CN107568790A - Cigarette filter tip and cigarette containing zeolite perfume (or spice) pearl zeolite perfume (or spice) pearl preparation method - Google Patents
Cigarette filter tip and cigarette containing zeolite perfume (or spice) pearl zeolite perfume (or spice) pearl preparation method Download PDFInfo
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- CN107568790A CN107568790A CN201710990114.9A CN201710990114A CN107568790A CN 107568790 A CN107568790 A CN 107568790A CN 201710990114 A CN201710990114 A CN 201710990114A CN 107568790 A CN107568790 A CN 107568790A
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- zeolite
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- perfume
- filter tip
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Abstract
Present invention is disclosed a kind of cigarette filter tip containing zeolite perfume (or spice) pearl and cigarette zeolite perfume (or spice) pearl preparation method.Include the zeolite perfume (or spice) pearl in cigarette filter tip of the present invention, the zeolite perfume (or spice) pearl has adsorbed the essence for being suitable for cigarette using zeolite as carrier.The zeolite perfume (or spice) pearl has open adsorption hole, and the adsorption hole is adsorbed with essence.The present invention is used for zeolite perfume (or spice) pearl as solid perfume (or spice) pearl in cigarette filter tip, because zeolite has open adsorption hole, it has very strong absorption property, and cause perfumery can be smoothly discharged when sucking cigarette after its densely covered adsorption hole absorption essence, ensures that stable fragrance can be obtained when sucking.
Description
Technical field
The present invention relates to cigarette technical field, more particularly to a kind of cigarette filter tip and cigarette zeolite containing zeolite perfume (or spice) pearl
The preparation method of fragrant pearl.
Background technology
The cigarette of cigarette filter tip is by the graininess capsule that is fabricated to of shell parcel liquid oily perfume with perfuming pearl at present, is put
Being pinched brokenly in finished cigarettes mouth rod, during use discharges internal spices, as the compensation to cigarette flavor.
Be present many defects in this liquid perfume pearl, comprise at least:1st, after liquid perfume release is in cigarette filter tip, can lead
Fragrance supply is unstable when cause is sucked, and fragrance is excessively dense when typically just starting to suck, with the rise of temperature in cigarette filter tip,
Liquid can volatilize, and fragrance when now sucking becomes very light again;2nd, the easy moisture absorption of shell, cause to be difficult to pinch brokenly, influence its use;
3rd, after liquid perfume release is in cigarette filter tip, the outward appearance of mouth rod can be usually polluted, is influenceed attractive in appearance.
Accordingly, it is desirable to provide a kind of new cigarette for cigarette filter tip is with solid perfume (or spice) pearl and preparation method thereof.
The content of the invention
It is an object of the invention to provide a kind of cigarette filter tip containing zeolite perfume (or spice) pearl and cigarette zeolite perfume (or spice) pearl preparation method,
To solve some problems existing for current technology.
The present invention provides a kind of cigarette filter tip containing zeolite perfume (or spice) pearl, and it is fragrant to include the zeolite in the cigarette filter tip
Pearl, the zeolite perfume (or spice) pearl are densely covered with open adsorption hole using zeolite as carrier on the zeolite perfume (or spice) pearl, the adsorption hole is adsorbed with
Essence.
Adsorption hole is adsorbed with fragrance solution on the zeolite perfume (or spice) pearl, and the solvent of the fragrance solution includes water, ethanol, the third two
One or more of mixing in alcohol, glycerine, Glycerin, mixed triester with caprylic acid capric acid and medium chain triglyceride, the perfume (or spice) of the zeolite perfume (or spice) pearl absorption
Smart solution is 0.1%~60% in the mass concentration of the zeolite perfume (or spice) pearl.
The cigarette filter tip includes a cavity, and some zeolite perfume (or spice) pearls are placed with the cavity and some are densely covered with out
Put the mixture of the zeolite grain of formula adsorption hole.
A kind of cigarette filter tip, include a cylinder, axle of the cylinder along the cigarette filter tip in the cigarette filter tip
To setting, the cylinder is molded by some zeolite perfume (or spice) pearls, and the zeolite perfume (or spice) pearl using zeolite as carrier, gather by the zeolite perfume (or spice) pearl
There is open adsorption hole, the adsorption hole is adsorbed with essence.
Axially direction is in breakthrough status for the inside of the cylinder, is filled in the internal run-through cavity of the cylinder
There are some zeolite grains, open adsorption hole is densely covered with the zeolite grain.
