KR102652799B1 - Cooling filter rod, application and cigarette - Google Patents
Cooling filter rod, application and cigarette Download PDFInfo
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- KR102652799B1 KR102652799B1 KR1020207036646A KR20207036646A KR102652799B1 KR 102652799 B1 KR102652799 B1 KR 102652799B1 KR 1020207036646 A KR1020207036646 A KR 1020207036646A KR 20207036646 A KR20207036646 A KR 20207036646A KR 102652799 B1 KR102652799 B1 KR 102652799B1
- Authority
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- South Korea
- Prior art keywords
- cooling
- powder
- filter rod
- particles
- cooling filter
- Prior art date
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- 238000001816 cooling Methods 0.000 title claims abstract description 143
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 58
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- 239000002808 molecular sieve Substances 0.000 claims description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims description 2
- 239000012188 paraffin wax Substances 0.000 claims description 2
- 235000020232 peanut Nutrition 0.000 claims description 2
- 239000004626 polylactic acid Substances 0.000 claims description 2
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- 229910002027 silica gel Inorganic materials 0.000 claims description 2
- 239000000741 silica gel Substances 0.000 claims description 2
- 229910052814 silicon oxide Inorganic materials 0.000 claims description 2
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims description 2
- 239000010902 straw Substances 0.000 claims description 2
- 235000020234 walnut Nutrition 0.000 claims description 2
- 244000061176 Nicotiana tabacum Species 0.000 claims 3
- 239000000779 smoke Substances 0.000 abstract description 39
- 230000000694 effects Effects 0.000 abstract description 19
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- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/067—Use of materials for tobacco smoke filters characterised by functional properties
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/04—Tobacco smoke filters characterised by their shape or structure
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/186—Treatment of tobacco products or tobacco substitutes by coating with a coating composition, encapsulation of tobacco particles
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/08—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/16—Use of materials for tobacco smoke filters of inorganic materials
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/16—Use of materials for tobacco smoke filters of inorganic materials
- A24D3/163—Carbon
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/20—Cigarettes specially adapted for simulated smoking devices
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
냉각 필터 로드, 적용 및 궐련이 제공된다. 냉각 필터 로드는 냉각 입자들에 의해 주로 형성되며; 냉각 입자는 입자 바디와 입자 바디 상에 코팅된 쉘을 포함하고, 쉘/또는 입자 바디는 상 변화 재료를 포함한다. 상 변화 재료는 냉각 입자들을 형성하기 위해 입자 재료의 표면에 코팅되고, 냉각 입자들은 냉각 필터 로드로 일체로 형성되며, 냉각 필터 로드는 기존의 필터 로드들과 조합된 후에 궐련 생산을 위해 직접 사용될 수 있으며; 냉각 효과는 상 변화 재료 및 냉각 필터 로드의 양에 따라 제어될 수 있고, 이러한 필터 로드는 산업 생산을 실현할 수 있고 낮은 비용과 양호한 냉각 효과를 가지며; 흡연 저항이 적고, 연기와 상 변화 재료 사이의 접촉 면적은 커서, 냉각 효율이 높다.Cooling filter rod, application and cigarette are provided. The cooling filter rod is mainly formed by cooling particles; The cooling particle includes a particle body and a shell coated on the particle body, and the shell/or particle body includes a phase change material. The phase change material is coated on the surface of the particle material to form cooling particles, and the cooling particles are integrally formed into a cooling filter rod, and the cooling filter rod can be used directly for cigarette production after being combined with existing filter rods. There is; The cooling effect can be controlled according to the amount of phase change material and cooling filter rod, such filter rod can realize industrial production and has low cost and good cooling effect; The smoking resistance is small, the contact area between the smoke and the phase change material is large, and the cooling efficiency is high.
Description
본 발명은 궐련 생산의 기술 분야에 속하는, 냉각 필터 로드, 그것의 적용 및 궐련에 관한 것이다.The present invention relates to cooling filter rods, their applications and cigarettes, belonging to the technical field of cigarette production.
전통적인 궐련의 흡연 과정에서, 궐련 연소 콘에 의해 발생된 열은 주류 연기에 의해 필터로 전달될 것이고, 흡연이 진행됨에 따라, 필터를 통과하는 연기의 온도는 점차 상승한다. 필터에서의 연기의 온도는 흡연이 끝날 무렵 70-80℃ 정도로 높을 수 있다는 것을 연구들이 보여주었다. 필터에서 너무 온도가 높으면 필터의 유지 효과에 영향을 미칠 것이고, 연기의 감각(sensory) 품질에 대한 소비자의 평가에 또한 영향을 미칠 것이다. 그러므로, 연기의 온도를 적절히 낮추는 것이 필요하다.In the traditional cigarette smoking process, the heat generated by the cigarette combustion cone will be transferred to the filter by the mainstream smoke, and as smoking progresses, the temperature of the smoke passing through the filter gradually increases. Studies have shown that the temperature of the smoke in the filter can be as high as 70-80 degrees Celsius by the end of the smoke. If the temperature in the filter is too high, it will affect the filter's retention effectiveness and will also affect the consumer's evaluation of the sensory quality of the smoke. Therefore, it is necessary to appropriately lower the temperature of the smoke.
궐련형 전자담배(heat-not-burn cigarette)는 외부 가열 엘리먼트로 담배 제품을 가열함으로써 연기를 생성한다. 일반적으로, 담배 제품은 250-350℃에서 무화 조건에 도달한다. 연기의 양을 보장하기 위하여, 흡착은 필터에서 적게 요구되거나 또는 요구되지 않는다. 필터를 통해 입에 들어가는 고온 무화된 연기의 온도는 전통적인 궐련 연소의 온도보다 더 높을 것이다. 그러므로, 연기의 온도의 적절한 감소 또한 저온 궐련들의 개발의 핵심 기술이다.Heat-not-burn cigarettes produce smoke by heating a tobacco product with an external heating element. Typically, tobacco products reach atomization conditions at 250-350°C. To ensure the volume of smoke, less or no adsorption is required in the filter. The temperature of the hot atomized smoke entering the mouth through the filter will be higher than that of traditional cigarette combustion. Therefore, appropriate reduction of the temperature of smoke is also a key technology in the development of low-temperature cigarettes.
중국 특허 CN201510045745.4호는 필터와 궐련을 제공한다. 연기의 온도는 상 변화 재료를 필터에 첨가함으로써 감소되며, 사용되는 상 변화 재료는 수화된 무기 염 및 요소(urea)의 혼합물이고, 그 혼합물은 셀룰로오스 아세테이트 로드에 분무되거나 또는 그것의 결정이 두 개의 필터들 사이에 배치된다. 업계에서 알려진 바와 같이, 이 수화된 염의 사용과 효과는 이상적이지 않다.Chinese patent CN201510045745.4 provides a filter and cigarette. The temperature of the smoke is reduced by adding a phase change material to the filter, the phase change material used being a mixture of hydrated inorganic salts and urea, the mixture being sprayed onto cellulose acetate rods or its crystals mixed into two It is placed between filters. As is known in the art, the use and effectiveness of these hydrated salts are not ideal.
중국 특허 CN101396173호는 궐련을 위한 와류 냉각 및 풍미 유지 방법과 궐련 구조를 제공한다. 와류 채널들은 공기와 동일한 냉각 효과를 성취하기 위해 궐련 필터의 앞에서 형성되지만, 그 구조가 복잡하고 궐련형 전자담배에 적합하지 않다.Chinese patent CN101396173 provides a vortex cooling and flavor retention method for cigarettes and a cigarette structure. Vortex channels are formed in front of the cigarette filter to achieve the same cooling effect as air, but their structure is complex and is not suitable for cigarette-type electronic cigarettes.
