CN102619134A - Aroma improvement method for filter stick forming paper - Google Patents
Aroma improvement method for filter stick forming paper Download PDFInfo
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- CN102619134A CN102619134A CN2012100611769A CN201210061176A CN102619134A CN 102619134 A CN102619134 A CN 102619134A CN 2012100611769 A CN2012100611769 A CN 2012100611769A CN 201210061176 A CN201210061176 A CN 201210061176A CN 102619134 A CN102619134 A CN 102619134A
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Abstract
The invention discloses an aroma improvement method for filter stick forming paper. The method comprises the following steps of: (1) mixing the Yunnan K326 planted in Yunnan and Yunnan Honghuadajinyuan tobacco leaves in a proportion of 1:(1-3), crushing or shredding to obtain a fragrance source, and performing normal-temperature extraction for 48 hours by use of 95-98% of ethanol solution to obtain fragrance extract; (2) performing pressure-reduced distillation of the filtrate under the conditions that the vacuum degree is 0.02-0.08MPa and the temperature is 60-85 DEG C, and separating to obtain an aromatic substance with a boiling point of 150-260 DEG C at normal pressure; and (3) coating the aromatic substance on the forming paper in a manner that the aromatic substance accounts for 0.5-4.0% of the mass of the dry forming paper. In the invention, the tobacco aromatic substance is added, and miscellaneous gas is not led in during cigarette suction so as to achieve the aims of increasing the cigarette aroma, regulating the cigarette flavor, improving the comfort and promoting the cigarette suction quality. By selecting proper fragrance and an extraction method and combining a coating method with a drying method, the invention develops a method capable of obviously increasing the aroma and effectively improving the cigarette suction quality without influencing the performance of the filter stick forming paper.
Description
Technical field
The present invention relates to a kind of cigarette material, more particularly, is a kind of cigarette filter rod shaping paper that has added the tobacco aroma component.
Background technology
Filter stick except cigarette smoke is carried out " cutting ", also need carry out " modification " to flue gas as the filtration system to cigarette smoke.Shaping paper is claimed filter rod paper again; Belong to industrial slim extraordinary stationery; Be mainly used in the tobacco business cigarette filter rod and wrap up acetate silk, in the cigarette filter stick structure, be between inner acetate silk and the outer tipping paper, be divided into plain edition and high-transparency.Shaping paper is to play the effect of parcel tow as one of the part of filter stick its function.Along with the development and the tobacco business keen competition day by day of tobacco technology, whether product technology content and differentiation personality elements become product can persistent existence and the key factor of tremendous development.Because the traditional limitation of cigarette supplementary on application characteristic, the application of cigarette functional auxiliary materials become the important technical that improves product technology content gradually.The Chinese style cigarette direction of the high fragrance of current China's tobacco business forward, low harm, low tar develops high-end cigarette brand, and this certainly will require constantly to provide the product development and the achievements conversion of new technologies and materials direction.Filter stick is as a chief component of cigarette material, because effective part harmful components in the filtering flue gas, thereby obtained paying attention to widely and application.Along with the development trend of tobacco business reducing tar and reducing harm and the propelling of reducing tar and reducing harm work, the research of shaping paper more and more receives tobacco worker's concern.But about the research of shaping paper, one type is through changing the air permeability of shaping paper, utilizing its dilution flue gas to realize the purpose of lowering harm and decreasing coking at present; Another kind of research is the purpose that reaches lowering harm and decreasing coking through the suction-operated of shaping paper and coating.And flue gas is carried out the research of " modification " to shaping paper; Remove Chinese patent 200610163871.0 and address the adding sweetener component; Can increase the sweet rhythm and abundant sense of flue gas; Improve outside the comfortableness of oral cavity, for for further promote the cigarette smoking quality, enrich cigarette odor-absorbing, the fragrant achievement in research that in shaping paper, adds the tobacco aroma component of harmony cigarette also do not appear in the newspapers.Because shaping paper is to moisture-sensitive, unfavorable factor such as shaping paper is easy to generate distortion, fold during high humidity, and air permeability is influenced.Therefore, in shaping paper, add aroma component, be the blank field in the production of cigarettes always.
Summary of the invention
The flavouring method that the purpose of this invention is to provide a kind of filter rod forming paper.
