CN105661651A - Aroma-increasing type low-temperature fuming body - Google Patents
Aroma-increasing type low-temperature fuming body Download PDFInfo
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- CN105661651A CN105661651A CN201610232921.XA CN201610232921A CN105661651A CN 105661651 A CN105661651 A CN 105661651A CN 201610232921 A CN201610232921 A CN 201610232921A CN 105661651 A CN105661651 A CN 105661651A
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- Prior art keywords
- low temperature
- temperature fuming
- plant
- fuming liquids
- carrier
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F47/00—Smokers' requisites not otherwise provided for
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/12—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
Abstract
The invention discloses an aroma-increasing type low-temperature fuming body. The aroma-increasing type low-temperature fuming body comprises a carrier and tobacco extract and plant essence which are adsorbed to the carrier, wherein the mass ratio of the tobacco extract to the plant essence is 100 to (1-20), the carrier is composed of plant adsorption materials, thermal conductive components and a binding agent, and the mass ratio of the plant adsorption materials to the tobacco extract in the low-temperature fuming body is not larger than 1 to 1. The aroma-increasing type low-temperature fuming body is formed according to the size of a smoking set heating cavity, adsorbs tobacco tar and packed in a sealed mode, the fuming body can be stored for a long time, the smoking feeling is not affected, and meanwhile, addition and cleaning of tobacco materials are easy; the aroma-increasing type low-temperature fuming body is loosened in structure, is internally provided with a large number of pores and is easy to smoke; meanwhile, the heating area and the heating uniformity of smoking materials can be improved, and good satisfaction can be given to a consumer; meanwhile, the aroma-increasing type low-temperature fuming body is low in raw material price, safe, environmentally friendly and suitable for serving as disposable consumer goods.
Description
Technical field
The present invention relates to a kind of flavored type low temperature fuming liquids, belong to electronic cigarette technical field.
Background technology
In conventional cigarette, the smog of result of combustion of tobacco exists tens of kinds of carcinogen, and full of smoke form the second hand smoking that hazardness is bigger in atmosphere, surrounding population can be caused bigger Health cost contaminated environment simultaneously.
The pursuit to healthy living along with scientific and technological progress and people, occurs in that a kind of smokeless cigarette system, toasts to produce smog by thing that the solids such as Medicated cigarette are fuming, it is not necessary to burning. At present, low temperature on market does not burn cigarette product mainly by filling tobacco-containing material such as cigarette, tobacco shred or smoked sheet etc. in special electric heater unit, the flue gas in tobacco fill material is made to evaporate by electrical heating, so that smoker obtains the suction impression being similar to tradition Nicotiana tabacum L.. But the electrical heating of prior art is substantially peripheral heating, firing rate is slow and heats uneven, and the time of generation smog is longer and concentration is not enough; The simultaneously filling of tobacco-containing material and remove after sucking pretty troublesome, thus having had a strong impact on Consumer's Experience.
Summary of the invention
Present invention solves the technical problem that and be, tobacco extract is liquid, when sucking, takes inconvenience; During heating, it is heated uneven.
The technical scheme is that, it is provided that a kind of flavored type low temperature fuming liquids, including carrier with the tobacco extract being adsorbed on carrier and plant essence; The mass ratio of described tobacco extract and plant essence is 100:1-20; Described carrier is made up of plant absorptive material, heat conduction component and binding agent; The mass ratio of the plant absorptive material in described low temperature fuming liquids and tobacco extract is less than 1:1.
The preparation method of flavored type low temperature fuming liquids comprises the following steps: (1), by plant absorptive material, heat conduction component and binding agent mix homogeneously, obtains carrier after molding; (2) being soaked in by described carrier in tobacco extract and plant essence, (tobacco extract, plant essence are generally all liquid, directly soak; If it is excessive to run into special circumstances such as viscosity, correspondingly add base solvent dilution), namely obtain low temperature fuming liquids after taking-up; In described low temperature fuming liquids, the mass ratio of plant absorptive material and tobacco extract is less than 1:1.