필터를 통한 향미(perfuming) 처리는 일반적으로 향미 입자들, 향미 스레드들 또는 캡슐들의 형태이다. 예를 들어, 중국 특허 CN101390657호는 박하 지속 방출 기능을 갖는 궐련 필터 로드와 그것의 제조 프로세스를 개시한다. 향미 수단은 향미가 함침된 면사들(cotton threads)을 사용하는 것이지만, 연속적인 향미를 성취하는 것은 어렵다.Perfuming through filters is usually in the form of flavor particles, flavor threads or capsules. For example, Chinese patent CN101390657 discloses a cigarette filter rod with peppermint sustained release function and its manufacturing process. A flavoring means is to use cotton threads impregnated with flavor, but it is difficult to achieve continuous flavor.
본 발명에 의해 해결하고자 하는 기술적 과제는, 궐련들(전통적인 궐련들과 궐련형 전자담배들을 포함함)이 흡연될 때, 연소에 의해 발생된 연기의 온도는 비교적 높아, 소비자들의 입에서의 작열감(burning sensation)이 흡연 경험에 영향을 미치게 한다는 것이다.The technical problem to be solved by the present invention is that when cigarettes (including traditional cigarettes and cigarette-type electronic cigarettes) are smoked, the temperature of the smoke generated by combustion is relatively high, causing a burning sensation in the mouth of consumers ( The burning sensation affects the smoking experience.
위의 기술적 과제를 해결하기 위하여, 본 발명의 기술적 해법은 다음과 같다:In order to solve the above technical problems, the technical solution of the present invention is as follows:
냉각 필터 로드가 냉각 입자들에 의해 주로 형성되며; 냉각 입자는 입자 바디와 입자 바디 상에 코팅된 쉘을 포함하고, 쉘/또는 입자 바디는 상 변화 재료를 포함한다.The cooling filter rod is mainly formed by cooling particles; The cooling particle includes a particle body and a shell coated on the particle body, and the shell/or particle body includes a phase change material.
이런 식으로, 사용되는 냉각 입자들은 코어-쉘 구조를 가지고, 표면 쉘들에는 냉각 기능을 갖는 상 변화 재료가 분산된다. 냉각 필터 로드는 요구된 형상에 따라 냉각 입자들의 성형(molding)에 의해 획득될 수 있으며; 냉각 입자들이 특정한 형상으로 적층된 후, 형성된 전체 냉각 필터 로드는 느슨하고 다공성 구조를 가지며; 냉각 필터 로드가 궐련 제품에 적용되고 고온 연기가 냉각 필터 로드를 통과할 때, 그 연기는 원활하게 통과할 수 있고; 한편, 고온 연기는 쉘들과의 큰 접촉 면적을 가지며, 그래서 냉각 효율은 높으며, 양호한 냉각 효과가 성취될 수 있고, 흡연자의 경험은 개선된다.In this way, the cooling particles used have a core-shell structure, and in the surface shells a phase change material with a cooling function is dispersed. The cooling filter rod can be obtained by molding the cooling particles according to the required shape; After the cooling particles are stacked into a specific shape, the entire cooling filter rod formed has a loose and porous structure; When the cooling filter rod is applied to the cigarette product and the high temperature smoke passes through the cooling filter rod, the smoke can pass smoothly; Meanwhile, the high temperature smoke has a large contact area with the shells, so the cooling efficiency is high, a good cooling effect can be achieved, and the smoker's experience is improved.
임의적으로, 쉘만이 상 변화 재료를 포함하며; 임의적으로, 입자 바디만이 상 변화 재료를 포함하며; 임의적으로, 쉘 및 입자 바디 둘 다가 상 변화 재료를 포함한다.Optionally, only the shell contains the phase change material; Optionally, only the particle body contains phase change material; Optionally, both the shell and particle body comprise a phase change material.
본 발명의 일부 실시예들에서, 쉘은 상 변화 재료로 이루어진다.In some embodiments of the invention, the shell is made of a phase change material.
게다가, 상 변화 재료는 PLA, 폴리에틸렌 글리콜, 스테아르 산, 팔미트 산, 파라핀, 미세결정질 왁스, EVA, 펜타에리트리톨, 스테아레이트-이소프로판올 에스테르, 및 스테아레이트-글리세롤 에스테르 중 적어도 하나를 포함한다. 적합한 상 변화 재료는 양호한 냉각 효과를 보장면서도 코팅 효과를 보장할 수 있음으로써, 냉각 필터 로드의 전체 냉각 성능을 개선시킨다. 바람직하게는, 상 변화 재료는 PLA, 폴리에틸렌 글리콜, 스테아레이트들(시리즈 스테아레이트들을 포함함) 및 EVA의 혼합물을 포함한다.Additionally, the phase change material includes at least one of PLA, polyethylene glycol, stearic acid, palmitic acid, paraffin, microcrystalline wax, EVA, pentaerythritol, stearate-isopropanol ester, and stearate-glycerol ester. A suitable phase change material can ensure good cooling effect and coating effect, thereby improving the overall cooling performance of the cooling filter rod. Preferably, the phase change material comprises a mixture of PLA, polyethylene glycol, stearates (including series stearates) and EVA.
본 발명의 일부 실시예들에서, 쉘은 게다가 풍미 증강제를 포함한다. 이런 식으로, 냉각 입자의 쉘은 상 변화 재료와 풍미 증강제를 포함하고, 냉각 입자들이 특정한 형상으로 적층된 후, 형성된 전체 냉각 필터 로드는 느슨하고 다공성 구조를 가지고, 그 연기는 원활하게 통과할 수 있으며; 덧붙여서, 냉각 필터 로드가 궐련 제품에 적용되고 고온 연기가 냉각 필터 로드를 통과할 때, 고온 연기는 쉘들과의 큰 접촉 면적을 가지고, 상 변화 재료는 연기의 열에 대한 높은 흡수 효율을 가지며, 그래서 냉각 효율은 높으며, 양호한 냉각 효과가 성취되고, 흡연자의 경험이 개선되며; 한편, 쉘들에서의 풍미 증강제는 풍미를 느리게 방출하도록 가열되고, 풍미는 연기와 함께 흡연자의 입에 들어가 연기에 개별 흡연 요구들을 충족시킬 수 있는 독특한 맛을 제공하고; 상 변화 재료가 열을 흡수함으로써 상 변화를 받을 때, 쉘 내부의 풍미 성분들은 서서히 방출되어 풍미를 지속적으로 첨가할 수 있다. 일반적으로, 풍미를 생성하기 위한 풍미 증강제의 휘발은 또한 열 흡수 프로세스이고 연기 온도의 감소에 또한 유익하다.In some embodiments of the invention, the shell further includes a flavor enhancer. In this way, the shell of the cooling particles contains the phase change material and the flavor enhancer, and after the cooling particles are laminated into a specific shape, the entire cooling filter rod formed has a loose and porous structure, and the smoke can pass through smoothly. There is; In addition, when the cooling filter rod is applied to the cigarette product and the high temperature smoke passes through the cooling filter rod, the high temperature smoke has a large contact area with the shells, and the phase change material has a high absorption efficiency for the heat of the smoke, so that the cooling The efficiency is high, a good cooling effect is achieved, and the smoker's experience is improved; Meanwhile, the flavor enhancer in the shells is heated to release the flavor slowly, and the flavor enters the smoker's mouth with the smoke, giving the smoke a unique taste that can meet individual smoking needs; When the phase change material undergoes a phase change by absorbing heat, the flavor components inside the shell are slowly released, allowing flavor to be continuously added. In general, volatilization of flavor enhancers to produce flavor is also a heat absorbing process and is also beneficial for reducing smoke temperature.