Invention realizes above-mentioned purpose through following technical scheme:
Invention provides a kind of flavouring method of filter rod forming paper; It is characterized in that may further comprise the steps: 1:1 ~ 3 mixed are pressed with the big gold dollar tobacco leaf of Yunnan K326, Yunnan safflower of Yunnan plantation in (1); Pulverizing or chopping are as spice source; Ethanolic solution with 95% ~ 98% carries out the normal temperature lixiviate and obtains the spices leaching liquor, and wherein the ratio of spice source and ethanolic solution is 1:3 ~ 1:20, and extraction time is 48 hours; (2) filtrating is that 0.02 ~ 0.08MPa, temperature are to carry out decompression distillation under 60 ~ 85 ℃ the condition in vacuum, separates that to obtain boiling point under the normal pressure be 150 ~ 260 ℃ aroma component material; (3) distillate is coated on the shaping paper according to 0.5%～4.0% amount.
The described spice source of step (1) need pass through and be crushed into 60 ~ 120 purpose powder particles.Carry out the normal temperature lixiviate after the pulverizing, extraction time is 48 hours.Preserve under the distillate sealed environment that step (2) is obtained.The described coating of step (3) is to coat the one side that shaping paper is used to wrap up acetate silk.
Through decompression distillation, obtain boiling point under the normal pressure and be 150 ~ 260 ℃ aroma component material.These compositions possibly mainly contain: dihydrogeraniol, beta-myrcene, leaf-alcohol, linalool, 2; 3-butanediol, geraniol, furfuryl alcohol, tetrahydrolinalool, α-pine needle alcohol, 5-methylfuran aldehyde, 6-methyl-5-hepten-2-one, maltol, isophorone, 4-oxidation isophorone, ethyl caprilate, ethyl pelargonate, butene dioic acid diethylester, gamma-butyrolacton, γ-second lactone, furfural, 5 methyl furfural, 2-acetyl furan, furfuryl acetate, 3-ethylpyridine, 2; 5-dimethyl pyrazine, 2,3-dimethyl pyrazine, 2,6-dimethyl pyrazine, 2; 3; 5,6-Tetramethylpyrazine, 2-ethyl-3,5-dimethyl pyrazine, 2; 3,5-trimethylpyrazine, 2-acetyl pyrrole.
Cigarette is when inhaling combustion, and is big near the pressure of the pressure ratio axial centre of shaping paper end.Adopt shaping paper of the present invention; Utilize the tangible underbalance effect that shaping paper is outer, inboard and all exist from shaping paper end to axial centre; The tobacco aroma component that makes dip-coating or coat shaping paper gets into main flume with diluent air; Reach raising cigarette flavor concentration, harmony cigarette perfume, improve comfortableness, promote the purpose of cigarette quality.
Through the shaping paper that the inventive method obtained, especially be suitable as the shaping paper of Guangdong China Tobacco Industry Co.,Ltd's double happiness series cigarette.
Compared with prior art, the present invention has following beneficial effect:
1. the present invention adds the tobacco aroma component, when cigarette smoking, does not introduce assorted gas, reaches raising cigarette flavor concentration, harmony cigarette perfume, improves comfortableness, promotes the purpose of cigarette quality.Selected spice source is to obtain through series of selection; This spice source can be so that when the very small amount of extract of coating; Even shaping paper produces tangible good aroma; Through combining with method for distilling and coating process, drying means, the present invention finds out and a kind ofly both can add obvious fragrance, does not influence the method for shaping paper shape and air permeability again.
2. the shaping paper that the present invention obtained especially is suitable as the shaping paper of Guangdong China Tobacco Industry Co.,Ltd's double happiness trade mark cigarette.The result of the test of smokeing panel test shows that the lifting amplitude of its score of smokeing panel test was the highest when it was used as double happiness trade mark filter rod forming paper, and the sense organ top score increases by 1.2 fens.
3. the selected tobacco aroma component of the present invention combines the process conditions and the know-why of shaping paper production; Having adopted the method for decompression distillation to separate to obtain boiling point under the normal pressure is 150 ~ 260 ℃ material; Avoided the loss of tobacco extract when shaping paper is produced, the tobacco aroma component gets into main flume when being more conducive to cigarette smoking simultaneously.
