CN105661651B - A kind of flavored type low temperature fuming liquids - Google Patents

A kind of flavored type low temperature fuming liquids Download PDF

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Publication number
CN105661651B
CN105661651B CN201610232921.XA CN201610232921A CN105661651B CN 105661651 B CN105661651 B CN 105661651B CN 201610232921 A CN201610232921 A CN 201610232921A CN 105661651 B CN105661651 B CN 105661651B
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low temperature
fuming liquids
plant
extract
temperature fuming
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CN105661651A (en
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陈潜
金勇�
李克
杜文
黄平
谭新良
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China Tobacco Hunan Industrial Co Ltd
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China Tobacco Hunan Industrial Co Ltd
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F47/00Smokers' requisites not otherwise provided for
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/12Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Disinfection, Sterilisation Or Deodorisation Of Air (AREA)

Abstract

The invention discloses a kind of flavored type low temperature fuming liquids, flavored type low temperature fuming liquids include carrier and the tobacco extract and plant essence that are adsorbed on carrier;The mass ratio of the tobacco extract and plant essence is 100:1-20;The carrier is made of plant absorptive material, thermally conductive component and binder;The mass ratio of plant absorptive material and tobacco extract in the low temperature fuming liquids is no more than 1:1.Flavored type low temperature fuming liquids provided by the invention according to the molding of smoking set heating chamber size, absorption tobacco tar and sealed package, can be stored without influencing to suck impression, while being easy to add and remove for a long time;There are a large amount of holes in flavored type low temperature fuming liquids short texture, inside, and suction easily, while can be improved the heating surface area of sucked material and being heated evenly property, can give the good satisfaction of consumer;Low in raw material price, safety and environmental protection are suitable as one-time consumption product simultaneously.