게다가, 풍미 증강제는 풍미 및/또는 담배 추출물을 포함하며; 바람직하게는, 상 변화 재료 대 풍미 증강제의 질량비는 100 : (0.5-10)이다. 임의적으로, 풍미는 요구된 대로 구체적으로 선택될 수 있는 멘톤과 커피 풍미 중 적어도 하나를 포함하고, 다른 유형들의 풍미들이 요구된 대로 또한 선택될 수 있다.Additionally, flavor enhancers include flavors and/or tobacco extracts; Preferably, the mass ratio of phase change material to flavor enhancer is 100:(0.5-10). Optionally, the flavor comprises at least one of menthone and coffee flavors, which may be specifically selected as required, and other types of flavors may also be selected as required.
게다가, 쉘의 질량은 냉각 입자의 총 질량의 0.5-30%, 바람직하게는 1-20%를 차지한다. 적절한 양의 상 변화 재료는 냉각 효과가 요건들을 충족시키는 것을 보장할 수 있고, 필터 로드의 채널들은 상 변화가 흡연 프로세스에서 반복될 때 차단되지 않을 것이다.Furthermore, the mass of the shell accounts for 0.5-30%, preferably 1-20%, of the total mass of the cooling particles. An appropriate amount of phase change material can ensure that the cooling effect meets the requirements, and the channels of the filter rod will not be blocked when the phase change is repeated in the smoking process.
본 발명의 일부 실시예들에서, 입자 바디는 식물 섬유 분말 및/또는 무기 재료 분말을 포함하고, 게다가, 식물 섬유 분말 및/또는 무기 재료 분말은 80-200 메시, 바람직하게는 100-180 메시의 입자 사이즈를 갖는다.In some embodiments of the invention, the particle body comprises plant fiber powder and/or inorganic material powder, furthermore the plant fiber powder and/or inorganic material powder has a mesh of 80-200 mesh, preferably 100-180 mesh. It has particle size.
게다가, 식물 섬유 분말은 담배 분말, 옥수숫대 분말, 왕겨 분말, 호두 껍질 분말, 코코넛 껍질 분말, 감귤 껍질 분말, 및 자몽 껍질 분말 중 적어도 하나를 포함한다. 식물 분말은 천연, 무공해이고 저렴하며, 흡착 효율을 줄이기 위해 밀한 입자들로 준비될 수 있으며, 저온 궐련들에 더 적합하고, 냉각 필터 로드 및 궐련들의 준비 동안 커터들의 손실을 감소시킬 수 있다. 게다가, 무기 재료 분말은 탄산 칼슘, 탄소 분말, 세라믹들, 실리카 겔, 및 분자체들 중 적어도 하나를 포함한다. 무기 재료들의 사용은 독특한 냄새를 도입하지 않고, 동시에, 다공성 성질이 부분적으로 이용되어서, 냉각 필터 로드는 더 나은 흡착 성능을 갖고 일반 궐련들에 더 적합하다. 게다가, 입자 바디는 보조 성형 재료를 더 포함하고, 보조 성형 재료는 결합제, 습윤제, 및 부형제 중 적어도 하나를 포함한다.Additionally, the plant fiber powder includes at least one of tobacco powder, corncob powder, rice husk powder, walnut shell powder, coconut shell powder, citrus peel powder, and grapefruit peel powder. Plant powder is natural, pollution-free and inexpensive, can be prepared with dense particles to reduce adsorption efficiency, is more suitable for low-temperature cigarettes, and can reduce the loss of cutters during cooling filter loading and preparation of cigarettes. Additionally, the inorganic material powder includes at least one of calcium carbonate, carbon powder, ceramics, silica gel, and molecular sieves. The use of inorganic materials does not introduce peculiar odor, and at the same time, the porous nature is partially exploited, so the cooling filter rod has better adsorption performance and is more suitable for ordinary cigarettes. In addition, the particle body further includes an auxiliary molding material, and the auxiliary molding material includes at least one of a binder, a wetting agent, and an excipient.
게다가, 결합제는 PVP, HPC, HPMC, SCMC, 및 변성 전분 중 적어도 하나를 포함하며; 습윤제는 물 또는 알코올을 포함하고; 부형제는 미세결정질 셀룰로스 및 락토스를 포함한다. 적합한 결합제 및 습윤제는 준비된 입자들이 양호한 형상 및 강도를 갖는 것을 보장할 수 있다.Additionally, the binder includes at least one of PVP, HPC, HPMC, SCMC, and modified starch; Humectants include water or alcohol; Excipients include microcrystalline cellulose and lactose. Suitable binders and wetting agents can ensure that the prepared particles have good shape and strength.
식물 섬유 분말 및 무기 재료 분말의 비율을 합리적으로 조정함으로써, 냉각 필터 로드의 흡착 성능은 적절한 범위로 조정될 수 있고, 상이한 궐련들의 필요도 또한 충족될 수 있다.By reasonably adjusting the ratio of plant fiber powder and inorganic material powder, the adsorption performance of the cooling filter rod can be adjusted to an appropriate range, and the needs of different cigarettes can also be met.
본 발명의 일부 실시예들에서, 입자 바디는 베이스 분말, 핫 멜트 접착제 분말, 부형제들, 및 물을 완전히 혼합하며, 과립화하며, 건조, 및 체질(sieving)함으로써 획득되며; 베이스 분말은 식물 재료들, 무기 재료들, 및 금속 분말 중 적어도 하나를 포함하며; 게다가, 식물 재료들은 담배 원료들, 짚, 땅콩 껍질들, 버개스, 옥수숫대들, 과피, 및 방향성 식물들 중 적어도 하나를 포함하며; 무기 재료들은 탄소 분말, 점토, 탄산 칼슘, 및 실리콘 산화물 중 적어도 하나를 포함하고; 금속 분말은 철 분말, 알루미늄 산화물, 및 구리 분말 중 적어도 하나를 포함한다. 일반적으로, 베이스 분말, 핫 멜트 접착제 분말, 부형제들, 및 물의 비율은 그것들이 정상적이고 고루 잘 섞인 입상화 및 형성을 위해 사용될 수 있는 한 필요에 따라 선택될 수 있다. 식물 재료들의 사용은 가능한 한 비용을 줄일 수 있고, 방향성 식물들은 또한 필터 로드에서 풍미 효과를 갖는다. 무기 재료들 및 금속 분말은 독특한 냄새가 나지 않을 것이고, 금속 분말은 냉각 효과에 더 많이 도움이 된다. 게다가, 방향성 식물들은 백단향, 침향나무, 정향들, 커피, 및 아니스(anise) 중 적어도 하나를 포함한다.In some embodiments of the invention, the particle body is obtained by thoroughly mixing the base powder, hot melt adhesive powder, excipients, and water, granulating, drying, and sieving; The base powder includes at least one of plant materials, inorganic materials, and metal powder; Additionally, the plant materials include at least one of tobacco raw materials, straw, peanut shells, bagasse, corn cobs, pericarp, and aromatic plants; The inorganic materials include at least one of carbon powder, clay, calcium carbonate, and silicon oxide; The metal powder includes at least one of iron powder, aluminum oxide, and copper powder. In general, the proportions of base powder, hot melt adhesive powder, excipients, and water can be selected as needed as long as they can be used for normal and well-mixed granulation and formation. The use of plant materials can reduce costs as much as possible, and aromatic plants also have a flavor effect in the filter rod. Inorganic materials and metal powders will not have a characteristic odor, and metal powders are more conducive to the cooling effect. Additionally, aromatic plants include at least one of sandalwood, agarwood, cloves, coffee, and anise.
