CN113229523A - Tobacco stem biomass charcoal loaded tobacco extract and application thereof in cigarette filter stick - Google Patents
Tobacco stem biomass charcoal loaded tobacco extract and application thereof in cigarette filter stick Download PDFInfo
- Publication number
- CN113229523A CN113229523A CN202110456040.7A CN202110456040A CN113229523A CN 113229523 A CN113229523 A CN 113229523A CN 202110456040 A CN202110456040 A CN 202110456040A CN 113229523 A CN113229523 A CN 113229523A
- Authority
- CN
- China
- Prior art keywords
- tobacco
- biomass charcoal
- extract
- loaded
- tobacco extract
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 241000208125 Nicotiana Species 0.000 title claims abstract description 225
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 225
- 239000002028 Biomass Substances 0.000 title claims abstract description 103
- 239000003610 charcoal Substances 0.000 title claims abstract description 102
- 239000000284 extract Substances 0.000 title claims abstract description 90
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 22
- 239000010902 straw Substances 0.000 claims abstract description 24
- 238000005507 spraying Methods 0.000 claims description 14
- 239000011246 composite particle Substances 0.000 claims description 12
- 238000002360 preparation method Methods 0.000 claims description 10
- 239000000834 fixative Substances 0.000 claims description 8
- 238000007865 diluting Methods 0.000 claims description 7
- 238000012216 screening Methods 0.000 claims description 7
- 239000012634 fragment Substances 0.000 claims description 6
- 238000000605 extraction Methods 0.000 claims description 5
- 239000000428 dust Substances 0.000 claims 1
- 239000002699 waste material Substances 0.000 abstract description 5
- 238000005516 engineering process Methods 0.000 abstract description 3
- 238000003763 carbonization Methods 0.000 abstract description 2
- 238000001179 sorption measurement Methods 0.000 abstract description 2
- 239000000843 powder Substances 0.000 description 5
- 235000013599 spices Nutrition 0.000 description 3
- SCCDQYPEOIRVGX-UHFFFAOYSA-N Acetyleugenol Chemical compound COC1=CC(CC=C)=CC=C1OC(C)=O SCCDQYPEOIRVGX-UHFFFAOYSA-N 0.000 description 2
- SESFRYSPDFLNCH-UHFFFAOYSA-N benzyl benzoate Chemical compound C=1C=CC=CC=1C(=O)OCC1=CC=CC=C1 SESFRYSPDFLNCH-UHFFFAOYSA-N 0.000 description 2
- GOLORTLGFDVFDW-UHFFFAOYSA-N 3-(1h-benzimidazol-2-yl)-7-(diethylamino)chromen-2-one Chemical compound C1=CC=C2NC(C3=CC4=CC=C(C=C4OC3=O)N(CC)CC)=NC2=C1 GOLORTLGFDVFDW-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 241000209140 Triticum Species 0.000 description 1
- 235000021307 Triticum Nutrition 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- ISAOCJYIOMOJEB-UHFFFAOYSA-N benzoin Chemical class C=1C=CC=CC=1C(O)C(=O)C1=CC=CC=C1 ISAOCJYIOMOJEB-UHFFFAOYSA-N 0.000 description 1
- 229960002903 benzyl benzoate Drugs 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000002309 gasification Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- MWOOGOJBHIARFG-UHFFFAOYSA-N vanillin Chemical compound COC1=CC(C=O)=CC=C1O MWOOGOJBHIARFG-UHFFFAOYSA-N 0.000 description 1
- FGQOOHJZONJGDT-UHFFFAOYSA-N vanillin Natural products COC1=CC(O)=CC(C=O)=C1 FGQOOHJZONJGDT-UHFFFAOYSA-N 0.000 description 1
- 235000012141 vanillin Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
Abstract
The invention relates to a tobacco extract loaded with tobacco straw biomass charcoal and application thereof in cigarette filter sticks. According to the technical scheme, the tobacco stalk biomass charcoal is prepared by adopting a carbonization technology for the waste tobacco stalks, the tobacco extract is sprayed on the tobacco stalk biomass charcoal, the adsorption of the tobacco extract is realized by utilizing the porous characteristic of the tobacco stalk biomass charcoal, the waste of resources can be avoided, and the quality of cigarettes can be improved.
