CN109938399B - Low-temperature non-combustible cigarette tobacco tar carrier - Google Patents
Low-temperature non-combustible cigarette tobacco tar carrier Download PDFInfo
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- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 2
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- HFHDHCJBZVLPGP-UHFFFAOYSA-N schardinger α-dextrin Chemical compound O1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2CO HFHDHCJBZVLPGP-UHFFFAOYSA-N 0.000 description 1
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- Manufacture Of Tobacco Products (AREA)
Abstract
The invention provides a low-temperature non-combustible cigarette tobacco tar carrier, which comprises a plant fiber adsorption carrier mainly adsorbing tobacco tar extracts and an inorganic material adsorption carrier mainly adsorbing plant essence, wherein the plant fiber adsorption carrier and the inorganic adsorption carrier form a core-shell structure. The tobacco tar carrier provided by the invention uses the core-shell structure of the plant fiber/inorganic porous material to respectively adsorb tobacco tar components with different viscosities, and replaces the current mode of directly using a tobacco filling material, so that the uniformity of the volatile taste of the tobacco tar is effectively improved.
Description
Technical Field
The invention belongs to the field of daily electronic products, and particularly relates to a low-temperature non-combustible cigarette tobacco tar carrier.
Background
Electronic cigarettes have the characteristics of being free of tar and free of harmful suspended particles, and have gradually become a new tobacco development direction for replacing smoking of traditional cigarettes, wherein low-temperature flue-cured tobacco hardly generates harmful substances by baking tobacco extracts at a temperature lower than the burning point of tobacco, and the taste of the electronic cigarettes is closer to that of traditional tobacco. At present, low-temperature non-combustion cigarette products in the market mainly utilize tobacco flakes filled in a special electric heating device and used for adsorbing tobacco extracts and other essence components, smoke in tobacco filling materials is volatilized through electric heating, and therefore smokers can obtain smoking feeling similar to that of traditional tobaccos. However, the electric heating in the prior art is peripheral heating basically, the heating speed is low, the heating is not uniform, the time for generating smoke is long, and the uniformity of the smoke concentration is poor; meanwhile, the tobacco material is troublesome to remove after being filled and sucked, so that the user experience is seriously influenced.
Patent CN 105815815 a discloses a low-temperature smoke generator, which comprises a carrier and a tobacco extract adsorbed on the carrier; the carrier consists of a plant adsorbing material, a heat conducting component and a binder; the mass ratio of the plant adsorbing material to the tobacco extract in the low-temperature fuming body is not more than 1: 1. On the basis of the structural components of the smoke body, the patent CN 105661651A increases the adsorption and the use of plant essence: the mass ratio of the tobacco extract to the plant essence is 100: 1-20. The tobacco extract and the plant essence are absorbed by mixing, adhering, molding and overall soaking. However, in the actual operation process, the components in the tobacco extract and the plant essence are complex, the time for the components with different viscosities to diffuse into the mixed smoke body is different, and similarly, in the actual working process of heating the smoke body, on one hand, because the components and the structure of the smoke body limit that most of the heat conduction components are not contacted together, the thermal resistance of the plant fiber in the gap area is still very large, and the improvement effect is limited; on the other hand, the components of tobacco tar molecules with different molecular weights and polarities are locally changed in the soaking process, the tobacco tar molecules with small molecular weights and low viscosities volatilize firstly after being heated, and the tobacco tar molecules with large molecular weights and high viscosities volatilize, so that the components of smoke can not always keep uniform mouthfeel in the temperature rising-stabilizing-reducing process.
Therefore, how to find a novel low-temperature non-combustion cigarette tobacco tar carrier and ensure good taste uniformity is a technical problem to be solved urgently in the technical field of electronic cigarettes.
Disclosure of Invention
In view of the above, the invention aims to provide a low-temperature non-combustible cigarette tobacco tar carrier, which uses a core-shell structure of plant fiber/inorganic porous material to respectively adsorb tobacco tar components with different viscosities, so as to replace the current mode of directly using a tobacco filling material, and effectively improve the uniformity of volatile taste of tobacco tar.
In order to achieve the purpose, the technical scheme of the invention is realized as follows:
a low-temperature non-combustible cigarette tobacco tar carrier comprises a plant fiber adsorption carrier mainly adsorbing tobacco tar extracts and an inorganic material adsorption carrier mainly adsorbing plant essence, wherein the plant fiber adsorption carrier and the inorganic adsorption carrier form a core-shell structure.