4. final products of the present invention derive from tobacco, its application on filter rod forming paper bring for this perfume (or spice) of tobacco, can not introduce the external source breath, for the design of cigarette provides new thinking and technological means.
5. production technology of the present invention is simple, need not transform and can produce existing shaping paper producing apparatus, is convenient to industrialization promotion.
The specific embodiment
Below further specify technical scheme of the present invention through concrete embodiment.But they are not to qualification of the present invention.In order further to verify beneficial effect of the present invention, the present invention is also with cigarette that makes and the contrast of undressed control group cigarette.
The specific embodiment
Embodiment 1
The flavouring method of shaping paper: with Yunnan plant Yunnan K326, the big gold dollar tobacco leaf of Yunnan safflower dry to moisture be about 10.0%, press the 1:1 mixed, be crushed to 120 orders, as spice source.According to the mixed of solid-liquid ratio 1:10, the ethanolic solution with 95% carried out the normal temperature lixiviate 48 hours, obtained the spices leaching liquor; (2) filtrating is that 0.02 ~ 0.08MPa, temperature are to carry out decompression distillation under 75 ℃ the condition in vacuum, and the cut that obtains is aroma component.
By account for the dried paper of shaping paper heavy 2.5% take by weighing the tobacco distillate, with the dilution of 20% ethanolic solution, obtain required coating fluid after stirring.Said coating fluid is added on the shaping paper that air permeability is 12000CU by routine shaping paper production technology profit, dries then, cut, pack, the cigarette filter that obtains adding the tobacco aroma component is used shaping paper.
On the shaping paper with above-mentioned acquisition, appoint and to get three zones and carry out the air permeability test, the result is: 11880CU, and 11950CU, 11850CU, and not through the shaping paper contrast of flavouring method, air permeability does not all have significant difference.
The shaping paper of above-mentioned acquisition is cut, packed; The cigarette filter that obtains adding the tobacco aroma component is used shaping paper; Be applied to the test of smokeing panel test on Guangdong China Tobacco Industry Co.,Ltd's double happiness, double happiness (WUYESHENG), double happiness (the red rose king) trade mark cigarette respectively, the result is as shown in table 1:
The smoking result of the shaping paper of table 1. embodiment 1
| The cigarette specification | The fragrance score improves | The harmony score improves | The pleasant impression score improves | Stimulate score to improve | The assorted branch of being so incensed that improves | PTS improves |
| Double happiness | 0.5 | 0.2 | 0.2 | 0.15 | 0.15 | 1.2 |
| Double happiness (WUYESHENG) | 0.5 | 0.1 | 0.1 | 0.05 | 0.1 | 0.85 |
| Double happiness (red rose king) | 0.25 | 0.1 | 0.1 | 0.05 | 0.05 | 0.55 |
According to smoking result, through the shaping paper that flavouring method obtained of embodiment 1, be applied in the cigarette fragrance and send out plentiful thoroughly, clear submissive, increase the sense of promoting the production of body fluid, harmony is comfortable.Especially in the application of double happiness cigarette, can make the score of smokeing panel test promote 1.2 fens.
Embodiment 2
The flavouring method of shaping paper: with Yunnan plant Yunnan K326, the big gold dollar tobacco leaf of Yunnan safflower dry to moisture be about 10.0%, press the 1:3 mixed, be crushed to 100 orders, as spice source.According to the mixed of solid-liquid ratio 1:10, the ethanolic solution with 98% carried out the normal temperature lixiviate 48 hours, obtained the spices leaching liquor; (2) filtrating is that 0.02 ~ 0.08MPa, temperature are to carry out decompression distillation under 80 ℃ the condition in vacuum, and the cut that obtains is aroma component. (3) by account for the dried paper of shaping paper heavy 3% take by weighing the tobacco distillate, distillate is coated on the common shaping paper on (0 CU).
The shaping paper of above-mentioned acquisition is cut, packed, and the cigarette filter that obtains adding the tobacco aroma component is used shaping paper, and gained shaping paper is applied to non-ventilation filter tip cigarette, can increase cigarette smoke concentration, makes cigarette flavor
Pass through and send out harmony.