Description

A kind of flavored type low temperature fuming liquids
Technical field
The present invention relates to a kind of flavored type low temperature fuming liquids, belong to electronic cigarette technical field.
Background technique
In conventional cigarette, there are tens of kinds of carcinogens in the smog of result of combustion of tobacco, and it is full of smoke in air The bigger secondhand smoke of harmfulness is formed, larger Health cost will cause to surrounding population while polluting environment.
There is a kind of smokeless cigarette system, by cigarette in pursuit with scientific and technological progress and people to healthy living Equal solids smoke object is toasted to generate smog, does not need to burn.Currently, low temperature in the market does not burn, cigarette product is main It is that tobacco filler is made by electric heating using tobacco-containing material such as cigarette, pipe tobacco or smoked sheet etc. is filled in special electric heater unit Flue gas in material evaporates, so that smoker be made to obtain the suction impression for being similar to traditional tobacco.However the prior art Electric heating is substantially peripheral heating, and heating speed is slow and heating is uneven, and the time for generating smog is longer and concentration is insufficient;Together When tobacco-containing material filling and remove after sucking it is pretty troublesome, to seriously affect user experience.
Summary of the invention
Present invention solves the technical problem that being, tobacco extract is liquid, when sucking, takes inconvenience;When heating, it is heated not Uniformly.
The technical scheme is that providing a kind of flavored type low temperature fuming liquids, including carrier and it is adsorbed on carrier Tobacco extract and plant essence;The mass ratio of the tobacco extract and plant essence is 100:1-20;The carrier is by planting Object adsorbent material, thermally conductive component and binder composition;Plant absorptive material and tobacco extract in the low temperature fuming liquids Mass ratio is no more than 1:1.
The preparation method of flavored type low temperature fuming liquids includes the following steps:(1) by plant absorptive material, thermally conductive component and Binder is uniformly mixed, and carrier is obtained after molding;(2) carrier is soaked in tobacco extract and plant essence(Tobacco Extract, plant essence are usually all liquid, are directly impregnated;If it is excessive to encounter special circumstances such as viscosity, correspondingly it is added Base solvent dilution), up to low temperature fuming liquids after taking-up;In the low temperature fuming liquids, plant absorptive material and tobacco extract Mass ratio be no more than 1:1.
Plant absorptive material refers to that the vegetable material with absorption property, plant absorptive material of the invention are selected from plant Fruit, and obtained after crushing, it can be whole fruits, be also possible to a part such as pericarp/shell of fruit.The present invention Using plant absorptive material as tobacco extract(Or tobacco tar, electronic cigarette liquid etc.)Carrier material, to make tobacco extract Be adsorbed on plant vector, it is contemplated that the problems such as the thermal conductivity and molding of plant absorptive material, by plant absorptive material with it is thermally conductive Component, binder mixed-forming, then carry out immersion absorption can be obtained and conveniently take, be heated and the uniform low temperature smoke of smoke Body.The adsorbance of plant absorptive material is to select the important indicator of carrier material, is typically chosen the plant of large amount of adsorption and free from extraneous odour Object material, the tobacco extract of plant absorptive material absorption should be not less than the weight of plant absorptive material itself, in order to avoid smoke It is thin.
Further, it is divided into conduction powder and/or heat conducting fiber for described thermally conductive group.Conduction powder and heat conducting fiber generation respectively Table two class heat-conducting modes different materials.Conduction powder is evenly distributed in low temperature fuming liquids, and low temperature fuming liquids can be improved Thermal conductivity, by the propagation of flue gas, conduction powder is easy to heated, so that the tobacco tar around conduction powder is heated evenly.Due to Heat conducting fiber has longer length, and heat conducting fiber, can also be thermally conductive using machine direction other than above-mentioned heat-conducting mode, so that Low temperature fuming liquids are more easier entirety and are equably heated.
Further, the conduction powder is spherical alumina aluminium powder;The heat conducting fiber is carbon fiber.
Further, the partial size of the conduction powder is 0.15-0.25mm;The diameter of the heat conducting fiber is 0.05- 0.2mm, length 1-10mm.
Further, the thermal coefficient of the thermally conductive component is 500-5000W/ (m K).Actually these materials are superconduction Hot material.Present invention discover that when the thermal coefficient of thermally conductive component reaches 500 W/ (m K) or more, preferably thermal coefficient be greater than The thermally conductive component of 1000 W/ (m K), the heat-conducting effect of the column of smoke improve obviously, and cigarette perfume release is uniform.
Further, the mass ratio of the plant absorptive material, thermally conductive component and binder is 100: (1-15) : (1-20), preferred mass ratio are 100: (5-10) : (5-15).
Further, before step (1), the moisture content of plant adsorption material is adjusted to 10-15%, and carry out disinfection and sterilization Processing;In step (1), the moisture content of carrier is adjusted to 3-6%;Step(2)The low temperature fuming liquids obtained afterwards are wrapped again Dress;The thin-film materials or aluminium-foil paper etc. such as the material of packaging optional PET, PA, PE, BOPP, LDPE.
Further, the binder is cigarette white glue with vinyl, in pre-gelatinized modified starch, cyclodextrin, chitosan, hot melt adhesive It is one or more.
Further, the plant absorptive material is one of maize cob meal, walnut shell powder, powdered rice hulls, shaddock peel powder Or it is a variety of.
Further, soaking time of the plant absorptive material in tobacco extract and plant essence is 5-15min, It is adsorbed in tobacco extract on carrier.After immersion, 4-8h is drained, is then packed again.
Further, the granularity of the plant absorptive material is 20-40 mesh, and the density of the carrier is 0.3-1.2g/ cm3.The granularity of plant absorptive material is related to absorption property, also related to the density of carrier;The density of carrier cannot be excessive, with It is insufficient to exempt from fuming liquids internal pore, flue gas is not easy to spread, and heat is not easy to transmit.Certainly, density is too low, illustrate the content of tobacco tar compared with Few, the flue gas that can take out food is few, and the tobacco is very mild.
Further, the plant essence is at least one of ethereal oil of flower, Chinese medical concrete, spice extract.
Further, the ethereal oil of flower is osmanthus essential oil, rose ethereal oil, cape jasmine flower essential oil, jasmine essential oil, tree orchid At least one of flower essential oil, chrysanthemum essential oil, lily essential oil, clove oil.
