CN110373266A - A kind of fragrance-enhancing tobacco agent and its application - Google Patents
A kind of fragrance-enhancing tobacco agent and its application Download PDFInfo
- Publication number
- CN110373266A CN110373266A CN201910574804.5A CN201910574804A CN110373266A CN 110373266 A CN110373266 A CN 110373266A CN 201910574804 A CN201910574804 A CN 201910574804A CN 110373266 A CN110373266 A CN 110373266A
- Authority
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- China
- Prior art keywords
- tobacco
- fragrance
- lotus
- enhancing
- conch meal
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Links
- 241000208125 Nicotiana Species 0.000 title claims abstract description 134
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 134
- 240000002853 Nelumbo nucifera Species 0.000 claims abstract description 128
- 235000006508 Nelumbo nucifera Nutrition 0.000 claims abstract description 128
- 235000006510 Nelumbo pentapetala Nutrition 0.000 claims abstract description 128
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 105
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 99
- 239000000284 extract Substances 0.000 claims abstract description 79
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 62
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 45
- 235000013311 vegetables Nutrition 0.000 claims abstract description 33
- 239000002994 raw material Substances 0.000 claims abstract description 16
- 235000012054 meals Nutrition 0.000 claims description 62
- XPPKVPWEQAFLFU-UHFFFAOYSA-N diphosphoric acid Chemical group OP(O)(=O)OP(O)(O)=O XPPKVPWEQAFLFU-UHFFFAOYSA-N 0.000 claims description 40
- 229940005657 pyrophosphoric acid Drugs 0.000 claims description 39
- 238000002360 preparation method Methods 0.000 claims description 36
- WNGSUWLDMZFYNZ-UHFFFAOYSA-N Leonurine Chemical compound COC1=CC(C(=O)OCCCCN=C(N)N)=CC(OC)=C1O WNGSUWLDMZFYNZ-UHFFFAOYSA-N 0.000 claims description 22
- 238000000605 extraction Methods 0.000 claims description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
- 239000007864 aqueous solution Substances 0.000 claims description 9
- 238000010438 heat treatment Methods 0.000 claims description 8
- 235000019441 ethanol Nutrition 0.000 claims description 7
- 238000007654 immersion Methods 0.000 claims description 2
- 210000003296 saliva Anatomy 0.000 claims 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract description 12
- 239000003546 flue gas Substances 0.000 abstract description 11
- 239000000463 material Substances 0.000 abstract description 8
- 238000002485 combustion reaction Methods 0.000 abstract description 5
- 239000002304 perfume Substances 0.000 abstract description 4
- 239000000843 powder Substances 0.000 description 26
- 238000002137 ultrasound extraction Methods 0.000 description 25
- 239000000706 filtrate Substances 0.000 description 19
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 description 17
- 239000000243 solution Substances 0.000 description 15
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 12
- 238000000227 grinding Methods 0.000 description 12
- 238000005374 membrane filtration Methods 0.000 description 12
- 238000007873 sieving Methods 0.000 description 12
- 238000001291 vacuum drying Methods 0.000 description 12
- XKABJYQDMJTNGQ-VIFPVBQESA-N n-nitrosonornicotine Chemical compound O=NN1CCC[C@H]1C1=CC=CN=C1 XKABJYQDMJTNGQ-VIFPVBQESA-N 0.000 description 7
- 238000001354 calcination Methods 0.000 description 6
- 239000003205 fragrance Substances 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- 239000000654 additive Substances 0.000 description 4
- 230000000996 additive effect Effects 0.000 description 4
- 238000012986 modification Methods 0.000 description 4
- 230000004048 modification Effects 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 239000000523 sample Substances 0.000 description 4
- 239000000779 smoke Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 230000007794 irritation Effects 0.000 description 3
- 244000269722 Thea sinensis Species 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 235000009508 confectionery Nutrition 0.000 description 2
- 239000013068 control sample Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- LELOWRISYMNNSU-UHFFFAOYSA-N hydrogen cyanide Chemical compound N#C LELOWRISYMNNSU-UHFFFAOYSA-N 0.000 description 2
- 239000006101 laboratory sample Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 150000008442 polyphenolic compounds Chemical class 0.000 description 2
- 235000013824 polyphenols Nutrition 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 235000019505 tobacco product Nutrition 0.000 description 2
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- VAJVDSVGBWFCLW-UHFFFAOYSA-N 3-Phenyl-1-propanol Chemical compound OCCCC1=CC=CC=C1 VAJVDSVGBWFCLW-UHFFFAOYSA-N 0.000 description 1
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- OVSQVDMCBVZWGM-SJWGPRHPSA-N Hyperin Natural products O[C@H]1[C@H](O)[C@@H](O)[C@@H](CO)O[C@H]1OC1=C(C=2C=C(O)C(O)=CC=2)OC2=CC(O)=CC(O)=C2C1=O OVSQVDMCBVZWGM-SJWGPRHPSA-N 0.000 description 1
- FVQOMEDMFUMIMO-UHFFFAOYSA-N Hyperosid Natural products OC1C(O)C(O)C(CO)OC1OC1C(=O)C2=C(O)C=C(O)C=C2OC1C1=CC=C(O)C(O)=C1 FVQOMEDMFUMIMO-UHFFFAOYSA-N 0.000 description 1
