CN110226774B - Dry cigarette bead tip rod capable of improving sweet feeling of cigarettes - Google Patents

Dry cigarette bead tip rod capable of improving sweet feeling of cigarettes Download PDF

Info

Publication number
CN110226774B
CN110226774B CN201910600952.XA CN201910600952A CN110226774B CN 110226774 B CN110226774 B CN 110226774B CN 201910600952 A CN201910600952 A CN 201910600952A CN 110226774 B CN110226774 B CN 110226774B
Authority
CN
China
Prior art keywords
dry
cigarette
beads
extract
hours
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201910600952.XA
Other languages
Chinese (zh)
Other versions
CN110226774A (en
Inventor
罗海涛
蔡继宝
苏加坤
何力
徐达
刘思奎
郭磊
邵灯寅
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Tobacco Jiangxi Industrial Co Ltd
Original Assignee
China Tobacco Jiangxi Industrial Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Tobacco Jiangxi Industrial Co Ltd filed Critical China Tobacco Jiangxi Industrial Co Ltd
Priority to CN201910600952.XA priority Critical patent/CN110226774B/en
Publication of CN110226774A publication Critical patent/CN110226774A/en
Application granted granted Critical
Publication of CN110226774B publication Critical patent/CN110226774B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00—Cigars; Cigarettes
    • A24D1/04—Cigars; Cigarettes with mouthpieces or filter-tips
    • A24D1/042—Cigars; Cigarettes with mouthpieces or filter-tips with mouthpieces
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/02—Manufacture of tobacco smoke filters
    • A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
    • A24D3/0212—Applying additives to filter materials
    • A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06—Use of materials for tobacco smoke filters
    • A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)

Abstract

The circumference of the bottom surface of the filter rod is 24mm, dry beads with the diameter of 3.25 +/-0.15 mm are loaded in the middle section of a tow, zeolite molecular sieves are used as main raw materials of the dry beads, the dry beads are prepared by pelletizing, fragrance adding and forming processes, and a sea buckthorn composite extract for improving the sweet feeling of cigarettes is adsorbed on the dry beads.

