CN104757703B - A kind of tobacco distillate and its preparation and application - Google Patents
A kind of tobacco distillate and its preparation and application Download PDFInfo
- Publication number
- CN104757703B CN104757703B CN201410848930.2A CN201410848930A CN104757703B CN 104757703 B CN104757703 B CN 104757703B CN 201410848930 A CN201410848930 A CN 201410848930A CN 104757703 B CN104757703 B CN 104757703B
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- tobacco
- distillate
- solvent
- cigarette
- product
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The present invention provides a kind of tobacco distillate, is the distillate that tobacco material is carried out to distillation acquisition.The present invention also provides the preparation methods of the tobacco distillate, comprising steps of 1) tobacco material is placed in solvent and extracts, the solvent is the ethanol solution that mass fraction is 40~99%；2) step 1) resulting material is heated, collecting temperature is distillate between 150~400 DEG C.The present invention is by the way that under gas atmosphere, in certain temperature range, distillation tobacco-containing material obtains distillate, which has the tobacco flavors such as strong burnt odor, faint scent and radix aucklandiae.
Description
Technical field
The invention belongs to Field of Tobacco, and in particular to a kind of preparation method and applications of tobacco curing straw-made articles again.
Background technique
Tobacco has fragrance complicated and changeable, has stimulation to nerve, tobacco product has extremely wide consumption market.
It is most commonly seen tobacco product that tobacco, which dries rear chopping cigarette,.Tobacco product also includes chewing tobacco, buccal cigarette, snuff, electric heating
Type tobacco product, fuel hot type tobacco product, tobacco spray product and electronic cigarette, but have the characteristics that common, an i.e. mouth
The taste of taste and traditional cigarette or cigar differs greatly, it is difficult to consumer be allowed to approve.The fragrance of tobacco extract simultaneously
Differ greatly with the cigarette of extracting combustion or the fragrance of cigar, it is difficult to provide sufficient burnt odor, Jiao Tianxiang, faint scent, it is fresh and sweet it is fragrant,
The complicated multi-level fragrance such as radix aucklandiae.Some producers or developer attempt to add various natural flavor substances, reach mould with expectation
The purpose of the taste of imitative cigarette or cigar, but still be difficult to reach and meet with cigarette or cigar fragrance.
Also there is existing tobacco product flavor component to be difficult to lasting defect.
(food industry is scientific and technological, the 10th phase in 2011 commonly used in extracting essential oil of tobaccos for the technology distilled to tobacco
388-390 pages), tobacco leaf and aqueous slkali mixing are distilled with steam distillation.This method can effective extraction nicotine, but
It cannot be used for the distillate that preparation keeps tobacco flavor.
Summary of the invention
In view of the deficiencies of the prior art, it the purpose of the present invention is to propose to a kind of tobacco distillate, can be well solved
Chewing tobacco, buccal cigarette, snuff, electric heating type tobacco product, fuel hot type tobacco product, tobacco spray product and electronic cigarette at present
The taste problem of equal products, and the unendurable defect of fragrance of some products can also be improved well.
It is another object of the present invention to propose the application of the tobacco distillate.
Third object of the present invention is the tobacco product for proposing to contain the tobacco distillate.
Realize above-mentioned purpose of the present invention the specific technical proposal is:
A kind of tobacco distillate is the distillate that tobacco material is carried out to distillation acquisition；
The tobacco material is tobacco extract, tobacco extract, tobacco leaf, is evaporated under reduced pressure distillating for tobacco extract acquisition
Object, vacuum distillation tobacco extract obtain difficult volatile materials, short-path distillation tobacco extract distillate, short-path distillation cigarette
One of difficult volatile materials of careless extract is a variety of.
Specifically, the tobacco extract is that Tobacco Leaf and/or stem shred after 50-180 DEG C of drying, and ethyl alcohol, water is added
One of or it is a variety of, the amount that volume is added is 1~100 times of Tobacco Leaf and/or stem quality, is depressurized after impregnating 0.5-50 hours
Concentration gained.The tobacco leaf can be tobacco leaf powder and/or sheet tobacco leaf.
The preparation method of tobacco distillate proposed by the present invention, comprising steps of
1) tobacco material is placed in solvent and extracts, the solvent be mass fraction be 40~99% ethanol solution, water, nothing
One of water-ethanol, supercritical carbon dioxide or a variety of combinations；
2) step 1) resulting material is heated, collecting temperature is distillate between 150~400 DEG C.