- DYUQAZSOFZSPHD-UHFFFAOYSA-N Phenylpropyl alcohol Natural products CCC(O)C1=CC=CC=C1 DYUQAZSOFZSPHD-UHFFFAOYSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 229910052785 arsenic Inorganic materials 0.000 description 1
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 1
- 208000011775 arteriosclerosis disease Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 231100000357 carcinogen Toxicity 0.000 description 1
- 231100000315 carcinogenic Toxicity 0.000 description 1
- 239000003183 carcinogenic agent Substances 0.000 description 1
- 208000026106 cerebrovascular disease Diseases 0.000 description 1
- 235000019506 cigar Nutrition 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000002526 effect on cardiovascular system Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 150000004005 nitrosamines Chemical class 0.000 description 1
- XKLJHFLUAHKGGU-UHFFFAOYSA-N nitrous amide Chemical compound ON=N XKLJHFLUAHKGGU-UHFFFAOYSA-N 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000035479 physiological effects, processes and functions Effects 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 238000004445 quantitative analysis Methods 0.000 description 1
- OVSQVDMCBVZWGM-DTGCRPNFSA-N quercetin 3-O-beta-D-galactopyranoside Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1OC1=C(C=2C=C(O)C(O)=CC=2)OC2=CC(O)=CC(O)=C2C1=O OVSQVDMCBVZWGM-DTGCRPNFSA-N 0.000 description 1
- BBFYUPYFXSSMNV-UHFFFAOYSA-N quercetin-7-o-galactoside Natural products OC1C(O)C(O)C(CO)OC1OC1=CC(O)=C2C(=O)C(O)=C(C=3C=C(O)C(O)=CC=3)OC2=C1 BBFYUPYFXSSMNV-UHFFFAOYSA-N 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 230000002227 vasoactive effect Effects 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
- A24B15/303—Plant extracts other than tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Wood Science & Technology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Agronomy & Crop Science (AREA)
- Botany (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Engineering & Computer Science (AREA)
- Manufacture Of Tobacco Products (AREA)
- Seasonings (AREA)
Abstract
The present invention relates to technical field of cigarettes, and in particular to a kind of fragrance-enhancing tobacco agent and its application.The present invention provides a kind of fragrance-enhancing tobacco agent, the raw material including following parts by weight: propylene glycol and 6-48 parts of vegetables glycerol, and 0.5-3 parts of seedpod of the lotus shell extract.Fragrance-enhancing tobacco agent provided by the invention can effectively reduce the burst size of tar in result of combustion of tobacco flue gas, while can also improve tobacco material suction quality, promote aroma quality and perfume quantity.
Description
Technical field
The present invention relates to technical field of cigarettes, and in particular to a kind of fragrance-enhancing tobacco agent and its application.
Background technique
Main product form of the traditional cigarette (or traditional point lit cigarettes) as tobacco consumption, has more than 100 years
History.Increasing with the public to the reinforcement and government of cigarette recognizing dangers to cigarette control dynamics, countries in the world tobacco
Enterprise strengthens the exploitation to new tobacco products.New tobacco products to be to heat non-combustion-type cigarette as representative at present, wherein
Closest to traditional cigarette in terms of physiology impression, sucking, there is good development potentiality.Heat non-combustion-type cigarette
Feature is heating tobacco rather than burning tobacco, avoids Pintsch process when result of combustion of tobacco, thus the main flume for generating it
The burst size of middle harmful components substantially reduces, and is supplied to the certain tobacco feature impression of consumer.However compared to conventional point
Lit cigarettes, heating non-combustion-type cigarette fragrance, in terms of still have larger gap, seriously affected consumer to it
Approve and receive degree.
Studies have shown that contain about 4000 kinds of known chemical substances in the smog discharged when result of combustion of tobacco, including
About 50 kinds of carcinogens such as smoke tar, hydrocyanic acid, carbon monoxide.Such as: contain a variety of carcinogenic substances in smoke tar, including phenylpropyl alcohol is simultaneously
Bi, every, arsenic, β-how amine etc., though its amount is atomic, have often, repeatedly, long-term accumulation effect.Dissolved with one in smoker's blood
Fixed tar ingredients, vasoactive tube wall can accelerate vascular sclerosis, lead to cardiovascular and cerebrovascular disease.Therefore, it reduces in tobacco
Tar content has become the common recognition of tobacco enterprise, however a large amount of the study found that while reducing tar, a large amount of perfume in tobacco
Taste substance can also greatly reduce, and eventually lead to cigarette perfume deficiency, be unable to satisfy consumer's hobby.How to realize is reducing tar content
While do not weaken tobacco flavor become tobacco industry one of problem.
Summary of the invention
It is an object of the invention to overcome that asking for tobacco flavor can be weakened while reducing tar content in the prior art
Topic, to provide a kind of fragrance-enhancing tobacco agent and its application.