Description

Dry cigarette bead tip rod capable of improving sweet feeling of cigarettes
Technical Field
The invention relates to the field of tobacco flavors and fragrances, in particular to a dry cigarette holder rod capable of improving the sweet feeling of cigarettes.
Background
In the tobacco industry, the cigarette stereoscopic flavor blending technology is developed rapidly, and particularly, a new method and a new technology in a cigarette filter rod are developed, wherein the new technology comprises cigarette blasting beads, microcapsules, nano particles, powdery particles and the like. At present, through the inspection of consumer market, the overall acceptance of the cigarette bead blasting is better, and additives such as microcapsules, nano particles, powder particles and the like easily cause the smoking safety worry of consumers due to fine particles. However, the addition of the cigarette popping beads and dropping pills also has certain disadvantages, including low forming rate, high cost and the like, and trace unpleasant odors exist in the popping beads, the dropping pill solvents such as olive oil, ODO and the like, so that the popping beads are mainly used for wrapping essence and spice with strong fragrance such as ginseng, mint and the like, and other types of essence and spice have obvious offensive odor when being used, thereby influencing smoking experience. Although the prior art has the cigarette filter rod prepared by silica gel flavor beads or zeolite flavor beads, the preparation process of the flavor beads is unstable, the forming rate is low, and the flavor beads are difficult to release the flavor for a long time to achieve the slow release effect due to the limitation of the microstructure of the flavor beads.
The sea-buckthorn contains rich nutrient substances and bioactive substances, has the effects of relieving cough, reducing phlegm and relieving asthma, and although the prior art tries to add the sea-buckthorn as cigarette spice into a cigarette holder filter stick, the smoking experience is not good all the time due to the sour and astringent taste. Therefore, it is also necessary to develop a method for removing astringent components from hippophae rhamnoides and retaining the fragrant components thereof, and making the smoke soft and sweet.
Disclosure of Invention
In order to solve the technical problems, the invention provides a novel dry bead adsorbed with a sea-buckthorn composite extract with a sweetening and moistening effect, which is applied to a cigarette filter rod.
The invention provides a cigarette dry bead filter rod capable of improving the sweet feeling of cigarettes, which is characterized in that the circumference of the bottom surface of the cigarette filter rod is 24mm, dry beads with the diameter of 3.25 +/-0.15 mm are loaded in the middle section of a tow, the dry beads are prepared by using a zeolite molecular sieve as a main raw material through pelletizing, fragrance adding and forming processes, and seabuckthorn compound extracts for improving the sweet feeling of cigarettes are adsorbed on the dry beads.
The invention also provides a preparation method of the dry cigarette bead tip rod capable of improving the sweet feeling of the cigarette, which is characterized by comprising the following steps:
1) pelletizing: taking a certain amount of zeolite molecular sieve, grinding, uniformly mixing the zeolite molecular sieve and silica sol (the solid content is 25-50%) in a mass ratio of 2: 1-5, placing the mixture in a pelletizer for rolling ball forming, screening qualified samples with the diameter of 3.25 +/-0.15 mm, calcining a bead-shaped blank at 1000-1300 ℃ for 2-6 hours, washing with water, and drying to obtain dry beads with porous structures;
2) adding fragrance: uniformly mixing the dry beads and the sea buckthorn compound extract according to the mass ratio of 1: 1-4, sealing, placing the mixture in a shaking table with 150 revolutions per minute for 6-12 hours, standing for 12 hours to enable essence to be uniformly adsorbed in porous channels of the dry beads, and air-drying the mixture for 2-4 hours at 40-50 ℃ to obtain dry attached-fragrance beads;
3) and (3) forming a filter tip: adding the dry bead with the fragrance into the middle section of the filter rod tows of the cigarette, and molding to obtain the cigarette.
Preferably, the preparation method of the sea buckthorn compound extract comprises the following steps:
1) cleaning sea-buckthorn, squeezing the pulp into juice, adding pectinase accounting for 0.1-0.2 percent of the mass of the sea-buckthorn juice and flavourzyme accounting for 0.05-0.1 percent of the mass of the sea-buckthorn juice, and carrying out enzymolysis at constant temperature for 0.5-4 hours at the temperature of 40-50 ℃ to obtain sea-buckthorn zymolyte; further, 0.1% of pectinase and 0.05% of flavourzyme are preferred, and the enzymolysis temperature is preferably 40-45 ℃.
2) Uniformly mixing the sea buckthorn zymolyte, the Jinba tobacco extract, the sun-cured tobacco extract and the dandelion extract according to the mass ratio of 100: 10-20: 2-5: 1-2, adding bacillus, and fermenting the fermentation substrate for 4-10 days to obtain the composite fermentation liquid.
3) Adding 95% ethanol with 3 times of the weight of the compound fermentation liquor for alcohol precipitation, standing for 24 hours at 4 ℃, filtering, and concentrating under reduced pressure until the density of the extract is 1.05-1.10 g/cm3Adding 1, 2-propylene glycol with the mass of 20% of the concentrate to obtain the sea-buckthorn compound extract.
The Jinba tobacco extract, the sun-cured yellow tobacco extract and the dandelion extract can be obtained from the market or prepared by self, and are preferably extract type extracts, and the addition amount is preferably 100: 10-15: 2-4: 1-2.
The pectinase and the flavourzyme of the invention are commercially available.
Further, the zeolite molecular sieve is preferably 4A, 5A or Y type.