Axially direction is in breakthrough status for the inside of the cylinder, is filled in the internal run-through cavity of the cylinder
There are some silicon particles, open adsorption hole is densely covered with the silicon particle.
A kind of cigarette preparation method of zeolite perfume (or spice) pearl, the described method comprises the following steps:
7.1 prepare zeolite pearl, and the zeolite pearl is seated in an absorption tower, and the fragrance solution prepared is sprayed in institute
State on the zeolite pearl in absorption tower;
Fragrance solution described in 7.2 circulated sprinklings, when the target compound concentration for entering tower feed liquid with going out tower feed liquid is identical, reach
To adsorption equilibrium, stop spray;
7.3 drain the material in the absorption tower, and discharging saves backup into closed container.
In the step 7.2, it is additionally included in when implementing circulated sprinkling and pressurization gas is inputted to the material in the absorption tower,
To promote the zeolite pearl to fully absorb the fragrance solution, the pressurization gas includes one in nitrogen, inert gas, air
The mixing of kind or several gases.
A kind of cigarette preparation method of zeolite perfume (or spice) pearl, the described method comprises the following steps:
9.1 prepare zeolite pearl, and the zeolite pearl is seated in an adsorption column, is passed through the essence gas through ultrasonic atomization
Stream;
9.2, when inlet air flow is with going out that target components are identical in air-flow, reaches adsorption equilibrium, stop ventilation;
9.3 are transferred to the material in the adsorption column in closed container, save backup.
The gas of essence air-flow in the step 9.1 includes one kind in nitrogen, inertia or air.
One of the advantages of the present invention, it is used for zeolite perfume (or spice) pearl as solid perfume (or spice) pearl in cigarette filter tip, is opened because zeolite has
Formula adsorption hole is put, it has very strong absorption property, can smoothly discharge cause perfumery after its densely covered adsorption hole absorption essence,
Ensure smoothly provide fragrance when sucking.Further, since zeolite contains the hydrone of potential phase in itself, it is heated when sucking
Afterwards, moisture content can be discharged, the moisture content can form fragrance solution with the essence of absorption, and fragrance solution can further lift fragrance
Stationarity, and solution can also absorb the nicotine and tar in flue gas, play cleaning action.
The two of advantages of the present invention, when sucking the cigarette for having used the present invention, with the rise of cigarette filter tip temperature, zeolite
On fragrant pearl gather adsorption hole can expanded by heating, preferably the essence adsorbed in adsorption hole can be discharged, with it is continuous not
Fragrance is provided disconnectedly.
The three of advantages of the present invention, the adsorption hole of zeolite perfume (or spice) pearl are also adsorbed with the fragrance solution (quality of certain mass concentration
Concentration is defined as 0.1%~60% by many experiments), it is possible to achieve form fragrance solution in absorption internal surface of hole and will not overflow
Go out, the solvent of the fragrance solution includes water, ethanol, propane diols, glycerine, Glycerin, mixed triester with caprylic acid capric acid (ODO) and medium chain triglyceride
(MCT) one or more of mixing in.When sucking, flue gas fully contacts after entering adsorption hole with fragrance solution, fragrant obtaining
While the fragrance of essence, the solvent (water, ethanol etc.) of fragrance solution can absorb nicotine and tar in flue gas well, this
Sample perfume (or spice) pearl can not only provide endlessly fragrance, can also effectively reduce harmful substance.
The four of advantages of the present invention, the cavity in the cigarette filter tip are placed with the mixing of some zeolite perfume (or spice) pearls and zeolite grain
Thing, zeolite grain without essence but has very strong adsorption capacity to the tar in flue gas and nicotine, after such flue gas is come in,
Fragrance is obtained from zeolite perfume (or spice) pearl, while the harmful substance of tar and nicotine is reduced from the contact of zeolite grain.
The five of advantage of the present invention, include a cylinder in the cigarette filter tip, the cylinder is by some zeolite perfume (or spice) pearls
Shaping, the internal run-through of cylinder are simultaneously filled with some zeolite grains.After cylinder is arranged in cigarette filter tip, it can be formed when sucking
Two exhaust gases passes, a flue gas Titian passage formed in cylinder periphery, flue gas can be with the bottom surface and outer surface of cylinder
Contact, fragrance is obtained in zeolite perfume (or spice) pearl;Another passage is the flue gas cleaning passage inside cylinder, and flue gas can be by logical
Zeolite grain reduces tar and nicotine content in road.
Brief description of the drawings
Fig. 1 is the structural representation of one embodiment of the invention.
Embodiment
Below in conjunction with the accompanying drawings technical scheme is further illustrated with embodiment.