게다가, 핫 멜트 접착제 분말은 EVA, TPU, PE, PA, 및 PES 중 적어도 하나를 포함한다. 핫 멜트 접착제 분말은 입자들의 형성과 입자 로드들의 형성을 보장할 수 있다. 한편, 핫 멜트 접착제 분말은 특정한 상 변화 능력을 가지며, 그래서 상 변화 냉각 효과를 어느 정도 성취할 수 있다. 냉각 입자들에서의 핫 멜트 접착제 분말의 질량비는 5%-50%, 바람직하게는 10%-40%이고, 다른 성분들의 함량은 요구된 대로 조정될 수 있다. 적절한 양의 핫 멜트 접착제는 충분한 접착을 보장할 수 있고, 과도한 양은 용융 중에 채널들을 차단하여 냉각 효과에 영향을 미칠 수 있다.Additionally, the hot melt adhesive powder includes at least one of EVA, TPU, PE, PA, and PES. The hot melt adhesive powder can ensure the formation of particles and the formation of particle rods. Meanwhile, hot melt adhesive powder has a certain phase change ability, so it can achieve a certain degree of phase change cooling effect. The mass ratio of hot melt adhesive powder to cooling particles is 5%-50%, preferably 10%-40%, and the contents of other components can be adjusted as required. An appropriate amount of hot melt adhesive can ensure sufficient adhesion, while an excessive amount may block channels during melting and affect the cooling effect.
임의적으로, 부형제들은 미세결정질 셀룰로스와 사전 젤라틴화된 전분을 포함한다. 게다가, 냉각 입자들은 10-50 메시, 바람직하게는 20-35 메시의 직경을 갖는다.Optionally, excipients include microcrystalline cellulose and pregelatinized starch. Furthermore, the cooling particles have a diameter of 10-50 mesh, preferably 20-35 mesh.
게다가, 궐련형 전자담배들을 냉각하는데 사용될 때, 냉각 입자들은 압출 라운딩에 의해 과립화되며, 구형 또는 대략 구형의 입자들이고, 0.8 내지 2.5 g/ml의 벌크 밀도를 갖는다. 구형 또는 대략 구형 형상은 냉각 필터 로드 내부에 충분히 복잡하고 연속적인 연기 채널들을 보장할 수 있고, 충분히 높은 입자 밀도는 흡착 성능이 궐련에 의해 생성된 연기의 양에 영향을 미치는 일 없이 최소화되는 것을 보장한다.Moreover, when used to cool cigarette-type electronic cigarettes, the cooling particles are granulated by extrusion rounding, are spherical or approximately spherical particles, and have a bulk density of 0.8 to 2.5 g/ml. A spherical or approximately spherical shape can ensure sufficiently complex and continuous smoke channels inside the cooling filter rod, and a sufficiently high particle density ensures that adsorption performance is minimized without affecting the amount of smoke produced by the cigarette. do.
게다가, 기존의 궐련들을 냉각시키는데 사용될 때, 냉각 입자들은 구형 또는 무정형이고, 0.4 내지 1.6 g/ml의 벌크 밀도를 갖는다. 이는 냉각 필터 로드 내부에 충분히 복잡하고 연속적인 연기 채널들을 보장할 수 있고, 낮은 입자 밀도는 입자들의 내부 기공들이 완전히 차단되지 않는 것을 보장할 수 있어서, 입자들은 특정한 흡착 성능을 여전히 갖는다. 바람직하게는, 냉각 입자들의 수분 함량은 5-15 wt%이고, 추가로 7-12 wt%이다. 수분 함량을 적절한 수분 함량 범위로 유지하면 흡연 중에 궐련을 양호한 입맛(mouthfeel)으로 유지할 수 있고, 식물 섬유 분말을 포함하는 냉각 필터 로드에 곰팡이(mildew)를 방지할 수 있다.Additionally, when used to cool conventional cigarettes, the cooling particles are spherical or amorphous and have a bulk density of 0.4 to 1.6 g/ml. This can ensure sufficiently complex and continuous smoke channels inside the cooling filter rod, and the low particle density can ensure that the internal pores of the particles are not completely blocked, so that the particles still have a certain adsorption performance. Preferably, the moisture content of the cooling particles is 5-15 wt%, further 7-12 wt%. Maintaining the moisture content in an appropriate moisture content range can maintain the cigarette with good mouthfeel during smoking and prevent mildew on the cooling filter rod containing plant fiber powder.
적절한 직경들의 입자들은 필터 로드 내부의 충분한 공기 투과성을 보장할 수 있고, 적절한 수분은 저장 및 성형 제어를 용이하게 한다.Particles of appropriate diameters can ensure sufficient air permeability inside the filter rod, and appropriate moisture facilitates storage and shaping control.
게다가, 냉각 필터 로드 내부의 유효 다공도는 65-95%이다. 이런 식으로, 전체 냉각 필터 로드는 복잡하고 연속적인 채널들이 내부에 형성된 다공성 구조를 갖고; 고온 연기가 냉각 필터 로드의 하나의 말단에서부터 냉각 필터 로드에 들어간 후, 고온 연기는 냉각 필터 로드의 기공들 안으로 빠르게 분산되고 냉각 입자들에 충분히 접촉하여 열을 교환하며, 따라서 냉각을 실현하며; 덧붙여서, 고온 연기는 냉각 필터 로드에서 긴 이동 거리를 가지며, 그래서 성취된 냉각 효과는 양호하다. 충분한 유효 다공도는 필터 로드 내부의 공기 투과성 요구를 충족시킬 수 있다.Moreover, the effective porosity inside the cooling filter rod is 65-95%. In this way, the entire cooling filter rod has a porous structure with complex, continuous channels formed inside; After the high-temperature smoke enters the cooling filter rod from one end of the cooling filter rod, the high-temperature smoke quickly disperses into the pores of the cooling filter rod and sufficiently contacts the cooling particles to exchange heat, thereby realizing cooling; In addition, the high temperature smoke has a long travel distance in the cooling filter rod, so the achieved cooling effect is good. Sufficient effective porosity can meet the air permeability requirements inside the filter rod.
게다가, 냉각 필터 로드 내의 유효 다공도는 80-95%이다.Additionally, the effective porosity within the cooling filter rod is 80-95%.
게다가, 다공성 구조는 벌집 모양이다.Moreover, the porous structure is honeycomb-shaped.
임의적으로, 냉각 필터 로드는 느슨하고 공기 투과 가능한 실린더이다.Optionally, the cooling filter rod is a loose, air-permeable cylinder.
게다가, 냉각 필터 로드는 결합제를 통해 냉각 입자들의 결속에 의해 형성된다.Additionally, the cooling filter rod is formed by binding cooling particles through a binder.
게다가, 냉각 필터 로드는 마이크로파 가열 또는 열 응고의 방식을 통해 냉각 입자들에 의해 주로 형성된다.Moreover, the cooled filter rod is mainly formed by cooled particles through the method of microwave heating or thermal coagulation.
게다가, 냉각 필터 로드는 절초(cut tobacco) 섹션 또는 흡연을 위한 흡연 섹션에 연결되는데, 냉각 필터 로드는 절초/흡연 섹션에 가깝다. 임의적으로, 냉각 필터 로드의 준비 방법이 다음의 단계들을 포함한다:Furthermore, the cooling filter rod is connected to a cut tobacco section or a smoking section for smoking, where the cooling filter rod is close to the cutting/smoking section. Optionally, the method of preparing the cooling filter rod includes the following steps:
(1) 식물 섬유 분말 및/또는 무기 재료 분말을 관련 보조 성형 재료들과 혼합하며, 과립화하며, 건조하고, 체질(screening)하여 입자 바디들을 획득하며; 그 다음에 냉각 입자들을 획득하기 위해 상 변화 재료로 입자 바디들을 코팅하는 단계; 및(1) Mixing plant fiber powder and/or inorganic material powder with relevant auxiliary molding materials, granulating, drying and screening to obtain particle bodies; then coating the particle bodies with a phase change material to obtain cooled particles; and
(2) 냉각 필터 로드를 획득하기 위해 단계 (1)에서 획득된 냉각 입자들을 성형하는 단계; 또는(2) shaping the cooling particles obtained in step (1) to obtain a cooling filter rod; or
1) 식물 재료들/무기 재료들/금속 분말, 핫 멜트 접착제 분말, 미세결정질 셀룰로스, 사전 젤라틴화된 전분, 물 등 중 적어도 하나를 완전히 혼합하며, 과립화하며, 건조, 체질하여 입자 바디들을 획득하며; 그 다음에 적절한 직경들의 냉각 입자들을 획득하기 위해 상 변화 재료로 입자 바디들을 코팅하는 단계; 및1) Thoroughly mix at least one of plant materials/inorganic materials/metal powder, hot melt adhesive powder, microcrystalline cellulose, pregelatinized starch, water, etc., granulate, dry, and sieve to obtain particle bodies. and; then coating the particle bodies with a phase change material to obtain cooling particles of appropriate diameters; and
2) 획득된 냉각 입자들을 일정한 사이즈를 갖는 실린더, 다시 말하면, 요구된 냉각 필터 로드로 성형하는 단계.2) Forming the obtained cooling particles into a cylinder with a certain size, that is, into the required cooling filter rod.