Further, the solid content of the silica sol is preferably 30-40%.
Preferably, the bacillus is bacillus BA-01, is separated and screened from the surface of tobacco leaves, and has better aroma-enhancing performance.
The Bacillus BA-01 is named as Bacillus amyloliquefaciens by classification, the preservation unit is Jiangxi Zhongyan tobacco industry Limited liability company, the preservation date is 2017, 4 and 26 days, and the Bacillus BA-01 is preserved in Guangdong province microbial strain preservation center, and the preservation number is GDMCC No. 60171. The address of the preservation unit is No. 59 building 5 of the Jie No. 100 Dazhou, Jieli, Guangzhou, Guangdong province.
Preferably, the flavor-attaching rate of the dry beads is controlled to be 15-30%, wherein the flavor-attaching rate is (weight after flavor-weight before flavor-attaching)/weight before flavor-attaching.
Preferably, the dry beads are in a micro porous structure, the average pore diameter is 0.5-1 nm, and the fragrance-attaching and slow-release performance is better.
Compared with the prior art, the invention has the advantages and positive effects that:
1) the dry beads in the filter tip are of a porous structure, have good essence adsorption and slow release performance, and can provide lasting and stable aroma enhancement experience.
2) According to the invention, the sea buckthorn extract, the Jinba tobacco, the sun-cured tobacco and the dandelion extract are compounded to prepare the sea buckthorn compound extract, and when cigarettes are smoked for slow release, because the sea buckthorn compound extract does not participate in combustion, on one hand, the acidic natural extract can be used for neutralizing the pH value of the cigarette smoke and playing a role in reducing the irritation of the cigarettes, and on the other hand, small molecular substances in the dandelion, the sea buckthorn and other extracts enter the throat along with the cigarette smoke and play a role in improving the sweet and moist feeling of the cigarettes, and the fragrance of the extracts is well blended with the fragrance of the Jinba tobacco and the sun-cured tobacco, so that the finally generated smoke has no astringent feeling and is rich and sweet.
3) The sea-buckthorn compound extract adopts enzymolysis and compound fermentation processes, so that the extract has prominent sweet and sour fragrance, has elegant tobacco fragrance, and can be coordinated with cigarette fragrance.
4) The circumference of the filter rod is 24mm, the middle section of the filament bundle of the filter rod is loaded with a dry attached flavor bead with the diameter of 3.25 +/-0.15 mm, the dry flavor bead is prepared by zeolite molecular sieve and silica sol, and is safer and more stable in flavor retention compared with the method of directly adopting small zeolite particles and microcapsules, the adsorption effect of the preparation process of the invention is better than that of the prior art, and the safety worry of the consumers about the safe absorption of fine additives such as charcoal powder, silica gel powder, zeolite powder, cyclodextrin particles and the like is avoided;
5) compared with the traditional bead blasting and dropping pills for cigarettes, consumers do not need to pinch and break the aroma beads when smoking cigarettes, no solvent exudes, and the use is safer and more convenient.
Drawings
FIG. 1 is a schematic view of a cigarette filter rod;
in the figure: 1-filter stick suction end, 2-dry bead, 3-cigarette coil paper and 4-tobacco shred.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
The preparation method of the cigarette dry bead tip rod comprises the following steps:
1) pelletizing: taking a certain amount of Y-type zeolite molecular sieve, grinding, uniformly mixing the zeolite molecular sieve and silica sol (solid content is 50%) according to the mass ratio of 2:3, placing the mixture into a pelletizer to perform rolling ball forming, screening qualified samples with the diameter of 3.25 +/-0.15 mm, calcining a bead-shaped blank at 1000 ℃ for 4 hours, washing with water, and drying to obtain dry beads with porous structures;
2) adding fragrance: uniformly mixing the dry beads and the sea buckthorn compound extract according to the mass ratio of 1:2, sealing, placing in a shaking table with 150 revolutions per minute for 12 hours, then standing for 12 hours to enable the essence to be uniformly adsorbed in porous channels of the dry beads, and air-drying at 40-50 ℃ for 4 hours to obtain dry attached-fragrance beads;
3) and (3) forming a filter tip: adding one dry bead with fragrance into the middle section of the filter rod filament bundle of the cigarette, and molding to obtain the cigarette filter rod with the circumference of the bottom surface of the cigarette being 24 mm.
The preparation method of the sea buckthorn compound extract comprises the following steps:
1) cleaning fructus Hippophae, squeezing pulp into juice, adding pectase 0.1% of the weight of fructus Hippophae juice and flavourzyme 0.05%, and performing enzymolysis at constant temperature for 2 hr at 40 deg.C to obtain fructus Hippophae zymolyte;
2) uniformly mixing the sea buckthorn zymolyte, the Jinba tobacco extract, the sun-cured yellow tobacco extract and the dandelion extract according to the mass ratio of 100:10:2:1, adding bacillus Simplex with the mass of 0.5% of the substrate, and fermenting the fermentation substrate for 5 days to obtain a composite fermentation liquid;
3) adding 95% ethanol with the weight 3 times of that of the compound fermentation liquor to carry out alcohol precipitation, standing at 4 ℃ for 24 hours, filtering, concentrating under reduced pressure until the density of the extract is 1.05-1.10 g/cm3, and adding 1, 2-propylene glycol with the mass of 20% of the concentrate to obtain the sea buckthorn compound extract.
The detection shows that the average pore diameter of the dry beads is 0.72nm, and the fragrance adding rate is 19.9%.