Further, the spice extract be fennel, fragrant nutmeg, cassia bark, spiceleaf, dried orange peel, turmeric, Chinese prickly ash, illiciumverum, At least one of thyme, purple perilla, peppermint, cloves, extract of lemon-grass.
Further, the Chinese medical concrete is extract of licorice root, Luo Han Guo Paste In Foods, Fructus Lycii extractum, campanulaceae medicinal extract, lotus leaf leaching At least one of cream, raspberry medicinal extract, purple perilla medicinal extract, wrinkled giant hyssop medicinal extract.
Compared with prior art, the beneficial effects of the invention are as follows:
1, low temperature fuming liquids provided by the invention form according to smoking set heating chamber size, adsorb tobacco tar and sealed package, It can store for a long time without influencing to suck impression, while be easy to add and remove.
2, there are a large amount of holes in low temperature fuming liquids short texture provided by the invention, inside, and easily, while pumping can be improved in suction Inhale the heating surface area of material and being heated evenly property.
3, carrier provided by the invention is splendid to tobacco tar absorption property, which can give consumer very when sucking Good satisfaction;Low in raw material price, safety and environmental protection are suitable as one-time consumption product simultaneously.
4, contain heat superconducting powder body material inside low temperature fuming liquids provided by the invention, inside is thermally conductive to be greatly speeded up, and have Smog is quickly formed conducive to being heated evenly property of raising and at a lower temperature.
5, there are also spice or fresh flower flavor ingredient, suctions in addition to tobacco tar in electric heating low temperature fuming liquids provided by the invention When have special fragrance, can to smoker's pleasure novel sense by.
Specific embodiment
Below with reference to embodiment, the invention will be further described.
Embodiment 1
1)The maize cob meal of 20-40 mesh is pre-adjusted moisture to 12%, using microwave sterilization sterilization processing 50s and is regulated and controled Moisture is to 5% or so;2)It will treated maize cob meal, heat superconducting ball-aluminium oxide powder(Thermal coefficient is 500 W/ (m K)), cigarette white glue with vinyl is according to 100:5:8 mass ratio is uniformly mixed, and is added in moulding press cavity and is pressed and molded, is prepared 17mm × thickness 6mm, 0.75 g/cm of density3Cylindric carrier;3)Microwave drying is spare to moisture content 5% or so;4)It will It is 10 that above-mentioned carrier, which is soaked in mass ratio,:10min in 0.5 tobacco extract and rose ethereal oil mixture, after taking-up drains Using aluminium-foil paper sealed package up to required electric heating low temperature fuming liquids.Main body both ends packing material is removed, smoking set is directly plugged into It can be sucked in heating chamber, fuming rate is fast when sucking, and suction is smooth, and satisfaction is strong, and waste material is still integral blocks after the completion of sucking Shape can easily take out, and smoking set less pollution is readily cleaned.
Embodiment 2
1)The walnut shell powder of 20-40 mesh is pre-adjusted moisture to 10%, using microwave sterilization sterilization processing 60s and is regulated and controled Moisture is to 5% or so;2)It will treated walnut shell powder, heat superconducting carbon fiber powder(Thermal coefficient is 1500 W/ (m K)), cigarette use White glue with vinyl, retardation PES hot melt adhesive powder are according to 100:5:5:3 mass ratio is uniformly mixed, and is added in moulding press cavity and is pressed and molded, and is prepared Obtain 17mm × thickness 6mm, 0.65 g/cm of density3Cylindric carrier;3)100 DEG C to be dried to moisture content 5% or so standby With;4)It is 10 that above-mentioned carrier, which is soaked in mass ratio,:15min in 0.4 tobacco extract and tree orchid anthosin oil mixture, takes out Using BOPP film sealed package up to required electric heating low temperature fuming liquids after draining.Fuming liquids packing material is removed, is directly filled in Entering in smoking set heating chamber can suck, and fuming rate is fast when sucking, and suction is smooth, and satisfaction is strong, and waste material is still after the completion of sucking Whole bulk can easily be taken out, and smoking set less pollution is readily cleaned.
Embodiment 3
1)By the powdered rice hulls of 20-40 mesh and shaddock peel powder mixture(Mass ratio 1:2)Moisture is pre-adjusted to 15%, is used Microwave sterilization sterilization processing 60s simultaneously regulates and controls moisture to 5% or so;2)It will treated mixed powder, heat superconducting carbon fiber powder(It leads Hot coefficient is 4000 W/ (m K)), chitosan, TPU hot-melt adhesive powder is according to 100:5:10:5 mass ratio is uniformly mixed, another to add 10% moisture again be uniformly mixed to obtain wet mixed material, be added into moulding press cavity and be pressed and molded, be prepared 6mm × Thickness 16mm, 0.5 g/cm of density3Disc-shaped carrier;3)100 DEG C to be dried to moisture content 5% or so spare;4)By mass ratio It is 10:0.5:0.5 tobacco extract, thyme extract and lemon-grass extract volume ratio is 5:1 propylene glycol and second Alcohol dilution, is made into the mixed solution of 40% mass fraction;5)Above-mentioned carrier is soaked the 12min in mixed solution, after taking-up drains It is packed using PE diaphragm seal up to required electric heating low temperature fuming liquids.Fuming liquids packing material is removed, smoking set is directly plugged into and adds It can be sucked in hot chamber, fuming rate is fast when sucking, and suction is smooth, and satisfaction is strong, and waste material is still whole bulk after the completion of sucking It can easily take out, smoking set less pollution is readily cleaned.
Embodiment 4
1)The maize cob meal of 20-40 mesh is pre-adjusted moisture to 12%, using microwave sterilization sterilization processing 50s and is regulated and controled Moisture is to 5% or so;2)It will treated maize cob meal, heat superconducting ball-aluminium oxide powder(Thermal coefficient is 500 W/ (m K)), cigarette white glue with vinyl, polyolefin hot-melt powder is according to 100:5:5:3 mass ratio is uniformly mixed, and mould in moulding press cavity is added It is molded, 17mm × thickness 6mm, 0.95 g/cm of density is prepared3Cylindric carrier;3)Microwave drying is to moisture content 5% or so is spare;4)It is 10 by mass ratio:1.0 tobacco extract and extract of licorice root is diluted with propylene glycol, is made into 50% mass ratio Mixed solution;5)Above-mentioned carrier is soaked the 10min in mixed solution, taking-up uses aluminium-foil paper sealed package up to institute after draining Need electric heating low temperature fuming liquids.Main body both ends packing material is removed, being directly plugged into smoking set heating chamber can suck, hair when sucking Cigarette speed is fast, aspirates smooth, and satisfaction is strong, and it is fragrant and sweet to accompany special Radix Glycyrrhizae in tobacco perfume, and waste material is still whole after the completion of sucking Bulk can easily be taken out, and smoking set less pollution is readily cleaned.