또는, 1) 식물 섬유 분말 및/또는 무기 재료 분말을 관련 보조 성형 재료들과 혼합하며, 과립화하며, 건조, 및 선별하여 베이스 입자들을 획득하는 단계;Alternatively, 1) mixing plant fiber powder and/or inorganic material powder with relevant auxiliary molding materials, granulating, drying, and screening to obtain base particles;
2) 상 변화 재료를 가열하여 녹이며, 적절한 양의 풍미 증강제를 칭량(weighing)하여 용융된 상 변화 재료에 첨가하며, 철저하고 균일한 혼합을 위해 고속으로 교반 및 전단하여 나중의 사용을 위한 혼합된 액체를 획득하는 단계;2) Heat and melt the phase change material, weigh and add an appropriate amount of flavor enhancer to the molten phase change material, and stir and shear at high speed for thorough and uniform mixing to form a mixed product for later use. Obtaining a liquid;
3) 단계 2)에서 준비된 혼합된 액체를 코팅 재료로 하여 단계 1)에서 준비된 베이스 입자들을 코팅하여 냉각 입자들을 획득하는 단계; 및3) obtaining cooling particles by coating the base particles prepared in step 1) using the mixed liquid prepared in step 2) as a coating material; and
4) 단계 3)에서 준비된 냉각 입자들을 일정한 사이즈의 실린더로 성형하여 풍미 향상된 냉각 필터 로드를 획득하는 단계.4) Obtaining a cooling filter rod with improved flavor by molding the cooling particles prepared in step 3) into a cylinder of a certain size.
동일한 발명적 개념에 기초하여, 본 발명은 궐련의 생산에서 전술한 냉각 필터 로드의 적용을 추가로 제공한다. 동일한 발명적 개념에 기초하여, 본 발명은 전술한 냉각 필터 로드를 포함하는 궐련을 추가로 제공한다.Based on the same inventive concept, the invention further provides for the application of the above-described cooling filter rod in the production of cigarettes. Based on the same inventive concept, the present invention further provides a cigarette comprising the above-described cooling filter rod.
게다가, 궐련이 순차적으로 연결된 흡연 부분 및 필터를 포함하는데, 전술한 냉각 필터 로드는 필터 내부에 배열된다.Furthermore, the cigarette includes a sequentially connected smoking portion and a filter, wherein the aforementioned cooling filter rod is arranged inside the filter.
임의적으로, 냉각 필터 로드는 기존의 궐련들 또는 궐련형 전자담배들을 위한 필터로서 특정한 비율로 기존의 필터 로드들과 조합(compound)되며, 예를 들어, 냉각 필터 로드는 궐련 필터 부분(필터)을 구성하기 위해 두 개의 기존의 필터 로드들 사이에 배열되고, 모든 고온 연기는 냉각 효과를 보장하기 위해 입에 들어가기 전에 냉각 필터 로드를 통과할 필요가 있다. 상이한 기존의 필터 로드들은 상이한 사용 요건들에 따라 선택된다.Optionally, the cooled filter rod is compounded with existing filter rods in a certain ratio as a filter for conventional cigarettes or cigarette-type electronic cigarettes, for example, the cooled filter rod can be used to form a cigarette filter portion (filter). To configure it, it is arranged between two conventional filter rods, and all hot smoke needs to pass through the cooling filter rod before entering the mouth to ensure the cooling effect. Different existing filter rods are selected according to different usage requirements.
게다가, 기존의 필터 로드들은 아세테이트 필터 로드들, 폴리프로필렌 섬유 필터 로드들, 종이 필터 로드들, 빈 튜브 로드들 등이다.Additionally, existing filter rods include acetate filter rods, polypropylene fiber filter rods, paper filter rods, empty tube rods, etc.
종래 기술과 비교하면, 본 발명의 기술적 해법이 가져다주는 기술적 효과는 다음과 같다:Compared with the prior art, the technical effects brought by the technical solution of the present invention are as follows:
(1) 상 변화 재료는 입자 재료의 표면에 코팅되어 냉각 입자들을 형성하고, 냉각 입자들은 냉각 필터 로드로 일체로 형성되며, 이는 기존의 필터 로드들과 조합된 후 궐련 생산에 직접 사용될 수 있다.(1) The phase change material is coated on the surface of the particle material to form cooling particles, and the cooling particles are integrally formed into a cooling filter rod, which can be directly used in cigarette production after being combined with existing filter rods.
(2) 냉각 효과는 상 변화 재료 및 냉각 필터 로드의 양에 따라 제어될 수 있다. 냉각 필터 로드의 형태는 단순하고 신규하고, 아주 새로운 필터 로드는 산업 생산을 용이하게 하고 낮은 비용과 양호한 냉각 효과를 갖는다.(2) The cooling effect can be controlled according to the amount of phase change material and cooling filter load. The shape of the cooling filter rod is simple and novel, and the brand-new filter rod facilitates industrial production and has low cost and good cooling effect.
(3) 흡연 저항은 작고, 연기와 상 변화 재료 사이의 접촉 면적은 크고, 그래서 냉각 효율은 높으며, 흡연자의 입에 들어가는 연기의 온도는 크게 감소될 수 있고, 경험은 개선된다.(3) The smoking resistance is small, the contact area between the smoke and the phase change material is large, so the cooling efficiency is high, the temperature of the smoke entering the smoker's mouth can be greatly reduced, and the experience is improved.
(4) 풍미 증강제는 상 변화 재료와 조합되어서, 냉각 필터 로드는 처음으로 풍미 기능을 실현하고, 그것의 적용 값은 크게 증가한다.(4) The flavor enhancer is combined with the phase change material, so that the cooling filter rod realizes the flavor function for the first time, and its application value is greatly increased.
(5) 입에 들어가는 연기의 온도는 냉각 필터 로드의 유효 다공도를 제어하고 물리적 냉각의 원리에 기초한 환기 또는 희석이 없는 수단을 사용함으로써 크게 감소되고, 냉각 진폭은 50%를 초과하여 도달할 수 있다.(5) The temperature of the smoke entering the mouth is greatly reduced by controlling the effective porosity of the cooling filter rod and using means without ventilation or dilution based on the principle of physical cooling, and the cooling amplitude can reach more than 50%. .
다음의 예들은 본 발명의 보호 범위를 추가로 제한하기 보다는, 본 발명의 내용을 예시하도록 의도된다.The following examples are intended to illustrate the content of the present invention, rather than further limit the protection scope of the present invention.
