPYLENE GLYCOL, fructose, honey etc..
6. the method according to claim 1 for heating cigarette sucked material of not burning using dry granulation preparation, special Sign is: the smoke agent in the S3 step is one of propylene glycol, glycerine, butanediol and triethylene glycol or a variety of groups It closes.
7. the method according to claim 1 for heating cigarette sucked material of not burning using dry granulation preparation, special Sign is: the density of atomized liquid is 1.1~1.25g/mL in the S3 step.
8. the method according to claim 1 for heating cigarette sucked material of not burning using dry granulation preparation, special Sign is: the obtained solid base in the S2 step further includes 50~100 parts by weight natural plant raw materials, the natural plants Raw material is added ultra micro tobacco powder obtained in S1 step after Ultra-Micro Grinding Equipment carries out pulverization process and is uniformly mixed.
9. the method according to claim 8 for heating cigarette sucked material of not burning using dry granulation preparation, special Sign is: the natural plant raw material is the combination of wild chrysanthemum, dandelion, pueraria lobata, lily, dried orange peel, Jasmine, rose.
CN201811082539.0A 2018-09-17 2018-09-17 Method for preparing smoking material for heating non-combustible cigarettes by dry granulation Active CN108936782B (en)

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CN112890270A (en) * 2021-03-31 2021-06-04 云南巴菰生物科技有限公司 Sweetening granule for heating non-burning cigarette and preparation method thereof
CN115445578A (en) * 2022-08-30 2022-12-09 南京植创生物技术研究院有限公司 Composite montmorillonite particles for cigarette filter tip and preparation method and application thereof

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CN112890270A (en) * 2021-03-31 2021-06-04 云南巴菰生物科技有限公司 Sweetening granule for heating non-burning cigarette and preparation method thereof
CN115445578A (en) * 2022-08-30 2022-12-09 南京植创生物技术研究院有限公司 Composite montmorillonite particles for cigarette filter tip and preparation method and application thereof
CN115445578B (en) * 2022-08-30 2024-03-01 南京植创生物技术研究院有限公司 Composite montmorillonite particle for cigarette filter tip and preparation method and application thereof

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