Preferably, in the step 1), tobacco material is placed in solvent ultrasonic extraction at normal temperature, tobacco material and solvent
Mass volume ratio be 1g:1~10mL.
Ultrasonic wave extraction is the supplementary means extracted, and the time is changeable, such as ultrasonic extraction 2.5-3.5 hours, tobacco
The mass volume ratio of raw material and solvent is preferably 1g:5~8mL.
Or, solvent is added in tobacco material in the step 1), in 38~45MPa extracting pressure, 48~55 DEG C of extraction temperature
Carbon dioxide draw is used under degree；The mass volume ratio of tobacco material and solvent is 100g:0~15mL.Tobacco material and solvent
Mass volume ratio is preferably 100g:4~7mL.
It is changeable with the time of carbon dioxide draw, preferably 2.5-3.5 hours.
Wherein, in the step 2), the heating is carried out in the atmosphere containing nitrogen, and the atmosphere is by volume parts
It is formed for 100 nitrogen and 0~10 part of air and/or oxygen.
Further, in the step 2), when material is heated to 150~340 DEG C, nitrogen protection is used above material；Material
When being heated to 340~400 DEG C, air conservation is used above material.
Wherein, in the step 2), the speed of material heating is 0.1~10 DEG C/min.Preferably, heating speed is 4~6
℃/min。
Tobacco distillate of the present invention is preparing the application in tobacco product, the tobacco product be cigarette, cigar,
Chewing tobacco, buccal cigarette, snuff, electric heating type tobacco product, fuel hot type tobacco product, tobacco spray product, chewing gum, tobacco
One of thin slice and electronic cigarette.
Tobacco product containing tobacco distillate of the present invention, which is characterized in that the tobacco product further includes porous
Starch, titanium dioxide, calgon, expanded cut tobacco, expanded cut stem, ethyl alcohol, water, ethylene glycol, glycerol, rapeseed oil, palm oil,
One of corn oil, calcium carbonate, surfactant are a variety of.
Wherein, in the tobacco product in terms of tobacco product gross mass, the tobacco distillate of addition is 0.3~10% mass
Than.
Specifically, the surfactant is selected from sorbierite, potassium citrate and guar gum, Sodium Polyacrylate, polypropylene
One of sour ammonium, polyvinylpyrrolidone and sodium alginate or two or more mixtures.
Further, tobacco distillate and glycerol, propylene glycol, water are mixed according to mass ratio 0.2~0.4:4:5:0.5~0.8
Close uniformly to get arrive tobacco juice for electronic smoke.
Tobacco distillate by mass fraction 4~6% addition obtain coating fluid, further include in coating fluid mass content be 20~
50% calcium carbonate, 0.3~0.6% calgon, 0.1~0.3% Sodium Polyacrylate and surplus water.
Tobacco distillate and porous-starch are uniformly mixed according to mass ratio 3:6~8, and are sealed 2 days to get to having
The material of slow-release function；The obtained material with slow-release function is added in 20g chewing gum base rubber, chewing gum is made.
Tobacco distillate is sprayed on pipe tobacco, and the two mass ratio is 0.2~0.4:100, is prepared into manual cigarette.
The beneficial effects of the present invention are:
The present invention provides a kind of tobacco distillate, preparation method and applications.By under gas atmosphere, certain temperature
In range, distillation tobacco-containing material obtains distillate, which has the tobacco flavors such as strong burnt odor, faint scent and radix aucklandiae.This
The preparation method of invention can be carried out in the case where stirring or not stirring；And the collection method of distillate can be distillate
It is collected into same container, the temperature and time that can also be distillated according to difference carries out Fractional Collections into different containers.
By the distillate be applied to chewing tobacco, buccal cigarette, snuff, electric heating tobacco product, fuel hot type tobacco product,
Tobacco spray product and electronic cigarette etc. can make these products largely close with traditional cigarette taste.This is distillated
When object is used as perfuming cigarette, have the effects that increase solid sense, fine and smooth flue gas to flue gas.
Specific embodiment
The present invention is now illustrated with following most preferred embodiment, but is not intended to limit the scope of the invention.In embodiment, such as nothing
Specified otherwise, used device and method are the device and method of fields routine.
Embodiment 1
Tobacco leaf (75g) is soaked in the ethyl alcohol (mass fraction, similarly hereinafter) of 450mL 95%, under the auxiliary of ultrasonic wave,
Room temperature is extracted 3 hours, and filtrate is concentrated after filtering and removes ethyl alcohol, obtains concentrate.