Example 2
The preparation method of the cigarette dry bead tip rod comprises the following steps:
1) pelletizing: taking a certain amount of 5A type zeolite molecular sieve, grinding, uniformly mixing the zeolite molecular sieve and silica sol (the solid content is 25 percent) in a mass ratio of 2:3, placing the mixture into a pelletizer to perform rolling ball forming, screening qualified samples with the diameter of 3.25 +/-0.15 mm, calcining a bead-shaped blank at 1000 ℃ for 4 hours, washing with water, and drying to obtain dry beads with porous structures;
2) adding fragrance: uniformly mixing the dry beads and the sea buckthorn compound extract according to the mass ratio of 1:2, sealing, placing the mixture in a shaking table with 150 revolutions per minute for 6 hours, then standing for 12 hours to enable the essence to be uniformly adsorbed in porous channels of the dry beads, and air-drying for 4 hours at 40-50 ℃ to obtain dry fragrance-coated beads;
3) and (3) forming a filter tip: adding one dry bead with fragrance into the middle section of the filter rod filament bundle of the cigarette, and molding to obtain the cigarette filter rod with the circumference of the bottom surface of the cigarette being 24 mm.
The preparation method of the sea buckthorn compound extract comprises the following steps:
1) cleaning fructus Hippophae, squeezing pulp into juice, adding pectase 0.1% of the weight of fructus Hippophae juice and flavourzyme 0.1%, and performing enzymolysis at constant temperature of 45 deg.C for 4 hr to obtain fructus Hippophae zymolyte;
2) uniformly mixing the sea buckthorn zymolyte, the Jinba tobacco extract, the sun-cured tobacco extract and the dandelion extract according to the mass ratio of 100:20:3:2, adding bacillus pumilus with the mass of 0.1% of that of a substrate, and fermenting the fermentation substrate for 5 days to obtain a composite fermentation liquid;
3) adding 95% ethanol with 3 times of the weight of the compound fermentation liquor for alcohol precipitation, standing for 24 hours at 4 ℃, filtering, and concentrating under reduced pressure until the density of the extract is 1.05-1.10 g/cm3Adding 1, 2-propylene glycol with the mass of 20% of the concentrate to obtain the sea-buckthorn compound extract.
The detection shows that the average pore diameter of the dry beads is 0.77nm, and the fragrance adding rate is 21.5%.
Example 3
The preparation method of the cigarette dry bead tip rod comprises the following steps:
1) pelletizing: grinding a certain amount of ZSM-5 type zeolite molecular sieve, uniformly mixing the zeolite molecular sieve and silica sol (the solid content is 35%) in a mass ratio of 2:3, placing the mixture in a pelletizer for rolling ball forming, screening qualified samples with the diameter of 3.25 +/-0.15 mm, calcining a bead-shaped blank body for 4 hours at 1000 ℃, washing with water and drying to obtain dry beads with porous structures;
2) adding fragrance: uniformly mixing the dry beads and the sea buckthorn compound extract according to the mass ratio of 1:3, sealing, placing in a shaking table with 150 revolutions per minute for 12 hours, then standing for 12 hours to enable the essence to be uniformly adsorbed in porous channels of the dry beads, and air-drying at 40-50 ℃ for 4 hours to obtain dry attached-fragrance beads;
3) and (3) forming a filter tip: adding one dry bead with fragrance into the middle section of the filter rod filament bundle of the cigarette, and molding to obtain the cigarette filter rod with the circumference of the bottom surface of the cigarette being 24 mm.
The preparation method of the sea buckthorn compound extract comprises the following steps:
1) cleaning fructus Hippophae, and squeezing pulp to obtain juice; adding pectinase 0.1% of the mass of the sea buckthorn juice and flavourzyme 0.1% of the mass of the sea buckthorn juice, and performing enzymolysis for 4 hours at a constant temperature of 45 ℃ to obtain sea buckthorn zymolyte;
2) uniformly mixing the sea buckthorn zymolyte, the Jinba tobacco extract, the sun-cured tobacco extract and the dandelion extract according to the mass ratio of 100:20:3:2, adding bacillus subtilis with the mass of 0.1% of that of a substrate, and fermenting the fermentation substrate for 5 days to obtain a composite fermentation liquid;
3) adding 95% ethanol with 3 times of the weight of the compound fermentation liquor for alcohol precipitation, standing for 24 hours at 4 ℃, filtering, and concentrating under reduced pressure until the density of the extract is 1.05-1.10 g/cm3Adding 1, 2-propylene glycol with the mass of 20% of the concentrate to obtain the sea-buckthorn compound extract.
The detection shows that the average pore diameter of the dry beads is 0.82nm, and the fragrance adding rate is 18.7%.
Example 4
The preparation method of the cigarette dry bead tip rod comprises the following steps:
1) pelletizing: taking a certain amount of Y-type zeolite molecular sieve, grinding, uniformly mixing the zeolite molecular sieve and silica sol (the solid content is 35 percent) according to the mass ratio of 1:1, placing the mixture into a pelletizer to perform rolling ball forming, screening qualified samples with the diameter of 3.25 +/-0.15 mm, calcining a bead-shaped blank at 1000 ℃ for 4 hours, washing with water, and drying to obtain dry beads with porous structures;
2) adding fragrance: uniformly mixing the dry beads and the sea buckthorn compound extract according to the mass ratio of 1:2, sealing, placing in a shaking table with 150 revolutions per minute for 12 hours, then standing for 12 hours to enable the essence to be uniformly adsorbed in porous channels of the dry beads, and air-drying at 40-50 ℃ for 4 hours to obtain dry attached-fragrance beads;
3) and (3) forming a filter tip: adding one dry bead with fragrance into the middle section of the filter rod filament bundle of the cigarette, and molding to obtain the cigarette filter rod with the circumference of the bottom surface of the cigarette being 24 mm.
