CN113234509A - Tobacco stem biomass charcoal composite particle and preparation method thereof - Google Patents
Tobacco stem biomass charcoal composite particle and preparation method thereof Download PDFInfo
- Publication number
- CN113234509A CN113234509A CN202110456046.4A CN202110456046A CN113234509A CN 113234509 A CN113234509 A CN 113234509A CN 202110456046 A CN202110456046 A CN 202110456046A CN 113234509 A CN113234509 A CN 113234509A
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- Prior art keywords
- tobacco
- biomass charcoal
- composite particle
- extract
- stalk biomass
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L5/00—Solid fuels
- C10L5/40—Solid fuels essentially based on materials of non-mineral origin
- C10L5/44—Solid fuels essentially based on materials of non-mineral origin on vegetable substances
- C10L5/445—Agricultural waste, e.g. corn crops, grass clippings, nut shells or oil pressing residues
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B5/00—Stripping tobacco; Treatment of stems or ribs
- A24B5/16—Other treatment of stems or ribs, e.g. bending, chopping, incising
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L5/00—Solid fuels
- C10L5/40—Solid fuels essentially based on materials of non-mineral origin
- C10L5/44—Solid fuels essentially based on materials of non-mineral origin on vegetable substances
- C10L5/447—Carbonized vegetable substances, e.g. charcoal, or produced by hydrothermal carbonization of biomass
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L9/00—Treating solid fuels to improve their combustion
- C10L9/10—Treating solid fuels to improve their combustion by using additives
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/30—Fuel from waste, e.g. synthetic alcohol or diesel
Abstract
The invention relates to a tobacco stalk biomass charcoal composite particle and a preparation method thereof, the tobacco stalk biomass charcoal prepared by tobacco stalks and the composite particle prepared by attachments attached in the tobacco stalk biomass charcoal; the attachment is tobacco extract, smoke agent or essence. According to the invention, the waste tobacco straws are carbonized to prepare the tobacco straw biomass charcoal, more than one of tobacco extract, smoke agent or essence and spice is attached into the tobacco straw biomass charcoal in an immersion manner to prepare the composite particles, and the porous characteristic of the tobacco straw biomass charcoal is utilized, so that the waste of resources can be avoided, the air permeability of the composite particles can be improved, and the quality of cigarettes can be improved in application.
Description
Technical Field
The invention belongs to the technical field of tobacco waste recycling, and particularly relates to tobacco stem biomass charcoal composite particles and a preparation method thereof.
Background
The tobacco straw is used as an accessory product in tobacco production, or discarded or dried and incinerated. Not only causes environmental pollution, but also causes waste of resources. The tobacco extract is used as an important raw material in the flavoring and casing of the cigarette, and the tobacco extract with a certain proportion is added into the cigarette, so that the aroma of the cigarette can be increased, part of miscellaneous gas can be masked, and the taste of the cigarette can be improved. At present, researches on biochar are mostly focused on crops such as wheat and rice, researches on converting tobacco stalks into biochar, such as Chinese patents (CN112191229A, CN112169760A and CN111943200A), are also mainly focused on the preparation direction of tobacco stalk and tobacco stalk biochar, and no report is found on researches on application of tobacco stalk biochar composite particles.
Disclosure of Invention
The invention aims to provide a tobacco stalk biomass charcoal composite particle and a preparation method thereof, and aims to solve the problem of resource waste caused by insufficient recycling importance of tobacco stalks in the prior art.
In order to realize the purpose, the invention is realized by the following technical scheme:
a composite particle of tobacco stalk biomass charcoal is prepared from tobacco stalk biomass charcoal and attachments attached to the tobacco stalk biomass charcoal.
Further, the weight percentage of attachments in the composite particles is 1-3%.
Furthermore, the attachment is more than one of tobacco extract, smoke agent or essence.
Further, the weight ratio of the tobacco extract, the smoke agent and the essence is (1-10): (0-5): (0-10).
Further, the tobacco extract is extracted from more than one of tobacco leaves, tobacco fragments, tobacco powder, tobacco stems or tobacco stalks.
Further, the smoke agent is more than one of glycerin, propylene glycol or glycerol; the flavors and fragrances include but are not limited to more than one of tobacco extract, tobacco absolute, tobacco flavor and fragrance, fruit flavor extract or flower extract.
The preparation method of the tobacco stalk biomass charcoal composite particle comprises the following steps:
s1, preparing tobacco straw into tobacco straw biomass charcoal;
s2, smashing the tobacco stalk biomass charcoal into tobacco stalk biomass charcoal particles with a set diameter range;
s3, diluting the attachments for immersing into the tobacco stalk biomass charcoal by 50-100 times to obtain attachment solution, immersing the tobacco stalk biomass charcoal particles in the step S2 into the attachment solution for 0.5-2 hours, filtering and drying to obtain composite particle blanks;
s4, spraying Peru extract accounting for 0.1 percent of the weight of the composite particle blank and fixative accounting for 0.1 to 1 percent of the weight of the composite particle blank onto the composite particle blank;
and S5, crushing the composite particle blank obtained in the step S4 by using a disc granulator, and then screening to obtain the tobacco stem biomass charcoal composite particles.