Plant absorptive material refers to the vegetable material with absorption property, and the plant absorptive material of the present invention is selected from the fruit of plant, and obtains after pulverizing, it is possible to be whole fruits, it is also possible to be a part such as peel/shell of fruit. The present invention is using the plant absorptive material carrier material as tobacco extract (or claim ree-oil, electronic cigarette liquid etc.), so that tobacco extract is adsorbed on plant vector, the problems such as heat conductivity and the molding of considering plant absorptive material, by plant absorptive material and heat conduction component, binding agent mixed-forming, carry out again soaking absorption, uniform low temperature fuming liquids of can conveniently being taken, be heated and be fuming. The adsorbance of plant absorptive material is the important indicator selecting carrier material, is typically chosen that adsorbance is big and the vegetable material of free from extraneous odour, and the tobacco extract of plant absorptive material absorption should be not less than the weight of plant absorptive material self, in order to avoid smoke is thin.
Further, described heat conduction component is conduction powder and/or heat conducting fiber. Conduction powder represents the material that two class heat-conducting modes are different respectively with heat conducting fiber. Conduction powder is evenly distributed in low temperature fuming liquids, it is possible to improving the thermal conductivity of low temperature fuming liquids, by the propagation of flue gas, conduction powder is prone to be heated so that the ree-oil around conduction powder is heated evenly. Owing to heat conducting fiber has longer length, heat conducting fiber is except above-mentioned heat-conducting mode, it is also possible to utilize machine direction heat conduction so that low temperature fuming liquids are more prone to entirety and are heated equably.
Further, described conduction powder is spherical alumina aluminium powder; Described heat conducting fiber is carbon fiber.
Further, the particle diameter of described conduction powder is 0.15-0.25mm; The diameter of described heat conducting fiber is 0.05-0.2mm, length is 1-10mm.
Further, the heat conductivity of described heat conduction component is 500-5000W/ (m K). Actually these materials are super heat conduction material. Present invention discover that when the heat conductivity of heat conduction component reaches more than 500W/ (m K), it is preferable that heat conductivity is the heat conduction component more than 1000W/ (m K), the heat-conducting effect of the column of smoke is improved substantially, and the release of cigarette perfume (or spice) is uniformly.
Further, the mass ratio of described plant absorptive material, heat conduction component and binding agent is 100:(1-15): (1-20), it is preferable that mass ratio is 100:(5-10): (5-15).
Further, front in step (1), the moisture content of plant adsorption material is regulated to 10-15%, and carries out disinfection process; In step (1), the moisture content of carrier is regulated to 3-6%; The low temperature fuming liquids obtained after step (2) are packed again; Thin-film material or the aluminium-foil papers etc. such as material optional PET, PA, PE, BOPP, LDPE of packaging.
Further, described binding agent is one or more in cigarette white glue with vinyl, pre-gelatinized modified starch, cyclodextrin, chitosan, PUR.
Further, described plant absorptive material is one or more in maize cob meal, walnut shell powder, powdered rice hulls, shaddock peel powder.
Further, described plant absorptive material soak time in tobacco extract and plant essence is 5-15min, makes tobacco extract be adsorbed on carrier. After immersion, drain 4-8h, then pack again.
Further, the granularity of described plant absorptive material is 20-40 order, and the density of described carrier is 0.3-1.2g/cm3. The granularity of plant absorptive material is relevant to absorption property, also relevant to the density of carrier; The density of carrier can not be excessive, in order to avoid fuming liquids internal pore is not enough, flue gas not easily spreads, and heat not easily transmits. Certainly, density is too low, illustrates that the content of ree-oil is less, and the flue gas that can take out food is few, and the tobacco is very mild.
Further, described plant essence is at least one in ethereal oil of flower, Chinese medical concrete, spice extract.
Further, described ethereal oil of flower is at least one in osmanthus essential oil, rose ethereal oil, Flos Gardeniae quintessence oil, Flos Jasmini Sambac quintessence oil, SHULANHUA quintessence oil, chrysanthemum essential oil, Bulbus Lilii quintessence oil, clove oil.