The preparation method of the sea buckthorn compound extract comprises the following steps:
1) cleaning fructus Hippophae, squeezing pulp into juice, adding pectase 0.1% of the weight of fructus Hippophae juice and flavourzyme 0.1%, and performing enzymolysis at constant temperature of 45 deg.C for 4 hr to obtain fructus Hippophae zymolyte;
2) uniformly mixing the sea buckthorn zymolyte, the Jinba tobacco extract, the sun-cured yellow tobacco extract and the dandelion extract according to the mass ratio of 100:20:3:2, adding bacillus BA-01 (the preservation date is 2017, 4 and 26 months, and is preserved in Guangdong province microbial strain preservation center, and the preservation number is GDMCC No.60171) with the mass of a substrate of 0.5%, and fermenting the fermentation substrate for 5 days to obtain a composite fermentation liquid;
3) adding 95% ethanol with 3 times of the weight of the compound fermentation liquor for alcohol precipitation, standing for 24 hours at 4 ℃, filtering, and concentrating under reduced pressure until the density of the extract is 1.05-1.10 g/cm3Adding 1, 2-propylene glycol with the mass of 20% of the concentrate to obtain the sea-buckthorn compound extract.
The detection shows that the average pore diameter of the dry beads is 0.55nm, and the fragrance adding rate is 26.4%.
Example 5
The preparation method of the cigarette dry bead tip rod comprises the following steps:
1) pelletizing: taking a certain amount of 5A type zeolite molecular sieve, grinding, uniformly mixing the zeolite molecular sieve and silica sol (the solid content is 35%) according to the mass ratio of 2:5, placing the mixture into a pelletizer to perform rolling ball forming, screening qualified samples with the diameter of 3.25 +/-0.15 mm, calcining a bead-shaped blank at 1000 ℃ for 2 hours, washing with water, and drying to obtain dry beads with porous structures;
2) adding fragrance: uniformly mixing the dry beads and the sea buckthorn compound extract according to the mass ratio of 1:2, sealing, placing in a shaking table with 150 revolutions per minute for 12 hours, then standing for 12 hours to enable the essence to be uniformly adsorbed in porous channels of the dry beads, and air-drying at 40-50 ℃ for 4 hours to obtain dry attached-fragrance beads;
3) and (3) forming a filter tip: adding one dry bead with fragrance into the middle section of the filter rod filament bundle of the cigarette, and molding to obtain the cigarette filter rod with the circumference of the bottom surface of the cigarette being 24 mm.
The preparation method of the sea buckthorn compound extract comprises the following steps:
1) cleaning fructus Hippophae, squeezing pulp into juice, adding pectase 0.1% of the weight of fructus Hippophae juice and flavourzyme 0.1%, and performing enzymolysis at constant temperature of 45 deg.C for 4 hr to obtain fructus Hippophae zymolyte;
2) uniformly mixing the sea buckthorn zymolyte, the Jinba tobacco extract, the sun-cured yellow tobacco extract and the dandelion extract according to the mass ratio of 100:20:3:2, adding bacillus BA-01 (the preservation date is 2017, 4 and 26 months, and is preserved in Guangdong province microbial strain preservation center, and the preservation number is GDMCC No.60171) with the mass of a substrate, and fermenting the fermentation substrate for 5 days to obtain a composite fermentation broth;
3) adding 95% ethanol with the weight 3 times of that of the compound fermentation liquor to carry out alcohol precipitation, standing at 4 ℃ for 24 hours, filtering, concentrating under reduced pressure until the density of the extract is 1.05-1.10 g/cm3, and adding 1, 2-propylene glycol with the mass of 20% of the concentrate to obtain the sea buckthorn compound extract.
The detection shows that the average pore diameter of the dry beads is 0.71nm, and the fragrance adding rate is 22.7%.
Example 6
The preparation method of the cigarette dry bead tip rod comprises the following steps:
1) pelletizing: taking a certain amount of 4A type zeolite molecular sieve, grinding, uniformly mixing the zeolite molecular sieve and silica sol (the solid content is 30 percent) according to the mass ratio of 1:2, placing the mixture into a pelletizer to perform rolling ball forming, screening qualified samples with the diameter of 3.25 +/-0.15 mm, calcining a bead-shaped blank at 1200 ℃ for 6 hours, washing with water, and drying to obtain dry beads with porous structures;
2) adding fragrance: uniformly mixing the dry beads and the sea buckthorn compound extract according to the mass ratio of 1:2, sealing, placing in a shaking table with 150 revolutions per minute for 12 hours, then standing for 12 hours to enable the essence to be uniformly adsorbed in porous channels of the dry beads, and air-drying at 40-50 ℃ for 4 hours to obtain dry attached-fragrance beads;
3) and (3) forming a filter tip: adding one dry bead with fragrance into the middle section of the filter rod filament bundle of the cigarette, and molding to obtain the cigarette filter rod with the circumference of the bottom surface of the cigarette being 24 mm.
The preparation method of the sea buckthorn compound extract comprises the following steps:
1) cleaning fructus Hippophae, squeezing pulp into juice, adding pectase 0.1% of the weight of fructus Hippophae juice and flavourzyme 0.1%, and performing enzymolysis at constant temperature of 45 deg.C for 1 hr to obtain fructus Hippophae zymolyte;
2) uniformly mixing the sea buckthorn zymolyte, the Jinba tobacco extract, the sun-cured yellow tobacco extract and the dandelion extract according to the mass ratio of 100:10:2:1, adding bacillus BA-01 (the preservation date is 2017, 4, 26 days, and is preserved in Guangdong province microbial strain preservation center, and the preservation number is GDMCC No.60171) with the mass of the substrate of 0.1%, and fermenting the fermentation substrate for 5 days to obtain a composite fermentation liquid;