실시예 1Example 1
이 실시예에서, 테스트 프로세스는 다음의 단계들을 포함하였다:In this example, the testing process included the following steps:
1) 100-150 메시 담배 원료 분말의 100 질량부, 변성 전분의 20 질량부 및 미세결정질 셀룰로스의 30 질량부가 취해지고, 균일하게 혼합된 다음 물의 30 질량부로 분무되며, 뒤이어서 균일하게 혼합되어 혼합된 연질 재료가 준비되었으며; 2) 연질 재료는 압출 라운딩에 의해 과립화되며, 건조 및 체질되었고, 20-50 메시 담배 입자들이 나중의 사용을 위해 취해졌으며; 3) 획득된 담배 입자들에는 용융된 PEG1500이 담배 입자들의 질량의 10%의 양으로 코팅되었으며, 뒤이어서 체질되었고, 20-40 메시 담배 입자들이 냉각 담배 입자들로서 취해졌으며; 4) 획득된 냉각 담배 입자들은 둘레 23.5 mm의 느슨하고 다공성 실린더에 마이크로파로 연속적으로 성형되었고, 실린더는 120 mm 길이의 냉각 필터 로드들로 절단되었고; 5) 냉각 필터 로드들은 궐련들을 준비하기 위해 10 : 15의 길이 비율로 아세테이트 섬유 섹션들과 조합되었는데, 냉각 섹션들은 절초에 가깝고, 아세테이트 섬유 로드들은 대조물(control)과 동일한 사양의 궐련들로 또한 준비되었다. 두 종류의 필터 로드 궐련들은 흡연되었으며, 필터 로드들의 출구 단부들에서의 온도들은 다섯 번째 흡연 시에 테스트되었고, 그 결과들은 표 1에 도시된다.1) 100 parts by mass of 100-150 mesh tobacco raw material powder, 20 parts by mass of modified starch and 30 parts by mass of microcrystalline cellulose are taken, mixed uniformly and then sprayed with 30 parts by mass of water, then mixed and mixed evenly. The soft material was prepared; 2) The soft material was granulated by extrusion rounding, dried and sieved, and 20-50 mesh tobacco particles were taken for later use; 3) The obtained tobacco particles were coated with molten PEG1500 in an amount of 10% of the mass of the tobacco particles, followed by sieving, and 20-40 mesh tobacco particles were taken as cooled tobacco particles; 4) The obtained cooled tobacco particles were continuously molded by microwave into loose, porous cylinders with a circumference of 23.5 mm, and the cylinders were cut into 120 mm long cooled filter rods; 5) Cooling filter rods were combined with acetate fiber sections in a length ratio of 10:15 to prepare cigarettes, where the cooling sections were close to each other and the acetate fiber rods were also used to prepare cigarettes with the same specifications as the control. Ready. Two types of filter rod cigarettes were smoked and the temperatures at the outlet ends of the filter rods were tested on the fifth smoke, and the results are shown in Table 1.
실시예 2Example 2
이 실시예에서, 테스트 프로세스는 다음의 단계들을 포함하였다:In this example, the testing process included the following steps:
1) 100-150 메시 옥수숫대 가루의 80 질량부, 탄산 칼슘의 20 질량부, HPMC의 10 질량부 및 미세결정질 셀룰로스의 40 질량부가 취해지고, 균일하게 혼합된 다음 물의 25 질량부로 분무되며, 뒤이어서 균일하게 혼합되어 혼합된 연질 재료가 준비되었으며; 2) 연질 재료는 압출 라운딩에 의해 과립화되며, 건조 및 체질되었고, 20-50 메시 옥수숫대 입자들이 나중의 사용을 위해 취해졌으며; 3) 1 : 1의 질량비의 스테아르 산 및 펜타에리트리톨이 용융되어 옥수숫대 입자들의 질량의 5%의 양으로 획득된 옥수숫대 입자들을 코팅하였으며, 뒤이어서 체질되었고, 10-50 메시 옥수숫대 입자들이 냉각 옥수숫대 입자들로서 취해졌으며; 4) 획득된 냉각 옥수숫대 입자들은 열 경화에 의해 둘레 23.5 mm의 느슨하고 다공성 실린더로 연속적으로 성형되었고, 실린더는 84 mm 길이의 냉각 필터 로드들로 절단되었고; 5) 냉각 필터 로드들은 궐련들을 준비하기 위해 7 : 18의 길이 비율로 아세테이트 섬유 섹션들과 조합되었는데, 냉각 섹션들은 절초에 가깝고, 아세테이트 섬유 로드들은 대조물과 동일한 사양의 궐련들로 또한 준비되었다. 두 종류의 필터 로드 궐련들은 흡연되었으며, 필터 로드들의 출구 단부들에서의 온도들은 다섯 번째 흡연 시에 테스트되었고, 그 결과들은 표 1에 도시된다.1) 80 parts by mass of 100-150 mesh corncob meal, 20 parts by mass of calcium carbonate, 10 parts by mass of HPMC and 40 parts by mass of microcrystalline cellulose are taken, mixed uniformly and then sprayed with 25 parts by mass of water, followed by uniform mixing. A soft material was prepared by mixing and mixing; 2) The soft material was granulated by extrusion rounding, dried and sieved, and 20-50 mesh corncob particles were taken for later use; 3) Stearic acid and pentaerythritol in a mass ratio of 1:1 were melted to coat the obtained corncob particles in an amount of 5% of the mass of the corncob particles, followed by sieving, and 10-50 mesh corncob particles were cooled as cooled corncob particles. taken; 4) The obtained cooled corncob particles were continuously formed by heat setting into loose, porous cylinders with a circumference of 23.5 mm, and the cylinders were cut into 84 mm long cooled filter rods; 5) The cooling filter rods were combined with acetate fiber sections in a length ratio of 7:18 to prepare cigarettes, the cooling sections were close to the cut, and the acetate fiber rods were also prepared into cigarettes with the same specifications as the control. Two types of filter rod cigarettes were smoked and the temperatures at the outlet ends of the filter rods were tested on the fifth smoke, and the results are shown in Table 1.
실시예 3Example 3
이 실시예에서, 테스트 프로세스는 다음의 단계들을 포함하였다:In this example, the testing process included the following steps:
1) 100-150 메시 자몽 껍질 분말의 60 질량부, 탄소 분말의 40 질량부, 변성 전분의 20 질량부, 미세결정질 셀룰로스의 20 질량부 및 락토스의 10 질량부가 취해지고, 균일하게 혼합된 다음 물의 25 질량부로 분무되며, 뒤이어서 균일하게 혼합되어 혼합된 연질 재료가 준비되었으며; 2) 연질 재료는 압출 라운딩에 의해 과립화되며, 건조 및 체질되었고, 20-50 메시 입자들은 나중의 사용을 위해 취해졌고; 3) 1 : 1: 1의 질량비의 PEG3000, 팔미트 산 및 스테아레이트 이소프로판올 에스테르는 용융되어 입자들의 질량의 15%의 양으로 획득된 입자들을 코팅하였고, 20-40 메시 입자들은 냉각 입자들로 취해졌고; 4) 획득된 냉각 입자들은 둘레 23.5 mm의 느슨하고 다공성 실린더에 마이크로파로 연속적으로 성형되었고, 그 실린더는 120 mm 길이 냉각 필터 로드들로 절단되었고; 5) 냉각 필터 로드들은 저온 궐련들을 준비하기 위해 10: 15의 길이 비율로 종이의 빈 튜브 섹션들과 조합되었는데, 냉각 섹션들은 절초에 가깝고, 아세테이트 섬유 로드들은 대조물과 동일한 사양의 저온 궐련들로 또한 준비되었다. 두 종류의 필터 로드 궐련들은 흡연되었으며, 필터 로드들의 출구 단부들에서의 온도들은 다섯 번째 흡연 시에 테스트되었고, 그 결과들은 표 1에 도시되었다.1) 60 parts by mass of 100-150 mesh grapefruit peel powder, 40 parts by mass of carbon powder, 20 parts by mass of modified starch, 20 parts by mass of microcrystalline cellulose and 10 parts by mass of lactose are taken, mixed uniformly and then added to water. 25 mass parts were sprayed, followed by uniform mixing to prepare a mixed soft material; 2) The soft material was granulated by extrusion rounding, dried and sieved, and 20-50 mesh particles were taken for later use; 3) PEG3000, palmitic acid and stearate isopropanol ester in a mass ratio of 1:1:1 were melted and coated the obtained particles in an amount of 15% of the mass of the particles, and 20-40 mesh particles were taken as cooled particles. lost; 4) The obtained cooling particles were continuously molded by microwave into a loose, porous cylinder with a circumference of 23.5 mm, and the cylinder was cut into 120 mm long cooling filter rods; 5) Cooling filter rods were combined with hollow tube sections of paper in a length ratio of 10:15 to prepare low-temperature cigarettes, the cooling sections were close to the cut, and acetate fiber rods were used to prepare low-temperature cigarettes with the same specifications as the control. Also ready. Two types of filter rod cigarettes were smoked and the temperatures at the outlet ends of the filter rods were tested on the fifth smoke, and the results are shown in Table 1.