Further, described spice extract is at least one in the extract of Fructus Foeniculi, fragrant Semen Myristicae, Cortex cinnamomi japonici (Ramulus Cinnamomi), Herba Pelargonii Graveolentis, Pericarpium Citri Reticulatae, Rhizoma Curcumae Longae, Pericarpium Zanthoxyli, anise, Herba thymi vulgaris, Folium Perillae, Herba Menthae, Flos Caryophylli, Herba Cymbopogonis Citrari.
Further, described Chinese medical concrete is at least one in Radix Glycyrrhizae extractum, Luo Han Guo Paste In Foods, Fructus Lycii extractum, Radix Platycodonis extractum, Folium Nelumbinis extractum, Fructus Rubi extractum, Folium Perillae extractum, Herba Pogostemonis extractum.
Compared with prior art, the invention has the beneficial effects as follows:
1, low temperature fuming liquids provided by the invention are according to smoking set heating chamber size molding, absorption ree-oil packing, it is possible to permanent storage and do not affect and suck impression, be prone to add and remove simultaneously.
2, low temperature fuming liquids short texture provided by the invention, there is a large amount of hole inside, and suction easily, can improve the heating surface area of sucked material and being heated evenly property simultaneously.
3, carrier provided by the invention is splendid to ree-oil absorption property, and these low temperature fuming liquids can give consumer good gratification when sucking; Low in raw material price, safety and environmental protection, be suitable as one-time consumption product simultaneously.
4, low temperature fuming liquids provided by the invention are internal containing heat superconducting powder body material, and internal heat conduction can greatly speed up, and is conducive to being heated evenly property of raising and quickly forms smog at a lower temperature.
5, electrical heating low temperature fuming liquids provided by the invention also have spice or fresh flower flavor composition outside smoke abatement oil, during suction, have special fragrance, the novel impression that smoker is joyful can be given.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described.
Embodiment 1
1) maize cob meal of 20-40 order is regulated moisture in advance to 12%, adopt microwave sterilization sterilization processing 50s and regulate and control moisture to about 5%; 2) maize cob meal after process, heat superconducting ball-aluminium oxide powder body (heat conductivity is 500W/ (m K)), cigarette white glue with vinyl are compared mix homogeneously according to the quality of 100:5:8, add compression molding in moulding press cavity, prepare 17mm × thickness 6mm, density 0.75g/cm3Cylindric carrier; 3) microwave drying is standby to moisture about 5%; 4) leaching of above-mentioned carrier is formed on tobacco extract and the 10min in rose ethereal oil mixture that mass ratio is 10:0.5, takes out and after draining, adopt aluminium-foil paper to pack and obtain required electrical heating low temperature fuming liquids. Being removed by main body two ends packing material, be directly plugged in smoking set heating chamber and can suck, speed of being fuming when sucking is fast, aspirates smooth and easy, and gratification is strong, has sucked rear waste material and still can easily take out for overall bulk, and smoking set less pollution is readily cleaned.
Embodiment 2
1) walnut shell powder of 20-40 order is regulated moisture in advance to 10%, adopt microwave sterilization sterilization processing 60s and regulate and control moisture to about 5%; 2) walnut shell powder after process, heat superconducting carbon fiber powder (heat conductivity is 1500W/ (m K)), cigarette white glue with vinyl, retardation PES hot melt adhesive powder are compared mix homogeneously according to the quality of 100:5:5:3, add compression molding in moulding press cavity, prepare 17mm × thickness 6mm, density 0.65g/cm3Cylindric carrier; 3) 100 DEG C of drying are standby to moisture about 5%; 4) leaching of above-mentioned carrier is formed on tobacco extract and the 15min in SHULANHUA blend of essential oils that mass ratio is 10:0.4, takes out and after draining, adopt BOPP diaphragm seal to pack and obtain required electrical heating low temperature fuming liquids.Being removed by fuming liquids packing material, be directly plugged in smoking set heating chamber and can suck, speed of being fuming when sucking is fast, aspirates smooth and easy, and gratification is strong, has sucked rear waste material and still can easily take out for overall bulk, and smoking set less pollution is readily cleaned.
