CN105725258A - Fragrant microcapsule for composite cigarettes and preparation method and application thereof - Google Patents
Fragrant microcapsule for composite cigarettes and preparation method and application thereof Download PDFInfo
- Publication number
- CN105725258A CN105725258A CN201610104050.3A CN201610104050A CN105725258A CN 105725258 A CN105725258 A CN 105725258A CN 201610104050 A CN201610104050 A CN 201610104050A CN 105725258 A CN105725258 A CN 105725258A
- Authority
- CN
- China
- Prior art keywords
- microcapsule
- rhodinol
- essence
- composite smoke
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
- B01J13/04—Making microcapsules or microballoons by physical processes, e.g. drying, spraying
- B01J13/043—Drying and spraying
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
- C11B9/003—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing less than six carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0042—Essential oils; Perfumes compounds containing condensed hydrocarbon rings
Abstract
The invention discloses a fragrant microcapsule for composite cigarettes.A nucleus of the microcapsule is prepared from novel methyl hesperidin dihydro chalcone, rhodinol and rhodinol-beta-D-glucopyranoside.A shell of the microcapsule is prepared from chitosan.The invention further discloses a preparation method of the fragrant microcapsule for composite cigarettes and application for increasing fragrance of cigarettes.The fragrant microcapsule for composite cigarettes can keep cigarette fragrance stability, durability and uniformity consistency of fragrance release along with time.
Description
Technical field
The invention belongs to the technical field that composite smoke essence microcapsule is applied in Medicated cigarette field, be specifically related to one
Plant composite smoke essence microcapsule, its preparation method and the application in Medicated cigarette.
Background technology
In medicated cigarette, essence and flavoring agent can play the effect improving captivation, boosting consumption, thus is in tobacco industry
An indispensable part.But owing to fragrance material major part is that molecular weight is relatively low, boiling point is low, volatility is stronger
Compound, in high temperature working processes, loss is serious, causes releasing fragrant uneven phenomenon, even during storing
Because volatilization loses fragrance, or unstable chemcial property is easy to be oxidized rotten.Research finds, though essence loss
The volatile matter of 2% also results in odor type and changes, and makes the quality of medicated cigarette be greatly affected.
High temperature resistant and the long-acting problem of flavouring essence for tobacco, major issue always urgently to be resolved hurrily in tobacco aromatics using industry.
The sixties in last century begin, and increasing producer begins to focus on how to overcome these shortcomings, and has some new
Fragrance product obtains development and application, is effectively improved the heat stability of spice, significantly improves perfuming effect,
Drastically increase value-added content of product, but still the requirement to thermostable type essence can not be met.
Microencapsulation technology is by the various natural or macromolecule of synthesis of a certain goal object (core or internal phase)
Compound continuous film (wall or foreign minister or shell) is coated with to get up to form nucleocapsid structure completely, and to goal object
Original chemical property is unaffected, then makes the merit of goal object increasingly by some outside stimulus or slow releasing function
Can again present in outside.The outer wall thin film (shell) of microcapsule prevents effective aroma component (core
Or internal phase or stratum nucleare) scatter and disappear, apply certain technological means to process capsule and can reach slow release or fixed point is released
The effect put；Liquid essence is changed into the pressed powder of microcapsule so that it is more convenient in processing uses,
Greatly reduce the consumption of essence；Reduce fragrance material to contact with extraneous, prevent volatilization and loss etc., improve
The stability of fragrance material.
Therefore, use microcapsule embedded technology to compound and can the sweet taste essence of flavouring essence for tobacco potentiation be added thermally-stabilised
Glucosides class fragrance precursor, the novel flavouring essence for tobacco of exploitation be widely used in medicated cigarette produce in, reach improve medicated cigarette
The purpose of the uniformity consistency of the stability of fragrance, persistency and/or fragrance release.
Summary of the invention
The present invention, for overcoming loss in fragrance material high temperature working processes serious, causes releasing fragrant non-uniform phenomenon, very
Lose fragrance to during storing because of volatilization, or unstable chemcial property is easy to be oxidized rotten and propose, this
Invention uses microencapsulation technology to prepare composite smoke essence microcapsule, and flavouring in Medicated cigarette, can keep
The stability of cigarette flavor, persistency and/or the uniformity consistency of fragrance release.
A first aspect of the present invention relates to a kind of composite smoke essence microcapsule, wherein the core of microcapsule or internal phase
Or stratum nucleare includes new hesperidin methyl dihydrochalcone, rhodinol and rhodinol-β-D-pyranglucoside, micro-
The macromolecular compound continuous film (wall or foreign minister or shell) of capsule completely encasement core or internal phase or stratum nucleare,
Preferably macromolecular compound is chitosan.
