CN108853168A - A kind of perfume (or spice) and preparation method thereof with chrysanthemum perfume - Google Patents

A kind of perfume (or spice) and preparation method thereof with chrysanthemum perfume Download PDF

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CN108853168A
CN108853168A CN201810768986.5A CN201810768986A CN108853168A CN 108853168 A CN108853168 A CN 108853168A CN 201810768986 A CN201810768986 A CN 201810768986A CN 108853168 A CN108853168 A CN 108853168A
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chrysanthemum
perfume
spice
parts
powder
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CN108853168B (en
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王磊
蔡忠弟
江洁
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Chuzhou Vocational and Technical College
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/28Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • A61K36/287Chrysanthemum, e.g. daisy
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/02Inorganic compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/30Macromolecular organic or inorganic compounds, e.g. inorganic polyphosphates
    • A61K47/32Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds, e.g. carbomers, poly(meth)acrylates, or polyvinyl pyrrolidone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/30Macromolecular organic or inorganic compounds, e.g. inorganic polyphosphates
    • A61K47/36Polysaccharides; Derivatives thereof, e.g. gums, starch, alginate, dextrin, hyaluronic acid, chitosan, inulin, agar or pectin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00Medicinal preparations characterised by special physical form
    • A61K9/0012Galenical forms characterised by the site of application
    • A61K9/007Pulmonary tract; Aromatherapy
    • A61K9/0073Sprays or powders for inhalation; Aerolised or nebulised preparations generated by other means than thermal energy
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P11/00Drugs for disorders of the respiratory system
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P27/00Drugs for disorders of the senses
    • A61P27/02Ophthalmic agents
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P29/00Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P9/00Drugs for disorders of the cardiovascular system
    • A61P9/12Antihypertensives

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  • Pharmacology & Pharmacy (AREA)
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Abstract

The invention discloses a kind of perfume (or spice) with chrysanthemum perfume, raw material includes by weight:50-82 parts of chrysanthemum aerial part, 0-20 parts of talcum powder, 0-20 parts of chrysanthemum essence, 4-10 parts of adhesive.The invention also discloses the above-mentioned fragrant preparation methods fragrant with chrysanthemum, include the following steps:Chrysanthemum aerial part dissection is crushed to 80-120 mesh, other surplus stocks are added and are uniformly mixed so as to obtain mixture;It adds water and stirs 45-60min and obtains dough material;It is then pressed into type, dries in the shade to obtain the perfume (or spice) with chrysanthemum perfume, wherein the weight ratio of mixture and water is 1:1-1.5, temperature of drying in the shade are 20-30 DEG C, and the time of drying in the shade is 2-3 days.Faint scent of the present invention overflows, and plays the role of dispelling wind calming the liver, tranquilizing and allaying excitement, antibacterial anti-inflammatory, and anti-folding, can effectively adsorb the fine particle discharged in combustion process.

Description

A kind of perfume (or spice) and preparation method thereof with chrysanthemum perfume
Technical field
The present invention relates to fragrant technical field more particularly to a kind of perfume (or spice) and preparation method thereof with chrysanthemum perfume.
Background technique
Traditional Xiang Gong effect is single.In recent years, have many perfume (or spice) with multiple efficacies to be studied and develop, such as cloud wood Fragrant, suspension culture of Aquilaria sinensis and the perfume (or spice) with green tea feature etc..Chrysanthemum is a kind of compositae plant of dual-purpose of drug and food, is mainly contained in flower and stem There are volatile oil, flavonoids, phenolic acid class isoreactivity substance, the faint scent come out has dispelling wind and heat from the body, calming the liver and improving eyesight, antibacterial The effect of anti-inflammatory and tranquilizing and allaying excitement.To anemopyretic cold, headache and dizziness, red eye, swell pain, eyes is dim-sighted, and hypertension etc. has certain Relaxation effect.
Chuzhou richness produces chrysanthemum, and chrysanthemum is commonly used to watch, and jasmine tea, Chinese medicine is made, or extract the effective component in chrysanthemum, and its Stem, leaf, inferior flower are often dropped, and are easy to produce a large amount of waste pollution environment, or do simple process to stem, leaf Pillow with health role is made, fails the utilization of further progress deep processing development.
Summary of the invention
Technical problems based on background technology, the invention proposes a kind of perfume (or spice) with chrysanthemum perfume and its preparation sides Method, faint scent of the present invention overflow, and play the role of dispelling wind calming the liver, tranquilizing and allaying excitement, antibacterial anti-inflammatory, and anti-folding, can effectively adsorb burned The fine particle discharged in journey.
A kind of perfume (or spice) with chrysanthemum perfume proposed by the present invention, raw material include by weight:Chrysanthemum aerial part 50-82 Part, 0-20 parts of talcum powder, 0-20 parts of chrysanthemum essence, 4-10 parts of adhesive.
Preferably, chrysanthemum aerial part is through shining dry-cure.
Preferably, chrysanthemum aerial part is chrysanthemum stem, the mixture of chrysanthemum stem and florists chrysanthemum leaf, chrysanthemum stem, chrysanthemum One of leaf and the mixture of chrysanthemum piece.
Preferably, adhesive is at least one of starch, guar gum, viscous powder, polyacrylamide.
Preferably, raw material further includes pigment, and the pigment has light yellow, Basic Orange, tea green plain, light green etc..
Preferably, raw material further includes adsorbent, wherein the weight ratio of chrysanthemum stem and adsorbent is 50-82:10-15.
Preferably, adsorbent is modified micaceous powder, straw biological powdered carbon and montmorillonite, wherein modified micaceous powder, stalk are raw Object powdered carbon and the weight ratio of montmorillonite are 1-3:1-2:0.5-1.
Preferably, in the preparation process of modified micaceous powder, it is 1-3wt% Guar glue that mass fraction, which is added, in mica powder It is mixed in solution, is swollen 20-24h, is cooled to -40 to -60 DEG C, vacuum freezedrying 24-36h obtains intermediate material;It will be intermediate Material is added in mass fraction 4-6wt% borax solution and mixes, and stands 10-30min, and washing is cooled to -40 to -60 DEG C, cold Freeze vacuum drying 24-36h, crushing obtains modified micaceous powder.
Preferably, in the preparation process of modified micaceous powder, mica powder, guar gum weight ratio be 7-8:2-3, guar gum The volume ratio of aqueous solution and borax solution is 1-1.5:1.
Preferably, modified micaceous powder is 80-120 mesh, and straw biological powdered carbon is 100-200 mesh, montmorillonite 400-600 Mesh.
The invention also provides the above-mentioned fragrant preparation methods fragrant with chrysanthemum, include the following steps:By chrysanthemum overground part Cutting section is crushed to 80-120 mesh, other surplus stocks are added and are uniformly mixed so as to obtain mixture;It adds water and stirs 45-60min and obtains dough Shape material;It is then pressed into type, dries in the shade to obtain the perfume (or spice) with chrysanthemum perfume, wherein the weight ratio of mixture and water is 1:1-1.5 Temperature of drying in the shade is 20-30 DEG C, and the time of drying in the shade is 2-3 days.
Above-mentioned talcum powder, chrysanthemum essence are food-grade.
The present invention selects chrysanthemum aerial part, chrysanthemum essence to cooperate, so that clear with chrysanthemum after present invention burning Perfume (or spice), faint scent overflow, and play the role of dispelling wind calming the liver, tranquilizing and allaying excitement, antibacterial anti-inflammatory, increase health properties of the invention, suitable house, Office uses;And chrysanthemum stem, florists chrysanthemum leaf, chrysanthemum piece is selected to be used as raw material, it is cheap and easy to get and it can be alleviated to environment Pollution, turns waste into wealth;In addition at least one of starch, guar gum, viscous powder, polyacrylamide are used as adhesive, can make Each substance close adhesion increases anti-folding of the invention, anti-bending strength, improves fragrant the problem of being easily broken off;Because perfume (or spice) is smoulder , in combustion, it is easy release fine particle, influences human health, reduction dispelling wind calming the liver of the present invention, resists tranquilizing and allaying excitement The health-care effect of bacterium anti-inflammatory, the present invention select mica powder, straw biological powdered carbon and montmorillonite to all have good absorption property, cloud Female powder is swollen in aqueous guar glue solution, so that guar gum is coated on mica powder surface and enters mica powder interlayer, then through borax Crosslinking on the surface of mica powder and interlayer is cross-linked into reticular structure, then by vacuum freezedrying on mica powder surface and Interlayer forms porous network structure, greatly increases the absorption property of mica powder, can effectively adsorb the fine particle of burning release, Greatly increase health properties of the invention;Modified micaceous powder, straw biological powdered carbon and montmorillonite are with proper ratio, appropriate particle size phase Mutually cooperation can further increase absorption property of the invention, and can cooperate with adhesive and increase anti-folding of the invention, resist Curved performance.
Specific embodiment
In the following, technical solution of the present invention is described in detail by specific embodiment.
Embodiment 1
A kind of perfume (or spice) with chrysanthemum perfume, raw material include by weight:70 parts of chrysanthemum aerial part, 10 parts of talcum powder, chrysanthemum 10 parts of extrait, 10 parts of adhesive.
The above-mentioned fragrant preparation method fragrant with chrysanthemum, includes the following steps:Chrysanthemum aerial part dissection is crushed to 100 Mesh is added other surplus stocks and is uniformly mixed so as to obtain mixture;It adds water and stirs 53min and obtains dough material;It is then pressed into type, yin The dry perfume (or spice) for obtaining that there is chrysanthemum perfume, wherein the weight ratio of mixture and water is 1:1.25, temperature of drying in the shade is 25 DEG C, is dried in the shade the time It is 3 days.
Embodiment 2
A kind of perfume (or spice) with chrysanthemum perfume, raw material include by weight:Dry 58 parts of chrysanthemum stem, 15 parts of talcum powder, chrysanthemum 20 parts of extrait, 7 parts of polyacrylamide.
The above-mentioned fragrant preparation method fragrant with chrysanthemum, includes the following steps:Dry chrysanthemum stem dissection is crushed to 80 Mesh is added other surplus stocks and is uniformly mixed so as to obtain mixture;It adds water and stirs 60min and obtains dough material;It is then pressed into type, yin The dry perfume (or spice) for obtaining that there is chrysanthemum perfume, wherein the weight ratio of mixture and water is 1:1, temperature of drying in the shade is 20 DEG C, and the time of drying in the shade is 3 It.
Embodiment 3
A kind of perfume (or spice) with chrysanthemum perfume, raw material include by weight:Dry 60 parts of chrysanthemum stem, dry florists chrysanthemum leaf 20 Part, 8 parts of chrysanthemum essence, 10 parts of polyacrylamide, light yellow 2 parts.
The above-mentioned fragrant preparation method fragrant with chrysanthemum, includes the following steps:Dry chrysanthemum stem, dry florists chrysanthemum leaf are cut Section is crushed to 100 mesh, other surplus stocks are added and are uniformly mixed so as to obtain mixture;It adds water and stirs 60min and obtains dough material;Then Compression moulding dries in the shade to obtain the perfume (or spice) with chrysanthemum perfume, wherein the weight ratio of mixture and water is 1:1.2, temperature of drying in the shade is 25 DEG C, the time of drying in the shade is 2 days.
Embodiment 4
A kind of perfume (or spice) with chrysanthemum perfume, raw material include by weight:Dry 36 parts of chrysanthemum stem, dry florists chrysanthemum leaf 46 Part, 10 parts of guar gum, tea green plain 4 parts.
The above-mentioned fragrant preparation method fragrant with chrysanthemum, includes the following steps:Dry chrysanthemum stem, dry florists chrysanthemum leaf are cut Section is crushed to 120 mesh, other surplus stocks are added and are uniformly mixed so as to obtain mixture;It adds water and stirs 45min and obtains dough material;Then Compression moulding dries in the shade to obtain the perfume (or spice) with chrysanthemum perfume, wherein the weight ratio of mixture and water is 1:1.2, temperature of drying in the shade is 30 DEG C, the time of drying in the shade is 2 days.
Embodiment 5
A kind of perfume (or spice) with chrysanthemum perfume, raw material include by weight:Dry 50 parts of chrysanthemum stem, 20 parts of talcum powder, chrysanthemum 10 parts of extrait, 4 parts of polyacrylamide, 10 parts of adsorbent;
Wherein, adsorbent is the modified micaceous powder of 120 mesh, 100 mesh straw biological powdered carbons and 600 mesh montmorillonites, wherein modified The weight ratio of mica powder, straw biological powdered carbon and montmorillonite is 1:2:0.5;
In the preparation process of modified micaceous powder, it is to mix in 3wt% aqueous guar glue solution that mass fraction, which is added, in mica powder It is even, it is swollen 20h, is cooled to -60 DEG C, vacuum freezedrying obtains intermediate material for 24 hours;Mass fraction is added in intermediate material It is mixed in 6wt% borax solution, stands 10min, washing is cooled to -60 DEG C, and for 24 hours, crushing is modified vacuum freezedrying Mica powder, wherein mica powder, guar gum weight ratio be 4:1, the volume ratio of aqueous guar glue solution and borax solution is 1.5: 1。
The above-mentioned fragrant preparation method fragrant with chrysanthemum, includes the following steps:Dry chrysanthemum stem dissection is crushed to 80 Mesh is added other surplus stocks and is uniformly mixed so as to obtain mixture;It adds water and stirs 55min and obtains dough material;It is then pressed into type, yin The dry perfume (or spice) for obtaining that there is chrysanthemum perfume, wherein the weight ratio of mixture and water is 1:1.1, temperature of drying in the shade is 28 DEG C, and the time of drying in the shade is 2 days.
Embodiment 6
A kind of perfume (or spice) with chrysanthemum perfume, raw material include by weight:Dry 60 parts of chrysanthemum aerial part, talcum powder 15 Part, 5 parts of chrysanthemum essence, 9 parts of adhesive, 15 parts of adsorbent;
Wherein, chrysanthemum aerial part is the mixture of chrysanthemum stem, florists chrysanthemum leaf and chrysanthemum piece;
Adhesive is starch, viscous powder and polyacrylamide;
Adsorbent is the modified micaceous powder of 80 mesh, 200 mesh straw biological powdered carbons and 400 mesh montmorillonites, wherein modified micaceous The weight ratio of powder, straw biological powdered carbon and montmorillonite is 3:1:1;
In the preparation process of modified micaceous powder, it is to mix in 1wt% aqueous guar glue solution that mass fraction, which is added, in mica powder Even, swelling for 24 hours, is cooled to -40 DEG C, vacuum freezedrying 36h obtains intermediate material;Mass fraction is added in intermediate material It is mixed in 4wt% borax solution, stands 30min, washing is cooled to -40 DEG C, vacuum freezedrying 36h, and crushing is modified Mica powder, wherein mica powder, guar gum weight ratio be 7:3, the volume ratio of aqueous guar glue solution and borax solution is 1:1.
The above-mentioned fragrant preparation method fragrant with chrysanthemum, includes the following steps:Dry chrysanthemum aerial part dissection is crushed To 120 mesh, other surplus stocks are added and are uniformly mixed so as to obtain mixture;It adds water and stirs 50min and obtains dough material;It is then pressed into Type dries in the shade to obtain the perfume (or spice) with chrysanthemum perfume, wherein the weight ratio of mixture and water is 1:1.4, temperature of drying in the shade is 25 DEG C, is dried in the shade Time is 3 days.
Test example 1
Embodiment 5, embodiment 6 are tested for the property, it is as a result as follows:
Detection project Fracture resistence force g Water content % Fume amount mg/g Fragrance
Embodiment 5 461 4.5 2.5 Chrysanthemum faint scent
Embodiment 6 463 4.0 2.6 Chrysanthemum faint scent
Fracture resistence force of the present invention is high as can be seen from the above table, and fume amount is few after burning, has chrysanthemum faint scent.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto, Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.

Claims (10)

1. a kind of perfume (or spice) with chrysanthemum perfume, which is characterized in that its raw material includes by weight:It is 50-82 parts of chrysanthemum aerial part, sliding 0-20 parts of mountain flour, 0-20 parts of chrysanthemum essence, 4-10 parts of adhesive.
2. according to claim 1 with the perfume (or spice) of chrysanthemum perfume, which is characterized in that chrysanthemum aerial part is through shining dry-cure.
3. the perfume (or spice) according to claim 1 or claim 2 with chrysanthemum perfume, which is characterized in that chrysanthemum aerial part is chrysanthemum stem, chrysanthemum The mixture of scape bar and florists chrysanthemum leaf, one of chrysanthemum stem, florists chrysanthemum leaf and mixture of chrysanthemum piece.
4. according to claim 1 described in -3 any one with chrysanthemum perfume perfume (or spice), which is characterized in that adhesive be starch, guar gum, At least one of viscous powder, polyacrylamide;Preferably, raw material further includes pigment.
5. according to claim 1 with the perfume (or spice) of chrysanthemum perfume described in -4 any one, which is characterized in that its raw material further includes adsorbent, Wherein, the weight ratio of chrysanthemum aerial part and adsorbent is 50-82:10-15.
6. according to claim 5 with the perfume (or spice) of chrysanthemum perfume, which is characterized in that adsorbent is modified micaceous powder, straw biological Powdered carbon and montmorillonite, wherein the weight ratio of modified micaceous powder, straw biological powdered carbon and montmorillonite is 1-3:1-2:0.5-1.
7. according to claim 6 with the perfume (or spice) of chrysanthemum perfume, which is characterized in that, will in the preparation process of modified micaceous powder It is to mix in 1-3wt% aqueous guar glue solution that mass fraction, which is added, in mica powder, is swollen 20-24h, is cooled to -40 to -60 DEG C, cold Freeze vacuum drying 24-36h and obtains intermediate material;Intermediate material is added in mass fraction 4-6wt% borax solution and is mixed, it is quiet 10-30min is set, is washed, is cooled to -40 to -60 DEG C, vacuum freezedrying 24-36h, crushing obtains modified micaceous powder.
8. according to claim 7 with the perfume (or spice) of chrysanthemum perfume, which is characterized in that in the preparation process of modified micaceous powder, cloud Female powder, the weight ratio of guar gum are 7-8:The volume ratio of 2-3, aqueous guar glue solution and borax solution is 1-1.5:1.
9. with the perfume (or spice) of chrysanthemum perfume according to claim any one of 6-8, which is characterized in that modified micaceous powder is 80-120 Mesh, straw biological powdered carbon are 100-200 mesh, and montmorillonite is 400-600 mesh.
10. a kind of preparation method with the fragrant perfume of chrysanthemum as described in claim any one of 1-9, which is characterized in that including such as Lower step:Chrysanthemum aerial part dissection is crushed to 80-120 mesh, other surplus stocks are added and are uniformly mixed so as to obtain mixture;Water is added to stir It mixes 45-60min and obtains dough material;It is then pressed into type, dries in the shade to obtain the perfume (or spice) with chrysanthemum perfume, wherein mixture and water Weight ratio be 1:1-1.5, temperature of drying in the shade are 20-30 DEG C, and the time of drying in the shade is 2-3 days.
CN201810768986.5A 2018-07-13 2018-07-13 Incense with chrysanthemum fragrance and preparation method thereof Active CN108853168B (en)

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CN111135795A (en) * 2020-01-21 2020-05-12 温州子久堂生物科技有限公司 Preparation method and application of adsorption material for gardenia essential oil head fragrance extraction
CN113425880A (en) * 2021-04-29 2021-09-24 河北古城香业集团股份有限公司 Environment-friendly smokeless incense and preparation method thereof
CN114470288A (en) * 2022-03-14 2022-05-13 浙江宋朝臻选科技有限公司 Fragrance with relieving effect and preparation method thereof

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111135795A (en) * 2020-01-21 2020-05-12 温州子久堂生物科技有限公司 Preparation method and application of adsorption material for gardenia essential oil head fragrance extraction
CN113425880A (en) * 2021-04-29 2021-09-24 河北古城香业集团股份有限公司 Environment-friendly smokeless incense and preparation method thereof
CN114470288A (en) * 2022-03-14 2022-05-13 浙江宋朝臻选科技有限公司 Fragrance with relieving effect and preparation method thereof
CN114470288B (en) * 2022-03-14 2023-08-22 浙江宋朝臻选科技有限公司 Fragrance with relieving effect and preparation method thereof

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