The preparation method of the tobacco stalk biomass charcoal composite particle comprises the following steps:
s10, preparing tobacco straw into tobacco straw biomass charcoal;
s20, diluting the attachment for immersing into the tobacco stalk biomass charcoal by 10-50 times to obtain an attachment solution, spraying the attachment solution on the tobacco stalk biomass charcoal according to 1-3% of the weight of the tobacco stalk biomass charcoal, and spraying Peru extract 0.1-1% of the weight of the tobacco stalk biomass charcoal and fixative 0.1-1% of the weight of the tobacco stalk biomass charcoal on the tobacco stalk biomass charcoal;
s30, crushing the tobacco stem biomass charcoal obtained in the step S20 by using a disc particle leaning machine, and then screening to obtain the tobacco stem biomass charcoal composite particles.
Further, the attachment is more than one of tobacco extract, smoke agent or essence.
Further, the weight ratio of the tobacco extract, the smoke agent and the essence is (1-10): (0-5): (0-10).
The invention has the beneficial effects that:
according to the invention, the waste tobacco straws are carbonized to prepare the tobacco straw biomass charcoal, more than one of tobacco extract, smoke agent or essence and spice is attached into the tobacco straw biomass charcoal in an immersion manner to prepare the composite particles, and the porous characteristic of the tobacco straw biomass charcoal is utilized, so that the waste of resources can be avoided, the air permeability of the composite particles can be improved, and the quality of cigarettes can be improved in application.
Detailed Description
The technical solutions of the present invention are described in detail below by examples, and the following examples are only exemplary and can be used only for explaining and explaining the technical solutions of the present invention, but not construed as limiting the technical solutions of the present invention.
The tobacco stalk biomass charcoal used in the present application is prepared by using tobacco stalks in a high-temperature low-oxygen environment, and the preparation method of the tobacco stalk biomass charcoal in the present application is a conventional technology, and a detailed description thereof is omitted, and all the tobacco stalk biomass charcoal prepared by the method for preparing the tobacco stalk biomass charcoal is suitable for the present invention.
The tobacco extract is prepared by extracting tobacco leaves, tobacco fragments, tobacco powder, tobacco stems or tobacco stalks and the like. In the technical scheme of the application, substances such as flavors and fragrances and the like can be mixed in the tobacco extract, and the flavors and fragrances are one or more than one of tobacco extract, tobacco absolute oil, tobacco flavor flavors and fragrances, fruit-flavor extract or flower extract which are conventionally used in the existing cigarettes. Also includes the use of a smoking agent, which in this application is one or more of glycerin, propylene glycol or glycerol.
In the present application, any fixative conventionally used may be used, including, for example, but not limited to peru resin, benzoin esters, vanillin, coumarin, acetyl eugenol, benzyl benzoate, and the like.
In the embodiments of the present application, the used apparatus, instruments, reagents, or the like are commercially available unless otherwise specified.
In the technical scheme of the application, the tobacco stalk biomass charcoal is prepared by adopting the prior art, namely, all the tobacco stalk biomass charcoal prepared by the method which can be used for preparing the tobacco stalk biomass charcoal can be used in the technical scheme of the application, and in this case, the preparation of the tobacco stalk biomass charcoal is not explained in detail.
Example 1
The preparation method of the tobacco stalk biomass charcoal composite particles comprises the following steps:
s1, preparing the tobacco stalks into the tobacco stalk biomass charcoal.
S2, smashing the tobacco stalk biomass charcoal into 10-30-mesh tobacco stalk biomass charcoal particles, and selecting 100 g of 10-30-mesh tobacco stalk biomass charcoal particles.
S3, adding water to dilute the tobacco extract 5 g for immersing into the tobacco straw biomass charcoal by 50 times to obtain a tobacco extract solution, immersing the tobacco straw biomass charcoal particles 100 g in the step S2 into the tobacco extract solution for 0.5 hour, filtering and drying to obtain the composite particle blank.
S4, spraying Peru extract accounting for 0.1 percent of the weight of the composite particle blank and fixative accounting for 0.1 percent of the weight of the composite particle blank onto the composite particle blank.
And S5, crushing the composite particle blank obtained in the step S4 by using a disc granulator, and then screening to obtain the tobacco stem biomass charcoal composite particles.
Example 2
The preparation method of the tobacco stalk biomass charcoal composite particles comprises the following steps:
s1, preparing the tobacco stalks into the tobacco stalk biomass charcoal.