Description
Technical Field
The invention belongs to the technical field of cigarette processing, and particularly relates to a tobacco stem biomass charcoal-loaded tobacco extract and application thereof in a cigarette filter stick.
Background
The tobacco straw is used as an accessory product in tobacco production, or discarded or dried and incinerated. Not only causes environmental pollution, but also causes waste of resources. The tobacco extract is used as an important raw material in the flavoring and casing of the cigarette, and the tobacco extract with a certain proportion is added into the cigarette, so that the aroma of the cigarette can be increased, part of miscellaneous gas can be masked, and the taste of the cigarette can be improved. At present, the research on the biochar is mostly concentrated on crops such as wheat and rice, and for the research on the gasification of the tobacco straw into the biochar, the research of Chinese patents (CN112191229A, CN112169760A and CN111943200A) is mainly concentrated on the preparation direction of the biomass carbon of the tobacco stems and the tobacco stalks, and the research on the application of the tobacco stem biochar loaded tobacco extract to cigarette filter sticks is not reported.
Disclosure of Invention
The invention aims to provide a tobacco straw biomass charcoal-loaded tobacco extract and application thereof in a cigarette filter stick, so as to solve the problem of application limitation of the existing tobacco straw.
In order to realize the purpose, the invention is realized by the following technical scheme:
a tobacco extract loaded with tobacco stem biomass charcoal comprises the tobacco stem biomass charcoal and a tobacco extract, wherein the tobacco extract is attached to the tobacco stem biomass charcoal.
Further, the tobacco stalk biomass charcoal loaded tobacco extract is composite particles.
Further, the composite particles are 20-30 meshes.
Further, the preparation method of the tobacco stalk biomass charcoal loaded tobacco extract comprises the following steps:
s1, preparing tobacco straw into tobacco straw biomass charcoal;
s2, preparing a tobacco extract from tobacco by an extraction method;
s3, diluting the tobacco extract prepared in the step S2 by 10-50 times to prepare a tobacco extract solution, spraying the tobacco extract solution onto the tobacco stalk biomass charcoal according to 1-3% of the weight of the tobacco stalk biomass charcoal, and spraying Peru extract accounting for 0.1% of the weight of the tobacco stalk biomass charcoal and a fixative accounting for 0.1-1% of the weight of the tobacco stalk biomass charcoal onto the tobacco stalk biomass charcoal;
s4, crushing the tobacco stem biomass charcoal obtained in the step S3 by using a disc granulator, and then screening to obtain the tobacco stem biomass charcoal-loaded tobacco extract composite particles.
Further, the tobacco used for preparing the tobacco extract in the step S2 is one or more of tobacco leaves, tobacco fragments, tobacco powder and tobacco stems.
The tobacco stalk biomass charcoal load tobacco extract is applied to cigarette filter sticks.
The invention has the beneficial effects that:
according to the invention, the waste tobacco straws are prepared into the tobacco stalk biomass charcoal by adopting a carbonization technology, the tobacco extract is sprayed on the tobacco stalk biomass charcoal, and the adsorption of the tobacco extract is realized by utilizing the porous characteristic of the tobacco stalk biomass charcoal, so that the waste of resources can be avoided, and the quality of cigarettes can be improved.
Detailed Description
The technical solutions of the present invention are described in detail below by examples, and the following examples are only exemplary and can be used only for explaining and explaining the technical solutions of the present invention, but not construed as limiting the technical solutions of the present invention.