In order to achieve the above objectives, the present invention adopts the following technical scheme:
A kind of fragrance-enhancing tobacco agent, the raw material including following parts by weight: propylene glycol and 6-48 parts of vegetables glycerol, lotus receptacle extract
0.5-3 parts of object.
It preferably, further include 0.02-0.4 parts of leonurine hydrochloride.
It preferably, further include that pyrophosphoric acid is conch meal 0.8-3 parts modified.
Preferably, the preparation method of the modified conch meal of the pyrophosphoric acid includes the following steps:
1) conch meal is calcined at 700-800 DEG C, obtains calcined conch meal；
2) calcined conch meal is placed in pyrophosphoric acid aqueous solution and is impregnated, is dried in vacuo after immersion, pulverize and sieve to obtain
The modified conch meal of the pyrophosphoric acid.
Preferably, the pyrophosphoric acid concentration of aqueous solution is 4-10wt%.
Preferably, the seedpod of the lotus shell extract is to be prepared from lotus receptacle by ethyl alcohol extraction.
Preferably, the preparation method of the seedpod of the lotus shell extract includes the following steps:
1) lotus receptacle is pulverized and sieved, obtains lotus receptacle powder；
2) lotus receptacle powder is added in ethanol water, mixes, obtains lotus receptacle mixed liquor；
3) ultrasonic extraction is carried out to lotus receptacle mixed liquor, extracting solution filtering, filtrate, which is concentrated and dried to obtain the lotus receptacle, to be mentioned
Take object.
Preferably, the mass concentration of the ethanol water is 40-60%.
It preferably, further include 0.1-0.6 parts of tobacco extract.
Preferably, the tobacco extract is to be prepared into from Yunnan tobacco and Zimbabwe's tobacco leaf by ethyl alcohol extraction
It arrives；
The weight ratio of the Yunnan tobacco and Zimbabwe's tobacco leaf is 1:0.8-1.2.
Preferably, the preparation method of the tobacco extract includes the following steps: Yunnan tobacco and Zimbabwe's tobacco leaf
It is added in the ethanol water that mass fraction is 40-60% and is extracted, filtered after extraction, obtain filtrate, filtrate concentration
Drying is to get the tobacco extract.
Preferably, the extraction temperature is 20-40 DEG C, and the extraction time is 6-8 hours.
Preferably, the propylene glycol is 3-45 parts, and the vegetables glycerol is 3-45 parts.
The present invention also provides a kind of fragrance-enhancing tobacco agent described above in point lit cigarettes and/or heating non-combustion-type cigarette
In application.
The fragrance-enhancing tobacco agent can be added in tobacco material in the present invention, and the moisture content in the tobacco material is
6-9%.Preferably, the tobacco material is Filamentous, particle or sheet.When the fragrance-enhancing tobacco agent is applied to heating non-combustion-type
When in cigarette, optionally, cigarette paper used is cigar roll paper.
Beneficial effects of the present invention:
1) present invention provides a kind of fragrance-enhancing tobacco agent, the raw material including following parts by weight: propylene glycol and vegetables glycerol 6-48
Part, 0.5-3 parts of seedpod of the lotus shell extract.Hyperin rich in seedpod of the lotus shell extract, carrotene, has procyanidine
The substances such as machine acid and vitamin, it has been investigated that, the present invention adds lotus receptacle extraction on the basis of propylene glycol, vegetables glycerol
Object can effectively reduce the burst size of tar in result of combustion of tobacco flue gas, while can also improve tobacco material suction quality, promote fragrance
Quality and perfume quantity, the organic acid in seedpod of the lotus shell extract can also neutralize nicotine, reduce the irritation of flue gas.
2) present invention provides a kind of fumet, further includes 0.02-0.4 parts of leonurine hydrochloride further.Inventor
By a large amount of experimental study, has been surprisingly found that and the leonurine hydrochloride of specific quantity is added in tobacco material, with lotus receptacle
Extract, which cooperates, can effectively reduce the burst size of N- nitrosonornicotine in flue gas, this may be due to leonurine uniqueness
Steric configuration make its be more conducive to have an effect with nitrosamines substance, to effectively reduce N- nitrosonornicotine in flue gas
Burst size.
3) present invention provides a kind of fumet, further includes that pyrophosphoric acid is conch meal 0.8-3 parts modified further.The present invention
The creative structure special using pyrophosphoric acid and polyhydroxy feature, is modified conch meal, makes modified conch meal can
The burst size of N- nitrosonornicotine in flue gas is effectively reduced.
4) present invention provides a kind of fumet, and further, the present invention calcines conch meal at 700-800 DEG C,
The organic matter inside conch meal is decomposed, on conch meal surface and internal formation pore structure abundant, then passes through pyrophosphoric acid
Solution is impregnated, and pyrophosphoric acid is made to be attached to conch meal surface and inside, and inventor is found surprisingly that modified by pyrophosphoric acid
Conch meal can effectively reduce the burst size of N- nitrosonornicotine in flue gas.