Embodiment 3
1) powdered rice hulls of 20-40 order and shaddock peel powder mixture (mass ratio 1:2) are regulated moisture in advance to 15%, adopt microwave sterilization sterilization processing 60s and regulate and control moisture to about 5%; 2) mixed powder after process, heat superconducting carbon fiber powder (heat conductivity is 4000W/ (m K)), chitosan, TPU hot-melt adhesive powder are compared mix homogeneously according to the quality of 100:5:10:5, separately add 10% moisture mix homogeneously again and must moisten mixed material, it is added into compression molding in moulding press cavity, prepares 6mm × thickness 16mm, density 0.5g/cm3Disc-shaped carrier; 3) 100 DEG C of drying are standby to moisture about 5%; 4) it is the tobacco extract of 10:0.5:0.5, Thymi Serpylli Herba extract and propylene glycol and ethanol dilution that Herba Cymbopogonis Citrari extract volume ratio is 5:1 by mass ratio, is made into the mixed solution of 40% mass fraction; 5) leaching of above-mentioned carrier is formed in mixed solution 12min, takes out and after draining, adopt PE diaphragm seal to pack and obtain required electrical heating low temperature fuming liquids. Being removed by fuming liquids packing material, be directly plugged in smoking set heating chamber and can suck, speed of being fuming when sucking is fast, aspirates smooth and easy, and gratification is strong, has sucked rear waste material and still can easily take out for overall bulk, and smoking set less pollution is readily cleaned.
Embodiment 4
1) maize cob meal of 20-40 order is regulated moisture in advance to 12%, adopt microwave sterilization sterilization processing 50s and regulate and control moisture to about 5%; 2) maize cob meal after process, heat superconducting ball-aluminium oxide powder body (heat conductivity is 500W/ (m K)), cigarette white glue with vinyl, polyolefin hot-melt powder are compared mix homogeneously according to the quality of 100:5:5:3, add compression molding in moulding press cavity, prepare 17mm × thickness 6mm, density 0.95g/cm3Cylindric carrier; 3) microwave drying is standby to moisture about 5%; 4) tobacco extract that mass ratio is 10:1.0 is diluted with Radix Glycyrrhizae extractum propylene glycol, be made into the mixed solution of 50% mass ratio; 5) leaching of above-mentioned carrier is formed in mixed solution 10min, takes out and after draining, adopt aluminium-foil paper to pack and obtain required electrical heating low temperature fuming liquids. Being removed by main body two ends packing material, be directly plugged in smoking set heating chamber and can suck, speed of being fuming when sucking is fast, aspirating smooth and easy, gratification is strong, accompanies special Radix Glycyrrhizae fragrant and sweet in Nicotiana tabacum L. perfume (or spice), having sucked rear waste material still can easily to take out for overall bulk, smoking set less pollution is readily cleaned.
Claims (10)
1. flavored type low temperature fuming liquids, it is characterised in that include carrier and the tobacco extract being adsorbed on carrier and plant essence; The mass ratio of described tobacco extract and plant essence is 100:1-20;
Described carrier is made up of plant absorptive material, heat conduction component and binding agent; The mass ratio of the plant absorptive material in described low temperature fuming liquids and tobacco extract is less than 1:1.
2. low temperature fuming liquids as claimed in claim 1, it is characterised in that described heat conduction component is conduction powder and/or heat conducting fiber; Described conduction powder is metal-oxide powder; Described heat conducting fiber is carbon fiber.
3. low temperature fuming liquids as claimed in claim 2, it is characterised in that described metal-oxide powder is spherical alumina aluminium powder.
4. low temperature fuming liquids as claimed in claim 2, it is characterised in that the particle diameter of described conduction powder is 0.15-0.25mm; The diameter of described heat conducting fiber is 0.05-0.2mm, length is 1-10mm; The heat conductivity of described heat conduction component is 500-5000W/ (m K).
5. low temperature fuming liquids as claimed in claim 1, it is characterised in that the granularity of described plant absorptive material is 20-40 order; The density of described carrier is 0.3-1.2g/cm3。
6. low temperature fuming liquids as claimed in claim 1, it is characterised in that the mass ratio of described plant absorptive material, heat conduction component and binding agent is 100:(1-15): (1-20).
7. low temperature fuming liquids as claimed in claim 1, it is characterised in that described plant essence is at least one in ethereal oil of flower, Chinese medical concrete, spice extract.