Preferably, the weight portion of each composition of composite smoke essence microcapsule of the present invention is: new hesperidin methyl two
Hydrogen chalcone 1～5 parts, rhodinol 50～70 parts, rhodinol-β-D-pyranglucoside 10～25, chitosan
35～40.
A second aspect of the present invention is the preparation method of composite smoke essence microcapsule, comprises the steps:
(1) new hesperidin methyl dihydrochalcone, rhodinol, rhodinol-β-D-glucopyra are weighed in proportion
Glucosides and emulsifying agent solids granule mix homogeneously obtain mixture；
(2) weighing chitosan solid granule to be dissolved in glacial acetic acid aqueous solution, preparation obtains the shell of 1%～4% and gathers
Sugar juice；
(3) mixture of described step (1) is joined in the solution of step (2), stir newborn
Liquid；
(4) aqueous solution of sodium hydroxide is sprayed by the emulsion of step (3), solution occurs solidification
Little granule；
(5) product of step (4) is carried out ultra-filtration filters；
(6) filtration product of step (5) is carried out microwave vacuum drying, i.e. obtain described compound flavouring essence for tobacco
Microcapsule.Product carries out pack packaging, can be as commodity selling.
Preferably, the addition of the emulsifying agent of above-mentioned steps (1) is new hesperidin methyl dihydrochalcone, rose
Rare alcohol, rhodinol-β-D-pyranglucoside and the 1 of emulsifying agent gross weight～5%；Described glacial acetic acid aqueous solution
Concentration be 1wt%, the pH value of described sodium hydrate aqueous solution is 7.5～8.0.
The emulsifying agent of above-mentioned steps (1) is that food service industry commonly uses emulsifying agent, as glyceryl monostearate is (single sweet
Fat), sucrose stearate C 1811 etc..
Preferably, the vacuum of above-mentioned steps (6) microwave vacuum drying is 0.080～0.095MPa, microwave
Power is 8～12W/g.
Third aspect present invention is that composite smoke essence microcapsule is for the purposes to Medicated cigarette flavouring.In using, can
This composite smoke essence microcapsule is added in cigarette shreds with flavouring.Preferably, this compound flavouring essence for tobacco is micro-
Capsule addition in Medicated cigarette is 0.1%～0.5% of the weight relative to tobacco shred.
A fourth aspect of the present invention is composite smoke essence microcapsule for keeping the stability, persistently of cigarette flavor
Property and/or the purposes of fragrance release uniformity consistency in time.
Beneficial effects of the present invention:
1, new hesperidin methyl dihydrochalcone is used as the compound micro-glue of flavouring essence for tobacco with remaining combinations of perfumes
The core of capsule, unexpectedly serves the effect reducing miscellaneous QI, improving pleasant impression, and decreases the usage amount of flavouring essence for tobacco.
New hesperidin methyl dihydrochalcone is a kind of sweeting agent being conventionally used in Food & Drink industry, mainly exists
Act on tongue under room temperature to produce sweet taste, the most never instruct it can act on nose after being heated through burning
Son plays the effect reducing miscellaneous QI, improving pleasant impression.
2, the rhodinol-β-D-pyranglucoside molecular weight that the present invention selects is relatively big, boiling point is higher, fragrance relatively
Less or itself do not have fragrance, but can discharge provide through high-temperature heating or burning cracking after adding Medicated cigarette as spice
There is the compound of fragrance fragrance, increase the fragrance of product.This compensate for effectively because cigarette combustion causes a large amount of normal
Rule spice volatilizees and makes the defect of cigarette combustion later stage insufficient fragrance.
3, chitosan is as shell, prevents the volatilization loss of each fragrance component.By adjusting chitosan shell
Thickness, it is also possible to adjust it and by the temperature of thermal fracture and rupture opportunity, adjusts fragrance release profile.
Accompanying drawing explanation
Fig. 1 is the preparation technology flow chart of the composite smoke essence microcapsule of the present invention.
Detailed description of the invention
The composite smoke essence microcapsule using the present invention adds in cigarette shreds, with the common flavouring essence for tobacco of interpolation
Medicated cigarette compare, choose 6 professionals and carry out scoring of smokeing panel test, appraisal result is as shown in table 1, standards of grading
As shown in table 2.