It takes concentrate (6g) to be placed under nitrogen atmosphere, and begins to warm up in 150 DEG C to 340 DEG C, to heat up per minute 5 DEG C
Speed collects distillate.When not apparent substance distillates, using the gas above air displacement bottoms, continue
It distills and is warming up to 400 DEG C with 5 DEG C of the speed of heating up per minute, when not apparent liquid distillate, stop heating.
Obtained distillate merges, and obtains 150~400 DEG C of fractions.
Same preparation method, distillate nonjoinder are labeled as 150~340 DEG C of fractions and 340~400 DEG C of fractions.
Embodiment 2
Tobacco leaf (1kg) and 50mL ethyl alcohol (95%) are added in means of supercritical extraction equipment, in the extracting pressure of 40MPa, and
Under 50 DEG C of extraction temperature, using carbon dioxide draw 3 hours, the obtained extract concentration containing ethyl alcohol is then removed into second
Alcohol obtains concentrate.It takes concentrate (6g) under nitrogen/air (volume ratio 20:1) atmosphere, and is begun to warm up in 150 DEG C
400 DEG C, with 5 DEG C of the speed of heating up per minute, in not apparent distillate, stop heating.Obtained distillate is cigarette
Careless distillate.
Embodiment 3
Tobacco leaf (50g) is soaked in 300mL ethyl alcohol (95%), under the auxiliary of ultrasonic wave, room temperature is extracted 3 hours, mistake
Filtrate is concentrated after filter and removes ethyl alcohol, obtains concentrate.Concentrate (6g) is taken to begin to warm up under nitrogen atmosphere, and in 150 DEG C
To 400 DEG C, with 5 DEG C of the speed of heating up per minute, in not apparent distillate, stop heating.Obtained distillate is
Tobacco distillate.
Embodiment 4
150~400 DEG C of fractions obtained in embodiment 1 are taken into 0.3g and glycerol (4g), propylene glycol (5g) and water (0.7g)
It is uniformly mixed to get tobacco juice for electronic smoke is arrived.It is similar with cigarette that suction taste can be obviously experienced when suction, and is had apparent burnt
Fragrant, faint scent and radix aucklandiae.
150~340 DEG C of fractions obtained in embodiment 1 are taken into 0.3g and glycerol (4g), propylene glycol (5g) and water (0.7g)
It is uniformly mixed to get tobacco juice for electronic smoke is arrived.Can be experienced when suction suction taste it is similar with cigarette, and have apparent faint scent and
Radix aucklandiae, and distant burnt odor.
Embodiment 5
Tobacco distillate will be obtained in embodiment 3 to be added in coating fluid by mass fraction 5%, is coated in painting process
To reconstituted tobacoo.Obtained thin slice is put in the device that can heat and have suction nozzle with battery unit, heating sheet is to 300 DEG C, suction
Suction taste can be obviously experienced when steam and cigarette is closely similar, and there is apparent burnt odor, faint scent.
Embodiment 6
It obtains tobacco distillate 0.3g in Example 2 to be uniformly mixed with 0.7g porous-starch respectively, and in sealing
2 days are saved in vial to get the material with slow-release function is arrived；The obtained material addition with slow-release function is existed
In 20g chewing gum base rubber, it is uniformly mixed to get Chewing gum tobacco product is arrived.The Chewing gum tobacco product has and cigarette
Taste is similar, and has the characteristics that flavor component discharges slow and apparent burnt odor.
Embodiment 7
150~400 DEG C of fractions of the gained of Example 1, embodiment 2 obtain each 0.3g of tobacco distillate in embodiment 3, point
Be not sprayed on 100g cigarette shreds, be prepared into manual cigarette, by comment cigarette teacher aspirate and respectively and without sprinkling distillate phase
It is compared with cigarette, can experience distillate has the effects that flue gas to increase solid sense, fine and smooth flue gas.Specifically, containing real
The manual cigarette for applying 1 150~400 DEG C of fractions of gained of example has solid sense and the exquisiteness sense of balance；Contain 2 gained tobacco of embodiment
The manual cigarette of distillate has more solid sense and less fine and smooth sense；Craft containing 3 gained tobacco distillate of embodiment
Cigarette has less solid sense and clearly fine and smooth sense.
Above embodiment be only preferred embodiments of the present invention will be described, not to the scope of the present invention into
Row limits, and without departing from the spirit of the design of the present invention, this field ordinary engineering and technical personnel is to technical side of the invention
The all variations and modifications that case is made, should fall within the scope of protection determined by the claims of the present invention.