8. low temperature fuming liquids as claimed in claim 7, it is characterised in that described ethereal oil of flower is at least one in osmanthus essential oil, rose ethereal oil, Flos Gardeniae quintessence oil, Flos Jasmini Sambac quintessence oil, SHULANHUA quintessence oil, chrysanthemum essential oil, Bulbus Lilii quintessence oil, clove oil.
9. low temperature fuming liquids as claimed in claim 7, it is characterized in that, described spice extract is at least one in the extract of Fructus Foeniculi, fragrant Semen Myristicae, Cortex cinnamomi japonici (Ramulus Cinnamomi), Herba Pelargonii Graveolentis, Pericarpium Citri Reticulatae, Rhizoma Curcumae Longae, Pericarpium Zanthoxyli, anise, Herba thymi vulgaris, Folium Perillae, Herba Menthae, Flos Caryophylli, Herba Cymbopogonis Citrari.
10. low temperature fuming liquids as claimed in claim 7, it is characterised in that described Chinese medical concrete is at least one in Radix Glycyrrhizae extractum, Luo Han Guo Paste In Foods, Fructus Lycii extractum, Radix Platycodonis extractum, Folium Nelumbinis extractum, Fructus Rubi extractum, Folium Perillae extractum, Herba Pogostemonis extractum.
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| CN106418704A (en) * | 2016-09-14 | 2017-02-22 | 河北中烟工业有限责任公司 | Application of clove bud oil in electronic tobacco tar |
| CN107752120A (en) * | 2017-10-17 | 2018-03-06 | 广州秘理普植物技术开发有限公司 | A kind of low temperature does not burn draft particle and preparation method thereof |
| CN107853750A (en) * | 2017-10-11 | 2018-03-30 | 吴雷 | A kind of solid tobacco tar and its processing method |
| CN108185524A (en) * | 2017-12-22 | 2018-06-22 | 安徽中烟工业有限责任公司 | A kind of inside electrical heating aerosol generation system comprising tobacco particle |
| CN108523205A (en) * | 2018-05-09 | 2018-09-14 | 四川三联新材料有限公司 | One kind is for mode of heating smoke membrane material and preparation method thereof |
| CN108669634A (en) * | 2018-08-09 | 2018-10-19 | 四川三联新材料有限公司 | The tobacco compositions of drink style, smoke section and heating are not burnt cigarette cigarette stick |
| CN108669636A (en) * | 2018-08-09 | 2018-10-19 | 四川三联新材料有限公司 | The tobacco compositions of fragrance of a flower style, smoke section and heating are not burnt cigarette cigarette stick |
| CN109363230A (en) * | 2018-10-31 | 2019-02-22 | 云南恒罡科技有限公司 | It is a kind of to heat cigarette smoker particles inside material and preparation method thereof of not burning |
| CN109363224A (en) * | 2018-11-01 | 2019-02-22 | 广西中烟工业有限责任公司 | A kind of cigarette solid perfume compounding method and application |
| CN110214982A (en) * | 2019-07-03 | 2019-09-10 | 深圳市长能汇科科技有限公司 | A kind of smoking article and preparation method thereof for suction |
| CN110373265A (en) * | 2019-06-27 | 2019-10-25 | 广东中烟工业有限责任公司 | A kind of sustained release fragrance and its application in Chinese style taste tobacco product |
| CN111011915A (en) * | 2020-01-06 | 2020-04-17 | 江苏中烟工业有限责任公司 | Cigarette core column suitable for heating cigarettes and preparation method thereof |
| CN112056613A (en) * | 2020-09-07 | 2020-12-11 | 广西中烟工业有限责任公司 | Preparation method of cigarette filter stick with gardenia fragrance |
| CN112120275A (en) * | 2020-09-18 | 2020-12-25 | 新火智造(深圳)有限公司 | Flavored fuming particles suitable for heating non-burning cigarettes |
| CN113925193A (en) * | 2021-09-29 | 2022-01-14 | 新火智造(深圳)有限公司 | Paper-based composite core base material capable of volatilizing effective components without burning and manufacturing and using method |