5) present invention provides a kind of fumet, and further, the invention also includes 0.1-0.6 parts of tobacco extract.It utilizes
Containing the volatile materials such as volatile alcohols, aldehydes, lower fatty acid and its ester in tobacco extract, can be effectively suppressed due to
The addition of PG (propylene glycol) and VG (vegetables glycerol) lead to the sweet sense of flue gas, greatly strengthen suction mouthfeel, improve simultaneously
Fragrance when suction keeps flue gas softer.Further, the tobacco extract is from Yunnan tobacco and Zimbabwe's tobacco leaf
It is prepared by ethyl alcohol extraction；The weight ratio of the Yunnan tobacco and Zimbabwe's tobacco leaf is 1:0.8-1.2.The present invention is from spy
Surely the tobacco extract extracted in the Yunnan tobacco and Zimbabwe's tobacco leaf matched by ethyl alcohol more conducively inhibits due to PG
The sweet sense for leading to flue gas with the addition of VG, makes that fragrance is plentiful, texture is obviously improved.
Specific embodiment
There is provided following embodiments is to preferably further understand the present invention, it is not limited to the best embodiment party
Formula is not construed as limiting the contents of the present invention and protection scope, anyone under the inspiration of the present invention or by the present invention and its
The feature of his prior art is combined and any and identical or similar product of the present invention for obtaining, all falls within of the invention
Within protection scope.
Specific experiment step or condition person are not specified in embodiment, according to the literature in the art described routine experiment
The operation of step or condition can carry out.Reagents or instruments used without specified manufacturer, being can be by commercially available acquisition
Conventional reagent product.
Embodiment 1
Present embodiments provide a kind of fragrance-enhancing tobacco agent, including the following raw material: 3g propylene glycol, 45g vegetables glycerol, 0.5g lotus
Fluffy shell extract.
The preparation method of the seedpod of the lotus shell extract includes the following steps:
1) by 100g lotus receptacle grinding and sieving, lotus receptacle powder is obtained；
2) lotus receptacle powder is added in the ethanol water that 300ml mass fraction is 40%, is uniformly mixed, obtains lotus
Fluffy shell mixed liquor；
3) lotus receptacle mixed liquor is put into ultrasonic extraction tank and is carried out ultrasonic extraction 2 hours, extracting solution membrane filtration
Fall filter residue, filtrate concentration, vacuum drying obtains the seedpod of the lotus shell extract.
Above-mentioned fragrance-enhancing tobacco agent the preparation method is as follows: propylene glycol, vegetables glycerol and seedpod of the lotus shell extract are uniformly mixed
Up to the fragrance-enhancing tobacco agent.
Embodiment 2
Present embodiments provide a kind of fragrance-enhancing tobacco agent, including the following raw material: 45g propylene glycol, 3g vegetables glycerol, the 3g seedpod of the lotus
Shell extract.
The preparation method of the seedpod of the lotus shell extract includes the following steps:
1) by 100g lotus receptacle grinding and sieving, lotus receptacle powder is obtained；
2) lotus receptacle powder is added in the ethanol water that 300ml mass fraction is 60%, is uniformly mixed, obtains lotus
Fluffy shell mixed liquor；
3) lotus receptacle mixed liquor is put into ultrasonic extraction tank and is carried out ultrasonic extraction 3 hours, extracting solution membrane filtration
Fall filter residue, filtrate concentration, vacuum drying obtains the seedpod of the lotus shell extract.
Above-mentioned fragrance-enhancing tobacco agent the preparation method is as follows: propylene glycol, vegetables glycerol and seedpod of the lotus shell extract are uniformly mixed
Up to the fragrance-enhancing tobacco agent.
Embodiment 3
Present embodiments provide a kind of fragrance-enhancing tobacco agent, including the following raw material: 14g propylene glycol, 10g vegetables glycerol, 2g lotus
Fluffy shell extract.
The preparation method of the seedpod of the lotus shell extract includes the following steps:
1) by 100g lotus receptacle grinding and sieving, lotus receptacle powder is obtained；
2) lotus receptacle powder is added in the ethanol water that 200ml mass fraction is 50%, is uniformly mixed, obtains lotus
Fluffy shell mixed liquor；
3) lotus receptacle mixed liquor is put into ultrasonic extraction tank and is carried out ultrasonic extraction 3 hours, extracting solution membrane filtration
Fall filter residue, filtrate concentration, vacuum drying obtains the seedpod of the lotus shell extract.
Above-mentioned fragrance-enhancing tobacco agent the preparation method is as follows: propylene glycol, vegetables glycerol and seedpod of the lotus shell extract are uniformly mixed
Up to the fragrance-enhancing tobacco agent.
Embodiment 4
Present embodiments provide a kind of fragrance-enhancing tobacco agent, including the following raw material: 3g propylene glycol, 3g vegetables glycerol, 1.8g lotus
Fluffy shell extract, 0.08g leonurine hydrochloride, the modified conch meal of 1.5g pyrophosphoric acid, 0.1g tobacco extract.
The preparation method of the seedpod of the lotus shell extract includes the following steps:
1) by 100g lotus receptacle grinding and sieving, lotus receptacle powder is obtained；
2) lotus receptacle powder is added in the ethanol water that 200ml mass fraction is 50%, is uniformly mixed, obtains lotus
Fluffy shell mixed liquor；
3) lotus receptacle mixed liquor is put into ultrasonic extraction tank and is carried out ultrasonic extraction 3 hours, extracting solution membrane filtration
Fall filter residue, filtrate concentration, vacuum drying obtains the seedpod of the lotus shell extract.