Claims (2)
1. a kind of tobacco distillate, which is characterized in that be the distillate that tobacco material is carried out to distillation acquisition；
The tobacco material is tobacco extract, tobacco extract, tobacco leaf, the distillate for being evaporated under reduced pressure tobacco extract acquisition, subtracts
The difficult volatile materials of pressure distillation tobacco extract acquisition, the distillate of short-path distillation tobacco extract, short-path distillation tobacco mention
Take one of difficult volatile materials of object or a variety of；
The tobacco distillate is prepared by following steps:
1) tobacco material is placed in solvent and extracts；
The solvent be mass fraction be 95~99% ethanol solution, tobacco material be placed in solvent that ultrasound mentions at normal temperature
It takes, the mass volume ratio of tobacco material and solvent is 1g:1~10mL；
Or, solvent is added in tobacco material, mentioned under 38~45MPa extracting pressure, 48~55 DEG C of extraction temperatures with carbon dioxide
It takes；The mass volume ratio of tobacco material and solvent is 100g:5~15mL；
2) step 1) resulting material is heated, the speed of material heat temperature raising is 0.1~10 DEG C/min, collect temperature be 150~
Distillate between 400 DEG C when material is heated to 150~340 DEG C, uses nitrogen protection above material；Material is heated to 340~400
DEG C when, use air conservation above material.
2. the tobacco product containing tobacco distillate described in claim 1, which is characterized in that the tobacco product is cigarette, snow
Eggplant cigarette, chewing tobacco, buccal cigarette, snuff, electric heating type tobacco product, fuel hot type tobacco product, tobacco spray product, mouth are fragrant
One of sugar, reconstituted tobacoo and electronic cigarette；
The tobacco product further include porous-starch, titanium dioxide, calgon, expanded cut tobacco, expanded cut stem, ethyl alcohol, water,
One of ethylene glycol, glycerol, rapeseed oil, palm oil, corn oil, calcium carbonate, surfactant are a variety of；
In the tobacco product in terms of tobacco product gross mass, the tobacco distillate of addition is 0.3~10% mass ratio.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410848930.2A CN104757703B (en) | 2014-12-31 | 2014-12-31 | A kind of tobacco distillate and its preparation and application |
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| CN201410848930.2A CN104757703B (en) | 2014-12-31 | 2014-12-31 | A kind of tobacco distillate and its preparation and application |
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| CN104757703A CN104757703A (en) | 2015-07-08 |
| CN104757703B true CN104757703B (en) | 2019-04-23 |
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| CN105146734A (en) * | 2015-08-14 | 2015-12-16 | 贵州中烟工业有限责任公司 | Maotai-flavor tobacco product capable of avoiding burning as being heated and preparation method of tobacco product |
| CN105105317A (en) * | 2015-08-14 | 2015-12-02 | 贵州中烟工业有限责任公司 | Strong-flavor type tobacco product being nonflammable while heating and preparation method thereof |
| CN105249524A (en) * | 2015-08-14 | 2016-01-20 | 贵州中烟工业有限责任公司 | Fragrance type heating nonflammable tobacco product and preparation method thereof |
| CN105639718B (en) * | 2016-02-29 | 2017-06-30 | 湖北中烟工业有限责任公司 | A kind of preparation method and application of the tobacco extract of easy low-temperature atomizing |
| CN106235391B (en) * | 2016-10-20 | 2018-09-21 | 云南瑞升烟草技术（集团）有限公司 | The preparation method of tobacco flavor compensating particles and its application in reconstituted tobacco |
| CN107361403B (en) * | 2017-08-07 | 2018-09-18 | 武汉纺织大学 | A kind of cigarette of additive in cigarette and preparation method thereof containing Extracts of Tupistra chinensis |
| TWI735834B (en) * | 2017-12-27 | 2021-08-11 | 日商日本煙草產業股份有限公司 | Tobacco extract, method of producing tobacco extract, and non-combustion type flavor aspirator using tobacco extract |
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| CN110432535A (en) * | 2019-08-22 | 2019-11-12 | 河南中烟工业有限责任公司 | A kind of buccal cigarette of tobacco extract fermentation preparation |
| WO2022137745A1 (en) | 2020-12-21 | 2022-06-30 | 日本たばこ産業株式会社 | Tobacco-component-concentrated liquid, method for manufacturing same, flavor-producing article, and method for manufacturing same |
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