| CN114745972A (en) * | 2019-12-17 | 2022-07-12 | 菲利普莫里斯生产公司 | Aerosol-forming substrate with nitrogen-containing nucleophilic compound |
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| CN107853750A (en) * | 2017-10-11 | 2018-03-30 | 吴雷 | A kind of solid tobacco tar and its processing method |
| CN107752120A (en) * | 2017-10-17 | 2018-03-06 | 广州秘理普植物技术开发有限公司 | A kind of low temperature does not burn draft particle and preparation method thereof |
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| CN108523205A (en) * | 2018-05-09 | 2018-09-14 | 四川三联新材料有限公司 | One kind is for mode of heating smoke membrane material and preparation method thereof |
| CN108669636B (en) * | 2018-08-09 | 2021-07-27 | 四川三联新材料有限公司 | Floral-style tobacco composition, smoking segment and heating non-combustible cigarette rod |
| CN108669634A (en) * | 2018-08-09 | 2018-10-19 | 四川三联新材料有限公司 | The tobacco compositions of drink style, smoke section and heating are not burnt cigarette cigarette stick |
| CN108669636A (en) * | 2018-08-09 | 2018-10-19 | 四川三联新材料有限公司 | The tobacco compositions of fragrance of a flower style, smoke section and heating are not burnt cigarette cigarette stick |
| CN108669634B (en) * | 2018-08-09 | 2021-05-28 | 四川三联新材料有限公司 | Tobacco composition with drink style, smoking section and heating non-combustion cigarette rod |
| CN109363230A (en) * | 2018-10-31 | 2019-02-22 | 云南恒罡科技有限公司 | It is a kind of to heat cigarette smoker particles inside material and preparation method thereof of not burning |
| CN109363224A (en) * | 2018-11-01 | 2019-02-22 | 广西中烟工业有限责任公司 | A kind of cigarette solid perfume compounding method and application |
| JP7177309B2 (en) | 2019-06-27 | 2022-11-24 | チャイナ・タバコ・カントン・インダストリアル・カンパニー・リミテッド | Chinese-flavored tobacco cigarette base material, reconstituted tobacco and heated non-combustible cigarettes |
| CN110373265A (en) * | 2019-06-27 | 2019-10-25 | 广东中烟工业有限责任公司 | A kind of sustained release fragrance and its application in Chinese style taste tobacco product |
| EP3800238A4 (en) * | 2019-06-27 | 2021-10-06 | China Tobacco Guangdong Industrial Co., Ltd. | Slow-release flavorant and application thereof in chinese-flavor tobacco product |
| JP2021530977A (en) * | 2019-06-27 | 2021-11-18 | チャイナ・タバコ・カントン・インダストリアル・カンパニー・リミテッドChina Tobacco Guangdong Industrial Co., Ltd. | Its application in sustained release flavors and Chinese flavored tobacco products |
| CN110214982A (en) * | 2019-07-03 | 2019-09-10 | 深圳市长能汇科科技有限公司 | A kind of smoking article and preparation method thereof for suction |
| CN114745972B (en) * | 2019-12-17 | 2023-08-04 | 菲利普莫里斯生产公司 | Aerosol-forming matrix with nitrogen-containing nucleophile |
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| CN114745972A (en) * | 2019-12-17 | 2022-07-12 | 菲利普莫里斯生产公司 | Aerosol-forming substrate with nitrogen-containing nucleophilic compound |
| CN111011915A (en) * | 2020-01-06 | 2020-04-17 | 江苏中烟工业有限责任公司 | Cigarette core column suitable for heating cigarettes and preparation method thereof |
| CN111011915B (en) * | 2020-01-06 | 2022-04-29 | 江苏中烟工业有限责任公司 | Cigarette core column suitable for heating cigarettes and preparation method thereof |
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| CN112120275A (en) * | 2020-09-18 | 2020-12-25 | 新火智造(深圳)有限公司 | Flavored fuming particles suitable for heating non-burning cigarettes |
| CN113925193A (en) * | 2021-09-29 | 2022-01-14 | 新火智造(深圳)有限公司 | Paper-based composite core base material capable of volatilizing effective components without burning and manufacturing and using method |
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