Further, the mass ratio of the tobacco tar extract to the plant fiber adsorption carrier is 1: (5-10).
Further, the mass ratio of the plant essence to the inorganic material adsorption carrier is 1: (3-25).
Furthermore, the apparent volume of the plant fiber adsorption carrier is 300-600mL/g, the specific surface area is not less than 100 square meters per gram, and the particle size is 20-300 μm.
Further, the plant fiber adsorption carrier is one or a mixture of several of dry apple pomace, wheat straw, dry orange peel, dry banana peel, corn cob, corn stalk, rice hull, barley hull, wood chips, palm fruit branches, sawdust, bark, leaves, coconut shell fiber, banana pith and bagasse pith.
Furthermore, the inorganic material adsorption carrier has an apparent volume of 50-300mL/g, a specific surface area of not more than 100 square meters per gram and a particle size of 5-20 μm.
Further, the inorganic adsorption carrier is one or a mixture of more of kaolinite, montmorillonite, bentonite, vermiculite, sepiolite, activated carbon, zeolite, hydrotalcite, diatomite, alumina and porous silica.
Further, the diameter of the low-temperature non-combustible cigarette tobacco tar carrier is 100-1500 mu m.
Further, the invention also provides a preparation method of the low-temperature non-combustible cigarette tobacco tar carrier, which comprises the following steps:
(1) stirring and uniformly mixing the plant essence and the inorganic material adsorption carrier, adding a plant adhesive, and granulating to obtain a sphere core pre-adsorption carrier;
(2) soaking the plant fiber in the tobacco tar extract, stirring and uniformly mixing to obtain the plant fiber which adsorbs the tobacco tar extract;
(3) adding the spherical core pre-adsorption carrier into the plant fiber which has adsorbed the tobacco tar extract, adding the plant adhesive, granulating and drying to obtain the spherical tobacco tar carrier with the one-shell multi-core-shell structure.
Further, the diameter of the sphere core pre-adsorption carrier is 1/20-1/5 of the diameter of the whole sphere tobacco tar carrier.
Further, the mass ratio of the plant essence to the plant adhesive in the step (1) is 1: (3-6). The plant adhesive can be one or more of white latex for cigarette, pregelatinized modified starch, cyclodextrin, chitosan, and hot melt adhesive.
Compared with the prior art, the invention adopts the inorganic material adsorption carrier and the core/shell structure carrier forming the plant fiber adsorption carrier, wherein the inorganic material adsorption carrier with small specific surface and apparent volume can effectively and uniformly adsorb plant essence or other components with low small molecular weight and low viscosity, and the plant fiber adsorption carrier with large specific surface and apparent volume can effectively and uniformly adsorb tobacco tar extract components with high molecular weight and high viscosity, thereby reducing the problem of uneven adsorption caused by viscosity difference and improving the overall effective adsorption capacity of the adsorption carrier.
In addition, the smoke body generally adopts the outer wall heating mode in the heating process, causes the inside and outside difference in temperature of the adsorption carrier, and the conventional mixing mode leads to that partial small molecular weight tobacco tar component volatilizes relatively fast in the stage of rising temperature and cooling, leads to that the difference is big around the taste of the smoke, adopts the separation adsorption mode, and the large molecular weight tobacco tar temperature that volatilizes slowly is high, and the essence temperature of small molecular weight is low, can effectively reconcile different molecular weights like this and cause the difference problem of volatilization speed, effectively guarantees the taste of the smoke when the cigarette bullet works.
Detailed Description
Unless defined otherwise, technical terms used in the following examples have the same meanings as commonly understood by one of ordinary skill in the art to which the present invention belongs. The test reagents used in the following examples, unless otherwise specified, are all conventional biochemical reagents; the experimental methods are conventional methods unless otherwise specified.
The present invention will be described in detail with reference to examples.