The preparation method of the modified conch meal of the pyrophosphoric acid includes the following steps:
1) 200g conch meal is carried out to calcining 1 hour at 800 DEG C, obtains calcined conch meal；
2) calcined conch meal is placed in the pyrophosphoric acid aqueous solution that 500ml concentration is 10wt% and is impregnated 0.5 hour, soaked
It is dried in vacuo after bubble, crushed 30 meshes and obtain the modified conch meal of the pyrophosphoric acid.
The preparation method of the tobacco extract includes the following steps: 100g Yunnan tobacco and 120g Zimbabwe tobacco leaf
It is added in the ethanol water that 1000ml mass fraction is 60% and is extracted, filtered after extraction, obtain filtrate, filtrate is dense
Contracting is dry to get the tobacco extract；The extraction temperature is 20 DEG C, and the extraction time is 8 hours.
Above-mentioned fragrance-enhancing tobacco agent the preparation method is as follows: by propylene glycol, vegetables glycerol, seedpod of the lotus shell extract, leonurine
The modified conch meal of hydrochloride, pyrophosphoric acid and tobacco extract are uniformly mixed up to the fragrance-enhancing tobacco agent.
Embodiment 5
Present embodiments provide a kind of fragrance-enhancing tobacco agent, including the following raw material: 12g propylene glycol, 15g vegetables glycerol, 1.0g
Seedpod of the lotus shell extract, 0.1g leonurine hydrochloride, the modified conch meal of 2.2g pyrophosphoric acid, 0.6g tobacco extract.
The preparation method of the seedpod of the lotus shell extract includes the following steps:
1) by 100g lotus receptacle grinding and sieving, lotus receptacle powder is obtained；
2) lotus receptacle powder is added in the ethanol water that 200ml mass fraction is 50%, is uniformly mixed, obtains lotus
Fluffy shell mixed liquor；
3) lotus receptacle mixed liquor is put into ultrasonic extraction tank and is carried out ultrasonic extraction 3 hours, extracting solution membrane filtration
Fall filter residue, filtrate concentration, vacuum drying obtains the seedpod of the lotus shell extract.
The preparation method of the modified conch meal of the pyrophosphoric acid includes the following steps:
1) 200g conch meal is carried out to calcining 1 hour at 800 DEG C, obtains calcined conch meal；
2) calcined conch meal is placed in the pyrophosphoric acid aqueous solution that 500ml concentration is 10wt% and is impregnated 0.5 hour, soaked
It is dried in vacuo after bubble, crushed 30 meshes and obtain the modified conch meal of the pyrophosphoric acid.
The preparation method of the tobacco extract includes the following steps: 100g Yunnan tobacco and 80g Zimbabwe tobacco leaf
It is added in the ethanol water that 1000ml mass fraction is 40% and is extracted, filtered after extraction, obtain filtrate, filtrate is dense
Contracting is dry to get the tobacco extract；The extraction temperature is 40 DEG C, and the extraction time is 6 hours.
Above-mentioned fragrance-enhancing tobacco agent the preparation method is as follows: by propylene glycol, vegetables glycerol, seedpod of the lotus shell extract, leonurine
The modified conch meal of hydrochloride, pyrophosphoric acid and tobacco extract are uniformly mixed up to the fragrance-enhancing tobacco agent.
Embodiment 6
Present embodiments provide a kind of fragrance-enhancing tobacco agent, including the following raw material: 14g propylene glycol, 10g vegetables glycerol, 2g lotus
Fluffy shell extract, 0.02g leonurine hydrochloride.
The preparation method of the seedpod of the lotus shell extract includes the following steps:
1) by 100g lotus receptacle grinding and sieving, lotus receptacle powder is obtained；
2) lotus receptacle powder is added in the ethanol water that 200ml mass fraction is 50%, is uniformly mixed, obtains lotus
Fluffy shell mixed liquor；
3) lotus receptacle mixed liquor is put into ultrasonic extraction tank and is carried out ultrasonic extraction 3 hours, extracting solution membrane filtration
Fall filter residue, filtrate concentration, vacuum drying obtains the seedpod of the lotus shell extract.
Above-mentioned fragrance-enhancing tobacco agent the preparation method is as follows: by propylene glycol, vegetables glycerol, seedpod of the lotus shell extract and leonurine
Hydrochloride is uniformly mixed up to the fragrance-enhancing tobacco agent.
Embodiment 7
Present embodiments provide a kind of fragrance-enhancing tobacco agent, including the following raw material: 9g propylene glycol, 15g vegetables glycerol, the 1g seedpod of the lotus
Shell extract, 0.4g leonurine hydrochloride.