The present invention provides a kind of cigarette filter tip containing zeolite perfume (or spice) pearl, includes the zeolite perfume (or spice) pearl in the cigarette filter tip,
The zeolite perfume (or spice) pearl is densely covered with open adsorption hole using zeolite as carrier on the zeolite perfume (or spice) pearl, the adsorption hole is adsorbed with perfume (or spice)
Essence, essence here is the essence for going for cigarette, including flavoring essence etc.., can be by zeolite perfume (or spice) pearl as an embodiment
It is placed in the acetate fiber in cigarette filter tip.Here zeolite perfume (or spice) pearl will pass through zeolite by specially preparing, during preparation
Its adsorption hole fully absorbs essence.When sucking cigarette, flue gas passes through zeolite perfume (or spice) pearl, many suctions that flue gas can enter in zeolite perfume (or spice) pearl
Contact in attached hole and with the essence of the inside absorption, then suctioned out with aromatic flue gas by smoker.With constantly sucking, cigarette
The temperature of mouth rod can raise (sometimes more than 100 degrees Celsius), and now zeolite perfume (or spice) pearl is heated, and its adsorption hole can also expand, the inside
Essence can also be heated volatilization, at this moment fragrance can be further strong, can be good to smoker suck impression.Further, since zeolite
Itself contains the hydrone of potential phase, after being heated when sucking, can discharge moisture content, the moisture content can form perfume (or spice) with the essence of absorption
Smart solution, fragrance solution can further lift the stationarity of fragrance, and solution can also absorb nicotine in flue gas and
Tar, play cleaning action.
Adsorption hole is adsorbed with fragrance solution on the zeolite perfume (or spice) pearl, and the solvent of the fragrance solution includes water, ethanol, the third two
One or more of mixing in alcohol, glycerine, Glycerin, mixed triester with caprylic acid capric acid (ODO) and medium chain triglyceride (MCT), the zeolite perfume (or spice) pearl inhale
The attached fragrance solution is 0.1%~60% in the mass concentration of the zeolite perfume (or spice) pearl.Here mass concentration is by multiple
Experiment draws, so both can guarantee that in adsorption hole (mainly hole inwall) and has formed fragrance solution, will not cause again solution overflow and
Pollute cigarette filter tip.
As an embodiment, the zeolite perfume (or spice) pearl pass through containing 30% calcium chloride fragrance solution impregnation and drying and
Into such zeolite perfume (or spice) pearl has just adsorbed calcium chloride and perfume materials, and calcium chloride belongs to chemosorbent, can be used for further
The harmful substances such as tar and nicotine when sucking cigarette in flue gas, zeolite belong to physical absorption, and the essence of absorption is carried
Supply flue gas, so as to obtain cleaned contain aromatic flue gas.Metal chloride (such as calcium chloride) chemosorbent carries
In the micropore of zeolite, the absorption property of micropore can be strengthened.The surface roughness increase of the zeolite after calcium chloride is impregnated, it is concavo-convex
Surface texture increases and more uniformly, this contributes to the enhancing of its absorption property.Determined through overtesting, containing 30% concentration calcium chloride
Fragrance solution dipping zeolite after, there is more preferable adsorption capacity.
As an embodiment, the cigarette filter tip includes a cavity, and cavity is located in the acetate fiber in cigarette filter tip, institute
State the mixture that some zeolite perfume (or spice) pearls and some zeolite grains for being densely covered with open adsorption hole are placed with cavity.Here
Zeolite grain is pure zeolite grain, does not adsorb the materials such as essence, and these zeolite grains have to the tar in flue gas and nicotine
Very strong adsorption capacity, after flue gas is come in when so sucking, fragrance is obtained from zeolite perfume (or spice) pearl, while from the contact of zeolite grain
Reduce the harmful substances such as tar and nicotine.
Referring to Fig. 1, the present invention also provides a kind of cigarette filter tip 1, includes a cylinder 3, the circle in the cigarette filter tip 1
Cylinder 3 is axially arranged along the cigarette filter tip 1, and the outer diameter face of cylinder 3 is wrapped up by acetate fiber 2, if the cylinder 3 by
Dry zeolite perfume (or spice) pearl 7 is molded, and the mode of shaping can have a variety of, can be molding bonded or compression molding etc..The boiling
Stone perfume (or spice) pearl 7 is using zeolite as carrier, and the zeolite perfume (or spice) pearl 7 is densely covered with open adsorption hole, and the adsorption hole is adsorbed with essence.