S2, smashing the tobacco stalk biomass charcoal into 10-30-mesh tobacco stalk biomass charcoal particles, and selecting 100 g of 10-30-mesh tobacco stalk biomass charcoal particles.
S3, adding 8 g of tobacco extract and tobacco absolute oil which are used for being immersed into the tobacco stalk biomass charcoal, wherein the weight ratio of the tobacco extract to the essence and the spice is 1:1, adding water to dilute by 100 times to obtain attachment solution, immersing 100 g of tobacco stalk biomass charcoal particles obtained in the step S2 into the attachment solution for 2 hours, filtering and drying to obtain composite particle blanks.
S4, spraying Peru extract accounting for 0.1 percent of the weight of the composite particle blank and a fixative accounting for 1 percent of the weight of the composite particle blank onto the composite particle blank.
And S5, crushing the composite particle blank obtained in the step S4 by using a disc granulator, and then screening to obtain the tobacco stem biomass charcoal composite particles.
Example 3
The preparation method of the tobacco stalk biomass charcoal composite particles comprises the following steps:
s1, preparing the tobacco stalks into the tobacco stalk biomass charcoal.
S2, smashing the tobacco stalk biomass charcoal into 10-30-mesh tobacco stalk biomass charcoal particles, and selecting 100 g of 10-30-mesh tobacco stalk biomass charcoal particles.
S3, 6 g of the tobacco extract and the tobacco extract which are used for being immersed in the tobacco stalk biomass charcoal, wherein the weight ratio of the tobacco extract to the essence and the spice is 2:1, water is added for dilution by 80 times to obtain attachment solution, 100 g of the tobacco stalk biomass charcoal particles obtained in the step S2 are immersed in the attachment solution for 1 hour, and the composite particle blank is obtained through filtration and drying.
S4, spraying Peru extract accounting for 0.1 percent of the weight of the composite particle blank and fixative accounting for 0.5 percent of the weight of the composite particle blank onto the composite particle blank.
And S5, crushing the composite particle blank obtained in the step S4 by using a disc granulator, and then screening to obtain the tobacco stem biomass charcoal composite particles.
Example 4
The preparation method of the tobacco stalk biomass charcoal composite particles comprises the following steps:
s10, preparing the tobacco stalks into the tobacco stalk biomass charcoal.
S20, diluting the tobacco extract for immersing into the tobacco stalk biomass charcoal by 10 times to obtain an attachment solution, spraying the attachment solution onto the tobacco stalk biomass charcoal according to 1% of the weight of the tobacco stalk biomass charcoal, and spraying Peru extract 0.1% of the weight of the tobacco stalk biomass charcoal and a fixative 0.1% of the weight of the tobacco stalk biomass charcoal onto the tobacco stalk biomass charcoal.
S30, crushing the tobacco stem biomass charcoal obtained in the step S20 by using a disc particle leaning machine, and then screening to obtain the tobacco stem biomass charcoal composite particles.
Example 5
The preparation method of the tobacco stalk biomass charcoal composite particles comprises the following steps:
s10, preparing the tobacco stalks into the tobacco stalk biomass charcoal.
S20, diluting the tobacco extract and the tobacco extract which are used for being immersed in the tobacco stalk biomass charcoal by 50 times to obtain attachment solution, spraying the attachment solution on the tobacco stalk biomass charcoal according to 3% of the weight of the tobacco stalk biomass charcoal, and spraying peru extract which is 0.1% of the weight of the tobacco stalk biomass charcoal and a fixative which is 1% of the weight of the tobacco stalk biomass charcoal on the tobacco stalk biomass charcoal.
S30, crushing the tobacco stem biomass charcoal obtained in the step S20 by using a disc particle leaning machine, and then screening to obtain the tobacco stem biomass charcoal composite particles.
Example 6
The preparation method of the tobacco stalk biomass charcoal composite particles comprises the following steps:
s10, preparing the tobacco stalks into the tobacco stalk biomass charcoal.
S20, diluting the tobacco extract and the tobacco absolute oil which are used for being immersed in the tobacco stalk biomass charcoal by 30 times to obtain attachment solution, spraying the attachment solution on the tobacco stalk biomass charcoal according to 2% of the weight of the tobacco stalk biomass charcoal, and spraying Peru extract which is 0.1% of the weight of the tobacco stalk biomass charcoal and a fixative which is 0.5% of the weight of the tobacco stalk biomass charcoal on the tobacco stalk biomass charcoal.
S30, crushing the tobacco stem biomass charcoal obtained in the step S20 by using a disc particle leaning machine, and then screening to obtain the tobacco stem biomass charcoal composite particles.
Although the present application has been described with reference to a few embodiments, it should be understood that various changes, substitutions and alterations can be made herein without departing from the spirit and scope of the application as defined by the appended claims.