표 1 온도 테스트 결과들Table 1 Temperature test results
테스트들은 본 발명에 의해 제공된 냉각 필터 로드가 매우 명백한 냉각 효과를 가졌고, 전통적인 필터 로드 궐련들과 비교하여, 출구 온도는 50%를 초과하여 감소되었음을 보여주었다.Tests showed that the cooling filter rod provided by the present invention had a very obvious cooling effect and, compared to traditional filter rod cigarettes, the outlet temperature was reduced by more than 50%.
실시예 4Example 4
이 실시예에서, 테스트 프로세스는 다음의 단계들을 포함하였다:In this example, the testing process included the following steps:
1) 100-150 메시 담배 원료 분말의 100 질량부, 변성 전분의 20 질량부 및 미세결정질 셀룰로스의 30 질량부가 취해졌으며, 균일하게 혼합된 다음 물의 30 질량부로 분무되었으며, 뒤이어서 균일하게 혼합되어 혼합된 연질 재료가 준비되었고; 2) 혼합된 연질 재료는 압출 라운딩에 의해 과립화되며, 건조 및 체질되었고, 20-50 메시 냉각 입자 코어들이 나중의 사용을 위해 취해졌고; 3) PEG2000은 열로 용융되고 100 : 0.5의 질량비로 멘톤과 완전히 혼합되어 혼합된 액체가 획득되었고; 4) 획득된 냉각 입자 코어들은 냉각 입자들의 질량의 10%의 양으로 혼합된 액체와 코팅되며, 뒤이어서 체질되고, 멘톤을 포함하는 30-50 메시 냉각 입자들이 취해졌고; 5) 획득된 냉각 입자들은 둘레 23.5 mm의 느슨하고 다공성 실린더에 마이크로파로 연속적으로 성형되었고, 실린더는 120 mm 길이 냉각 필터 로드 섹션들로 절단되었고; 6) 냉각 필터 로드 섹션들은 궐련들을 준비하기 위해 10 : 15의 길이 비율로 아세테이트 섬유 섹션들과 조합되었는데, 냉각 섹션들은 절초에 가깝고, 아세테이트 섬유 로드들은 대조물과 동일한 사양의 궐련들로 또한 준비되었다. 두 종류의 필터 로드 궐련들은 흡연되었으며, 필터 로드들의 출구 단부들에서의 온도들은 다섯 번째 흡연 시에 테스트되었고, 온도 테스트 결과들은 표 2에 도시되었다. 동시에, 흡연된 두 종류의 궐련들은 평가되었고, 그 결과들은 표 3에 도시되었다.1) 100 parts by mass of 100-150 mesh tobacco raw material powder, 20 parts by mass of modified starch and 30 parts by mass of microcrystalline cellulose were taken, mixed uniformly and then sprayed with 30 parts by mass of water, followed by mixing and mixing evenly. The soft material was prepared; 2) The mixed soft material was granulated by extrusion rounding, dried and sieved, and 20-50 mesh cooled particle cores were taken for later use; 3) PEG2000 was melted by heat and thoroughly mixed with menthone at a mass ratio of 100:0.5 to obtain a mixed liquid; 4) The obtained cooling particle cores were coated with mixed liquid in an amount of 10% of the mass of the cooling particles, followed by sieving, and 30-50 mesh cooling particles containing menthone were taken; 5) The obtained cooled particles were continuously molded by microwave into a loose, porous cylinder with a circumference of 23.5 mm, and the cylinder was cut into 120 mm long cooled filter rod sections; 6) Cooling filter rod sections were combined with acetate fiber sections in a length ratio of 10:15 to prepare cigarettes, the cooling sections were close to the cut, and the acetate fiber rods were also prepared with cigarettes of the same specifications as the control. . Two types of filter rod cigarettes were smoked and the temperatures at the outlet ends of the filter rods were tested on the fifth smoke, and the temperature test results are shown in Table 2. At the same time, the two types of cigarettes smoked were evaluated, and the results are shown in Table 3.
실시예 5Example 5
이 실시예에서, 테스트 프로세스는 다음의 단계들을 포함하였다:In this example, the testing process included the following steps:
1) 100-150 메시 옥수숫대 가루의 80 질량부, 탄산 칼슘의 20 질량부, HPMC의 10 질량부 및 미세결정질 셀룰로스의 40 질량부가 취해지며, 균일하게 혼합되고 물의 25 질량부로 분무되었고, 뒤이어서 균일하게 혼합되어 혼합된 연질 재료가 준비되었고; 2) 혼합된 연질 재료는 압출 라운딩에 의해 과립화되며, 건조되고 체질되었고, 20-50 메시 냉각 입자 코어들이 나중의 사용을 위해 취해졌고; 3) 1 : 1의 질량비의 스테아르 산과 펜타에리트리톨이 가열에 의해 용융되고, 100 : 5의 질량비로 담배 추출물과 완전히 그리고 균일하게 혼합되어 혼합된 액체가 획득되었고; 4) 획득된 냉각 입자들은 냉각 입자들의 질량의 5%의 양으로 혼합된 액체로 코팅되었으며, 뒤이어서 체질되고, 담배 추출물을 포함하는 20-40 메시 풍미 향상된 냉각 입자들이 취해졌고; 5) 획득된 냉각 입자들은 열 경화에 의해 둘레 23.5 mm의 느슨하고 다공성 실린더로 연속적으로 성형되었고, 실린더는 84 mm 길이 냉각 필터 로드 섹션들로 절단되었고; 6) 냉각 필터 로드 섹션들은 궐련들을 준비하기 위해 7 : 18의 길이 비율로 아세테이트 섬유 섹션들과 조합되었는데, 냉각 섹션들은 절초에 가깝고, 아세테이트 섬유 로드들은 대조물과 동일한 사양의 궐련들로 또한 준비되었다. 두 종류의 필터 로드 궐련들은 흡연되었으며, 필터 로드들의 출구 단부들에서의 온도들은 다섯 번째 흡연 시에 테스트되었고, 그 결과들은 표 2에 도시되었다. 동시에, 흡연된 두 종류의 궐련들은 평가되었고, 그 결과들은 표 3에 도시되었다.1) 80 parts by mass of 100-150 mesh corncob meal, 20 parts by mass of calcium carbonate, 10 parts by mass of HPMC and 40 parts by mass of microcrystalline cellulose are taken, mixed uniformly and sprayed with 25 parts by mass of water, followed by uniformly mixing. A mixed soft material was prepared; 2) The mixed soft material was granulated by extrusion rounding, dried and sieved, and 20-50 mesh cooled particle cores were taken for later use; 3) Stearic acid and pentaerythritol at a mass ratio of 1:1 were melted by heating and mixed completely and uniformly with tobacco extract at a mass ratio of 100:5 to obtain a mixed liquid; 4) The obtained cooling particles were coated with mixed liquid in an amount of 5% of the mass of the cooling particles, followed by sieving, and 20-40 mesh flavor enhanced cooling particles containing tobacco extract were taken; 5) The obtained cooling particles were continuously molded into loose, porous cylinders with a circumference of 23.5 mm by heat setting, and the cylinders were cut into 84 mm long cooling filter rod sections; 6) Cooling filter rod sections were combined with acetate fiber sections in a length ratio of 7:18 to prepare cigarettes, the cooling sections were close to the cut, and the acetate fiber rods were also prepared with cigarettes of the same specifications as the control. . Two types of filter rod cigarettes were smoked and the temperatures at the outlet ends of the filter rods were tested on the fifth smoke, and the results are shown in Table 2. At the same time, the two types of cigarettes smoked were evaluated, and the results are shown in Table 3.