The preparation method of the seedpod of the lotus shell extract includes the following steps:
1) by 100g lotus receptacle grinding and sieving, lotus receptacle powder is obtained；
2) lotus receptacle powder is added in the ethanol water that 200ml mass fraction is 50%, is uniformly mixed, obtains lotus
Fluffy shell mixed liquor；
3) lotus receptacle mixed liquor is put into ultrasonic extraction tank and is carried out ultrasonic extraction 3 hours, extracting solution membrane filtration
Fall filter residue, filtrate concentration, vacuum drying obtains the seedpod of the lotus shell extract.
Above-mentioned fragrance-enhancing tobacco agent the preparation method is as follows: by propylene glycol, vegetables glycerol, seedpod of the lotus shell extract and leonurine
Hydrochloride is uniformly mixed up to the fragrance-enhancing tobacco agent.
Embodiment 8
Present embodiments provide a kind of fragrance-enhancing tobacco agent, including the following raw material: 9g propylene glycol, 15g vegetables glycerol, the 1g seedpod of the lotus
Shell extract, 0.4g leonurine hydrochloride, the modified conch meal of 0.8g pyrophosphoric acid.
The preparation method of the seedpod of the lotus shell extract includes the following steps:
1) by 100g lotus receptacle grinding and sieving, lotus receptacle powder is obtained；
2) lotus receptacle powder is added in the ethanol water that 200ml mass fraction is 50%, is uniformly mixed, obtains lotus
Fluffy shell mixed liquor；
3) lotus receptacle mixed liquor is put into ultrasonic extraction tank and is carried out ultrasonic extraction 3 hours, extracting solution membrane filtration
Fall filter residue, filtrate concentration, vacuum drying obtains the seedpod of the lotus shell extract.
The preparation method of the modified conch meal of the pyrophosphoric acid includes the following steps:
1) 200g conch meal is carried out to calcining 1 hour at 700 DEG C, obtains calcined conch meal；
2) calcined conch meal is placed in the pyrophosphoric acid aqueous solution that 500ml concentration is 4wt% and is impregnated 0.5 hour, soaked
It is dried in vacuo after bubble, crushed 30 meshes and obtain the modified conch meal of the pyrophosphoric acid.
Above-mentioned fragrance-enhancing tobacco agent the preparation method is as follows: by propylene glycol, vegetables glycerol, seedpod of the lotus shell extract, leonurine
Hydrochloride and the modified conch meal of pyrophosphoric acid are uniformly mixed up to the fragrance-enhancing tobacco agent.
Embodiment 9
Present embodiments provide a kind of fragrance-enhancing tobacco agent, including the following raw material: 10g propylene glycol, 10g vegetables glycerol, 1.2g
Seedpod of the lotus shell extract, 0.2g leonurine hydrochloride, the modified conch meal of 3g pyrophosphoric acid.
The preparation method of the seedpod of the lotus shell extract includes the following steps:
1) by 100g lotus receptacle grinding and sieving, lotus receptacle powder is obtained；
2) lotus receptacle powder is added in the ethanol water that 200ml mass fraction is 50%, is uniformly mixed, obtains lotus
Fluffy shell mixed liquor；
3) lotus receptacle mixed liquor is put into ultrasonic extraction tank and is carried out ultrasonic extraction 3 hours, extracting solution membrane filtration
Fall filter residue, filtrate concentration, vacuum drying obtains the seedpod of the lotus shell extract.
The preparation method of the modified conch meal of the pyrophosphoric acid includes the following steps:
1) 200g conch meal is carried out to calcining 1 hour at 800 DEG C, obtains calcined conch meal；
2) calcined conch meal is placed in the pyrophosphoric acid aqueous solution that 500ml concentration is 10wt% and is impregnated 0.5 hour, soaked
It is dried in vacuo after bubble, crushed 30 meshes and obtain the modified conch meal of the pyrophosphoric acid.
Above-mentioned fragrance-enhancing tobacco agent the preparation method is as follows: by propylene glycol, vegetables glycerol, seedpod of the lotus shell extract, leonurine
Hydrochloride and the modified conch meal of pyrophosphoric acid are uniformly mixed up to the fragrance-enhancing tobacco agent.
Embodiment 10
Present embodiments provide a kind of fragrance-enhancing tobacco agent, including the following raw material: 10g propylene glycol, 12g vegetables glycerol, 1g lotus
Fluffy shell extract, the modified conch meal of 1.0g pyrophosphoric acid.
The preparation method of the seedpod of the lotus shell extract includes the following steps:
1) by 100g lotus receptacle grinding and sieving, lotus receptacle powder is obtained；
2) lotus receptacle powder is added in the ethanol water that 200ml mass fraction is 50%, is uniformly mixed, obtains lotus
Fluffy shell mixed liquor；
3) lotus receptacle mixed liquor is put into ultrasonic extraction tank and is carried out ultrasonic extraction 3 hours, extracting solution membrane filtration
Fall filter residue, filtrate concentration, vacuum drying obtains the seedpod of the lotus shell extract.
The preparation method of the modified conch meal of the pyrophosphoric acid includes the following steps:
1) 200g conch meal is carried out to calcining 1 hour at 700 DEG C, obtains calcined conch meal；
2) calcined conch meal is placed in the pyrophosphoric acid aqueous solution that 500ml concentration is 4wt% and is impregnated 0.5 hour, soaked
It is dried in vacuo after bubble, crushed 30 meshes and obtain the modified conch meal of the pyrophosphoric acid.