Embodiment 3
The flavouring method of shaping paper: with Yunnan plant Yunnan K326, the big gold dollar tobacco leaf of Yunnan safflower dry to moisture be about 10.0%, press the 1:2 mixed, be crushed to 100 orders, as spice source.According to the mixed of solid-liquid ratio 1:3, the ethanolic solution with 98% carried out the normal temperature lixiviate 48 hours, obtained the spices leaching liquor; (2) filtrating is carried out decompression distillation under 0.02 ~ 0.08MPa, temperature are 80 ℃ condition, and the cut that obtains is aroma component; (3) by account for the dried paper of shaping paper heavy 4% take by weighing the tobacco distillate, be coated on the 5000CU shaping paper.Gained shaping paper is applied to the filter tip cigarette that ventilates, and makes the cigarette flavor exquisiteness soft, enriches harmony.
Embodiment 4
The flavouring method of shaping paper: with Yunnan plant Yunnan K326, the big gold dollar tobacco leaf of Yunnan safflower dry to moisture be about 10.0%, press the 1:2.5 mixed, be crushed to 100 orders, as spice source.According to the mixed of solid-liquid ratio 1:8, the ethanolic solution with 95% carried out the normal temperature lixiviate 48 hours, obtained the spices leaching liquor; (2) filtrating is that 0.02 ~ 0.08MPa, temperature are to carry out decompression distillation under 80 ℃ the condition in vacuum, and the cut that obtains is aroma component; (3) by account for the dried paper of shaping paper heavy 2% take by weighing the tobacco distillate, be coated on the common shaping paper.Gained shaping paper is applied to non-ventilation filter tip cigarette, can make cigarette flavor send out plentiful thoroughly, and is clear submissive, increases the sense of promoting the production of body fluid, and harmony is comfortable.
Embodiment 5
The flavouring method of shaping paper: with Yunnan plant Yunnan K326, the big gold dollar tobacco leaf of Yunnan safflower dry to moisture be about 10.0%, press the 1:2 mixed, be crushed to 120 orders, as spice source.According to the mixed of solid-liquid ratio 1:15, the ethanolic solution with 95% carried out the normal temperature lixiviate 48 hours, obtained the spices leaching liquor; (2) filtrating is that 0.02 ~ 0.08MPa, temperature are to carry out decompression distillation under 70 ℃ the condition in vacuum, and the cut that obtains is aroma component; (3) by account for the dried paper of shaping paper heavy 4% take by weighing the tobacco distillate, be coated on the 6000CU shaping paper, gained shaping paper is applied to the filter tip cigarette that ventilates, it is rich to promote cigarette flavor, makes fragrance pure and mild abundant, the pure Hui Tian of pleasant impression.
Embodiment 5
Like embodiment 1, but the tobacco of adopting separately is Yunnan K326.Be used for the double happiness cigarette, the result is as shown in table 2 for evaluation and analysis:
The smoking result of the shaping paper of table 2. embodiment 5
| The cigarette specification | The fragrance score improves (branch) | The harmony score improves (branch) | The pleasant impression score improves (branch) | Stimulate score to improve (branch) | The assorted branch of being so incensed that improves (branch) | PTS improves (branch) |
| The double happiness cigarette | 0.1 | 0.1 | 0.1 | 0.05 | 0.05 | 0.4 |
Claims (6)
1. the flavouring method of a filter rod forming paper; The big gold dollar tobacco leaf of Yunnan K326, Yunnan safflower that it is characterized in that Yunnan is planted is by 1:1 ~ 3 mixed; Adopt ethanol to carry out lixiviate after pulverizing or the chopping; Tobacco extract is that 0.02 ~ 0.08MPa, temperature are to carry out decompression distillation under 60 ~ 85 ℃ the condition in vacuum, separates obtaining the aroma component material; The aroma component material is coated on the shaping paper according to 0.5%～4.0% the amount that accounts for the dried paper weight of shaping paper.
2. the flavouring method of filter rod forming paper as claimed in claim 1 is characterized in that it is that boiling point is 150 ~ 260 ℃ an aroma component material under the normal pressure that described decompression distillation separates what obtain.