3) adding 95% ethanol with 3 times of the weight of the compound fermentation liquor for alcohol precipitation, standing for 24 hours at 4 ℃, filtering, and concentrating under reduced pressure until the density of the extract is 1.05-1.10 g/cm3Adding 1, 2-propylene glycol with the mass of 20% of the concentrate to obtain the sea-buckthorn compound extract.
Comparative example 1
1) Cleaning fructus Hippophae, squeezing pulp to obtain juice, adding 5 times of 75% ethanol solution, reflux-extracting at 70 deg.C for 2 times, mixing extractive solutions, concentrating to obtain extract, and adding 20% 1, 2-propylene glycol to obtain fructus Hippophae extract;
1) adding calcium chloride with the mass of 30% of the extract into the sea buckthorn extract, uniformly stirring to obtain an essence solution, taking a certain amount of 5A zeolite molecular sieve, calcining for 6 hours at 1300 ℃, washing with water, drying, then adding the essence solution, sealing, placing the mixture in a 150 r/m shaking table for 12 hours, then standing for 12 hours, and air-drying for 2 hours at 40-50 ℃ to obtain dry attached spice beads;
2) adding the same weight of the one dry attached spice bead prepared in the example 1 into the filament bundle of the cigarette filter rod with the circumference of the bottom surface being 24mm to obtain the cigarette filter rod.
The detection shows that the average pore diameter of the dry beads is 0.68nm, and the fragrance adding rate is 12.4%.
Comparative example 2
1) Taking a certain amount of 4A zeolite molecular sieve, grinding, uniformly mixing the zeolite molecular sieve and silica sol (the solid content is 25 percent) in a mass ratio of 2:1, placing the mixture into a pelletizer to perform rolling ball forming, screening qualified samples with the diameter of 3.25 +/-0.15 mm, calcining a bead-shaped blank at 800 ℃ for 6 hours, washing with water, and drying to obtain dry beads;
2) cleaning fructus Hippophae, squeezing pulp to obtain juice, adding 5 times of 75% ethanol solution, reflux-extracting at 70 deg.C for 2 times, mixing extractive solutions, concentrating to obtain extract, and adding 20% 1, 2-propylene glycol to obtain fructus Hippophae extract;
3) uniformly mixing the dry beads and the sea buckthorn extract according to the mass ratio of 1:2, sealing, placing the mixture in a table with 150 revolutions per minute for 12 hours, standing for 12 hours, and air-drying at 40-50 ℃ for 2 hours to prepare the dry beads with the fragrance;
4) adding one dry bead with fragrance into the middle section of the filter rod filament bundle of the cigarette, and molding to obtain the cigarette with circumference of 24mm on the bottom surface of the filter rod.
The detection shows that the average pore diameter of the dry beads is 0.76nm, and the fragrance adding rate is 18.8%.
Comparative example 3
1) Taking a certain amount of 5A zeolite molecular sieve, grinding, uniformly mixing the zeolite molecular sieve and silica sol (the solid content is 30 percent) in a mass ratio of 2:5, placing the mixture into a pelletizer to perform rolling ball forming, screening qualified samples with the diameter of 3.25 +/-0.15 mm, calcining a bead-shaped blank at 1200 ℃ for 4 hours, washing with water, and drying to obtain dry beads;
2) cleaning fructus Hippophae, squeezing pulp to obtain juice, mixing fructus Hippophae juice, JINBA tobacco extract, sun-dried yellow tobacco extract and herba Taraxaci extract at a mass ratio of 100:10:5:2, adding 0.1% cellulose hydrolase and 0.1% compound plant protease, fermenting at 35 deg.C for 5 days to obtain compound fermentation liquid,
3) adding 95% ethanol with 3 times of the weight of the compound fermentation liquor for alcohol precipitation, standing for 24 hours at 4 ℃, filtering, and concentrating under reduced pressure until the density of the extract is 1.05-1.10 g/cm3Adding 1, 2-propylene glycol with the mass of 20% of the concentrate to obtain a sea buckthorn compound extract;
4) uniformly mixing the dry beads and the sea buckthorn compound extract according to the mass ratio of 1:2, sealing, placing the mixture in a table with 150 revolutions per minute for 12 hours, standing for 12 hours, and air-drying at 40-50 ℃ for 2 hours to prepare the dry beads with the fragrance;
5) adding one dry bead with fragrance into the middle section of the filter rod filament bundle of the cigarette, and molding to obtain the cigarette with circumference of 24mm on the bottom surface of the filter rod.
The detection shows that the average pore diameter of the dry beads is 0.74nm, and the fragrance adding rate is 21.9%.
The test effect is as follows:
the cigarette dry bead filter rods prepared in the examples 1 to 6 and the comparative examples 1 to 3 were applied to cigarettes, and ordinary cigarettes prepared without the dry bead filter rods were used as a control. An expert smoking group organized to qualify for national cigarette smoking according to the five ginseng standard GB5606.4-2005 cigarette part 4: sensory technical requirements and YC/T497-.
TABLE 1 cigarette sensory evaluation results
Figure RE-GDA0002152852170000081
Figure RE-GDA0002152852170000091
Compared with a control sample, the dry cigarette bead tip rod products of the embodiments 1-6 of the invention have more obvious sour and sweet taste style, obviously increased richness of aroma and improved moistening feeling. The cigarette prepared by the filter tip of the embodiment 6 has the highest score mainly because the seabuckthorn compound extract is more harmonious with the smoking taste of the cigarette, and the slow release performance of the solid flavor bead is optimal.
The above embodiments are merely preferred embodiments of the present invention, and any simple modifications and alternative changes made to the above embodiments according to the technical spirit of the present invention are within the technical scope of the present invention.