Above-mentioned fragrance-enhancing tobacco agent the preparation method is as follows: propylene glycol, vegetables glycerol, seedpod of the lotus shell extract and pyrophosphoric acid are changed
Property conch meal be uniformly mixed up to the fragrance-enhancing tobacco agent.
Embodiment 11
Present embodiments provide a kind of fragrance-enhancing tobacco agent, including the following raw material: 14g propylene glycol, 10g vegetables glycerol, 2g lotus
Fluffy shell extract, 0.02g tea polyphenols.
The preparation method of the seedpod of the lotus shell extract includes the following steps:
1) by 100g lotus receptacle grinding and sieving, lotus receptacle powder is obtained；
2) lotus receptacle powder is added in the ethanol water that 200ml mass fraction is 50%, is uniformly mixed, obtains lotus
Fluffy shell mixed liquor；
3) lotus receptacle mixed liquor is put into ultrasonic extraction tank and is carried out ultrasonic extraction 3 hours, extracting solution membrane filtration
Fall filter residue, filtrate concentration, vacuum drying obtains the seedpod of the lotus shell extract.
Above-mentioned fragrance-enhancing tobacco agent the preparation method is as follows: propylene glycol, vegetables glycerol, seedpod of the lotus shell extract and tea polyphenols are mixed
It closes uniformly up to the fragrance-enhancing tobacco agent.
Embodiment 12
Present embodiments provide a kind of fragrance-enhancing tobacco agent, including the following raw material: 9g propylene glycol, 15g vegetables glycerol, the 1g seedpod of the lotus
Shell extract, 0.4g leonurine hydrochloride, 0.8g hydrochloric Acid Modification conch meal.
The preparation method of the seedpod of the lotus shell extract includes the following steps:
1) by 100g lotus receptacle grinding and sieving, lotus receptacle powder is obtained；
2) lotus receptacle powder is added in the ethanol water that 200ml mass fraction is 50%, is uniformly mixed, obtains lotus
Fluffy shell mixed liquor；
3) lotus receptacle mixed liquor is put into ultrasonic extraction tank and is carried out ultrasonic extraction 3 hours, extracting solution membrane filtration
Fall filter residue, filtrate concentration, vacuum drying obtains the seedpod of the lotus shell extract.
The preparation method of the hydrochloric Acid Modification conch meal includes the following steps:
1) 200g conch meal is carried out to calcining 1 hour at 700 DEG C, obtains calcined conch meal；
2) calcined conch meal is placed in the aqueous hydrochloric acid solution that 500ml concentration is 4wt% and is impregnated 0.5 hour, impregnated
After be dried in vacuo, crushed 30 meshes and obtain the hydrochloric Acid Modification conch meal.
Above-mentioned fragrance-enhancing tobacco agent the preparation method is as follows: by propylene glycol, vegetables glycerol, seedpod of the lotus shell extract, leonurine
Hydrochloride and hydrochloric Acid Modification conch meal are uniformly mixed up to the fragrance-enhancing tobacco agent.
Test example 1
It selects Yunnan brand cigarette (point lit cigarettes) as blank cigarette, extracts laboratory sample by GB/T5606.1,
6 blank cigarette samples are prepared, as control sample, the tobacco for then obtaining embodiment 1-5 increases one of blank cigarette sample
Pastil is uniformly sprayed onto (each implementation on the pipe tobacco of the remaining blank cigarette according to 1% additive amount for accounting for pipe tobacco weight respectively
One blank cigarette sample of the corresponding sprinkling of the fumet of example), according to " cigarette " GB5606.4-2005 Sensory Quality of Cigarette technical requirements
The aesthetic quality of evaluating cigarette, wherein being that score value more high organoleptic quality is better in each index.
Influence of the 1 fragrance-enhancing tobacco agent of table to Sensory Quality of Cigarette
From the data in table 1, it can be seen that the present invention adds seedpod of the lotus shell extract, three kinds of groups on the basis of propylene glycol, vegetables glycerol
Divide to cooperate and significantly improve the suction quality of cigarette, effectively improves the irritation of flue gas.
Test example 2
It selects Yunnan brand cigarette (point lit cigarettes) as blank cigarette, extracts laboratory sample by GB/T5606.1,
13 blank cigarette samples are prepared, one of blank cigarette sample is as control sample, the tobacco that then obtains embodiment 1-12
Fumet is uniformly sprayed onto (each reality on the pipe tobacco of the remaining blank cigarette according to 1% additive amount for accounting for pipe tobacco weight respectively
Apply one blank cigarette sample of the corresponding sprinkling of fumet of example), using the tobacco business standard tobacco of YC/T184-2004 and tobacco system
Gas-chromatography-thermal energy analysis combined instrument (GC-TEA) quantitative analysis in the measurement of the peculiar N- nitrosamine of product tobacco detects cigarette cigarette
The burst size of distinctive N- nitrosonornicotine (NNN) in gas.According to tar in 1996 standard test cigarette smoke of YC/T29-
Amount.
