CN107594621A - A kind of fruity flavor composite particles and its preparation method and application - Google Patents
A kind of fruity flavor composite particles and its preparation method and application Download PDFInfo
- Publication number
- CN107594621A CN107594621A CN201710873672.7A CN201710873672A CN107594621A CN 107594621 A CN107594621 A CN 107594621A CN 201710873672 A CN201710873672 A CN 201710873672A CN 107594621 A CN107594621 A CN 107594621A
- Authority
- CN
- China
- Prior art keywords
- mass parts
- cigarette
- composite particles
- dry plate
- shaping
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Abstract
A kind of fruity flavor composite particles and its preparation method and application,It is related to cigarette auxiliary material production technical field,It is characterized in that,The composite particles are by by dried orange peel dry plate,Green apple dry plate,The mixing dry plate of lemon dryslice and Kiwi berry dry plate composition adds new hesperidin methyl dihydrochalcone,Raspberry ketone,Cigarette ketone,Malic acid,Citric acid and adhesive are simultaneously mixed,Ultramicro grinding is carried out to the mixed material under cryogenic conditions,Successively by mixing,Shaping,It is broken,It is granulated and sieves process,And the composite particles of 20 80 mesh formed,Described composite particles are the composite particles that 10 20 mass parts are added in the pipe tobacco of 100 mass parts,The sweet sense of gained cigarette smoke and sense increase of promoting the production of body fluid,Reduce cigarette smoke excitant,Abundant cigarette flavor,And assign cigarette fruity notes feature sucks style,Bioactivity is farthest remained using superfine communication technique,Effect is truly had to remain nutritional ingredient,The suction quality of cigarette is set to be lifted with obtaining conspicuousness.
Description
Technical field
The present invention relates to cigarette auxiliary material production technical field, more particularly to a kind of fruity flavor composite particles and its system
Preparation Method and application.
Background technology
With the progress of society and the improvement of living standards of the people, " smoking with health " turn into tobacco business can not avoid and
The social concern that must be faced.In order to alleviate this contradictory problems, it is necessary to cigarette smoke tar content is greatly lowered, but reduces
Tarry matters in smoke inevitably lose the graceful fragrance component of cigarette again, reduce the suction quality of cigarette.Therefore, tobacco scientific research
Guiding of the personnel using " flavouring humectation " as low burnt cigarette product exploitation, enters from essence spice for cigarette and smoking material both direction
Row technological innovation and trial, tar reduction and this contradictory problems of suction taste are efficiently solved, and achieve a large amount of scientific achievements.
A kind of relatively effective technological means that flavoring and casing is cigarette " flavouring humectation " is carried out to cigarette leaf group, by spy
The various spices that different technology extraction or separation obtain are added to the perfume (or spice) that can be made up in cigarette leaf group after Harm reduction techniques tar reduction
Gas loss, the sweet sense for improving cigarette smoke, the excitant for reducing cigarette smoke.Although essence spice for cigarette is in cigarette " flavouring
There is more obvious effect in terms of humectation ", but fragrant loss be present for the stronger spices of some volatility, to cigarette
The stability of suction quality has an impact, such as the spices that the volatility such as menthol, menthones is stronger.
There are filter stick perfuming, forming paper perfuming for technology of the smoking material in terms of " flavouring humectation ", cigarette paper perfuming, take
Chewing-gum perfuming etc., a kind of mode of the filter stick by the use of particle as filter stick perfuming, by cigarette smoke elute physical action directly
The fragrance matter with cigarette flavor phase harmony is introduced into cigarette smoke, to reach the purpose for improving smoking property of cigarette quality.With filter
Bar spices stockline, filter stick are compared with capsule and other smoking materials, different in terms of on filter stick particle have positive effect,
Fragrance is stable, the advantage that manufacturing process is simple, cost is cheap.At present, tobacco researcher in the research that this side up
Achieve some achievements.
Chinese Patent Application No.：ZL201510689854.X, Publication No. CN105595421A, disclose a kind of cigarette filter
Rod plant compound granular and preparation method thereof, disclosed plant compound granular is with Chinese yam, the root of kudzu vine, hawthorn, honeysuckle, emblic
Son, Momordica grosvenori, gynostemma pentaphylla, green plum are primary raw material, by crushing, pelletizing, drying, shaping and screening process, the particle of formation
Shape vegetable material can increase the sweet sense of cigarette smoke and sense of promoting the production of body fluid, and reduces cigarette smoke excitant, enriches cigarette flavor, makes
The suction quality of cigarette is lifted with obtaining conspicuousness；Chinese Patent Application No.：ZL201710032545.4, Publication No.
CN106723306A, disclose a kind of method that cigarette filter rod additive is prepared with American mint, described cigarette filter additive
Using American mint, fireworks petal, red big tobacco leaf and tobacco jelly powder as raw material, by crushing, mixing, extruding, crushing, shaping and
Process is sieved, forms finished particle, has the function that to lift cigarette smoking quality；Chinese Patent Application No.：
ZL201410076539.5, Publication No. CN103876285B, disclose a kind of flavored type filter stick particulate additive and its preparation
Methods and applications, the flavored type filter stick particle of announcement is by having dulcet edible powder, plant granule powder, binding agent and swollen
Agent is prepared by solution mixing, extruding granulation, microwave drying, and this kind of particle is added in cigarette filter rod with special
Compound fragrant, the sense of taste abundanter to smoker, scent experience.
All kinds of plant granules disclosed in patent pass through wet method and dry granulation mainly using vegetable material as body material at present
Various types of cigarette filter rod particles are obtained, the embodiment of its odor characteristic is mainly derived from the intrinsic Studies of The Aromatic Substances of vegetable material,
And Studies of The Aromatic Substances content is relatively low in vegetable material, under the soil washing of cigarette smoke, the Studies of The Aromatic Substances migrated into cigarette smoke contains
Amount also just seems very small, it is difficult to obvious fragrance characteristic and taste perception are provided for cigarette.Selection is fragrant with vegetable material
The synthesis class solid spice of the mutual harmony of gas phase aids in natural plant material with taste material is inhaled, and improves plant granule in fragrance and taste
The degree being felt in terms of feel, is a kind of more satisfactory technology, a kind of more satisfactory method.
Plants particles material needs to carry perfume, could more efficiently improve its contribution to cigarette smoking quality.Such as chankings
Perfume is carried by the way of spice solution is sprayed to carry out particle to face, it is necessary first to the problem of considering solvent, water and difficult volatilization
Solvent is not suitable for particle and carries perfume, generally selects absolute ethyl alcohol as perfume solvent, it not only volatilizees soon, nor shadow
Ring the physical state of particle.If using absolute ethyl alcohol as perfume solvent, because deliquescent problem, part spices certainly will be caused
It is difficult to use with taste material is inhaled.In addition, taking sprinkling to carry fragrant mode, not only spices addition is limited, and there is also perfume damage
Lose, fragrant stability problem, it is difficult to give full play to spices or inhale the booster action of taste material.
Ultramicro grinding, refer to overcome solid interior cohesiveness to be allowed to broken using mechanical or hydrokinetic method, so as to
More than 3 millimeters of material particles are crushed to the operating technology of 10-25 microns, can be crushed under low-temperature condition, speed is fast,
Moment can complete, thus retain the bioactive ingredients of powder to greatest extent, in favor of required high quality of products is made,
Therefore low-temperature submicron powder is broken is increasingly paid attention in the manufacturing field of plants particles material, to developing for its availability
To extensive concern.
The shortcomings that for current filter stick granular materials and technology, how to select appropriate material and technology, meet and
Lifting it is increasing the sweet sense of cigarette smoke and sense of promoting the production of body fluid, and reduces cigarette smoke excitant, enriches the effect in terms of cigarette flavor,
It is that cigarette improves and lifted a kind of new technology of suction quality.
The content of the invention
It is an object of the invention to for insufficient existing for currently available technology described above, there is provided a kind of fruity flavor
Composite particles and its preparation method and application.
A kind of fruity flavor composite particles, it is characterised in that the particle is by dried orange peel dry plate, green apple dry plate, lemon
New hesperidin methyl dihydrochalcone, raspberry ketone, cigarette ketone, apple are added in the mixed material of dry plate and Kiwi berry dry plate composition
Acid, citric acid and adhesive, and ultramicro grinding is carried out to the mixed material under cryogenic, then pass through mix successively, be molded,
Broken, granulation and screening process, with the composite particles of manufactured 20-80 mesh.
The mass parts of each component are as follows in described mixed material：
Dried orange peel dry plate is 30-45 mass parts, green apple dry plate is 10-20 mass parts, lemon dryslice is 5-10 mass parts, Kiwi berry
Dry plate is 10-15 mass parts, new hesperidin methyl dihydrochalcone is 1-5 mass parts, raspberry ketone is 1-5 mass parts, cigarette ketone
For 0.5-2 mass parts, malic acid be 0.1-1 mass parts, citric acid is 0.5-2 mass parts, adhesive is 5-10 mass parts.
Described adhesive is by the one or more in hydroxypropyl methyl cellulose, carboxymethyl cellulose or xanthans
Material be mixed to prepare.
Present invention also offers a kind of preparation method of fruity wind composite particles, it is characterised in that described preparation method
Step is as follows：
（1）Stock：The outfit of mixed material is carried out by the component of following mass percent：
Dried orange peel dry plate is 30-45 mass parts, green apple dry plate is 10-20 mass parts, lemon dryslice is 5-10 mass parts, Kiwi berry
Dry plate is 10-15 mass parts, new hesperidin methyl dihydrochalcone is 1-5 mass parts, raspberry ketone is 1-5 mass parts, cigarette ketone
For 0.5-2 mass parts, malic acid be 0.1-1 mass parts, citric acid is 0.5-2 mass parts, adhesive is 5-10 mass parts；
（2）Ultramicro grinding：Using the broken machine of low-temperature submicron powder to step（1）Described in mixed material carry out ultramicro grinding, make it
As granular material, granular material crosses 160 eye mesh screens, and in crushing process, control pulverizer circulating cooling coolant-temperature gage is in 25-40
℃；
（3）Mixing：Gained granular material is poured into mixer, carrying out agitation is sufficiently mixed it, makes various material distribution equal
It is even；
（4）Shaping：Granular material is poured into water-cooled dry granulating machine, tabletting is carried out to it, granular material forms tablet
Material, sheet material thickness is 1.5-2.5 millimeters；
（5）It is broken：Sheet material is poured into hammer crusher and carries out break process, becomes comminuting matter；
（6）It is granulated：Comminuting matter is poured into pelletizing machine, shaping is carried out to comminuting matter using pelletizing machine, is passed to 20 mesh
Shaping net；
（7）Screening：The comminuting matter after shaping is sorted using vibratory sieve, granular of isolated 20-60 mesh grade
Grain material, you can obtain described composite particles.
Present invention also offers a kind of application of described fruity flavor composite particles, it is characterised in that described is compound
Particle is the composite particles that 10-20 mass parts are added in the pipe tobacco of 100 mass parts, so that charge bar is prepared, then by charge bar
Compound, formation binary compound filter candle, finally by composite filter tip cigarette on plume, formation cigarette finished product are carried out with white rod.
The representative aroma substance that the dried orange peel dry plate that the present invention selects contains mainly has limonene, firpene, farnesene, big
Root myrcene etc.；The representative aroma substance that green apple dry plate contains mainly has hexenoic aldehyde, ethyl butyrate, hexenol etc.；Lemon
The representative aroma substance that dry plate contains mainly has limonene, citral, geraniol ester, flores aurantii ester etc.；Kiwi berry dry plate contains
Representative aroma substance mainly has ethyl butyrate, benzoic ether, hexenoic aldehyde, phenmethylol etc., and these compositions are fragrance graces
Flavor matter, while be also the important fragrance component in cigarette smoke, it can not only enrich cigarette flavor, and can be
Cigarette provides a kind of fruity flavor for distributing nature fragrance.
In addition, the sugariness for the new hesperidin methyl dihydrochalcone that the present invention selects is 1500-1800 times of sucrose, its mouth
Sense is salubrious, and pleasant impression is lasting, there is splendid shielding bitter taste effect, and it is migrated to oral cavity with flue gas, by increasing capacitance it is possible to increase the sweet tea in terms of the sense of taste
Sense；Cigarette ketone has natural tobacco fragrant and sweet, by increasing capacitance it is possible to increase the sweet tea sense in terms of cigarette perfume, lifting cigarette smell；Raspberry ketone, which has, to be covered
The characteristic perfume and fruit sweet taste of basin, it can further lift the fruity flavor of composite particles；Malic acid and citric acid are in fruit
Used in fragrant composite particles as acid, primarily serve and promote the production of body fluid, improve jealous effect, it is equal in tobacco leaf and cigarette smoke
There is presence, there is preferable matching with cigarette flavor；Hydroxypropyl methyl cellulose, carboxymethyl cellulose, xanthans are to cigarette
Fragrance is had no adverse effect, and itself and other components are assembled, and can improve the processability of pulverulent material.
A kind of fruity flavor composite particles provided by the invention and its preparation method and application, can effectively increase cigarette cigarette
The sweet sense of volume of gas and sense of promoting the production of body fluid, improve cigarette smoke comfortableness, enrich cigarette flavor, and assign cigarette fruity notes feature
Style is sucked, the suction quality of cigarette is lifted with obtaining conspicuousness, the particle produced using superfine communication technique is most
Big degree remains bioactivity, truly has effect to remain nutritional ingredient, and ultramicro grinding is advantageous to save raw material, improves raw material
Utilization rate, crush that speed is high, and efficiency is fast, there is preferable economic benefit；The composite particles of the present invention have advantages below simultaneously
And effect：1）With the fruit character fragrance with the mutual harmony of cigarette flavor：Because dried orange peel dry plate, green apple dry plate, lemon do
Piece, Kiwi berry dry plate have dense natural fruit aroma, and the volatile ingredient contained by these four raw materials is cigarette flavor
Flavor matter, make addition fruity flavor composite particles in cigarette that there is dense and natural fruity fragrance, be effectively improved smoker
Smoking experience, make us being in a cheerful frame of mind；2）A kind of abundant taste and smell experience can be provided for cigarette consumption person：Composite particles
Under the soil washing of cigarette smoke, it migrates a small amount of cigarette ketone, malic acid, citric acid, raspberry ketone to cigarette mainstream flue gas
With new hesperidin methyl dihydrochalcone, this just provides a kind of sour-sweet, fragrant and sweet taste and smell impression for smoker, and
Tart flavour and sweet taste can promote oral cavity to promote the production of body fluid, and the comfortableness and fragrance of cigarette are sucked in increase；3）The fragrant and sweet gas of fruit is more stable：My god
Right fruit raw material is assembled with synthesizing the solid spice of class and inhaling taste material, can further improve the fruit sweet tea of composite particles
Fragrance, increase the persistence of the fragrant and sweet gas of fruit.
Embodiment
The present invention is described in further details with reference to embodiment.
Embodiment 1：
A kind of fruity flavor composite particles, the preparation method step of the particle are as follows：
（1）Stock：The outfit of mixed material is carried out by the component of following mass parts：
Dried orange peel dry plate is 45 mass parts, green apple dry plate is 15 mass parts, lemon dryslice is 10 mass parts, Kiwi berry dry plate is 15
Mass parts, new hesperidin methyl dihydrochalcone are 2 mass parts, raspberry ketone is 1 mass parts, cigarette ketone is 1 mass parts, malic acid
It is made up of 0.5 mass parts, citric acid of 2 mass parts, adhesive of carboxymethyl cellulose, is 8.5 mass parts；
（2）Ultramicro grinding：Using the broken machine of low-temperature submicron powder to step（1）Described in mixed material carry out ultramicro grinding, make it
As granular material, granular material crosses 160 eye mesh screens, and in crushing process, control pulverizer circulating cooling coolant-temperature gage is at 25 DEG C；
（3）Mixing：Gained granular material is poured into mixer, carrying out agitation is sufficiently mixed it, makes various material distribution equal
It is even；
（4）Shaping：Granular material is poured into water-cooled dry granulating machine, tabletting is carried out to it, granular material forms tablet
Material, sheet material thickness are 1.5 millimeters；
（5）It is broken：Sheet material is poured into hammer crusher and carries out break process, becomes comminuting matter；
（6）It is granulated：Comminuting matter is poured into pelletizing machine, shaping is carried out to comminuting matter using pelletizing machine, is passed to 20 mesh
Shaping net；
（7）Screening：The comminuting matter after shaping is sorted using vibratory sieve, the granular solid matter material of isolated 40 mesh grade
Material, you can obtain the composite particles.
The composite particles of gained are the composite particles that 20 mass parts are added in the pipe tobacco of 100 mass parts, to be prepared
Charge bar, then charge bar is carried out to compound, formation binary compound filter candle, finally by composite filter tip cigarette on plume, shape with white rod
Into cigarette finished product.
It will be evaluated and analysed using the cigarette obtained by the present embodiment with regular-size cigarette, smoking result is as shown in table 1.
Embodiment 2：
A kind of fruity flavor composite particles, it is as follows the step of described composite particles preparation method：
（1）Stock：The outfit of mixed material is carried out by the component of following mass percent：
Dried orange peel dry plate is 39 mass parts, green apple dry plate is 20 mass parts, lemon dryslice is 8 mass parts, Kiwi berry dry plate is 12
Mass parts, new hesperidin methyl dihydrochalcone are 5 mass parts, raspberry ketone is 3 mass parts, cigarette ketone is 2 mass parts, malic acid
For 0.1 mass parts, citric acid be 0.9 mass parts, adhesive is made using hydroxypropyl methyl cellulose, is 10 mass parts；
（2）Ultramicro grinding：Using the broken machine of low-temperature submicron powder to step（1）Described in mixed material carry out ultramicro grinding, make it
As granular material, granular material crosses 160 eye mesh screens, and in crushing process, control pulverizer circulating cooling coolant-temperature gage is at 30 DEG C；
（3）Mixing：Gained granular material is poured into mixer, carrying out agitation is sufficiently mixed it, makes various material distribution equal
It is even；
（4）Shaping：Granular material is poured into water-cooled dry granulating machine, tabletting is carried out to it, granular material forms tablet
Material, sheet material thickness are 1.5 millimeters；
（5）It is broken：Sheet material is poured into hammer crusher and carries out break process, becomes comminuting matter；
（6）It is granulated：Comminuting matter is poured into pelletizing machine, shaping is carried out to comminuting matter using pelletizing machine, is passed to 20 mesh
Shaping net；
（7）Screening：The comminuting matter after shaping is sorted using vibratory sieve, the granular solid matter material of isolated 40 mesh grade
Material, you can obtain the composite particles.
The composite particles of gained are the composite particles that 20 mass parts are added in the pipe tobacco of 100 mass parts, to be prepared
Charge bar, then charge bar is carried out to compound, formation binary compound filter candle, finally by composite filter tip cigarette on plume, shape with white rod
Into cigarette finished product.
It will be evaluated and analysed using the cigarette obtained by the present embodiment with regular-size cigarette, smoking result is as shown in table 2.
Embodiment 3：
A kind of fruity flavor composite particles, it is as follows the step of described composite particles preparation method：
（1）Stock：The outfit of mixed material is carried out by the component of following mass percent：
Dried orange peel dry plate is 30 mass parts, green apple dry plate is 20 mass parts, lemon dryslice is 10 mass parts, Kiwi berry dry plate is 15
Mass parts, new hesperidin methyl dihydrochalcone are 5 mass parts, raspberry ketone is 5 mass parts, cigarette ketone is 2 mass parts, malic acid
For 1 mass parts, citric acid be 2 mass parts, adhesive using xanthans make, it is 10 mass parts；
（2）Ultramicro grinding：Using the broken machine of low-temperature submicron powder to step（1）Described in mixed material carry out ultramicro grinding, make it
As granular material, granular material crosses 160 eye mesh screens, and in crushing process, control pulverizer circulating cooling coolant-temperature gage is at 35 DEG C；
（3）Mixing：Gained granular material is poured into mixer, carrying out agitation is sufficiently mixed it, makes various material distribution equal
It is even；
（4）Shaping：Granular material is poured into water-cooled dry granulating machine, tabletting is carried out to it, granular material forms tablet
Material, sheet material thickness are 1.0 millimeters；
（5）It is broken：Sheet material is poured into hammer crusher and carries out break process, becomes comminuting matter；
（6）It is granulated：Comminuting matter is poured into pelletizing machine, shaping is carried out to comminuting matter using pelletizing machine, is passed to 20 mesh
Shaping net；
（7）Screening：The comminuting matter after shaping is sorted using vibratory sieve, the granular solid matter material of isolated 60 mesh grade
Material, you can obtain the composite particles.
It is the composite particles that 20 mass parts are added in the pipe tobacco of 100 mass parts by the composite particles of gained, to be prepared into
To charge bar, then charge bar is carried out to compound, formation binary compound filter candle with white rod, finally by composite filter tip cigarette on plume,
Form cigarette finished product.
It will be evaluated and analysed using the cigarette obtained by the present embodiment with regular-size cigarette, smoking result is as shown in table 3.
Embodiment 4：
A kind of fruity flavor composite particles, it is as follows the step of described composite particles preparation method：
（1）Stock：The outfit of mixed material is carried out by the component of following mass parts：
Dried orange peel dry plate is 45 mass parts, green apple dry plate is 10 mass parts, lemon dryslice is 10 mass parts, Kiwi berry dry plate is 15
Mass parts, new hesperidin methyl dihydrochalcone are 4 mass parts, raspberry ketone is 4 mass parts, cigarette ketone is 0.5 mass parts, apple
Acid is 1 mass parts, citric acid is 0.5 mass parts, adhesive is xanthans and the mixture of hydroxypropyl methyl cellulose, is 10 matter
Part is measured, wherein xanthans is 5 mass parts, and hydroxypropyl methyl cellulose is 5 mass parts；
（2）Ultramicro grinding：Using the broken machine of low-temperature submicron powder to step（1）Described in mixed material carry out ultramicro grinding, make it
As granular material, granular material crosses 160 eye mesh screens, and in crushing process, control pulverizer circulating cooling coolant-temperature gage is at 30 DEG C；
（3）Mixing：Gained granular material is poured into mixer, carrying out agitation is sufficiently mixed it, makes various material distribution equal
It is even；
（4）Shaping：Granular material is poured into water-cooled dry granulating machine, tabletting is carried out to it, granular material forms tablet
Material, sheet material thickness are 2 millimeters；
（5）It is broken：Sheet material is poured into hammer crusher and carries out break process, becomes comminuting matter；
（6）It is granulated：Comminuting matter is poured into pelletizing machine, shaping is carried out to comminuting matter using pelletizing machine, is passed to 20 mesh
Shaping net；
（7）Material screening：The comminuting matter after shaping is sorted using vibratory sieve, granular of isolated 40 mesh grade
Grain material, you can obtain the composite particles.
It is the composite particles that 10-20 mass parts are added in the pipe tobacco of 100 mass parts by the composite particles of gained, to prepare
Charge bar is obtained, then charge bar is carried out to compound, formation binary compound filter candle, finally by composite filter tip cigarette in plume with white rod
On, form cigarette finished product.
It will be evaluated and analysed using the cigarette obtained by the present embodiment with regular-size cigarette, smoking result is as shown in table 4.
Embodiment 5：
A kind of fruity flavor composite particles, the preparation method step of the particle are as follows：
（1）Stock：The outfit of mixed material is carried out by the component of following mass percent：
Dried orange peel dry plate is 45 mass ratioes, green apple dry plate is 20 mass ratioes, lemon dryslice is 5 mass ratioes, Kiwi berry dry plate is 15
Mass ratio, new hesperidin methyl dihydrochalcone are 1 mass ratio, raspberry ketone is 2 mass ratioes, cigarette ketone is 1 mass ratio, malic acid
It is 9 mass ratioes for the mixture that 0.8 mass ratio, citric acid are 1.2 mass ratioes, adhesive is xanthans and carboxymethyl cellulose,
Wherein xanthans is 5 mass ratioes, and carboxymethyl cellulose is 4 mass ratioes；
（2）Ultramicro grinding：Using the broken machine of low-temperature submicron powder to step（1）Described in mixed material carry out ultramicro grinding, make it
As granular material, granular material crosses 160 eye mesh screens, and in crushing process, control pulverizer circulating cooling coolant-temperature gage is in 25-40
℃；
（3）Mixing：Gained granular material is poured into mixer, carrying out agitation is sufficiently mixed it, makes various material distribution equal
It is even；
（4）Shaping：Granular material is poured into water-cooled dry granulating machine, tabletting is carried out to it, granular material forms tablet
Material, sheet material thickness are 2.5 millimeters；
（5）It is broken：Sheet material is poured into hammer crusher and carries out break process, becomes comminuting matter；
（6）It is granulated：Comminuting matter is poured into pelletizing machine, shaping is carried out to comminuting matter using pelletizing machine, is passed to 20 mesh
Shaping net；
（7）Screening：The comminuting matter after shaping is sorted using vibratory sieve, granular of isolated 20-60 mesh grade
Grain material, you can obtain the composite particles.
It is the composite particles that 20 mass parts are added in the pipe tobacco of 100 mass parts by the composite particles of gained, to be prepared into
To charge bar, then charge bar is carried out to compound, formation binary compound filter candle with white rod, finally by composite filter tip cigarette on plume,
Form cigarette finished product.
It will be evaluated and analysed using the cigarette obtained by the present embodiment with regular-size cigarette, smoking result is as shown in table 5.
Embodiment 6：
A kind of fruity flavor composite particles, the preparation method step of the particle are as follows：
（1）Stock：The outfit of mixed material is carried out by the component of following mass percent：
Dried orange peel dry plate is 45 mass ratioes, green apple dry plate is 20 mass ratioes, lemon dryslice is 8 mass ratioes, Kiwi berry dry plate is 10
Mass ratio, new hesperidin methyl dihydrochalcone are 5 mass ratioes, raspberry ketone is 4 mass ratioes, cigarette ketone is 1.5 mass ratioes, apple
Acid is 0.4 mass ratio, citric acid is 1.1 mass ratioes, adhesive is carboxymethyl cellulose, is 5 mass ratioes；
（2）Ultramicro grinding：Using the broken machine of low-temperature submicron powder to step（1）Described in mixed material carry out ultramicro grinding, make it
As granular material, granular material crosses 160 eye mesh screens, and in crushing process, control pulverizer circulating cooling coolant-temperature gage is at 25 DEG C；
（3）Mixing：Gained granular material is poured into mixer, carrying out agitation is sufficiently mixed it, makes various material distribution equal
It is even；
（4）Shaping：Granular material is poured into water-cooled dry granulating machine, tabletting is carried out to it, granular material forms tablet
Material, sheet material thickness are 1.5 millimeters；
（5）It is broken：Sheet material is poured into hammer crusher and carries out break process, becomes comminuting matter；
（6）It is granulated：Comminuting matter is poured into pelletizing machine, shaping is carried out to comminuting matter using pelletizing machine, is passed to 20 mesh
Shaping net；
（7）Screening：The comminuting matter after shaping is sorted using vibratory sieve, granular of isolated 20-60 mesh grade
Grain material, you can obtain the composite particles.
It is the composite particles that 10 mass parts are added in the pipe tobacco of 100 mass parts by the composite particles of gained, to be prepared into
To charge bar, then charge bar is carried out to compound, formation binary compound filter candle with white rod, finally by composite filter tip cigarette on plume,
Form cigarette finished product.
It will be evaluated and analysed using the cigarette obtained by the present embodiment with regular-size cigarette, smoking result is as shown in table 6.
Inhaled from the cigarette obtained by above-described embodiment and regular-size cigarette and comment contrast, a kind of fruity flavor of present invention gained
Composite particles are added to the sweet sense that can increase cigarette smoke in cigarette filter rod tow and sense of promoting the production of body fluid, and reducing cigarette smoke stimulates
Property, cigarette flavor is enriched, and the style of sucking of cigarette fruity notes feature is assigned, make the suction quality of cigarette with obtaining conspicuousness
Lifting.
Claims (5)
1. a kind of fruity flavor composite particles, it is characterised in that the particle is done by dried orange peel dry plate, green apple dry plate, lemon
New hesperidin methyl dihydrochalcone, raspberry ketone, cigarette ketone, apple are added in the mixed material of piece and Kiwi berry dry plate composition
Acid, citric acid and adhesive, and ultramicro grinding is carried out to the mixed material under cryogenic, then pass through mix successively, be molded,
Broken, granulation and screening process, with the composite particles of manufactured 20-80 mesh.
2. according to a kind of fruity flavor composite particles of claims 1, it is characterised in that each component in described mixed material
Mass parts are as follows：
Dried orange peel dry plate is 30-45 mass parts, green apple dry plate is 10-20 mass parts, lemon dryslice is 5-10 mass parts, Kiwi berry
Dry plate is 10-15 mass parts, new hesperidin methyl dihydrochalcone is 1-5 mass parts, raspberry ketone is 1-5 mass parts, cigarette ketone
For 0.5-2 mass parts, malic acid be 0.1-1 mass parts, citric acid is 0.5-2 mass parts, adhesive is 5-10 mass parts.
3. according to a kind of fruity flavor composite particles of claims 1, it is characterised in that described adhesive is by hydroxypropyl methyl
One or more kinds of materials in cellulose, carboxymethyl cellulose or xanthans are mixed to prepare.
4. a kind of preparation method of fruity wind composite particles, it is characterised in that as follows the step of the preparation method：
（1）Stock：The outfit of mixed material is carried out by the component of following mass percent：
Dried orange peel dry plate is 30-45 mass parts, green apple dry plate is 10-20 mass parts, lemon dryslice is 5-10 mass parts, Kiwi berry
Dry plate is 10-15 mass parts, new hesperidin methyl dihydrochalcone is 1-5 mass parts, raspberry ketone is 1-5 mass parts, cigarette ketone
For 0.5-2 mass parts, malic acid be 0.1-1 mass parts, citric acid is 0.5-2 mass parts, adhesive is 5-10 mass parts；
（2）Ultramicro grinding：Using the broken machine of low-temperature submicron powder to step（1）Described in mixed material carry out ultramicro grinding, make it
As granular material, granular material crosses 160 eye mesh screens, and in crushing process, control pulverizer circulating cooling coolant-temperature gage is in 25-40
℃；
（3）Mixing：Gained granular material is poured into mixer, carrying out agitation is sufficiently mixed it, makes various material distribution equal
It is even;
（4）Shaping：Granular material is poured into water-cooled dry granulating machine, tabletting is carried out to it, granular material forms tablet
Material, sheet material thickness is 1.5-2.5 millimeters；
（5）It is broken：Sheet material is poured into hammer crusher and carries out break process, becomes comminuting matter；
（6）It is granulated：Comminuting matter is poured into pelletizing machine, shaping is carried out to comminuting matter using pelletizing machine, is passed to 20 mesh
Shaping net；
（7）Screening：The comminuting matter after shaping is sorted using vibratory sieve, granular of isolated 20-60 mesh grade
Grain material, you can obtain described composite particles.
A kind of 5. application of fruity flavor composite particles as described in claim 1, it is characterised in that described composite particles
It is the composite particles that 10-20 mass parts are added in the pipe tobacco of 100 mass parts, so that charge bar is prepared, then by charge bar and in vain
Rod carries out compound, formation binary compound filter candle, finally by composite filter tip cigarette on plume, formation cigarette finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710873672.7A CN107594621A (en) | 2017-09-25 | 2017-09-25 | A kind of fruity flavor composite particles and its preparation method and application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710873672.7A CN107594621A (en) | 2017-09-25 | 2017-09-25 | A kind of fruity flavor composite particles and its preparation method and application |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107594621A true CN107594621A (en) | 2018-01-19 |
Family
ID=61058376
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710873672.7A Pending CN107594621A (en) | 2017-09-25 | 2017-09-25 | A kind of fruity flavor composite particles and its preparation method and application |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107594621A (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108936780A (en) * | 2018-09-17 | 2018-12-07 | 中烟施伟策（云南）再造烟叶有限公司 | The method for heating cigarette sucked material of not burning using centrifugal process granulation preparation |
| CN109517664A (en) * | 2018-12-18 | 2019-03-26 | 河南中烟工业有限责任公司 | A kind of width skin orange peel powder, preparation method and its application in cigarette filter rod |
| CN109645567A (en) * | 2018-12-04 | 2019-04-19 | 云南中烟工业有限责任公司 | It reduces cigarette and endangers fruit particle material of sex index and its preparation method and application |
| CN110184122A (en) * | 2019-06-24 | 2019-08-30 | 云南中烟工业有限责任公司 | A kind of cigarette particle of quick sensing fragrance and its preparation method and application |
| CN111616404A (en) * | 2020-06-05 | 2020-09-04 | 安徽中烟工业有限责任公司 | Microwave drying method for heating particles for cigarettes |
| CN113576020A (en) * | 2021-08-02 | 2021-11-02 | 云南中烟工业有限责任公司 | Preparation method of smoke generating material for smoking product |
| CN115226932A (en) * | 2022-08-16 | 2022-10-25 | 湖北中烟工业有限责任公司 | Heated cigarette with uniformly blended aroma-carrying particles and heated cigarette tobacco shreds and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN202030987U (en) * | 2010-12-27 | 2011-11-09 | 吉林烟草工业有限责任公司 | Paper for cigarette filter stick and cigarette filter stick |
| CN105725258A (en) * | 2016-02-25 | 2016-07-06 | 云南中烟工业有限责任公司 | Fragrant microcapsule for composite cigarettes and preparation method and application thereof |
| CN106387995A (en) * | 2016-08-31 | 2017-02-15 | 刘迎春 | Controlled-release filter tip containing aroma-increasing and moisture-retaining sheets |
| CN107057853A (en) * | 2017-01-16 | 2017-08-18 | 云南中烟新材料科技有限公司 | A kind of cigarette rose composite particles and its application |