실시예 6Example 6
이 실시예에서, 테스트 프로세스는 다음의 단계들을 포함하였다:In this example, the testing process included the following steps:
1) 100-150 메시 자몽 껍질 분말의 60 질량부, 탄소 분말의 40 질량부, 변성 전분의 20 질량부, 미세결정질 셀룰로스의 20 질량부 및 락토스의 10 질량부가 취해지며, 균일하게 혼합된 다음 물의 25 질량부로 분무되었고, 뒤이어서 균일하게 혼합되어 혼합된 연질 재료가 준비되었고; 2) 혼합된 연질 재료는 압출 라운딩에 의해 과립화되며, 건조 및 체질되었고, 20-50 메시 냉각 입자 코어들이 나중의 사용을 위해 취해졌고; 3) 1 : 1 : 1의 질량비의 PEG3000, 팔미트 산 및 스테아레이트-이소프로판올 에스테르가 가열에 의해 용융되고, 100 : 2의 질량비로 커피 풍미와 완전히 그리고 균일하게 혼합되어 혼합된 액체가 획득되었고; 4) 획득된 냉각 입자 코어들은 냉각 입자들의 질량의 15%의 양으로 혼합된 액체로 코팅되며, 뒤이어서 체질되고, 20-40 메시 냉각 입자들이 취해졌고; 5) 획득된 냉각 입자들은 둘레 23.5 mm의 느슨하고 다공성 실린더에 마이크로파로 연속적으로 성형되었고, 실린더는 120 mm 길이 냉각 필터 로드 섹션들로 절단되었고; 6) 냉각 필터 로드 섹션들은 저온 궐련들을 준비하기 위해 10: 15의 길이 비율로 종이의 빈 튜브 섹션들과 조합되었는데, 냉각 섹션들은 절초에 가깝고, 아세테이트 섬유 로드들은 대조물과 동일한 사양의 저온 궐련들로 또한 준비되었다. 두 종류의 필터 로드 궐련들은 흡연되었으며, 필터 로드들의 출구 단부들에서의 온도들은 다섯 번째 흡연 시에 테스트되었고, 그 결과들은 표 2에 도시되었다. 동시에, 흡연된 두 종류의 궐련들은 평가되었고, 그 결과들은 표 3에 도시되었다.1) 60 parts by mass of 100-150 mesh grapefruit peel powder, 40 parts by mass of carbon powder, 20 parts by mass of modified starch, 20 parts by mass of microcrystalline cellulose and 10 parts by mass of lactose are taken, mixed uniformly and then added to water. 25 mass parts were sprayed, followed by uniform mixing to prepare a mixed soft material; 2) The mixed soft material was granulated by extrusion rounding, dried and sieved, and 20-50 mesh cooled particle cores were taken for later use; 3) PEG3000, palmitic acid and stearate-isopropanol ester in a mass ratio of 1:1:1 were melted by heating, and mixed completely and uniformly with coffee flavor in a mass ratio of 100:2 to obtain a mixed liquid; 4) The obtained cooling particle cores were coated with mixed liquid in an amount of 15% of the mass of cooling particles, followed by sieving, and 20-40 mesh cooling particles were taken; 5) The obtained cooled particles were continuously molded by microwave into a loose, porous cylinder with a circumference of 23.5 mm, and the cylinder was cut into 120 mm long cooled filter rod sections; 6) Cooling filter rod sections were combined with hollow tube sections of paper in a length ratio of 10:15 to prepare low temperature cigarettes, the cooling sections were close to the cutting edge, and acetate fiber rods were used to prepare low temperature cigarettes with the same specifications as the control. was also prepared. Two types of filter rod cigarettes were smoked and the temperatures at the outlet ends of the filter rods were tested on the fifth smoke, and the results are shown in Table 2. At the same time, the two types of cigarettes smoked were evaluated, and the results are shown in Table 3.
표 2 온도 테스트 결과들Table 2 Temperature test results
테스트들은 본 발명에 의해 제공된 냉각 필터 로드가 매우 명백한 냉각 효과를 가졌음을 보여주었다.Tests have shown that the cooling filter rod provided by the invention has a very pronounced cooling effect.
표 3 궐련 흡연 평가의 결과들Table 3 Results of cigarette smoking assessment
위의 실시예들에 의해 예시된 내용들은 이들 실시예들이 본 발명의 범위를 제한하는 것이 아니라, 본 발명을 더 명확하게 예시하기 위해서만 단순히 사용되어야 하는 것으로 이해되어야 한다. 본 발명을 읽은 후의 본 기술분야의 통상의 기술자들에 의해 본 발명에 대해 이루어진 다양한 동등한 수정들은 모두가 본 출원의 첨부의 청구항들에 의해 정의된 범위 내에 속한다.It should be understood that the content illustrated by the above embodiments does not limit the scope of the present invention, but should be used simply to more clearly illustrate the present invention. Various equivalent modifications made to the present invention by those skilled in the art after reading the present invention all fall within the scope defined by the appended claims of this application.
Claims (12)
상기 냉각 입자는 입자 바디와 상기 입자 바디 상에 코팅된 쉘을 포함하고, 상기 쉘은 상 변화 재료를 포함하고,
상기 상 변화 재료는 PLA, 폴리에틸렌 글리콜, 스테아르 산, 팔미트 산, 파라핀, 미세결정질 왁스, EVA, 펜타에리트리톨, 스테아레이트-이소프로판올 에스테르, 및 스테아레이트-글리세롤 에스테르 중 적어도 하나를 포함하는, 냉각 필터 로드.A cooling filter rod formed by cooling particles,
The cooling particle comprises a particle body and a shell coated on the particle body, the shell comprising a phase change material,
The phase change material includes at least one of PLA, polyethylene glycol, stearic acid, palmitic acid, paraffin, microcrystalline wax, EVA, pentaerythritol, stearate-isopropanol ester, and stearate-glycerol ester. road.
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CN201810486861.3A CN110506991B (en) | 2018-05-21 | 2018-05-21 | Cooling filter rod, application and cigarette |
CN201810486835.0A CN110506990A (en) | 2018-05-21 | 2018-05-21 | Flavored type cooling filter stick, application and cigarette |
CN201810486815.3 | 2018-05-21 | ||
CN201810486815.3A CN110506989A (en) | 2018-05-21 | 2018-05-21 | A kind of cooling filter stick, application and cigarette |
CN201810486861.3 | 2018-05-21 | ||
PCT/CN2019/078660 WO2019223412A1 (en) | 2018-05-21 | 2019-03-19 | Cooling filter rod, application and cigarette |
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CN114532588A (en) * | 2022-03-17 | 2022-05-27 | 湖北中烟工业有限责任公司 | Cigarette filter stick master batch and cigarette filter stick |
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