3. the flavouring method of filter rod forming paper as claimed in claim 1; It is characterized in that described aroma component contains dihydrogeraniol, beta-myrcene, leaf-alcohol, linalool, 2,3-butanediol, geraniol, furfuryl alcohol, tetrahydrolinalool, α-pine needle alcohol, 5-methylfuran aldehyde, 6-methyl-5-hepten-2-one, maltol, isophorone, 4-oxidation isophorone, ethyl caprilate, ethyl pelargonate, butene dioic acid diethylester, gamma-butyrolacton, γ-second lactone, furfural, 5 methyl furfural, 2-acetyl furan, furfuryl acetate, 3-ethylpyridine, 2,5-dimethyl pyrazine, 2; 3-dimethyl pyrazine, 2; 6-dimethyl pyrazine, 2,3,5; 6-Tetramethylpyrazine, 2-ethyl-3; 5-dimethyl pyrazine, 2,3,5-trimethylpyrazine and 2-acetyl pyrrole.
4. the flavouring method of filter rod forming paper as claimed in claim 1; It is characterized in that tobacco extract is to be obtained by following steps: 1:1 ~ 3 mixed are pressed with the big gold dollar tobacco leaf of Yunnan K326, Yunnan safflower of Yunnan plantation in (1); Pulverizing or chopping are as spice source; Ethanolic solution with 95% ~ 98% carries out the normal temperature lixiviate and obtains the spices leaching liquor, and wherein the ratio of spice source and ethanolic solution is 1:3 ~ 1:20, and extraction time is 48 hours; (2) filtrating is that 0.02 ~ 0.08MPa, temperature are to carry out decompression distillation under 60 ~ 85 ℃ the condition in vacuum, separates that to obtain boiling point under the normal pressure be 150 ~ 260 ℃ aroma component material; (3) distillate is coated on the shaping paper according to 0.5%～4.0% amount.
5. the flavouring method of filter rod forming paper as claimed in claim 1 is characterized in that the described coating of step (3) is to coat the one side that shaping paper is used to wrap up acetate silk.
6. the shaping paper that flavouring method obtained of filter rod forming paper as claimed in claim 1 is characterized in that being applied on Guangdong China Tobacco Industry Co.,Ltd's double happiness series cigarette.
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| CN104757703A (en) * | 2014-12-31 | 2015-07-08 | 贵州中烟工业有限责任公司 | Tobacco distillate, and preparation and application thereof |
| CN105105310A (en) * | 2015-08-19 | 2015-12-02 | 湖北中烟工业有限责任公司 | Preparation method of cigar wrapper tobacco |
| CN107348556A (en) * | 2017-07-31 | 2017-11-17 | 云南中烟新材料科技有限公司 | A kind of preparation method for being used to prepare forming paper and its cigarette core that English fire-cured tobacco type heats the cigarette cigarette core that do not burn |
| CN108420106A (en) * | 2018-03-22 | 2018-08-21 | 宝可科技（上海）有限公司 | A kind of filter tip perfume (or spice) and its preparation method and application |
| CN110514760A (en) * | 2019-08-26 | 2019-11-29 | 上海烟草集团有限责任公司 | A kind of evaluation method of the cigarette package leakproofness based on chemical marker |
| CN112064405A (en) * | 2020-09-07 | 2020-12-11 | 云南中烟工业有限责任公司 | Special aroma forming paper prepared from rice dyeing flower and method and application thereof |
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| CN107348556B (en) * | 2017-07-31 | 2019-08-30 | 云南中烟新材料科技有限公司 | A kind of preparation method for being used to prepare English fire-cured tobacco type and heating the forming paper and its cigarette core of the cigarette cigarette core that do not burn |
| CN108420106A (en) * | 2018-03-22 | 2018-08-21 | 宝可科技（上海）有限公司 | A kind of filter tip perfume (or spice) and its preparation method and application |
| CN110514760A (en) * | 2019-08-26 | 2019-11-29 | 上海烟草集团有限责任公司 | A kind of evaluation method of the cigarette package leakproofness based on chemical marker |
| CN112064405A (en) * | 2020-09-07 | 2020-12-11 | 云南中烟工业有限责任公司 | Special aroma forming paper prepared from rice dyeing flower and method and application thereof |
| CN112064405B (en) * | 2020-09-07 | 2022-09-13 | 云南中烟工业有限责任公司 | Special fragrant forming paper prepared from rice dyeing flower and method and application thereof |
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