Claims (10)
1. The composite particle is characterized by comprising tobacco straw biomass carbon prepared from tobacco straws and composite particles prepared from attachments attached in the tobacco straw biomass carbon.
2. The tobacco straw biomass charcoal composite particle according to claim 1, wherein the weight percentage of attachments in the composite particle is 1-3%.
3. The tobacco stem biomass charcoal composite particle according to claim 1, wherein the attachment is one or more of a tobacco extract, a smoke agent, or an aroma and flavor.
4. The tobacco stem biomass charcoal composite particle according to claim 3, wherein the weight ratio of the tobacco extract, the smoke agent and the flavors and fragrances is (1-10): (0-5): (0-10).
5. The tobacco stem biomass char composite particle according to claim 3, wherein the tobacco extract is extracted from one or more of tobacco leaves, tobacco leaf fragments, tobacco dust, tobacco stems, or tobacco stalks.
6. The tobacco stem biomass charcoal composite particle according to claim 3, wherein the fuming agent is one or more of glycerin, propylene glycol or glycerol; the flavors and fragrances include but are not limited to more than one of tobacco extract, tobacco absolute, tobacco flavor and fragrance, fruit flavor extract or flower extract.
7. The method for preparing the tobacco stalk biomass charcoal composite particle as claimed in any one of the above claims 1 to 6, characterized by comprising the steps of:
s1, preparing tobacco straw into tobacco straw biomass charcoal;
s2, smashing the tobacco stalk biomass charcoal into tobacco stalk biomass charcoal particles with a set diameter range;
s3, diluting the attachments for immersing into the tobacco stalk biomass charcoal by 50-100 times to obtain attachment solution, immersing the tobacco stalk biomass charcoal particles in the step S2 into the attachment solution for 0.5-2 hours, filtering and drying to obtain composite particle blanks;
s4, spraying Peru extract accounting for 0.1 percent of the weight of the composite particle blank and fixative accounting for 0.1 to 1 percent of the weight of the composite particle blank onto the composite particle blank;
and S5, crushing the composite particle blank obtained in the step S4 by using a disc granulator, and then screening to obtain the tobacco stem biomass charcoal composite particles.
8. The method for preparing the tobacco stalk biomass charcoal composite particle as claimed in any one of the above claims 1 to 6, characterized by comprising the steps of:
s10, preparing tobacco straw into tobacco straw biomass charcoal;
s20, diluting the attachment for immersing into the tobacco stalk biomass charcoal by 10-50 times to obtain an attachment solution, spraying the attachment solution on the tobacco stalk biomass charcoal according to 1-3% of the weight of the tobacco stalk biomass charcoal, and spraying Peru extract 0.1-1% of the weight of the tobacco stalk biomass charcoal and fixative 0.1-1% of the weight of the tobacco stalk biomass charcoal on the tobacco stalk biomass charcoal;
s30, crushing the tobacco stem biomass charcoal obtained in the step S20 by using a disc particle leaning machine, and then screening to obtain the tobacco stem biomass charcoal composite particles.
9. The method for preparing straw biomass charcoal composite particles according to claim 7 or 8, wherein the attachment is one or more of a tobacco extract, a smoke agent or an essence and flavor.
10. The method for preparing straw biomass charcoal composite particles according to claim 9, wherein the weight ratio of the tobacco extract, the smoke agent and the flavors and fragrances is (1-10): (0-5): (0-10).
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| Application Number | Priority Date | Filing Date | Title |
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| CN202110456046.4A CN113234509A (en) | 2021-04-26 | 2021-04-26 | Tobacco stem biomass charcoal composite particle and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202110456046.4A CN113234509A (en) | 2021-04-26 | 2021-04-26 | Tobacco stem biomass charcoal composite particle and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114195118A (en) * | 2021-11-30 | 2022-03-18 | 暨南大学 | Method for preparing biomass conductive carbon by taking straws as raw materials |
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| CN112191229A (en) * | 2020-10-19 | 2021-01-08 | 农业农村部环境保护科研监测所 | Preparation method and application of Mg/Ca-loaded modified tobacco stalk biochar |
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2021
- 2021-04-26 CN CN202110456046.4A patent/CN113234509A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101148594A (en) * | 2007-11-09 | 2008-03-26 | 曾勇 | Method for preparing formed charcoal from tobacco solid castoff |
| CN102488329A (en) * | 2011-11-11 | 2012-06-13 | 广东中烟工业有限责任公司 | Concentric filter tip sticks and preparation method thereof |
| CN104544548A (en) * | 2014-12-31 | 2015-04-29 | 贵州中烟工业有限责任公司 | Electronic cigarette smoke solution prepared through yellow tea leaf extract |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN114195118A (en) * | 2021-11-30 | 2022-03-18 | 暨南大学 | Method for preparing biomass conductive carbon by taking straws as raw materials |
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