The tobacco stalk biomass charcoal used in the present application is prepared by using tobacco stalks in a high-temperature low-oxygen environment, and the preparation method of the tobacco stalk biomass charcoal in the present application is a conventional technology, and a detailed description thereof is omitted, and all the tobacco stalk biomass charcoal prepared by the method for preparing the tobacco stalk biomass charcoal is suitable for the present invention.
The tobacco extract is prepared by extracting tobacco leaves, tobacco fragments, tobacco powder or tobacco stems and the like, in the technical scheme of the application, substances such as essence and spice can be mixed in the tobacco extract, the mass ratio of the essence and the spice to the tobacco extract is 1:1-1:10, and the essence and the spice are conventionally used in cigarettes. In the present application, any fixative conventionally used may be used, including, for example, but not limited to peru resin, benzoin esters, vanillin, coumarin, acetyl eugenol, benzyl benzoate, and the like.
The application provides a tobacco stalk biomass charcoal load tobacco extract, including tobacco stalk biomass charcoal and tobacco extract, the tobacco extract adhere to in the tobacco stalk biomass charcoal. The tobacco stalk biomass charcoal loaded tobacco extract is composite particles of 20-30 meshes.
The preparation method of the tobacco stalk biomass charcoal loaded tobacco extract is shown in the following examples:
example 1
The preparation method of the tobacco stalk biomass charcoal-loaded tobacco extract comprises the following steps:
s1, preparing tobacco straw biomass charcoal from the tobacco straws.
S2, preparing the tobacco extract from the tobacco fragments by an extraction method.
S3, diluting the tobacco extract prepared in the step S2 by 10 times to prepare a tobacco extract solution, spraying the tobacco extract solution onto the tobacco stalk biomass charcoal according to 1% of the weight of the tobacco stalk biomass charcoal, and spraying Peru extract accounting for 0.1% of the weight of the tobacco stalk biomass charcoal and a fixative accounting for 0.1% of the weight of the tobacco stalk biomass charcoal onto the tobacco stalk biomass charcoal.
S4, crushing the tobacco stem biomass charcoal obtained in the step S3 by using a disc granulator, and then screening to obtain 20-30-mesh composite particles of the tobacco stem biomass charcoal-loaded tobacco extract.
The prepared tobacco stalk biomass charcoal loaded tobacco extract is added into a cigarette filter stick.
Example 2
The preparation method of the tobacco stalk biomass charcoal-loaded tobacco extract comprises the following steps:
s1, preparing tobacco straw biomass charcoal from the tobacco straws.
S2, preparing the tobacco extract by extracting the tobacco powder and the tobacco fragments according to the weight ratio of 1: 1.
S3, diluting the tobacco extract prepared in the step S2 by 50 times to prepare a tobacco extract solution, spraying the tobacco extract solution onto the tobacco stalk biomass charcoal according to 3% of the weight of the tobacco stalk biomass charcoal, and spraying Peru extract accounting for 0.1% of the weight of the tobacco stalk biomass charcoal and a fixative accounting for 1% of the weight of the tobacco stalk biomass charcoal onto the tobacco stalk biomass charcoal.
S4, crushing the tobacco stem biomass charcoal obtained in the step S3 by using a disc granulator, and then screening to obtain 20-30-mesh composite particles of the tobacco stem biomass charcoal-loaded tobacco extract.
The prepared tobacco stalk biomass charcoal loaded tobacco extract is added into a cigarette filter stick.
Example 3
The preparation method of the tobacco stalk biomass charcoal-loaded tobacco extract comprises the following steps:
s1, preparing tobacco straw biomass charcoal from the tobacco straws.
S2, preparing the tobacco extract from the tobacco stems by an extraction method.
S3, diluting the tobacco extract prepared in the step S2 by 20 times to prepare a tobacco extract solution, spraying the tobacco extract solution onto the tobacco stalk biomass charcoal according to 2% of the weight of the tobacco stalk biomass charcoal, and spraying Peru extract accounting for 0.1% of the weight of the tobacco stalk biomass charcoal and a fixative accounting for 0.5% of the weight of the tobacco stalk biomass charcoal onto the tobacco stalk biomass charcoal.
