CN111150108B - Functional barrier sheet for heating non-combustible cigarettes and preparation method and application thereof - Google Patents
Functional barrier sheet for heating non-combustible cigarettes and preparation method and application thereof Download PDFInfo
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- CN111150108B CN111150108B CN202010050328.XA CN202010050328A CN111150108B CN 111150108 B CN111150108 B CN 111150108B CN 202010050328 A CN202010050328 A CN 202010050328A CN 111150108 B CN111150108 B CN 111150108B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F47/00—Smokers' requisites not otherwise provided for
Abstract
The functional barrier sheet is placed in a cigarette bullet of the heating non-combustion cigarette and is arranged close to a smoke particle section, and the functional barrier sheet comprises a functional material, a binder, an excipient and a wetting agent. The barrier sheet is applied to the cigarette bullet of the non-burning cigarette, has good supporting effect on the fuming particle section, and can achieve the effects of improving the smoke concentration, enhancing the satisfaction, enriching the cigarette fragrance and improving the smoking quality.
Description
Technical Field
The invention relates to the technical field of auxiliary materials of cigarette cartridges for heating non-combustion cigarettes.
Background
In recent years, the heated non-burning cigarettes have shown a rapidly increasing trend in the tobacco sales market. The heating non-combustible cigarette cartridge mainly comprises a cigarette cartridge based on paper hollow pipe integrated molding and a multi-section combined type cigarette cartridge, and the structural forms of the two kinds of cigarette cartridges are respectively composed of a smoking section, a supporting section, a cooling section and a filtering section. Wherein the supporting section mainly adopts a hollow paper tube, a hollow polyethylene tube or a hollow polyvinyl chloride tube and the like. A non-combustible heated cigarette product features that an external heat source is used to heat the tobacco sheets or particles to be smoked at 400 deg.C or lower. At present, the main means for improving the smoking quality of the non-burning heated cigarette is to adjust the tobacco sheets and the smoking particles of the smoking section or add the particles, the bead blasting and the like into the filter section. Chinese patent CN 109363230A discloses a heating non-combustion cigarette smoking particle material and a preparation method thereof, wherein the particle material comprises a heating non-combustion particle material carrier, a smoking agent, a surface wrapping agent and a fragrance-emitting extract, and a smoking unit finished product is mixed with smoking agents with different flavor fragrance-emitting components, so that the problems of single type of smoke cartridge and complex processing technology in the field of heating non-combustion are solved. Chinese patent CN110169606A discloses a heating non-combustion fuming particle and a preparation method and application thereof, wherein the fuming particle is prepared by uniformly mixing plant porous expanded particles with the mesh number of 30-40, water and plant extracts, when the fuming particle is heated to 300-350 ℃, fuming can be carried out, the smoke amount is close to that of a traditional cigarette, the smoke amount is stable, and the smoking sense organ comfort degree is good. Chinese patent CN1099998160A discloses a cigarette which is not combusted by heating, the pipe wall of a supporting element can rebound after passing through a cutter, the adaptability of the supporting element on a machine is high, the production efficiency and the product quality of the cigarette can be improved, the supporting element is not easy to collapse, and the supporting performance of the cigarette is high. However, the prior art has a single function, or only can improve the smoking quality, or only can improve the cigarette supporting performance, and cannot meet the requirements of not only improving the smoking quality but also improving the supporting performance of the cigarette cartridge supporting section, which are required in the development of heating non-burning cigarettes.
Disclosure of Invention
The invention aims to make up the vacancy in the prior art and provide a functional barrier sheet which has the function of a supporting section and can improve the smoking quality and is used for heating non-combustible cigarettes.
The purpose of the invention is realized by the following technical scheme:
a functional barrier for heating a non-combustible cigarette, the barrier being disposed in a heated non-combustible cigarette cartridge proximate to a smoking particle segment, the functional barrier comprising a functional material, a binder, an excipient, and a wetting agent.