Example 1
Mixing porous silica gel, white silica gel for cigarettes and plant essence according to the weight ratio of 20: 4.5: 1, wherein the apparent volume of the porous silica gel is 300mL/g, the specific surface area is 90 square meters per gram, and the particle size is 15 mu m. The method comprises the steps of pre-adjusting the water content of rice hull powder to 10%, carrying out microwave disinfection and sterilization treatment for 60s, and adjusting the water content to about 5%, wherein the apparent volume of the rice hull powder is 400mL/g, the specific surface area is 150 square meter/g, and the particle size is 150 mu m; and then soaking the mixture in the tobacco tar extract for 15min, taking out the mixture and draining the mixture, then adding the spherical core pre-adsorption porous silica gel into the rice hull powder fiber which adsorbs the tobacco tar extract, and carrying out vacuum granulation to obtain the tobacco tar carrier with a one-shell and multi-core-shell structure. And finally, filling the tobacco tar carrier with the core-shell structure into a paper cigarette cartridge, and hermetically packaging by adopting a BOPP film. The smoking body wrapper is removed, and the smoking body wrapper can be directly plugged into the smoking set heating cavity for smoking, the smoking speed is high during smoking, the smoking is smooth, the taste is uniform, the waste material is still in a whole block shape after smoking is completed, the smoking set can be easily taken out, and the smoking set is less in pollution and is easy to clean.
Example 2
Mixing activated carbon, white latex for cigarettes and plant essence according to the weight ratio of 22: 5: 1, wherein the apparent volume of the activated carbon is 100mL/g, the specific surface area is 100 square meters per gram, and the particle size is 10 mu m. Pre-adjusting the moisture of coconut powder to 10%, performing microwave disinfection and sterilization treatment for 60s, and adjusting the moisture to about 5%, wherein the apparent volume of the coconut powder is 450mL/g, the specific surface area is 100 square meters per gram, and the particle size is 250 μm; and then soaking the mixture in the tobacco tar extract for 15min, taking out and draining, then adding the sphere core pre-adsorption activated carbon into the coconut powder fiber which adsorbs the tobacco tar extract, and carrying out vacuum granulation to obtain the tobacco tar carrier with the core-shell structure with one shell and multiple cores. And finally, filling the tobacco tar carrier with the core-shell structure into a paper cigarette cartridge, and hermetically packaging by adopting a BOPP film. The smoking body wrapper is removed, and the smoking body wrapper can be directly plugged into the smoking set heating cavity for smoking, the smoking speed is high during smoking, the smoking is smooth, the taste is uniform, the waste material is still in a whole block shape after smoking is completed, the smoking set can be easily taken out, and the smoking set is less in pollution and is easy to clean.
Example 3
Mixing hydrotalcite, gelatinized starch and plant essence according to a weight ratio of 10: 2.5: 1, vacuum mixing and granulating, wherein the apparent volume of the hydrotalcite is 50mL/g, the specific surface area is 50 square meters per gram, and the particle size is 15 mu m. Pre-adjusting the water content of the corn stalk powder to 10 percent, adopting microwave disinfection and sterilization for 60s, and adjusting the water content to about 5 percent, wherein the apparent volume of the corn stalk powder is 250mL/g, the specific surface area is 150 square meters/g, and the particle size is 120 mu m; and then soaking the core-shell structure tobacco tar carrier in the tobacco tar extract for 15min, taking out and draining, then adding the spherical core-shaped pre-adsorption hydrotalcite into the corn stalk fiber which has adsorbed the tobacco tar extract, and carrying out vacuum granulation to obtain the core-shell structure tobacco tar carrier with one shell and multiple cores. And finally, filling the tobacco tar carrier with the core-shell structure into a paper cigarette cartridge, and hermetically packaging by adopting a BOPP film. The smoking body wrapper is removed, and the smoking body wrapper can be directly plugged into the smoking set heating cavity for smoking, the smoking speed is high during smoking, the smoking is smooth, the taste is uniform, the waste material is still in a whole block shape after smoking is completed, the smoking set can be easily taken out, and the smoking set is less in pollution and is easy to clean.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (6)
1. The low-temperature non-combustible cigarette tobacco tar carrier is characterized in that: the tobacco tar adsorption carrier comprises a plant fiber adsorption carrier mainly used for adsorbing tobacco tar extracts and an inorganic material adsorption carrier mainly used for adsorbing plant essence, wherein the plant fiber adsorption carrier and the inorganic adsorption carrier form a core-shell structure;
the mass ratio of the tobacco tar extract to the plant fiber adsorption carrier is 1: (5-10);
the apparent volume of the plant fiber adsorption carrier is 300-600mL/g, the specific surface area is not less than 100 square meters per gram, and the particle size is 20-300 mu m;
the apparent volume of the inorganic material adsorption carrier is 50-300mL/g, the specific surface area is not more than 100 square meters per gram, and the particle size is 5-20 mu m;
the preparation method of the tobacco tar carrier comprises the following steps:
(1) stirring and uniformly mixing the plant essence and the inorganic material adsorption carrier, adding a plant adhesive, and granulating to obtain a sphere core pre-adsorption carrier;
(2) soaking the plant fiber in the tobacco tar extract, stirring and uniformly mixing to obtain the plant fiber which adsorbs the tobacco tar extract;
(3) adding the spherical core pre-adsorption carrier into the plant fiber which has adsorbed the tobacco tar extract, adding the plant adhesive, granulating and drying to obtain the spherical tobacco tar carrier with the one-shell multi-core-shell structure.