S4, crushing the tobacco stem biomass charcoal obtained in the step S3 by using a disc granulator, and then screening to obtain 20-30-mesh composite particles of the tobacco stem biomass charcoal-loaded tobacco extract.
The prepared tobacco stalk biomass charcoal loaded tobacco extract is added into a cigarette filter stick.
Example 4
The preparation method of the tobacco stalk biomass charcoal-loaded tobacco extract comprises the following steps:
s1, preparing tobacco straw biomass charcoal from the tobacco straws.
S2, preparing the tobacco extract from the tobacco powder by an extraction method.
S3, diluting the tobacco extract prepared in the step S2 by 25 times to prepare a tobacco extract solution, spraying the tobacco extract solution onto the tobacco stalk biomass charcoal according to 1% of the weight of the tobacco stalk biomass charcoal, and spraying Peru extract accounting for 0.1% of the weight of the tobacco stalk biomass charcoal and a fixative accounting for 0.5% of the weight of the tobacco stalk biomass charcoal onto the tobacco stalk biomass charcoal.
S4, crushing the tobacco stem biomass charcoal obtained in the step S3 by using a disc granulator, and then screening to obtain 20-30-mesh composite particles of the tobacco stem biomass charcoal-loaded tobacco extract.
The prepared tobacco stalk biomass charcoal loaded tobacco extract is added into a cigarette filter stick.
Example 5
The preparation method of the tobacco stalk biomass charcoal-loaded tobacco extract comprises the following steps:
s1, preparing tobacco straw biomass charcoal from the tobacco straws.
S2, preparing the tobacco extract by extracting the tobacco powder and the tobacco fragments according to the weight ratio of 1: 2.
S3, diluting the tobacco extract and the essence (the conventional essence used in cigarettes currently, and the specific types are not described in detail) prepared in the step S2 by 30 times according to the mass ratio of 3:1, preparing a tobacco extract solution, spraying the tobacco extract solution onto the tobacco stalk biomass charcoal according to 3% of the weight of the tobacco stalk biomass charcoal, and spraying a Peru extract of 0.1% of the weight of the tobacco stalk biomass charcoal and a fixative of 1% of the weight of the tobacco stalk biomass charcoal onto the tobacco stalk biomass charcoal.
S4, crushing the tobacco stem biomass charcoal obtained in the step S3 by using a disc granulator, and then screening to obtain 20-30-mesh composite particles of the tobacco stem biomass charcoal-loaded tobacco extract.
The prepared tobacco stalk biomass charcoal loaded tobacco extract is added into a cigarette filter stick.
Although the present application has been described with reference to a few embodiments, it should be understood that various changes, substitutions and alterations can be made herein without departing from the spirit and scope of the application as defined by the appended claims.
Claims (6)
1. The tobacco extract loaded with the tobacco stalk biomass charcoal is characterized by comprising the tobacco stalk biomass charcoal and a tobacco extract, wherein the tobacco extract is attached to the tobacco stalk biomass charcoal.
2. The tobacco straw biomass charcoal-loaded tobacco extract as claimed in claim 1, wherein the tobacco straw biomass charcoal-loaded tobacco extract is a composite particle.
3. The tobacco stem biomass charcoal-loaded tobacco extract as claimed in claim 2, wherein the composite particles are between 20-30 mesh.