Claims (8)

1. a kind of flavored type low temperature fuming liquids, which is characterized in that including carrier and the tobacco extract being adsorbed on carrier and plant Object essence;The mass ratio of the tobacco extract and plant essence is 100:1-20;
The carrier is made of plant absorptive material, thermally conductive component and binder;Plant adsorption material in the low temperature fuming liquids The mass ratio of material and tobacco extract is no more than 1:1;
Described thermally conductive group is divided into conduction powder and/or heat conducting fiber;The conduction powder is metal oxide powder;The thermally conductive fibre Dimension is carbon fiber;The partial size of the conduction powder is 0.15-0.25mm;The diameter of the heat conducting fiber is 0.05-0.2mm, length Degree is 1-10mm;The thermal coefficient of the thermally conductive component is 500-5000W/ (m K).
2. low temperature fuming liquids as described in claim 1, which is characterized in that the metal oxide powder is spherical alumina aluminium powder.
3. low temperature fuming liquids as described in claim 1, which is characterized in that the granularity of the plant absorptive material is 20-40 mesh; The density of the carrier is 0.3-1.2g/cm3
4. low temperature fuming liquids as described in claim 1, which is characterized in that the plant absorptive material, thermally conductive component and bonding The mass ratio of agent is 100: (1-15) : (1-20).
5. low temperature fuming liquids as described in claim 1, which is characterized in that the plant essence be ethereal oil of flower, Chinese medical concrete, At least one of spice extract.
6. low temperature fuming liquids as claimed in claim 5, which is characterized in that the ethereal oil of flower is osmanthus essential oil, rose anthosin At least one of oil, cape jasmine flower essential oil, jasmine essential oil, tree orchid flower essential oil, chrysanthemum essential oil, lily essential oil, clove oil.
7. low temperature fuming liquids as claimed in claim 5, which is characterized in that the spice extract is fennel, fragrant nutmeg, osmanthus At least one of skin, spiceleaf, dried orange peel, turmeric, Chinese prickly ash, illiciumverum, thyme, purple perilla, peppermint, cloves, extract of lemon-grass.
8. low temperature fuming liquids as claimed in claim 5, which is characterized in that the Chinese medical concrete is extract of licorice root, Siraitia grosvenorii leaching At least one of cream, Fructus Lycii extractum, campanulaceae medicinal extract, lotus leaf medicinal extract, raspberry medicinal extract, purple perilla medicinal extract, wrinkled giant hyssop medicinal extract.
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WO2021122583A1 (en) * 2019-12-17 2021-06-24 Philip Morris Products S.A. Aerosol-forming substrate with nitrogen-containing nucleophilic compound
RU2798258C1 (en) * 2019-12-17 2023-06-20 Филип Моррис Продактс С.А. Aerosol substrate with nitrogen-containing nucleophilic compound

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