Influence of the 2 fragrance-enhancing tobacco agent of table to N- nitrosonornicotine and tar content in cigarette smoke
Test example 3
The fragrance-enhancing tobacco agent that embodiment 4 is obtained is as heating one of non-combustion-type cigarette additive formulations, according to accounting for
1% additive amount of pipe tobacco weight is added in new cigarette tobacco material, and smoking result shows compared to being not added with the present invention
The heating non-combustion-type cigarette of fragrance-enhancing tobacco agent, the heating non-combustion type cigarette of fragrance-enhancing tobacco agent prepared by addition embodiment 4
Gas fragrance obviously increases, irritation decline.
Obviously, the above embodiments are merely examples for clarifying the description, and does not limit the embodiments.It is right
For those of ordinary skill in the art, can also make on the basis of the above description it is other it is various forms of variation or
It changes.There is no necessity and possibility to exhaust all the enbodiments.And it is extended from this it is obvious variation or
It changes still within the protection scope of the invention.
Claims (10)
1. a kind of fragrance-enhancing tobacco agent, which is characterized in that the raw material including following parts by weight: propylene glycol and 6-48 parts of vegetables glycerol,
0.5-3 parts of seedpod of the lotus shell extract.
2. fragrance-enhancing tobacco agent according to claim 1, which is characterized in that further include leonurine hydrochloride 0.02-0.4
Part.
3. fragrance-enhancing tobacco agent according to claim 1 or 2, which is characterized in that further include the modified conch meal 0.8-3 of pyrophosphoric acid
Part.
4. fragrance-enhancing tobacco agent according to claim 3, which is characterized in that the preparation method of the modified conch meal of the pyrophosphoric acid
Include the following steps:
1) conch meal is calcined at 700-800 DEG C, obtains calcined conch meal；
2) calcined conch meal is placed in pyrophosphoric acid aqueous solution and is impregnated, is dried in vacuo after immersion, pulverize and sieve to obtain described
Pyrophosphoric acid is modified conch meal.
5. fragrance-enhancing tobacco agent according to claim 4, which is characterized in that the pyrophosphoric acid concentration of aqueous solution is 4-
10wt%.
6. fragrance-enhancing tobacco agent according to claim 1-5, which is characterized in that the seedpod of the lotus shell extract is from lotus
It is prepared in fluffy shell by ethyl alcohol extraction.
7. dual-purpose type fragrance-enhancing tobacco agent according to claim 1-6, which is characterized in that further include tobacco extract
0.1-0.6 parts.
8. fragrance-enhancing tobacco agent according to claim 7, which is characterized in that the tobacco extract is from Yunnan tobacco and saliva
It is prepared in Ba Buwei tobacco leaf by ethyl alcohol extraction；
The weight ratio of the Yunnan tobacco and Zimbabwe's tobacco leaf is 1:0.8-1.2.
9. fragrance-enhancing tobacco agent according to claim 1-8, which is characterized in that the propylene glycol is 3-45 parts, institute
Stating vegetables glycerol is 3-45 parts.
10. the described in any item fragrance-enhancing tobacco agent of claim 1-9 are in point lit cigarettes and/or heating non-combustion-type cigarette
Using.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111920081A (en) * | 2020-08-11 | 2020-11-13 | 云南中烟工业有限责任公司 | Method for regulating and controlling distribution of roasting aroma substances under heating condition of heating cigarettes |
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| JPH11169154A (en) * | 1997-12-09 | 1999-06-29 | Osaka Maeda Seika:Kk | Substitute for cigarette paper by food material and its production |
| CN101606981A (en) * | 2008-06-18 | 2009-12-23 | 湖北汇特生物医药技术有限公司 | From lotus (lotus) plant, extract the method for antimicrobial and antiphlogistic activity composition |
| CN102793264A (en) * | 2012-08-31 | 2012-11-28 | 中国烟草总公司郑州烟草研究院 | Preparation method of magnolia fruit extract and application thereof in cigarette |
| CN109875098A (en) * | 2019-03-18 | 2019-06-14 | 广东中烟工业有限责任公司 | A kind of cigarette blending coating medium and its application |
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| JPH11169154A (en) * | 1997-12-09 | 1999-06-29 | Osaka Maeda Seika:Kk | Substitute for cigarette paper by food material and its production |
| CN101606981A (en) * | 2008-06-18 | 2009-12-23 | 湖北汇特生物医药技术有限公司 | From lotus (lotus) plant, extract the method for antimicrobial and antiphlogistic activity composition |
| CN102793264A (en) * | 2012-08-31 | 2012-11-28 | 中国烟草总公司郑州烟草研究院 | Preparation method of magnolia fruit extract and application thereof in cigarette |
| CN109875098A (en) * | 2019-03-18 | 2019-06-14 | 广东中烟工业有限责任公司 | A kind of cigarette blending coating medium and its application |
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| CN111920081A (en) * | 2020-08-11 | 2020-11-13 | 云南中烟工业有限责任公司 | Method for regulating and controlling distribution of roasting aroma substances under heating condition of heating cigarettes |
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