2. The low temperature non-combustible cigarette liquid carrier of claim 1, wherein: in the step (1), the diameter of the sphere core pre-adsorption carrier is 1/20-1/5 of the diameter of the whole sphere tobacco tar carrier, and the mass ratio of the plant essence to the plant adhesive is 1: (3-6).
3. The low temperature non-combustible cigarette liquid carrier of claim 1, wherein: the mass ratio of the plant essence to the inorganic material adsorption carrier is 1: (3-25).
4. The low temperature non-combustible cigarette liquid carrier of claim 1, wherein: the plant fiber adsorption carrier is one or a mixture of several of dry apple pomace, wheat straw, dry orange peel, dry banana peel, corn cob, corn stalk, rice hull, barley husk, wood chips, palm fruit branches, sawdust, bark, leaves, coconut shell fiber, banana pith and bagasse pith.
5. The low temperature non-combustible cigarette liquid carrier of claim 1, wherein: the inorganic adsorption carrier is one or a mixture of more of kaolinite, montmorillonite, bentonite, vermiculite, sepiolite, activated carbon, zeolite, hydrotalcite, diatomite, alumina and porous silica.
6. The low temperature non-combustible cigarette liquid carrier of claim 1, wherein: the diameter of the low-temperature non-combustible cigarette tobacco tar carrier is 100-1500 mu m.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910226599.3A CN109938399B (en) | 2019-03-25 | 2019-03-25 | Low-temperature non-combustible cigarette tobacco tar carrier |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910226599.3A CN109938399B (en) | 2019-03-25 | 2019-03-25 | Low-temperature non-combustible cigarette tobacco tar carrier |
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| CN109938399A CN109938399A (en) | 2019-06-28 |
| CN109938399B true CN109938399B (en) | 2021-12-21 |
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| KR102402062B1 (en) * | 2020-01-03 | 2022-05-24 | 주식회사 케이티앤지 | A smoking material wrapper with grain husk and a smoking article including the same, and manufacturing method of the smoking article |
| CN111011915B (en) * | 2020-01-06 | 2022-04-29 | 江苏中烟工业有限责任公司 | Cigarette core column suitable for heating cigarettes and preparation method thereof |
| CN113229521A (en) * | 2021-06-23 | 2021-08-10 | 张家港外星人新材料科技有限公司 | Electronic atomized liquid composition and packaging container thereof |
| CN114557476A (en) * | 2022-03-30 | 2022-05-31 | 湖北中烟工业有限责任公司 | Cigarette blasting bead capable of giving off blasting sound and cigarette containing same |
| CN115627058B (en) * | 2022-10-24 | 2023-07-18 | 湖北中烟工业有限责任公司 | High-void-ratio fiber composite material for flavoring pipe and preparation method thereof |
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2019
- 2019-03-25 CN CN201910226599.3A patent/CN109938399B/en not_active Expired - Fee Related
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|---|---|---|---|---|
| US7815878B1 (en) * | 2006-08-29 | 2010-10-19 | American Covers, Inc. | Aromatherapy puffer ball |
| CN106993824A (en) * | 2016-01-25 | 2017-08-01 | 上海翰淼新材料科技有限公司 | Anti-oxidant slow-releasing granules preparation method |
| CN105815815A (en) * | 2016-04-15 | 2016-08-03 | 湖南中烟工业有限责任公司 | Low-temperature smoke formation body |
| CN109419043A (en) * | 2017-09-04 | 2019-03-05 | 湖南中烟工业有限责任公司 | It is a kind of for heating the sucked material for the tobacco product that do not burn |
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| CN109938399A (en) | 2019-06-28 |
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