Referring to Fig. 1, as an embodiment, axially direction is in breakthrough status for the inside of the cylinder 3, circle now
For cylinder 3 equivalent to the cylinder of an internal run-through, the internal run-through cavity of the cylinder 3 is interior to be filled with some zeolite grains 6, institute
State and open adsorption hole is densely covered with zeolite grain 6.It is clear that Through-cavity of the inside of cylinder 3 filled with zeolite grain 6 forms flue gas
Clean passage 4, flue gas contact zeolite grain 6 in this passage, and the adsorption hole of zeolite grain 6, which adsorbs tar and nicotine in flue gas etc., to be had
Evil material, greatly reduces the harmful substance in flue gas.The periphery (space beyond outer diameter face) of cylinder 3 forms flue gas Titian
Passage 5, flue gas are fully contacted with the essence out of zeolite perfume (or spice) pearl 7 adsorption hole in this passage with the outer wall surface of cylinder 3
Fragrance is extracted, by being mixed after flue gas cleaning passage 4 and flue gas Titian passage 5, formed not only has fragrance but also drop flue gas
The low flue gas of harmful substance.
As an embodiment, axially direction is in breakthrough status for the inside of the cylinder, the inside of the cylinder
Some silicon particles are filled with Through-cavity, open adsorption hole is densely covered with the silicon particle.It is same with epimere word description
Sample reason, the adsorption hole of silicon particle adsorb the harmful substances such as tar and nicotine in flue gas, greatly reduce having in flue gas
Evil material.And above-mentioned two passage is similarly formed, i.e. flue gas Titian passage 5 and flue gas cleaning passage 4.
Zeolite of the present invention is exactly molecular sieve, and it has the hydrone of potential phase, after being heated when sucking, can discharge water
Part, the adsorption hole in the moisture content and zeolite can adsorb nicotine and tar in flue gas, play cleaning action.
The present invention provides a kind of cigarette preparation method of zeolite perfume (or spice) pearl, the described method comprises the following steps:
8.1 prepare zeolite pearl, and the zeolite pearl is seated in an absorption tower, and the fragrance solution prepared is sprayed in institute
State on the zeolite pearl in absorption tower;
Fragrance solution described in 8.2 circulated sprinklings, when the target compound concentration for entering tower feed liquid with going out tower feed liquid is identical, reach
To adsorption equilibrium, stop spray;
8.3 drain the material in the absorption tower, and discharging saves backup into closed container.
As an embodiment, in the step 8.2, it is additionally included in when implementing circulated sprinkling to the material in the absorption tower
Pressurization gas is inputted, to promote the zeolite pearl to fully absorb the fragrance solution, the pressurization gas includes nitrogen, indifferent gas
The mixing of one or more of gases in body, air.
The present invention provides a kind of cigarette preparation method of zeolite perfume (or spice) pearl, the described method comprises the following steps:
10.1 prepare zeolite pearl, and the zeolite pearl is seated in an adsorption column, is passed through the essence gas through ultrasonic atomization
Stream;
10.2, when inlet air flow is with going out that target components are identical in air-flow, reaches adsorption equilibrium, stop ventilation;
10.3 are transferred to the material in the adsorption column in closed container, save backup.
The gas of essence air-flow in the step 10.1 includes one kind in nitrogen, inertia or air.
Those of ordinary skill in the art is it should be appreciated that the embodiment of the above is intended merely to illustrate this hair
It is bright, and be not used as limitation of the invention, as long as in the spirit of the present invention, the change to embodiment of above
Change, modification will all fall in the range of claims of the present invention.
Claims (10)
1. a kind of cigarette filter tip containing zeolite perfume (or spice) pearl, it is characterised in that include the zeolite perfume (or spice) pearl, institute in the cigarette filter tip
Zeolite perfume (or spice) pearl is stated using zeolite as carrier, open adsorption hole is densely covered with the zeolite perfume (or spice) pearl, the adsorption hole is adsorbed with essence.
2. cigarette filter tip as claimed in claim 1, it is characterised in that it is molten to be adsorbed with essence for adsorption hole on the zeolite perfume (or spice) pearl
Liquid, the solvent of the fragrance solution include one in water, ethanol, propane diols, glycerine, Glycerin, mixed triester with caprylic acid capric acid and medium chain triglyceride
Kind or several mixing, the fragrance solution of zeolite perfume (or spice) pearl absorption the zeolite perfume (or spice) pearl mass concentration for 0.1%~
60%.
3. cigarette filter tip as claimed in claim 1, it is characterised in that the zeolite perfume (or spice) pearl passes through the essence containing 30% calcium chloride
Solution impregnation and drying form.