Claims (6)

1. A dry bead filter rod capable of improving the sweet and moist feeling of cigarettes is characterized in that the circumference of the bottom surface of the cigarette filter rod is 24mm, dry beads with the diameter of 3.25 +/-0.15 mm are loaded in the middle section of a tow, the dry beads are prepared by taking a zeolite molecular sieve as a main raw material through pelletizing, fragrance adding and forming processes, and a sea buckthorn compound extract for improving the sweet and moist feeling of cigarettes is adsorbed on the dry beads; and the preparation method of the dry bead tip rod comprises the following steps:
1) pelletizing: taking a certain amount of zeolite molecular sieve, grinding, uniformly mixing the zeolite molecular sieve and silica sol with the solid content of 25-50% in a mass ratio of 2: 1-5, placing the mixture in a pelletizer for rolling ball forming, screening qualified samples with the diameter of 3.25 +/-0.15 mm, calcining a bead-shaped blank body at 1000-1300 ℃ for 2-6 hours, washing with water, and drying to obtain dry beads with porous structures;
2) adding fragrance: uniformly mixing the dry beads and the sea buckthorn compound extract according to the mass ratio of 1: 1-4, sealing, placing the mixture in a shaking table with 150 revolutions per minute for 6-12 hours, standing for 12 hours to enable essence to be uniformly adsorbed in porous channels of the dry beads, and air-drying the mixture for 2-4 hours at 40-50 ℃ to obtain dry fragrance-coated beads;
3) and (3) forming a filter tip: adding the dry aromatic bead into the middle section of the filter rod tows of the cigarette, and molding to obtain the cigarette;
the preparation method of the sea buckthorn compound extract comprises the following steps:
1) cleaning sea-buckthorn, squeezing the pulp into juice, adding pectinase accounting for 0.1-0.2 percent of the mass of the sea-buckthorn juice and flavourzyme accounting for 0.05-0.1 percent of the mass of the sea-buckthorn juice, and carrying out enzymolysis at constant temperature for 0.5-4 hours at the temperature of 40-50 ℃ to obtain sea-buckthorn zymolyte;
2) uniformly mixing the sea buckthorn zymolyte, the Jinba tobacco extract, the sun-cured tobacco extract and the dandelion extract according to the mass ratio of 100: 10-20: 2-5: 1-2, adding bacillus, and fermenting a fermentation substrate for 4-10 days to obtain a composite fermentation liquid;
3) adding 95% ethanol with the weight 3 times of that of the compound fermentation liquor to carry out alcohol precipitation, standing at 4 ℃ for 24 hours, filtering, concentrating under reduced pressure until the density of the extract is 1.05-1.10 g/cm3, and adding 1, 2-propylene glycol with the mass of 20% of the concentrate to obtain the sea buckthorn compound extract.
2. The dry bead filter rod for cigarette capable of improving cigarette sweetness according to claim 1, wherein the zeolite molecular sieve is one of 4A type, 5A type, Y type and ZSM-5 type.
3. The dry cigarette holder stick capable of improving the sweetness of cigarettes according to claim 1, characterized in that the bacillus is bacillus BA-01, which is isolated and screened from the surface of tobacco leaves, and the preservation date is 2017, 4 and 26 days, which is preserved in the Guangdong province microorganism culture collection with the preservation number being GDMCC No. 60171.
4. The dry cigarette bead tip rod capable of improving the sweetness of cigarettes according to claim 1, wherein the addition amount of the bacillus is 0.1-0.5% of the mass of the substrate.
5. The dry bead filter rod capable of improving the sweetness of cigarettes according to claim 1, wherein the flavor attaching rate of the dry beads is controlled to be 15-30%.
6. The dry bead filter rod capable of improving the sweetness of cigarettes according to claim 1, wherein the dry beads have a micro-porous structure and the average pore diameter is 0.5-1 nm.
CN201910600952.XA 2019-07-04 2019-07-04 Dry cigarette bead tip rod capable of improving sweet feeling of cigarettes Active CN110226774B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910600952.XA CN110226774B (en) 2019-07-04 2019-07-04 Dry cigarette bead tip rod capable of improving sweet feeling of cigarettes