The dosage of the binder is not more than 20% of the mass of the functional material, and the dosage of the excipient is not more than 5% of the mass of the functional material.
The functional material is one or more of inorganic mineral material, plant material and tobacco material with the particle size of less than 80 meshes. The inorganic mineral material is one or more of molecular sieve, diatomite and montmorillonite. The plant material is one or more of fructus Siraitiae Grosvenorii, radix Puerariae, pericarpium Citri Tangerinae, radix Ophiopogonis, and Ginseng radix.
The dosage of the wetting agent is 0.6 to 1.2 times of the mass of the mixture of the functional material, the binder and the excipient.
The wetting agent is one or more of water, natural plant extract water solution, glycerin water solution and propylene glycol water solution. The natural plant extract is one or more of fructus Phyllanthi, lemon balm, herba Menthae and fructus Lycii.
The functional barrier sheet also contains characteristic essence, wherein the characteristic essence is oil-soluble essence and is one or more of dried orange peel essence, juicy peach essence, milk essence, mint essence and Hami melon essence.
The preparation method of the functional barrier sheet for heating non-combustible cigarettes comprises the following steps:
(1) Uniformly mixing the functional material, the binder and the excipient;
(2) Adding a wetting agent into the mixture of the functional material, the binder and the excipient to prepare a soft material;
(3) Embedding the soft material into a mold in an extrusion forming mode, drying the mold embedded with the soft material at 80-100 ℃ for 1-2h, cooling the dried and formed soft material, and then demolding to obtain the functional barrier sheet.
The functional barrier sheet can also be subjected to characteristic fragrance loading to obtain the characteristic fragrance functional barrier sheet.
The functional barrier sheet can be used in a cigarette cartridge or a multi-section combined type cigarette cartridge which is integrally formed based on a paper hollow tube.
Compared with the prior art, the invention has the following advantages:
(1) The invention provides a brand new method for improving the supporting performance of a cigarette bullet supporting section.
(2) The functional barrier sheet prepared by the invention has good supporting effect, can load water-soluble essence and oil-soluble essence at the same time, can obviously enrich the cigarette fragrance, improve the satisfaction, improve the smoke fineness and improve the smoking quality of the heated non-combustible cigarette;
(3) The production and preparation method of the functional barrier sheet is simple, has strong operability and standardability, is convenient for realizing industrial production, and has good application prospect.
Drawings
Figure 1 is a schematic view of the present invention disposed in a heated non-combustible cigarette cartridge.
In the figure, 1 is a smoke particle section, 2 is a functional barrier section, 3 is a hollow section, and 4 is a filtering section.
Detailed Description
The present invention is further illustrated by the following examples, which are not intended to be limiting in any way, and any alterations and modifications based on the teachings of the present invention are intended to fall within the scope of the present invention.
A functional barrier for heating a non-combustible cigarette, the barrier being disposed in a heated non-combustible cigarette cartridge proximate to a smoking particle segment, the functional barrier comprising a functional material, a binder, an excipient, and a wetting agent.
The dosage of the binder is not more than 20% of the mass of the functional material, and the dosage of the excipient is not more than 5% of the mass of the functional material.
The functional material is one or more of inorganic mineral materials with the grain size of less than 80 meshes, plant materials and tobacco materials. The inorganic mineral material is one or more of molecular sieve, diatomite and montmorillonite. The plant material is one or more of fructus Siraitiae Grosvenorii, radix Puerariae, pericarpium Citri Tangerinae, radix Ophiopogonis, and Ginseng radix. The tobacco raw material is one or two of tobacco leaves and tobacco stems.
The binder used in the invention is a binder commonly used in food and medicine production, such as povidone, hypromellose, sodium carboxymethylcellulose and the like.
The excipient used by the invention is microcrystalline cellulose, calcium sulfate, mannitol and the like.
The dosage of the wetting agent is 0.6 to 1.2 times of the mass of the mixture of the functional material, the binder and the excipient. The wetting agent is one or more of water, natural plant extract water solution, glycerin water solution and propylene glycol water solution. The natural plant extract is one or more of fructus Phyllanthi, lemon balm, herba Menthae and fructus Lycii.
The functional barrier sheet also contains characteristic essence, wherein the characteristic essence is oil-soluble essence, such as one or more of tangerine peel essence, juicy peach essence, milk essence, mint essence and Hami melon essence.
The preparation method of the functional barrier sheet for heating non-combustible cigarettes comprises the following steps:
(1) Uniformly mixing a functional material, a binder and an excipient; the dosage of the binder is not more than 20% of the mass of the functional material, and the dosage of the excipient is not more than 5% of the mass of the functional material;
(2) Adding a wetting agent with the weight 0.6-1.2 times of that of the mixture into the mixture of the functional material, the binder and the excipient to prepare a soft material;
(3) Embedding the soft material into a mold in an extrusion forming mode, drying the mold embedded with the soft material at 80-100 ℃ for 1-2h, cooling the dried and formed soft material, and then demolding to obtain the functional barrier sheet.
The functional barrier sheet prepared by the method can be further subjected to characteristic fragrance loading to obtain the characteristic fragrance functional barrier sheet. The characteristic perfume loading method can adopt the prior art method.
The functional barrier sheet can be used in the prior art of integrally formed cigarettes based on paper hollow tubes or multi-section composite cigarettes. Fig. 1 shows the situation that the functional barrier sheet 2 is placed in the cigarette cartridge integrally formed by the paper hollow tube, the cigarette cartridge integrally formed by the paper hollow tube comprises a smoking particle section 1, a hollow section 3 and a filter section 4 which are connected in sequence, and the functional barrier sheet 2 is placed between the smoking particle section 1 and the hollow section 3 and is close to the smoking particle section.
Example 1
Weighing 80g of molecular sieve powder, 20g of fructus momordicae powder, 10g of dried orange peel powder, 5g of sodium carboxymethylcellulose and 1g of microcrystalline cellulose, and uniformly mixing. Weighing 10g of lemon balm extract, 90g of water, 1g of glycerol and 5g of propylene glycol, and uniformly mixing the lemon balm extract, the water, the glycerol and the propylene glycol with the mixed powder to prepare a soft material. And embedding the soft material into a mold in an extrusion forming mode, drying in an oven at 80 ℃ for 2h, cooling and demolding to obtain the functional barrier sheet with the diameter of 5.2 mm.
Example 2
Weighing 30g of molecular sieve powder, 70g of tobacco powder, 8g of hydroxypropyl methylcellulose and 2g of microcrystalline cellulose, and uniformly mixing. Weighing 20g of mint extract, 80g of water, 2g of glycerol and 8g of propylene glycol, and uniformly mixing the mint extract, the water, the glycerol and the propylene glycol with the mixed powder to prepare a soft material. And embedding the soft material into a mold in an extrusion forming mode, drying in a drying oven at 90 ℃ for 1.5h, cooling and demolding to obtain the functional barrier sheet with the diameter of 5.3 mm.
Example 3
Weighing 90g of diatomite powder, 10g of kudzu root powder, 13g of sodium carboxymethylcellulose and 3g of calcium sulfate, and uniformly mixing. Weighing 15g of fructus phyllanthi extract, 110g of water, 2g of glycerol and 8g of propylene glycol, and uniformly mixing with the mixed powder to prepare a soft material. And embedding the soft material into a mold in an extrusion forming mode, drying in a drying oven at 100 ℃ for 1h, cooling and demolding to obtain the functional barrier sheet with the diameter of 6.9 mm.
Example 4
Weighing 70g of diatomite powder, 10g of radix ophiopogonis powder, 20g of ginseng powder, 18g of povidone and 5g of microcrystalline cellulose, and uniformly mixing. Weighing 10g of the medlar extract, 100g of water, 2g of glycerol and 5g of propylene glycol, and uniformly mixing the medlar extract, the water, the glycerol and the propylene glycol with the mixed powder to prepare a soft material. And embedding the soft material into a mold in an extrusion forming mode, drying in a drying oven at 100 ℃ for 1h, cooling and demolding to obtain the functional barrier sheet with the diameter of 7.0 mm.
Example 5
Weighing 100g of molecular sieve powder, 20g of sodium carboxymethylcellulose and 5g of mannitol, and uniformly mixing. Weighing 100g of water, 1g of glycerol and 5g of propylene glycol, and uniformly mixing the water, the glycerol and the propylene glycol with the mixed powder to prepare a soft material. Embedding the soft material into a mold in an extrusion forming mode, drying for 1h in a drying oven at 100 ℃, demolding after cooling, and then negatively spraying 5% of oil-soluble tangerine peel essence on the demolded barrier sheet to obtain the functional barrier sheet with the diameter of 5.2 mm.
Example 6
Weighing 100g of molecular sieve powder, 20g of polyvidone and 5g of microcrystalline cellulose, and uniformly mixing. 75g of water, 1g of glycerol and 1g of propylene glycol are uniformly mixed with the mixed powder to prepare a soft material. Embedding the soft material into a mold in an extrusion forming mode, drying for 1h in a drying oven at 100 ℃, cooling, demolding, and then spraying 10% of oil-soluble juicy peach essence on the demolded barrier sheet to obtain the functional barrier sheet with the diameter of 6.9 mm.
Example 7
Weighing 110g of diatomite powder, 20g of sodium carboxymethylcellulose and 5g of calcium sulfate, and uniformly mixing. Weighing 90g of water, 1g of glycerol and 2g of propylene glycol, and uniformly mixing the water, the glycerol and the propylene glycol with the mixed powder to prepare a soft material. Embedding the soft material into a mold in an extrusion forming mode, drying in a drying oven at 100 ℃ for 1h, demolding after cooling, and then spraying 8% of milk flavor negatively onto the demolded barrier sheet to obtain the functional barrier sheet with the diameter of 7.0 mm.
Example 8
Weighing 115g of montmorillonite powder, 20g of sodium carboxymethylcellulose and 5g of microcrystalline cellulose, and uniformly mixing. Weighing 90g of water, 1g of glycerol and 1g of propylene glycol, and uniformly mixing the water, the glycerol and the propylene glycol with the mixed powder to prepare a soft material. Embedding the soft material into a mold in an extrusion forming mode, drying for 1h in a drying oven at 100 ℃, demolding after cooling, and then negatively spraying 6% Hami melon essence on the demolded barrier sheet to obtain the functional barrier sheet with the diameter of 7.1 mm.
Sensory quality evaluation was performed by putting the functional barrier sheets prepared in examples 1 to 8 into a non-burning heated cigarette pack, and sensory quality evaluation results are shown in fig. 1 with respect to the case where the functional barrier sheet was not added. As can be seen from table 1, the sensory quality of smoking a non-burning cigarette is significantly improved after the functional barrier sheet of the present invention is disposed in a heated non-burning cigarette cartridge. Production trial production also proves that after the functional barrier sheet, the support performance of the cigarette bullet support section is obviously improved, and the product quality is improved.
TABLE 1 sensory evaluation results
| Name (R) | Sensory quality evaluation results |
| Control of | The cigarette has flat and light fragrance and poor richness |
| Example 1 | The sample cigarette has sweet fragrance, good richness and clean aftertaste |
| Example 2 | The sample has strong fragrance, good satisfaction and clean aftertaste |
| Example 3 | The sample has fine and smooth tobacco fragrance, good harmony and clean aftertaste |
| Example 4 | The sample has clear cigarette fragrance, good comfort and clean aftertaste |
| Example 5 | The cigarette fragrance is clear, and the characteristic of the dried orange peel fragrance is obvious |
| Example 6 | The cigarette fragrance is clear, and the honey peach fragrance is relatively obvious in characteristic |
| Example 7 | The cigarette fragrance is clear, and the milk fragrance characteristic is obvious |
| Example 8 | Clear cigarette fragrance, hami melon fragranceIs marked more obviously |
Claims (9)
1. A functional barrier sheet for heating a non-combustible cigarette, wherein the barrier sheet is disposed in a heated non-combustible cigarette cartridge proximate to a smoker particle segment, the functional barrier sheet comprising a functional material, a binder, an excipient, and a wetting agent; the functional material is one or more of an inorganic mineral material, a plant material and a tobacco material with the grain size of less than 80 meshes; the method of making the functional barrier sheet is as follows:
(1) Uniformly mixing a functional material, a binder and an excipient;
(2) Adding a wetting agent into the mixture of the functional material, the binder and the excipient to prepare a soft material;
(3) And embedding the soft material into a mold in an extrusion molding manner, drying the mold embedded with the soft material at 80-100 ℃ for 1-2h, cooling the dried and molded soft material, and demolding to obtain the functional barrier sheet.
2. The functional barrier sheet for heating non-combustible cigarettes according to claim 1, characterized in that: the dosage of the binder is not more than 20% of the mass of the functional material, and the dosage of the excipient is not more than 5% of the mass of the functional material.
3. The functional barrier sheet for heating non-combustible cigarettes according to claim 1, characterized in that: the inorganic mineral material is one or more of molecular sieve, diatomite and montmorillonite.
4. The functional barrier sheet for heating non-combustible cigarettes according to claim 1, characterized in that: the plant material is one or more of fructus Siraitiae Grosvenorii, radix Puerariae, pericarpium Citri Tangerinae, radix Ophiopogonis, and Ginseng radix.
5. The functional barrier sheet for heating non-combustible cigarettes according to claim 1, characterized in that: the dosage of the wetting agent is 0.6 to 1.2 times of the mass of the mixture of the functional material, the binder and the excipient.
6. The functional barrier sheet for heating non-combustible cigarettes according to claim 5, characterized in that: the wetting agent is one or more of water, natural plant extract water solution, glycerol water solution and propylene glycol water solution.
7. The functional barrier sheet for heating non-combustible cigarettes according to claim 6, characterized in that: the natural plant extract is one or more of fructus Phyllanthi, lemon balm, herba Menthae and fructus Lycii.
8. The functional barrier sheet for heating non-combustible cigarettes according to any one of claims 1 to 7, characterized in that: the functional barrier sheet also contains characteristic essence, wherein the characteristic essence is oil-soluble essence and is one or more of pericarpium citri reticulatae essence, juicy peach essence, milk essence, mint essence and Hami melon essence.
9. Use of a functional barrier sheet for heating a non-combustible cigarette according to any one of claims 1 to 8, wherein: the functional barrier sheet is used in a cigarette cartridge or a multi-section combined type cigarette cartridge which is integrally formed based on a paper hollow tube.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111567870B (en) * | 2020-06-02 | 2023-05-30 | 四川三联新材料有限公司 | Flavoring and moisturizing tube for heating cigarettes and preparation method thereof |
| CN111728267A (en) * | 2020-07-04 | 2020-10-02 | 上海华宝生物科技有限公司 | Heating cigarette, plant firmware and manufacturing method thereof |
| CN112341134B (en) * | 2020-11-10 | 2021-11-12 | 中南大学 | Heat insulation material for heating non-combustible appliance and preparation method and application thereof |
| CN114158767B (en) * | 2021-12-22 | 2024-03-26 | 安徽中烟工业有限责任公司 | Bio-based firmware material for granular heating cigarette and preparation method thereof |
| CN114158766B (en) * | 2021-12-22 | 2024-02-23 | 安徽中烟工业有限责任公司 | Biodegradable firmware material for granular heating cigarettes and preparation method thereof |
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