4. the cigarette filter tip as described in claim 1 or 2 or 3, it is characterised in that the cigarette filter tip includes a cavity, described
The mixture of some zeolite perfume (or spice) pearls and some zeolite grains for being densely covered with open adsorption hole is placed with cavity.
5. a kind of cigarette filter tip, it is characterised in that include a cylinder in the cigarette filter tip, the cylinder is along the cigarette
Mouth rod it is axially arranged, the cylinder is molded by some zeolite perfume (or spice) pearls, and the zeolite perfume (or spice) pearl is using zeolite as carrier, the zeolite
Fragrant pearl is densely covered with open adsorption hole, and the adsorption hole is adsorbed with essence.
6. cigarette filter tip as claimed in claim 5, it is characterised in that axially direction is in insertion for the inside of the cylinder
State, the internal run-through cavity of the cylinder is interior to be filled with some zeolite grains, and open absorption is densely covered with the zeolite grain
Hole.
7. cigarette filter tip as claimed in claim 5, it is characterised in that axially direction is in insertion for the inside of the cylinder
State, the internal run-through cavity of the cylinder is interior to be filled with some silicon particles, and open absorption is densely covered with the silicon particle
Hole.
8. a kind of cigarette preparation method of zeolite perfume (or spice) pearl, it is characterised in that the described method comprises the following steps:
8.1 prepare zeolite pearl, and the zeolite pearl is seated in an absorption tower, and the fragrance solution prepared is sprayed in the suction
Receive on the zeolite pearl in tower;
Fragrance solution described in 8.2 circulated sprinklings, when the target compound concentration for entering tower feed liquid with going out tower feed liquid is identical, reach suction
Attached balance, stop spray;
8.3 drain the material in the absorption tower, and discharging saves backup into closed container.
9. preparation method as claimed in claim 8, it is characterised in that in the step 8.2, be additionally included in implementation circulated sprinkling
When in the absorption tower material input pressurization gas, it is described to promote the zeolite pearl to fully absorb the fragrance solution
Pressurization gas includes the mixing of nitrogen, inert gas, one or more of gases in air.
10. a kind of cigarette preparation method of zeolite perfume (or spice) pearl, it is characterised in that the described method comprises the following steps:
10.1 prepare zeolite pearl, and the zeolite pearl is seated in an adsorption column, is passed through the essence air-flow through ultrasonic atomization, institute
The gas stated in essence air-flow includes one kind in nitrogen, inert gas or air;
10.2, when inlet air flow is with going out that target components are identical in air-flow, reaches adsorption equilibrium, stop ventilation;
10.3 are transferred to the material in the adsorption column in closed container, save backup.
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CN201710990114.9A CN107568790A (en) | 2017-10-23 | 2017-10-23 | Cigarette filter tip and cigarette containing zeolite perfume (or spice) pearl zeolite perfume (or spice) pearl preparation method |
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CN201710990114.9A CN107568790A (en) | 2017-10-23 | 2017-10-23 | Cigarette filter tip and cigarette containing zeolite perfume (or spice) pearl zeolite perfume (or spice) pearl preparation method |
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CN201710990114.9A Pending CN107568790A (en) | 2017-10-23 | 2017-10-23 | Cigarette filter tip and cigarette containing zeolite perfume (or spice) pearl zeolite perfume (or spice) pearl preparation method |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110226774A (en) * | 2019-07-04 | 2019-09-13 | 江西中烟工业有限责任公司 | A kind of dry pearl mouth stick of cigarette that can promote cigarette sweet moisture feeling |
CN111165874A (en) * | 2020-02-28 | 2020-05-19 | 广西中烟工业有限责任公司 | Solid aromatic bead with core-shell structure and application thereof in cigarette filter stick |
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CN110226774A (en) * | 2019-07-04 | 2019-09-13 | 江西中烟工业有限责任公司 | A kind of dry pearl mouth stick of cigarette that can promote cigarette sweet moisture feeling |
CN110226774B (en) * | 2019-07-04 | 2021-07-27 | 江西中烟工业有限责任公司 | Dry cigarette bead tip rod capable of improving sweet feeling of cigarettes |
CN111165874A (en) * | 2020-02-28 | 2020-05-19 | 广西中烟工业有限责任公司 | Solid aromatic bead with core-shell structure and application thereof in cigarette filter stick |
CN111165874B (en) * | 2020-02-28 | 2022-02-18 | 广西中烟工业有限责任公司 | Solid aromatic bead with core-shell structure and application thereof in cigarette filter stick |
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