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910600952.XA CN110226774B (en) 2019-07-04 2019-07-04 Dry cigarette bead tip rod capable of improving sweet feeling of cigarettes

Publications (2)

Publication Number Publication Date
CN110226774A CN110226774A (en) 2019-09-13
CN110226774B true CN110226774B (en) 2021-07-27

Family

ID=67858090

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201910600952.XA Active CN110226774B (en) 2019-07-04 2019-07-04 Dry cigarette bead tip rod capable of improving sweet feeling of cigarettes

Country Status (1)

Country Link
CN (1) CN110226774B (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110916240B (en) * 2019-12-16 2021-11-02 云南中烟新材料科技有限公司 Method for preparing cigarette filter stick aroma-enhancing pellets by using thin and short tobacco stems
CN110982625A (en) * 2019-12-29 2020-04-10 亿利耐雀生物科技有限公司 Licorice-flavored dried beads for cigarette filter tips and preparation method thereof
CN113229523A (en) * 2021-04-26 2021-08-10 河南中烟工业有限责任公司 Tobacco stem biomass charcoal loaded tobacco extract and application thereof in cigarette filter stick

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104957768A (en) * 2015-06-05 2015-10-07 滁州卷烟材料厂 Health care cigarette filter tip composite adsorbent for promoting sleep and preparing method thereof
CN106520380A (en) * 2016-12-29 2017-03-22 云南省玉溪市云溪香精香料有限责任公司 Fruit extract and application
WO2017193495A1 (en) * 2016-05-10 2017-11-16 Lik Hon A kind of microburst-microcapsule used for cigarettes and smoking articles with such microburst-microcapsules
CN107568790A (en) * 2017-10-23 2018-01-12 上海聚华科技股份有限公司 Cigarette filter tip and cigarette containing zeolite perfume (or spice) pearl zeolite perfume (or spice) pearl preparation method
CN109123775A (en) * 2018-08-06 2019-01-04 江西中烟工业有限责任公司 A kind of heating of the perfume (or spice) of solid-state containing herbal odor type pearl is not burnt cigarette and preparation method thereof
CN109645561A (en) * 2019-02-18 2019-04-19 重庆中烟工业有限责任公司 Cigarette capsule and preparation method thereof and cigarette filter

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH02308784A (en) * 1989-05-22 1990-12-21 Tdk Corp Filter for tobacco

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104957768A (en) * 2015-06-05 2015-10-07 滁州卷烟材料厂 Health care cigarette filter tip composite adsorbent for promoting sleep and preparing method thereof
WO2017193495A1 (en) * 2016-05-10 2017-11-16 Lik Hon A kind of microburst-microcapsule used for cigarettes and smoking articles with such microburst-microcapsules
CN106520380A (en) * 2016-12-29 2017-03-22 云南省玉溪市云溪香精香料有限责任公司 Fruit extract and application
CN107568790A (en) * 2017-10-23 2018-01-12 上海聚华科技股份有限公司 Cigarette filter tip and cigarette containing zeolite perfume (or spice) pearl zeolite perfume (or spice) pearl preparation method
CN109123775A (en) * 2018-08-06 2019-01-04 江西中烟工业有限责任公司 A kind of heating of the perfume (or spice) of solid-state containing herbal odor type pearl is not burnt cigarette and preparation method thereof
CN109645561A (en) * 2019-02-18 2019-04-19 重庆中烟工业有限责任公司 Cigarette capsule and preparation method thereof and cigarette filter

Also Published As

Publication number Publication date
CN110226774A (en) 2019-09-13

Similar Documents

Publication Publication Date Title
CN110226774B (en) Dry cigarette bead tip rod capable of improving sweet feeling of cigarettes
KR102288257B1 (en) Functional cigarette filter comprising natural plant material, cigarette containing the same, and method for producing the same
CN106987314B (en) Citrus reticulata flavor essence for bead blasting of cigarettes and application of citrus reticulata flavor essence in cigarettes
CN110013806B (en) Graphene-plant porous composite microsphere and preparation method and application thereof
CN104403794A (en) Preparation method and application of Pu'er tea extract to cigarettes
CN104687246B (en) A kind of Moringa porous particle, preparation method and the cigarette filter rod containing the porous particle
CN112273717A (en) Aroma-enhancing and cooling particles for cigarettes, and preparation method and application thereof
CN103054181B (en) Coffee or cocoa composite particle filtering bar and manufacturing method thereof
CN103054186A (en) Chinese medicinal composite particle filter stick and preparation method thereof
CN106215818A (en) The preparation method of a kind of fragility capsule, fragility capsule and purposes
CN108851215B (en) Cigarette filter rod containing double solid flavor bead particles and preparation method thereof
CN108851173A (en) A kind of cigarette preparation method of mango fragrance and the application in cigarette
CN101637303A (en) Lemon extract, preparation method thereof and application thereof in cigarette flavoring
CN108851213B (en) Cigarette filter rod containing large-particle solid aromatic beads and preparation method thereof
CN110982625A (en) Licorice-flavored dried beads for cigarette filter tips and preparation method thereof
CN110403236B (en) Cigarette dry bead filter rod with function of improving smoke permeation
CN107022415B (en) Semen Scaphii Lychnophori essence for cigarette bead blasting and application thereof in cigarette
CN106947597B (en) Pine pollen essence for cigarette bead blasting and application of pine pollen essence in cigarettes
CN113876028A (en) Preparation method and application of porous plant particles with scorched fragrance
CN101642286A (en) Filtering agent for harmful gas in cigarette, production method thereof and application thereof
CN107418730B (en) Kumquat flavor essence for bead blasting of cigarettes and application of kumquat flavor essence in cigarettes
CN111718797A (en) Method for finely extracting tobacco essence
CN111084417A (en) Preparation method and application of cigarette filter stick aroma-enhancing ball
CN109247616A (en) A kind of cigarette filter tip
CN115644494A (en) Preparation method and application of mixed tobacco reconstituted essence

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant