CN110946317A - Granular industrial hemp core material for heating non-combustion cigarette and preparation method thereof - Google Patents
Granular industrial hemp core material for heating non-combustion cigarette and preparation method thereof Download PDFInfo
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- CN110946317A CN110946317A CN201911252065.4A CN201911252065A CN110946317A CN 110946317 A CN110946317 A CN 110946317A CN 201911252065 A CN201911252065 A CN 201911252065A CN 110946317 A CN110946317 A CN 110946317A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
Abstract
The invention discloses a granular industrial hemp tobacco core material for heating non-combustible cigarettes and a preparation method thereof, wherein the granular industrial hemp tobacco core material for heating non-combustible cigarettes comprises the following raw materials: industrial hemp raw material, plant auxiliary material, excipient, adhesive, smoke agent and perfume. The preparation method comprises the steps of processing industrial hemp raw materials, processing plant auxiliary materials, preparing solid base materials, preparing mixed liquid and preparing finished products. The industrial hemp tobacco core material prepared by the invention can load more than 10% of smoke agent in the process of granulating the solid industrial hemp ultrafine powder, can quickly generate smoke in a short time under the condition of lower heating temperature, and atomizes and brings out cannabidiol in industrial hemp, so that a smoker can have physiological satisfaction. The number of the suction ports can be effectively increased while the normal suction experience is kept, and the number of the suction ports can reach more than 15.
Description
Technical Field
The invention belongs to the technical field of industrial hemp products, and particularly relates to a granular industrial hemp tobacco core material for heating non-combustible cigarettes and a preparation method thereof.
Background
The 'hemp legalization' is gradually accepted in countries in Europe and America, but consumers in the market mainly consume the hemp by burning and smoking the rolled hemp and smoking the electronic cigarette added with tetrahydrocannabinol. The consumption mode has great potential safety hazard, and the main reason is that Tetrahydrocannabinol (THC) has a fantastic effect on human bodies. Industrial cannabis refers to cannabis with a tetrahydrocannabinol content of less than 0.3%, and is therefore considered to have no drug utilization value, while Cannabidiol (CBD) is a main chemical component in industrial cannabis and is also a non-addictive component, has pharmacological actions of anti-spasm, anti-anxiety and anti-inflammation, can not only be used for treating various difficult and complicated diseases, but also can effectively eliminate the hallucinogenic action of Tetrahydrocannabinol (THC) on human body, and is called as an "anti-drug compound".
By utilizing the design principle of low-harm heating tobacco in the current tobacco industry, the industrial hemp is made into the smokable heating industrial hemp, so that not only can the common hemp consumers obtain safer hemp products, but also the tobacco heating machine can play a role in the consumers: antispasmodic, anxiolytic, sedative, anti-insomnia, antiemetic, anti-inflammatory, anti-epileptic, anti-tumor, neuroprotective, metabolic and immunoregulatory, cardiovascular, hepatoprotective, and antibacterial effects.
Based on the above factors, it is necessary to develop a heating industrial hemp tobacco core material with simple process, low cost, good smoking quality and physiological satisfaction.
Disclosure of Invention
The first purpose of the invention is to provide a granular industrial hemp tobacco core material for heating non-combustible cigarettes.
The second purpose of the invention is to provide a preparation method of the granular industrial hemp tobacco core material for the cigarette which is not combusted by heating.
The first purpose of the invention is realized by the following raw materials in parts by weight: 10-80 parts of industrial hemp raw material, 0-10 parts of plant auxiliary material, 0-10 parts of excipient, 0-5 parts of adhesive, 0-20 parts of smoke agent and 0-15 parts of spice.
The second object of the present invention is achieved by comprising the steps of:
s1, processing the industrial hemp raw material: taking industrial hemp raw material with the mass percentage of 0-80%, extracting and concentrating to obtain concentrated extract, and then blending with distilled waterThe pitch density is 1.0 to 1.5g/m3Obtaining a liquid material A; crushing the rest industrial hemp raw materials to 400-1000 meshes, and spraying water to adjust the water content to 5-10% to obtain powder A;
s2, processing of plant auxiliary materials: taking plant auxiliary materials with the mass percent of 0-100%, extracting and concentrating to obtain a concentrated extract, and then adjusting the density to 1.0-1.5 g/m by using distilled water3Obtaining a liquid material B; crushing the rest plant auxiliary materials to 400-1000 meshes, and spraying water to adjust the water content to 5-10% to obtain powder B;
s3, preparing a solid base material: uniformly mixing the powder A, the powder B and an excipient to obtain a solid base material;
s4, preparing a mixed solution: uniformly mixing the adhesive and the spice, then adding the smoke agent and uniformly mixing, then adding the liquid material A and the liquid material B and uniformly mixing, standing for 2 hours at normal temperature, and filtering by using a 200-mesh filter screen to obtain a mixed solution;
s5, preparing a finished product: granulating the solid base material and the mixed solution to obtain particles with the particle size of 5-200 meshes, drying the particles, adjusting the moisture content of the particles to be below 10%, and screening.
The invention has the beneficial effects that: the solid industrial hemp ultrafine powder can be loaded with more than 10 percent of smoke agent in the granulation process, can quickly generate smoke in a short time under the condition of lower heating temperature, atomizes and brings out cannabidiol in industrial hemp, and ensures that a smoker can have physiological satisfaction. The number of the suction ports can be effectively increased while the normal suction experience is maintained, and the number of the suction ports can reach more than 15.
Drawings
FIG. 1 is a 1000-fold scanning electron microscope of a conventional filamentous core material;
FIG. 2 is a 2000 times scanning electron microscope of a conventional filamentous core material;
FIG. 3 is a 3000 times scanning electron microscope image of a conventional filamentous core material
FIG. 4 is a 100-fold electron microscope scan of a particulate tobacco core material of the present invention;
FIG. 5 is a scanning electron microscope image of the particulate core material of the present invention at 200 times;
FIG. 6 is a 500 times electron microscope scan of a particulate tobacco core material of the present invention;
FIG. 7 is a 1000 times electron microscope scan of the particulate core material of the present invention;
FIG. 8 is a thermogravimetric analysis of a conventional filamentary core material;
figure 9 is a thermogravimetric analysis of a particulate tobacco core material.
Detailed Description
The present invention is further illustrated by the following examples, which are not intended to be limiting in any way, and any modifications or alterations based on the teachings of the present invention are within the scope of the present invention.
The invention comprises the following raw materials in parts by weight: comprises the following raw materials in parts by weight: 10-80 parts of industrial hemp raw material, 0-10 parts of plant auxiliary material, 0-10 parts of excipient, 0-5 parts of adhesive, 0-20 parts of smoke agent and 0-15 parts of spice.
Preferably, the industrial hemp raw material is one or more of industrial hemp leaves, stems and extracted solid residues.
Preferably, the plant auxiliary materials are one or more of vetiver, vanilla, iris, mangnolia, jasmine and tree moss.
Preferably, the excipient is one or more of light calcium carbonate, heavy calcium carbonate, bentonite and diatomite, and the moisture of the excipient is controlled to be 5-10%.
Preferably, the excipient is in the form of a spindle or a sphere, and the particle size is 800-4500 meshes.
Preferably, the binder is one or more of water, ethanol, guar gum, starch gum, chitosan, carboxymethyl cellulose, pectin, acacia, sodium alginate, gelatin, glucose, polyallyl alcohol and fructose.
Preferably, the smoking agent is propylene glycol and/or glycerol.
Preferably, the fragrance is an aromatic plant extract.
The preparation method of the granular industrial hemp cigarette core material for the cigarette to be heated and burned comprises the following steps:
s1, processing the industrial hemp raw material: taking mass percentExtracting and concentrating 0-80% industrial hemp raw material to obtain concentrated extract, and then adjusting the density to 1.0-1.5 g/m with distilled water3Obtaining a liquid material A; crushing the rest industrial hemp raw materials to 400-1000 meshes, and spraying water to adjust the water content to 5-10% to obtain powder A;
s2, processing of plant auxiliary materials: taking plant auxiliary materials with the mass percent of 0-100%, extracting and concentrating to obtain a concentrated extract, and then adjusting the density to 1.0-1.5 g/m by using distilled water3Obtaining a liquid material B; crushing the rest plant auxiliary materials to 400-1000 meshes, and spraying water to adjust the water content to 5-10% to obtain powder B;
s3, preparing a solid base material: uniformly mixing the powder A, the powder B and an excipient to obtain a solid base material;
s4, preparing a mixed solution: uniformly mixing the adhesive and the spice, then adding the smoke agent and uniformly mixing, then adding the liquid material A and the liquid material B and uniformly mixing, standing for 2 hours at normal temperature, and filtering by using a 200-mesh filter screen to obtain a mixed solution;
s5, preparing a finished product: granulating the solid base material and the mixed solution to obtain particles with the particle size of 5-200 meshes, drying the particles, adjusting the moisture content of the particles to be below 10%, and screening.
S5, granulating by a dry granulator, specifically, tabletting the solid base material and the mixed solution by the dry granulator, cutting into small pieces, and granulating by two-stage granulation to obtain granules.
And S5, granulating by a wet granulator, specifically, adding the solid base material into the wet granulator, uniformly stirring and mixing, spraying the mixed solution to the solid base material by a spray gun, and granulating under the action of a stirring paddle and a cutter.
S5, granulating by a boiling one-step granulator, specifically, adding a solid base material into a bin of the boiling one-step granulator, adding a mixed solution into a top spraying system of the boiling one-step granulator, boiling the solid base material into a reaction kettle under the action of compressed air, simultaneously atomizing the mixed solution from the top of the reaction kettle by using clean compressed air, combining with the solid base material, and continuously accumulating and enlarging the solid base material in particle form to prepare particles through repeated and continuous boiling combination.
The present invention will be further described with reference to examples 1 to 67.
Example 1
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 10 parts of industrial hemp raw material.
Example 2
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 10 parts of industrial hemp raw material and 0.1 part of plant auxiliary material.
Example 3
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 80 parts of industrial hemp raw material and 10 parts of plant auxiliary material.
Example 4
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 45 parts of industrial hemp raw material and 5 parts of plant auxiliary material.
Example 5
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 10 portions of industrial hemp raw material, 0.1 portion of plant auxiliary material and 0.1 portion of excipient.
Example 6
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 80 parts of industrial hemp raw material, 10 parts of plant auxiliary material and 10 parts of excipient.
Example 7
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 45 parts of industrial hemp raw material, 5 parts of plant auxiliary material and 5 parts of excipient.
Example 8
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 10 portions of industrial hemp raw material, 0.1 portion of plant auxiliary material, 0.1 portion of excipient and 0.1 portion of adhesive.
Example 9
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 80 parts of industrial hemp raw material, 10 parts of plant auxiliary material, 10 parts of excipient and 5 parts of adhesive.
Example 10
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 45 parts of industrial hemp raw material, 5 parts of plant auxiliary material, 5 parts of excipient and 2.5 parts of adhesive.
Example 11
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 10 portions of industrial hemp raw material, 0.1 portion of plant auxiliary material, 0.1 portion of excipient, 0.1 portion of adhesive and 0.1 portion of smoke agent.
Example 12
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 80 parts of industrial hemp raw material, 10 parts of plant auxiliary material, 10 parts of excipient, 5 parts of adhesive and 20 parts of smoke agent.
Example 13
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 45 parts of industrial hemp raw material, 5 parts of plant auxiliary material, 5 parts of excipient, 2.5 parts of adhesive and 10 parts of smoke agent.
Example 14
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 10 portions of industrial hemp raw material, 0.1 portion of plant auxiliary material, 0.1 portion of excipient, 0.1 portion of adhesive, 0.1 portion of smoke agent and 0.1 portion of perfume.
Example 15
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 80 parts of industrial hemp raw material, 10 parts of plant auxiliary material, 10 parts of excipient, 5 parts of adhesive, 20 parts of smoke agent and 15 parts of spice.
Example 16
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 45 parts of industrial hemp raw material, 5 parts of plant auxiliary material, 5 parts of excipient, 2.5 parts of adhesive, 10 parts of smoke agent and 7.5 parts of spice.
Example 17
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 10 parts of industrial hemp leaves.
Example 18
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 10 portions of industrial hemp stalk.
Example 19
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 10 portions of industrial hemp extraction solid residue.
Example 20
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 10 parts of industrial hemp leaves and 0.1 part of vetiver.
Example 21
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 80 parts of industrial hemp stems and 10 parts of vanilla.
Example 22
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 45 parts of industrial hemp extraction solid residue and 5 parts of iris.
Example 23
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 10 parts of industrial hemp raw material, 0.1 part of orchid and 0.1 part of light calcium carbonate; the industrial hemp raw material is industrial hemp leaf and industrial hemp stalk.
Example 24
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 80 parts of industrial hemp raw material, 10 parts of jasmine flower and 10 parts of heavy calcium carbonate; the industrial hemp raw material is industrial hemp leaf and industrial hemp extraction solid residue.
Example 25
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 45 parts of industrial hemp raw material, 5 parts of tree moss and 5 parts of bentonite; the industrial hemp raw material is industrial hemp leaf, industrial hemp stalk and industrial hemp extraction solid residue.
Example 26
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 10 parts of industrial hemp leaves, 0.1 part of plant auxiliary materials, 0.1 part of diatomite and 0.1 part of water; the plant adjuvants are vetiver, vanilla, iris, mangnolia, jasmine and tree moss.
Example 27
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 80 parts of industrial hemp stems, 10 parts of vetiver, 10 parts of excipient and 5 parts of ethanol; the excipient is light calcium carbonate, heavy calcium carbonate, bentonite and diatomite.
Example 28
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 45 parts of industrial hemp extraction solid residue, 5 parts of vanilla, 5 parts of light calcium carbonate and 2.5 parts of guar gum; the water content of the light calcium carbonate is controlled to be 5 percent.
Example 29
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 10 parts of industrial hemp raw material, 0.1 part of iris, 0.1 part of heavy calcium carbonate, 0.1 part of starch glue and 0.1 part of propylene glycol; the industrial hemp raw materials are industrial hemp leaves and industrial hemp stalks; the water content of the heavy calcium carbonate is controlled to be 10 percent.
Example 30
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 80 parts of industrial hemp raw material, 10 parts of orchid, 10 parts of bentonite, 5 parts of chitosan and 20 parts of glycerol; the industrial hemp raw material is industrial hemp leaves and industrial hemp extraction solid residue; the bentonite is in a spindle shape, and the particle size is 800 meshes; the moisture of the bentonite is controlled to be 7.5 percent.
Example 31
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 45 parts of industrial hemp raw material, 5 parts of jasmine flower, 5 parts of diatomite, 2.5 parts of carboxymethyl cellulose and 10 parts of smoke agent; the industrial hemp raw materials are industrial hemp leaves, industrial hemp stalks and industrial hemp extraction solid residues; the smoke agent is propylene glycol and glycerol.
Example 32
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 30 parts of industrial hemp raw material, 1 part of plant auxiliary material, 1 part of excipient, 1 part of adhesive, 1 part of smoke agent and 1 part of spice.
Example 33
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 45 parts of industrial hemp raw material, 3 parts of plant auxiliary material, 3 parts of excipient, 5 parts of adhesive, 20 parts of smoke agent and 15 parts of spice.
Example 34
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 60 parts of industrial hemp raw material, 3 parts of plant auxiliary material, 5 parts of excipient, 10 parts of adhesive, 10 parts of smoke agent and 10 parts of spice.
Example 35
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 10 parts of industrial hemp leaves, 0.1 part of tree moss, 0.1 part of excipient, 0.1 part of pectin, 0.1 part of propylene glycol and 0.1 part of spice; the excipient is light calcium carbonate, heavy calcium carbonate, bentonite and diatomite.
Example 36
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 80 parts of industrial hemp stems, 10 parts of plant auxiliary materials, 10 parts of light calcium carbonate, 5 parts of Arabic gum, 20 parts of glycerol and 15 parts of spices; the plant auxiliary materials are vetiver, vanilla, iris, mangnolia, jasmine and tree moss; the light calcium carbonate is in a spindle shape, and the particle size is 4500 meshes.
Example 37
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 45 parts of industrial hemp extraction solid residue, 5 parts of plant auxiliary materials, 5 parts of ground limestone, 2.5 parts of sodium alginate, 10 parts of smoke agent and 7.5 parts of spice; the plant auxiliary materials are vetiver, vanilla, iris, mangnolia, jasmine and tree moss; the heavy calcium carbonate is spherical, and the particle size is 2650 meshes; the smoke agent is propylene glycol and glycerol.
Example 38
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 45 parts of industrial hemp extraction solid residue, 5 parts of iris tectorum and 0.1 part of gelatin.
Example 39
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 10 parts of industrial hemp raw material, 0.1 part of orchid, 0.1 part of light calcium carbonate and 10 parts of glucose; the industrial hemp raw material is industrial hemp leaf and industrial hemp stalk.
Example 40
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 80 parts of industrial hemp raw material, 10 parts of jasmine flower, 10 parts of ground calcium carbonate and 5 parts of polypropylene glycol; the industrial hemp raw material is industrial hemp leaf and industrial hemp extraction solid residue.
EXAMPLE 41
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 45 parts of industrial hemp raw material, 5 parts of tree moss, 5 parts of bentonite and 5 parts of fructose; the industrial hemp raw material is industrial hemp leaf, industrial hemp stalk and industrial hemp extraction solid residue.
Example 42
The granular industrial hemp cigarette core material for heating and non-burning cigarettes comprises the following raw materials in parts by weight: 45 parts of industrial hemp raw material, 5 parts of plant auxiliary material, 5 parts of excipient, 5 parts of adhesive, 10 parts of smoke agent and 7.5 parts of aromatic plant extract; the industrial hemp raw materials are industrial hemp leaves, industrial hemp stalks and industrial hemp extraction solid residues; the plant adjuvants are vetiver, vanilla, iris, mangnolia, jasmine and tree moss; the excipient is light calcium carbonate, heavy calcium carbonate, bentonite and diatomite, and the water content of the excipient is controlled to be 7.5%; the excipient is in the form of a spindle, and the particle size is 2650 meshes; the binder is water, ethanol, guar gum, starch gum, chitosan, carboxymethyl cellulose, pectin, acacia, sodium alginate, gelatin, glucose, polyallyl alcohol and fructose; the smoke agent is propylene glycol and glycerol.
Example 43
According to the embodiment 1, the preparation method of the granular industrial hemp core material for the heating non-combustion cigarette comprises the following steps:
s1, processing the industrial hemp raw material: crushing industrial hemp raw materials to 400 meshes, and spraying water to adjust the water content to 5% to obtain powder A, wherein the powder A is a solid base material;
s2, preparing a finished product: granulating the solid base material to obtain granules with the particle size of 5 meshes, drying the granules, adjusting the moisture of the granules to 1%, and then screening to obtain the compound feed.
Example 44
According to the embodiment 1, the preparation method of the granular industrial hemp core material for the heating non-combustion cigarette comprises the following steps:
s1, processing the industrial hemp raw material: taking industrial hemp raw material with the mass percentage of 0.1%, extracting and concentrating to obtain concentrated extract, and then adjusting the density to 1.0g/m by using distilled water3Obtaining a liquid material A; crushing other industrial hemp raw materials to 400 meshes, and spraying water to adjust the water content to 5% to obtain powder A, wherein the powder A is a solid base material;
s2, preparing a mixed solution: filtering the liquid material A by using a 200-mesh filter screen to obtain a mixed liquid;
s3, preparing a finished product: granulating the solid base material and the mixed solution to obtain particles with the particle size of 5 meshes, drying the particles, adjusting the moisture content of the particles to 1%, and then screening to obtain the particle.
Example 45
According to the embodiment 1, the preparation method of the granular industrial hemp core material for the heating non-combustion cigarette comprises the following steps:
s1, processing the industrial hemp raw material: taking industrial hemp raw material with the mass percent of 80%, extracting and concentrating to obtain concentrated extract, and then adjusting the density to 1.0-1.5 g/m by using distilled water3Obtaining a liquid material A; crushing the rest industrial hemp raw material to 1000 meshes, spraying water to adjust the water content to 10 percent to obtain powder A,the powder A is a solid base material;
s2, preparing a mixed solution: filtering the liquid material A by using a 200-mesh filter screen to obtain a mixed liquid;
s3, preparing a finished product: granulating the solid base material and the mixed solution to obtain granules with the particle size of 200 meshes, drying the granules, adjusting the moisture of the granules to 9.9%, and then screening to obtain the compound fertilizer.
Example 46
According to the embodiment 1, the preparation method of the granular industrial hemp core material for the heating non-combustion cigarette comprises the following steps:
s1, processing the industrial hemp raw material: taking 40% industrial hemp raw material by mass, extracting, concentrating to obtain concentrated extract, and then adjusting the density to 1.25g/m with distilled water3Obtaining a liquid material A; crushing other industrial hemp raw materials to 700 meshes, and spraying water to adjust the water content to 7.5% to obtain powder A, wherein the powder A is a solid base material;
s2, preparing a mixed solution: filtering the liquid material A by using a 200-mesh filter screen to obtain a mixed liquid;
s3, preparing a finished product: granulating the solid base material and the mixed solution to obtain particles with the particle size of 103 meshes, drying the particles, adjusting the moisture content of the particles to 5%, and then screening to obtain the particle.
Example 47
According to the embodiment 2, the preparation method of the granular industrial hemp core material for the heating non-combustion cigarette comprises the following steps:
s1, processing the industrial hemp raw material: crushing industrial hemp raw materials to 400 meshes, and spraying water to adjust the water content to 5% to obtain powder A;
s2, processing of plant auxiliary materials: crushing the plant auxiliary materials to 400 meshes, and spraying water to adjust the water content to 5% to obtain powder B;
s3, preparing a solid base material: uniformly mixing the powder A and the powder B to obtain a solid base material;
s4, preparing a finished product: granulating the solid base material to obtain granules with the particle size of 5 meshes, drying the granules, adjusting the moisture of the granules to 1%, and then screening to obtain the compound feed.
Example 48
According to the embodiment 2, the preparation method of the granular industrial hemp core material for the heating non-combustion cigarette comprises the following steps:
s1, processing the industrial hemp raw material: taking industrial hemp raw material with the mass percentage of 0.1%, extracting and concentrating to obtain concentrated extract, and then adjusting the density to 1.0g/m by using distilled water3Obtaining a liquid material A; crushing other industrial hemp raw materials to 400 meshes, and spraying water to adjust the water content to 5% to obtain powder A;
s2, processing of plant auxiliary materials: taking plant auxiliary materials with the mass percent of 0.1%, extracting and concentrating to obtain concentrated extract, and then adjusting the density to 1.0g/m by using distilled water3Obtaining a liquid material B; crushing the rest plant auxiliary materials to 400 meshes, and spraying water to adjust the water content to 5% to obtain powder B;
s3, preparing a solid base material: uniformly mixing the powder A and the powder B to obtain a solid base material;
s4, preparing a mixed solution: uniformly mixing the liquid material A and the liquid material B, standing for 2 hours at normal temperature, and filtering by using a 200-mesh filter screen to obtain a mixed solution;
s5, preparing a finished product: granulating the solid base material and the mixed solution to obtain particles with the particle size of 5 meshes, drying the particles, adjusting the moisture content of the particles to 1%, and then screening to obtain the particle.
Example 49
According to the embodiment 2, the preparation method of the granular industrial hemp core material for the heating non-combustion cigarette comprises the following steps:
s1, processing the industrial hemp raw material: taking industrial hemp raw material with the mass percent of 80%, extracting and concentrating to obtain concentrated extract, and then adjusting the density to 1.5g/m by using distilled water3Obtaining a liquid material A; crushing other industrial hemp raw materials to 1000 meshes, and then spraying water to adjust the water content to 10 percent to obtain powder A, wherein the powder is a solid base material;
s2, processing of plant auxiliary materials: taking plant auxiliary materials with the mass percent of 100%, extracting and concentrating to obtain concentrated extract, and then adjusting the density to 1.5g/m by using distilled water3Obtaining a liquid material B;
s3, preparing a mixed solution: uniformly mixing the liquid material A and the liquid material B, standing for 2 hours at normal temperature, and filtering by using a 200-mesh filter screen to obtain a mixed solution;
s4, preparing a finished product: granulating the solid base material and the mixed solution to obtain particles with the particle size of 103 meshes, drying the particles, adjusting the moisture content of the particles to 5%, and then screening to obtain the particle.
Example 50
According to the embodiment 2, the preparation method of the granular industrial hemp core material for the heating non-combustion cigarette comprises the following steps:
s1, processing the industrial hemp raw material: taking 40% industrial hemp raw material by mass, extracting, concentrating to obtain concentrated extract, and then adjusting the density to 1.25g/m with distilled water3Obtaining a liquid material A; crushing other industrial hemp raw materials to 700 meshes, and spraying water to adjust the water content to 7.5% to obtain powder A;
s2, processing of plant auxiliary materials: taking 50% of plant auxiliary materials by mass percent, extracting and concentrating to obtain a concentrated extract, and then adjusting the density to 1.25g/m by using distilled water3Obtaining a liquid material B; crushing the rest plant auxiliary materials to 700 meshes, and spraying water to adjust the water content to 7.5% to obtain powder B;
s3, preparing a solid base material: uniformly mixing the powder A and the powder B to obtain a solid base material;
s4, preparing a mixed solution: uniformly mixing the liquid material A and the liquid material B, standing for 2 hours at normal temperature, and filtering by using a 200-mesh filter screen to obtain a mixed solution;
s5, preparing a finished product: granulating the solid base material and the mixed solution to obtain particles with the particle size of 103 meshes, drying the particles, adjusting the moisture content of the particles to 5%, and then screening to obtain the particle.
Example 51
According to the embodiment 5, the preparation method of the granular industrial hemp core material for the heating non-combustion cigarette comprises the following steps:
s1, processing the industrial hemp raw material: crushing industrial hemp raw materials to 400 meshes, and spraying water to adjust the water content to 5% to obtain powder A;
s2, processing of plant auxiliary materials: crushing the plant auxiliary materials to 400 meshes, and spraying water to adjust the water content to 5% to obtain powder B;
s3, preparing a solid base material: uniformly mixing the powder A, the powder B and an excipient to obtain a solid base material;
s4, preparing a mixed solution: uniformly mixing the adhesive and the spice, then adding the smoke agent and uniformly mixing, then adding the liquid material A and the liquid material B and uniformly mixing, standing for 2 hours at normal temperature, and filtering by using a 200-mesh filter screen to obtain a mixed solution;
s5, preparing a finished product: granulating the solid base material and the mixed solution to obtain particles with the particle size of 5 meshes, drying the particles, adjusting the moisture content of the particles to 5%, and then screening to obtain the particle.
Example 52
According to the embodiment 5, the preparation method of the granular industrial hemp core material for the heating non-combustion cigarette comprises the following steps:
s1, processing the industrial hemp raw material: taking industrial hemp raw material with the mass percentage of 0.1%, extracting and concentrating to obtain concentrated extract, and then adjusting the density to 1.0g/m by using distilled water3Obtaining a liquid material A; crushing other industrial hemp raw materials to 400 meshes, and spraying water to adjust the water content to 5% to obtain powder A;
s2, processing of plant auxiliary materials: taking plant auxiliary materials with the mass percent of 0.1%, extracting and concentrating to obtain concentrated extract, and then adjusting the density to 1.0g/m by using distilled water3Obtaining a liquid material B; crushing the rest plant auxiliary materials to 400 meshes, and spraying water to adjust the water content to 5% to obtain powder B;
s3, preparing a solid base material: uniformly mixing the powder A, the powder B and an excipient to obtain a solid base material;
s4, preparing a mixed solution: uniformly mixing the liquid material A and the liquid material B, standing for 2 hours at normal temperature, and filtering by using a 200-mesh filter screen to obtain a mixed solution;
s5, preparing a finished product: granulating the solid base material and the mixed solution to obtain particles with the particle size of 5 meshes, drying the particles, adjusting the moisture content of the particles to 1%, and then screening to obtain the particle.
Example 53
According to the embodiment 5, the preparation method of the granular industrial hemp core material for the heating non-combustion cigarette comprises the following steps:
s1, processing the industrial hemp raw material: taking industrial hemp raw material with the mass percent of 80%, extracting and concentrating to obtain concentrated extract, and then adjusting the density to 1.5g/m by using distilled water3Obtaining a liquid material A; crushing other industrial hemp raw materials to 1000 meshes, and spraying water to adjust the water content to 10% to obtain powder A;
s2, processing of plant auxiliary materials: taking plant auxiliary materials with the mass percent of 100%, extracting and concentrating to obtain concentrated extract, and then adjusting the density to 1.5g/m by using distilled water3Obtaining a liquid material B;
s3, preparing a solid base material: uniformly mixing the powder A and the excipient to obtain a solid base material;
s4, preparing a mixed solution: uniformly mixing the liquid material A and the liquid material B, standing for 2 hours at normal temperature, and filtering by using a 200-mesh filter screen to obtain a mixed solution;
s5, preparing a finished product: granulating the solid base material and the mixed solution to obtain granules with the particle size of 200 meshes, drying the granules, adjusting the moisture of the granules to 9.9%, and then screening to obtain the compound fertilizer.
Example 54
According to the embodiment 5, the preparation method of the granular industrial hemp core material for the heating non-combustion cigarette comprises the following steps:
s1, processing the industrial hemp raw material: taking 40% industrial hemp raw material by mass, extracting, concentrating to obtain concentrated extract, and then adjusting the density to 1.25g/m with distilled water3Obtaining a liquid material A; crushing other industrial hemp raw materials to 700 meshes, and spraying water to adjust the water content to 7.5% to obtain powder A;
s2, processing of plant auxiliary materials: taking 50% of plant auxiliary materials by mass percent, extracting and concentrating to obtain a concentrated extract, and then adjusting the density to 1.25g/m by using distilled water3Obtaining a liquid material B; crushing the rest plant auxiliary materials to 700 meshes, and spraying water to adjust the water content to 7.5% to obtain powder B;
s3, preparing a solid base material: uniformly mixing the powder A, the powder B and an excipient to obtain a solid base material;
s4, preparing a mixed solution: uniformly mixing the liquid material A and the liquid material B, standing for 2 hours at normal temperature, and filtering by using a 200-mesh filter screen to obtain a mixed solution;
s5, preparing a finished product: granulating the solid base material and the mixed solution to obtain particles with the particle size of 103 meshes, drying the particles, adjusting the moisture content of the particles to 5%, and then screening to obtain the particle.
Example 55
According to the embodiment 8, the preparation method of the granular industrial hemp core material for the heating non-combustion cigarette comprises the following steps:
s1, processing the industrial hemp raw material: crushing industrial hemp raw materials to 400 meshes, and spraying water to adjust the water content to 5% to obtain powder A;
s2, processing of plant auxiliary materials: crushing the plant auxiliary materials to 400 meshes, and spraying water to adjust the water content to 5% to obtain powder B;
s3, preparing a solid base material: uniformly mixing the powder A, the powder B and an excipient to obtain a solid base material;
s4, preparing a mixed solution: filtering the adhesive by using a 200-mesh filter screen to obtain a mixed solution;
s5, preparing a finished product: granulating the solid base material and the mixed solution to obtain particles with the particle size of 5 meshes, drying the particles, adjusting the moisture content of the particles to 1%, and then screening to obtain the particle.
Example 56
According to the embodiment 8, the preparation method of the granular industrial hemp core material for the heating non-combustion cigarette comprises the following steps:
s1, processing the industrial hemp raw material: taking industrial hemp raw material with the mass percentage of 0.1%, extracting and concentrating to obtain concentrated extract, and then adjusting the density to 1.0g/m by using distilled water3Obtaining a liquid material A; crushing other industrial hemp raw materials to 400 meshes, and spraying water to adjust the water content to 5% to obtain powder A;
s2, processing of plant auxiliary materials: taking plant auxiliary materials with the mass percent of 0.1%, extracting and concentrating to obtain concentrated extract, and then using distilled waterAdjusting the density to 1.0g/m3Obtaining a liquid material B; crushing the rest plant auxiliary materials to 400 meshes, and spraying water to adjust the water content to 5% to obtain powder B;
s3, preparing a solid base material: uniformly mixing the powder A, the powder B and an excipient to obtain a solid base material;
s4, preparing a mixed solution: adding the liquid material A and the liquid material B into the adhesive, uniformly mixing, standing at normal temperature for 2 hours, and filtering by using a 200-mesh filter screen to obtain a mixed solution;
s5, preparing a finished product: granulating the solid base material and the mixed solution to obtain particles with the particle size of 5 meshes, drying the particles, adjusting the moisture content of the particles to 1%, and then screening to obtain the particle.
Example 57
According to the embodiment 8, the preparation method of the granular industrial hemp core material for the heating non-combustion cigarette comprises the following steps:
s1, processing the industrial hemp raw material: taking industrial hemp raw material with the mass percent of 80%, extracting and concentrating to obtain concentrated extract, and then adjusting the density to 1.5g/m by using distilled water3Obtaining a liquid material A; crushing other industrial hemp raw materials to 1000 meshes, and spraying water to adjust the water content to 10% to obtain powder A;
s2, processing of plant auxiliary materials: taking plant auxiliary materials with the mass percent of 100%, extracting and concentrating to obtain concentrated extract, and then adjusting the density to 1.5g/m by using distilled water3Obtaining a liquid material B;
s3, preparing a solid base material: uniformly mixing the powder A and the excipient to obtain a solid base material;
s4, preparing a mixed solution: adding the liquid material A and the liquid material B into the adhesive, uniformly mixing, standing at normal temperature for 2 hours, and filtering by using a 200-mesh filter screen to obtain a mixed solution;
s5, preparing a finished product: granulating the solid base material and the mixed solution to obtain granules with the particle size of 200 meshes, drying the granules, adjusting the moisture of the granules to 9.9%, and then screening to obtain the compound fertilizer.
Example 58
According to the embodiment 8, the preparation method of the granular industrial hemp core material for the heating non-combustion cigarette comprises the following steps:
s1, processing the industrial hemp raw material: taking 40% industrial hemp raw material by mass, extracting, concentrating to obtain concentrated extract, and then adjusting the density to 1.25g/m with distilled water3Obtaining a liquid material A; crushing other industrial hemp raw materials to 700 meshes, and spraying water to adjust the water content to 7.5% to obtain powder A;
s2, processing of plant auxiliary materials: taking 50% of plant auxiliary materials by mass percent, extracting and concentrating to obtain a concentrated extract, and then adjusting the density to 1.25g/m by using distilled water3Obtaining a liquid material B; crushing the rest plant auxiliary materials to 700 meshes, and spraying water to adjust the water content to 7.5% to obtain powder B;
s3, preparing a solid base material: uniformly mixing the powder A, the powder B and an excipient to obtain a solid base material;
s4, preparing a mixed solution: adding the liquid material A and the liquid material B into the adhesive, uniformly mixing, standing at normal temperature for 2 hours, and filtering by using a 200-mesh filter screen to obtain a mixed solution;
s5, preparing a finished product: granulating the solid base material and the mixed solution to obtain particles with the particle size of 103 meshes, drying the particles, adjusting the moisture content of the particles to 5%, and then screening to obtain the particle.
Example 59
According to example 11, the preparation method of the granular industrial hemp core material for the cigarette without heat combustion comprises the following steps:
s1, processing the industrial hemp raw material: crushing industrial hemp raw materials to 400 meshes, and spraying water to adjust the water content to 5% to obtain powder A;
s2, processing of plant auxiliary materials: crushing the plant auxiliary materials to 400 meshes, and spraying water to adjust the water content to 5% to obtain powder B;
s3, preparing a solid base material: uniformly mixing the powder A, the powder B and an excipient to obtain a solid base material;
s4, preparing a mixed solution: adding a smoke agent into the adhesive, uniformly mixing, standing at normal temperature for 2h, and filtering by using a 200-mesh filter screen to obtain a mixed solution;
s5, preparing a finished product: granulating the solid base material and the mixed solution to obtain particles with the particle size of 5 meshes, drying the particles, adjusting the moisture content of the particles to 1%, and then screening to obtain the particle.
Example 60
According to example 11, the preparation method of the granular industrial hemp core material for the cigarette without heat combustion comprises the following steps:
s1, processing the industrial hemp raw material: taking industrial hemp raw material with the mass percentage of 0.1%, extracting and concentrating to obtain concentrated extract, and then adjusting the density to 1.0g/m by using distilled water3Obtaining a liquid material A; crushing other industrial hemp raw materials to 400 meshes, and spraying water to adjust the water content to 5% to obtain powder A;
s2, processing of plant auxiliary materials: taking plant auxiliary materials with the mass percent of 0.1%, extracting and concentrating to obtain concentrated extract, and then adjusting the density to 1.0g/m by using distilled water3Obtaining a liquid material B; crushing the rest plant auxiliary materials to 400 meshes, and spraying water to adjust the water content to 5% to obtain powder B;
s3, preparing a solid base material: uniformly mixing the powder A, the powder B and an excipient to obtain a solid base material;
s4, preparing a mixed solution: adding a smoke agent into the adhesive, uniformly mixing, adding the liquid material A and the liquid material B, uniformly mixing, standing at normal temperature for 2 hours, and filtering by using a 200-mesh filter screen to obtain a mixed solution;
s5, preparing a finished product: granulating the solid base material and the mixed solution to obtain particles with the particle size of 5 meshes, drying the particles, adjusting the moisture content of the particles to 1%, and then screening to obtain the particle.
Example 61
According to example 11, the preparation method of the granular industrial hemp core material for the cigarette without heat combustion comprises the following steps:
s1, processing the industrial hemp raw material: taking industrial hemp raw material with the mass percent of 80%, extracting and concentrating to obtain concentrated extract, and then adjusting the density to 1.5g/m by using distilled water3Obtaining a liquid material A; crushing other industrial hemp raw materials to 1000 meshes, and spraying water to adjust the water content to 10% to obtain powder A;
s2, processing of plant auxiliary materials: taking plant auxiliary materials with the mass percent of 100%, extracting and concentrating to obtain concentrated extract, and then adjusting the density to 1.5g/m by using distilled water3Obtaining a liquid material B;
s3, preparing a solid base material: uniformly mixing the powder A and the excipient to obtain a solid base material;
s4, preparing a mixed solution: adding a smoke agent into the adhesive, uniformly mixing, adding the liquid material A and the liquid material B, uniformly mixing, standing at normal temperature for 2 hours, and filtering by using a 200-mesh filter screen to obtain a mixed solution;
s5, preparing a finished product: granulating the solid base material and the mixed solution to obtain granules with the particle size of 200 meshes, drying the granules, adjusting the moisture of the granules to 9.9%, and then screening to obtain the compound fertilizer.
Example 62
According to example 11, the preparation method of the granular industrial hemp core material for the cigarette without heat combustion comprises the following steps:
s1, processing the industrial hemp raw material: taking 40% industrial hemp raw material by mass, extracting, concentrating to obtain concentrated extract, and then adjusting the density to 1.25g/m with distilled water3Obtaining a liquid material A; crushing other industrial hemp raw materials to 700 meshes, and spraying water to adjust the water content to 7.5% to obtain powder A;
s2, processing of plant auxiliary materials: taking 50% of plant auxiliary materials by mass percent, extracting and concentrating to obtain a concentrated extract, and then adjusting the density to 1.25g/m by using distilled water3Obtaining a liquid material B; crushing the rest plant auxiliary materials to 700 meshes, and spraying water to adjust the water content to 7.5% to obtain powder B;
s3, preparing a solid base material: uniformly mixing the powder A, the powder B and an excipient to obtain a solid base material;
s4, preparing a mixed solution: adding a smoke agent into the adhesive, uniformly mixing, adding the liquid material A and the liquid material B, uniformly mixing, standing at normal temperature for 2 hours, and filtering by using a 200-mesh filter screen to obtain a mixed solution;
s5, preparing a finished product: granulating the solid base material and the mixed solution to obtain particles with the particle size of 103 meshes, drying the particles, adjusting the moisture content of the particles to 5%, and then screening to obtain the particle.
Example 63
According to example 14, a method for preparing a granular industrial hemp core material for a cigarette to be heated without combustion comprises the following steps:
s1, processing the industrial hemp raw material: crushing industrial hemp raw materials to 400 meshes, and spraying water to adjust the water content to 5% to obtain powder A;
s2, processing of plant auxiliary materials: crushing the plant auxiliary materials to 400 meshes, and spraying water to adjust the water content to 5% to obtain powder B;
s3, preparing a solid base material: uniformly mixing the powder A, the powder B and an excipient to obtain a solid base material;
s4, preparing a mixed solution: uniformly mixing the adhesive and the spice, then adding the smoke agent, uniformly mixing, standing for 2 hours at normal temperature, and filtering by using a 200-mesh filter screen to obtain a mixed solution;
s5, preparing a finished product: granulating the solid base material and the mixed solution to obtain particles with the particle size of 5 meshes, drying the particles, adjusting the moisture content of the particles to 1%, and then screening to obtain the particle.
Example 64
According to example 14, a method for preparing a granular industrial hemp core material for a cigarette to be heated without combustion comprises the following steps:
s1, processing the industrial hemp raw material: taking industrial hemp raw material with the mass percentage of 0.1%, extracting and concentrating to obtain concentrated extract, and then adjusting the density to 1.0g/m by using distilled water3Obtaining a liquid material A; crushing other industrial hemp raw materials to 400 meshes, and spraying water to adjust the water content to 5% to obtain powder A;
s2, processing of plant auxiliary materials: taking plant auxiliary materials with the mass percent of 0.1%, extracting and concentrating to obtain concentrated extract, and then adjusting the density to 1.0g/m by using distilled water3Obtaining a liquid material B; crushing the rest plant auxiliary materials to 400 meshes, and spraying water to adjust the water content to 5% to obtain powder B;
s3, preparing a solid base material: uniformly mixing the powder A, the powder B and an excipient to obtain a solid base material;
s4, preparing a mixed solution: uniformly mixing the adhesive and the spice, then adding the smoke agent and uniformly mixing, then adding the liquid material A and the liquid material B and uniformly mixing, standing for 2 hours at normal temperature, and filtering by using a 200-mesh filter screen to obtain a mixed solution;
s5, preparing a finished product: granulating the solid base material and the mixed solution to obtain particles with the particle size of 5 meshes, drying the particles, adjusting the moisture content of the particles to 1%, and then screening to obtain the particle.
Example 65
According to example 14, a method for preparing a granular industrial hemp core material for a cigarette to be heated without combustion comprises the following steps:
s1, processing the industrial hemp raw material: taking industrial hemp raw material with the mass percent of 80%, extracting and concentrating to obtain concentrated extract, and then adjusting the density to 1.5g/m by using distilled water3Obtaining a liquid material A; crushing other industrial hemp raw materials to 1000 meshes, and spraying water to adjust the water content to 10% to obtain powder A;
s2, processing of plant auxiliary materials: taking plant auxiliary materials with the mass percent of 100%, extracting and concentrating to obtain concentrated extract, and then adjusting the density to 1.5g/m by using distilled water3Obtaining a liquid material B;
s3, preparing a solid base material: uniformly mixing the powder A and the excipient to obtain a solid base material;
s4, preparing a mixed solution: uniformly mixing the adhesive and the spice, then adding the smoke agent and uniformly mixing, then adding the liquid material A and the liquid material B and uniformly mixing, standing for 2 hours at normal temperature, and filtering by using a 200-mesh filter screen to obtain a mixed solution;
s5, preparing a finished product: granulating the solid base material and the mixed solution to obtain granules with the particle size of 200 meshes, drying the granules, adjusting the moisture of the granules to 9.9%, and then screening to obtain the compound fertilizer.
Example 66
According to example 14, a method for preparing a granular industrial hemp core material for a cigarette to be heated without combustion comprises the following steps:
s1, processing the industrial hemp raw material: taking 40 percent of industrial hemp raw material by massExtracting, concentrating to obtain concentrated extract, and adjusting density to 1.25g/m with distilled water3Obtaining a liquid material A; crushing other industrial hemp raw materials to 700 meshes, and spraying water to adjust the water content to 7.5% to obtain powder A;
s2, processing of plant auxiliary materials: taking 50% of plant auxiliary materials by mass percent, extracting and concentrating to obtain a concentrated extract, and then adjusting the density to 1.25g/m by using distilled water3Obtaining a liquid material B; crushing the rest plant auxiliary materials to 700 meshes, and spraying water to adjust the water content to 7.5% to obtain powder B;
s3, preparing a solid base material: uniformly mixing the powder A, the powder B and an excipient to obtain a solid base material;
s4, preparing a mixed solution: uniformly mixing the adhesive and the spice, then adding the smoke agent and uniformly mixing, then adding the liquid material A and the liquid material B and uniformly mixing, standing for 2 hours at normal temperature, and filtering by using a 200-mesh filter screen to obtain a mixed solution;
s5, preparing a finished product: granulating the solid base material and the mixed solution to obtain particles with the particle size of 103 meshes, drying the particles, adjusting the moisture content of the particles to 5%, and then screening to obtain the particle.
Example 67: microscopic morphology and thermogravimetric analysis of tobacco core material
TABLE 1 thermogravimetric analysis results of conventional filamentous core material and granular core material
Compared with the traditional filamentous core material on the market at present, the granular core material is similar in microstructure; compared with the traditional filamentous core material, the particle-type core material has higher release efficiency of active substances in the core material at a low temperature section below 400 ℃; the traditional filamentous core material is shown in figures 1-3 by 1000, 2000 and 3000 times of electron microscope scanning, and the granular core material of the invention is shown in figures 4-7 by 100, 200, 500 and 1000 times of electron microscope scanning; the results of thermogravimetric analysis of the conventional filamentous core material and granular core material are shown in FIGS. 8 to 9 and Table 1; note: in fig. 8 and 9, the solid curve is a TG curve, and the dotted curve is a DTG curve.
Claims (9)
1. A granular industrial hemp cigarette core material for heating non-combustible cigarettes is characterized by comprising the following raw materials in parts by weight: 10-80 parts of industrial hemp raw material, 0-10 parts of plant auxiliary material, 0-10 parts of excipient, 0-5 parts of adhesive, 0-20 parts of smoke agent and 0-15 parts of spice.
2. The granular industrial hemp core material for cigarette heated without combustion according to claim 1, wherein the industrial hemp raw material is one or more of industrial hemp leaves, stems, and extracted solid residues.
3. The granular industrial hemp core material for cigarette heated without combustion as claimed in claim 1, wherein said plant auxiliary material is one or more of vetiver, vanilla, iris, mangrove, jasmine, tree moss, etc.
4. The granular industrial hemp core material for a cigarette heated without combustion according to claim 1, wherein the excipient is one or more of light calcium carbonate, heavy calcium carbonate, bentonite and diatomaceous earth, and the moisture content of the excipient is controlled to 5-10%.
5. The granular industrial hemp core material for a cigarette to be heated without combustion according to claim 1 or 4, wherein the excipient is in the form of a spindle or a sphere having a particle size of 800 to 4500 mesh.
6. The granular industrial hemp core material for a heat non-combustible cigarette according to claim 1, wherein the binder is one or more of water, ethanol, guar gum, starch gum, chitosan, carboxymethyl cellulose, pectin, acacia gum, sodium alginate, gelatin, glucose, polyallyl alcohol and fructose.
7. The granular industrial hemp core material for a heat non-combustible cigarette according to claim 1, wherein the smoking agent is propylene glycol and/or glycerin.
8. The granular industrial hemp core material for a heat non-combustible cigarette according to claim 1, wherein the perfume is an aromatic plant extract.
9. A method for preparing a granular industrial hemp core material for a cigarette which is not burned by heating according to any one of claims 1 to 8, characterized by comprising the steps of:
s1, processing the industrial hemp raw material: taking industrial hemp raw material with the mass percentage of 0-80%, extracting and concentrating to obtain concentrated extract, and then adjusting the density to 1.0-1.5 g/m by using distilled water3Obtaining a liquid material A; crushing other industrial hemp raw materials to 400-1000 meshes, and spraying water to adjust the water content to 5-10% to obtain powder A;
s2, processing of plant auxiliary materials: taking plant auxiliary materials with the mass percent of 0-100%, extracting and concentrating to obtain a concentrated extract, and then adjusting the density to 1.0-1.5 g/m by using distilled water3Obtaining a liquid material B; crushing the rest plant auxiliary materials to 400-1000 meshes, and spraying water to adjust the water content to 5-10% to obtain powder B;
s3, preparing a solid base material: uniformly mixing the powder A, the powder B and an excipient to obtain a solid base material;
s4, preparing a mixed solution: uniformly mixing the adhesive and the spice, then adding the smoke agent and uniformly mixing, then adding the liquid material A and the liquid material B and uniformly mixing, standing for 2 hours at normal temperature, and filtering by using a 200-mesh filter screen to obtain a mixed solution;
s5, preparing a finished product: granulating the solid base material and the mixed solution to obtain particles with the particle size of 5-200 meshes, drying the particles, adjusting the moisture content of the particles to be below 10%, and screening.
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| WO2022077219A1 (en) * | 2020-10-13 | 2022-04-21 | 深圳市舜宝科技有限公司 | Composition, preparation method, and tea cartridge |
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| CN111480877A (en) * | 2020-04-17 | 2020-08-04 | 云南佩林科技有限公司 | Preparation method of cigarette core material capable of being heated and not combusted |
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