-
2017
- 2017-09-25 CN CN201710873672.7A patent/CN107594621A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN202030987U (en) * | 2010-12-27 | 2011-11-09 | 吉林烟草工业有限责任公司 | Paper for cigarette filter stick and cigarette filter stick |
| CN105725258A (en) * | 2016-02-25 | 2016-07-06 | 云南中烟工业有限责任公司 | Fragrant microcapsule for composite cigarettes and preparation method and application thereof |
| CN106387995A (en) * | 2016-08-31 | 2017-02-15 | 刘迎春 | Controlled-release filter tip containing aroma-increasing and moisture-retaining sheets |
| CN107057853A (en) * | 2017-01-16 | 2017-08-18 | 云南中烟新材料科技有限公司 | A kind of cigarette rose composite particles and its application |
Non-Patent Citations (2)
| Title |
|---|
| 任凌波 等: "《生物化工产品生产工艺技术及应用》", 30 June 2001 * |
| 粉体技术导论: "《粉体技术导论》", 31 March 1998 * |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108936780A (en) * | 2018-09-17 | 2018-12-07 | 中烟施伟策（云南）再造烟叶有限公司 | The method for heating cigarette sucked material of not burning using centrifugal process granulation preparation |
| CN108936780B (en) * | 2018-09-17 | 2021-07-23 | 中烟施伟策（云南）再造烟叶有限公司 | Method for preparing smoking material for heating non-combustible cigarettes by utilizing centrifugal granulation |
| CN109645567A (en) * | 2018-12-04 | 2019-04-19 | 云南中烟工业有限责任公司 | It reduces cigarette and endangers fruit particle material of sex index and its preparation method and application |
| CN109517664A (en) * | 2018-12-18 | 2019-03-26 | 河南中烟工业有限责任公司 | A kind of width skin orange peel powder, preparation method and its application in cigarette filter rod |
| CN110184122A (en) * | 2019-06-24 | 2019-08-30 | 云南中烟工业有限责任公司 | A kind of cigarette particle of quick sensing fragrance and its preparation method and application |
| CN111616404A (en) * | 2020-06-05 | 2020-09-04 | 安徽中烟工业有限责任公司 | Microwave drying method for heating particles for cigarettes |
| CN113576020A (en) * | 2021-08-02 | 2021-11-02 | 云南中烟工业有限责任公司 | Preparation method of smoke generating material for smoking product |
| CN115226932A (en) * | 2022-08-16 | 2022-10-25 | 湖北中烟工业有限责任公司 | Heated cigarette with uniformly blended aroma-carrying particles and heated cigarette tobacco shreds and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107594621A (en) | A kind of fruity flavor composite particles and its preparation method and application | |
| CN105595421B (en) | A kind of cigarette filter rod plant compound granular and preparation method thereof | |
| JP5323064B2 (en) | Tobacco filters made from natural herb plants and tobacco using the same | |
| CN106174684A (en) | The preparation method of a kind of natural perfume material superfine powder and the application in reconstituted tobacoo thereof | |
| CN107752120A (en) | A kind of low temperature does not burn draft particle and preparation method thereof | |
| CN105230940A (en) | Functional hard candy and preparation method thereof | |
| CN106036998A (en) | Blast bead capable of making up for deficiencies in cigarette fragrance and moist sense and preparation method of blast bead | |
| CN110250565A (en) | A kind of plant granule perfume (or spice) pearl and the preparation method and application thereof | |
| CN101322851A (en) | Method for producing Tibetan medicinal herb incense with foot | |
| CN103054180A (en) | Aromatized composite particle filter stick and production method thereof | |
| CN107156903A (en) | A kind of cigarette of double-decker filter tip granular materials and its manufacture method | |
| CN102499447A (en) | Chinese style smoke-free tobacco product containing corsvenor momordica fruits | |
| CN104687246A (en) | Porous moringa oleifera particles, preparation method of porous moringa oleifera particles as well as cigarette filter stick containing porous particles | |
| CN103060093A (en) | Fragrance-invigorating and moisture-retention particles in cigarette and their preparation method and use | |
| CN105747267A (en) | Dissolvable smoke-free tobacco product and preparation method thereof | |
| CN110946317A (en) | Granular industrial hemp core material for heating non-combustion cigarette and preparation method thereof | |
| CN106723306B (en) | A kind of method that cigarette filter rod additive is prepared with American mint | |
| CN105831797B (en) | A kind of cabo particle and its application for being applied to prepare buccal cigarette | |
| CN107057853A (en) | A kind of cigarette rose composite particles and its application | |
| CN108936783B (en) | Method for preparing smoking material for cigarette by heating and non-burning through granulation by boiling method | |
| CN106867667A (en) | The preparation and its application of a kind of essence spice for cigarette | |
| CN107048464A (en) | One reuse method for growing tobacco useless thing | |
| CN101327041B (en) | Pu'er cooked tea alcohol extract and preparation and use thereof | |
| CN1072825A (en) | Five-leaved ginseng scented tea and preparation method thereof | |
| CN104663959A (en) | Preparation method of Anji white tea lozenge |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180119 |