4. The tobacco straw biomass charcoal-loaded tobacco extract as claimed in claim 1, wherein the preparation method of the tobacco straw biomass charcoal-loaded tobacco extract comprises the following steps:
s1, preparing tobacco straw into tobacco straw biomass charcoal;
s2, preparing a tobacco extract from tobacco by an extraction method;
s3, diluting the tobacco extract prepared in the step S2 by 10-50 times to prepare a tobacco extract solution, spraying the tobacco extract solution onto the tobacco stalk biomass charcoal according to 1-3% of the weight of the tobacco stalk biomass charcoal, and spraying Peru extract accounting for 0.1% of the weight of the tobacco stalk biomass charcoal and a fixative accounting for 0.1-1% of the weight of the tobacco stalk biomass charcoal onto the tobacco stalk biomass charcoal;
s4, crushing the tobacco stem biomass charcoal obtained in the step S3 by using a disc granulator, and then screening to obtain the composite particles of the tobacco stem biomass charcoal loaded tobacco extracts.
5. The tobacco stalk biomass charcoal-loaded tobacco extract as claimed in claim 4, wherein the tobacco used for preparing the tobacco extract in step S2 is one or more of tobacco leaves, tobacco fragments, tobacco dust or tobacco stems.
6. The tobacco stem biomass charcoal-loaded tobacco extract as claimed in any one of claims 1 to 5, which is applied to a cigarette filter stick.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN202110456040.7A CN113229523A (en) | 2021-04-26 | 2021-04-26 | Tobacco stem biomass charcoal loaded tobacco extract and application thereof in cigarette filter stick |
Applications Claiming Priority (1)
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CN202110456040.7A CN113229523A (en) | 2021-04-26 | 2021-04-26 | Tobacco stem biomass charcoal loaded tobacco extract and application thereof in cigarette filter stick |
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CN202110456040.7A Pending CN113229523A (en) | 2021-04-26 | 2021-04-26 | Tobacco stem biomass charcoal loaded tobacco extract and application thereof in cigarette filter stick |
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US20070000505A1 (en) * | 2005-02-24 | 2007-01-04 | Philip Morris Usa Inc. | Smoking article with tobacco beads |
CN102488329A (en) * | 2011-11-11 | 2012-06-13 | 广东中烟工业有限责任公司 | Concentric filter tip sticks and preparation method thereof |
CN105146754A (en) * | 2015-09-15 | 2015-12-16 | 中烟施伟策(云南)再造烟叶有限公司 | Method for preparing activated carbon cigarette filter stick from tobacco straw |
CN109898359A (en) * | 2019-04-11 | 2019-06-18 | 湖北中烟工业有限责任公司 | A kind of preparation method of the papery cigarette filter stick paper material of natural baccy fragrance |
CN110226774A (en) * | 2019-07-04 | 2019-09-13 | 江西中烟工业有限责任公司 | A kind of dry pearl mouth stick of cigarette that can promote cigarette sweet moisture feeling |
CN110419777A (en) * | 2019-08-12 | 2019-11-08 | 云南中烟新材料科技有限公司 | A kind of preparation method of cigarette class active carbon particle |
-
2021
- 2021-04-26 CN CN202110456040.7A patent/CN113229523A/en active Pending
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20070000505A1 (en) * | 2005-02-24 | 2007-01-04 | Philip Morris Usa Inc. | Smoking article with tobacco beads |
CN102488329A (en) * | 2011-11-11 | 2012-06-13 | 广东中烟工业有限责任公司 | Concentric filter tip sticks and preparation method thereof |
CN105146754A (en) * | 2015-09-15 | 2015-12-16 | 中烟施伟策(云南)再造烟叶有限公司 | Method for preparing activated carbon cigarette filter stick from tobacco straw |
CN109898359A (en) * | 2019-04-11 | 2019-06-18 | 湖北中烟工业有限责任公司 | A kind of preparation method of the papery cigarette filter stick paper material of natural baccy fragrance |
CN110226774A (en) * | 2019-07-04 | 2019-09-13 | 江西中烟工业有限责任公司 | A kind of dry pearl mouth stick of cigarette that can promote cigarette sweet moisture feeling |
CN110419777A (en) * | 2019-08-12 | 2019-11-08 | 云南中烟新材料科技有限公司 | A kind of preparation method of cigarette class active carbon particle |
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Application publication date: 20210810 |
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