Table 1 adds medicated cigarette and the interpolation of composite smoke essence microcapsule (embodiment)
The sensory evaluation scores contrast of the medicated cigarette of common flavouring essence for tobacco (comparative example)
Table 2 Medicated cigarette Sensory quality index and standards of grading
As it can be seen from table 1 use the composite smoke essence microcapsule of the present invention to be applied to perfuming cigarette, and add
The Medicated cigarette comparison adding common flavouring essence for tobacco is compared, and fragrance is good, perfume quantity is sufficient, almost without miscellaneous QI, and good after-taste,
Most importantly fragrance is lasting, good stability, starts suction from lighting medicated cigarette, and to last after-flame, fragrance discharges
Uniform and stable, concordance is good, and comprehensive grading is better than adding the Medicated cigarette of common flavouring essence for tobacco, achieves expectation not
The effect arrived.
Using the composite smoke essence microcapsule of the present invention, during medicated cigarette long-term storage, fragrance is still stable
Persistently, the medicated cigarette of long-term storage, during burning and sucking, fragrance is uniform and stable from the beginning to the end, releases fragrant uniform.And
The then volatile aroma loss during medicated cigarette is deposited of common flavouring essence for tobacco, forms above fragrance dense during burning and sucking,
The phenomenon that fragrance is boring below, and during burning and sucking, owing to flue-gas temperature is high, make essence volatilization loss fast,
There is also above fragrance dense, after the boring phenomenon of fragrance.
Use the composite smoke essence microcapsule of the present invention, the consumption of flavouring essence for tobacco can be reduced, improve essence
Flavouring essence quality, reduces production cost.Compound essence with the addition of rhodinol-β-D-pyranglucoside, be one
Planting the sweeting agent being usually used in Food & Drink industry, present inventors have surprisingly found that, it can be when burning and sucking medicated cigarette
Discharge fragrance, and fragrance is lasting, play the synergism of fragrance with other essence.
Use microcapsule embedded technology, compound essence ratio uniform can be made, also to a certain degree improve essence
Stability.Use NEW TYPE OF COMPOSITE microcapsule essence, significantly improve the aroma quality of medicated cigarette.The present invention is by right
Improve cigarette quality, promote the development of tobacco business, significant.
Claims (7)
1. a composite smoke essence microcapsule, it is characterised in that: the core of microcapsule includes new hesperidin methyl
Dihydrochalcone, rhodinol and rhodinol-β-D-pyranglucoside, the shell of microcapsule includes chitosan.
Composite smoke essence microcapsule the most according to claim 1, it is characterised in that compound flavouring essence for tobacco is micro-
The weight portion of each composition of capsule is: new hesperidin methyl dihydrochalcone 1～5 parts, rhodinol 50～70 parts, rose
Rare alcohol-β-D-pyranglucoside 10～25, chitosan: 35～40.
The preparation method of composite smoke essence microcapsule the most according to claim 1, it is characterised in that include
Following steps:
(1) new hesperidin methyl dihydrochalcone, rhodinol, rhodinol-β-D-glucopyra are weighed in proportion
Glucosides and emulsifying agent solids granule mix homogeneously obtain mixture；
(2) weighing chitosan solid granule to be dissolved in glacial acetic acid aqueous solution, preparation obtains the shell of 1%～4% and gathers
Sugar juice；
(3) mixture of described step (1) is joined in the solution of step (2), stir newborn
Liquid；
(4) aqueous solution of sodium hydroxide is sprayed by the emulsion of step (3), solution occurs solidification
Little granule；
(5) product of step (4) is carried out ultra-filtration filters；
(6) filtration product of step (5) is carried out microwave vacuum drying, i.e. obtain described compound flavouring essence for tobacco
Microcapsule.
The preparation method of composite smoke essence microcapsule the most according to claim 3, it is characterised in that:
The addition of described emulsifying agent is new hesperidin methyl dihydrochalcone, rhodinol, rhodinol-β-D-glucopyra
Glucosides and the 1 of emulsifying agent gross weight～5%；The concentration of described glacial acetic acid aqueous solution is 1wt%, described hydroxide
The pH value of sodium water solution is 7.5～8.0.
The preparation method of composite smoke essence microcapsule the most according to claim 3, it is characterised in that institute
The vacuum stating microwave vacuum drying is 0.080～0.095MPa, and microwave power is 8～12W/g.
Composite smoke essence microcapsule the most according to claim 1 is for the purposes of Medicated cigarette flavouring.
Composite smoke essence microcapsule the most according to claim 1 for keep cigarette flavor stability,
Persistency and/or the purposes of fragrance release uniformity consistency in time.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610104050.3A CN105725258A (en) | 2016-02-25 | 2016-02-25 | Fragrant microcapsule for composite cigarettes and preparation method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610104050.3A CN105725258A (en) | 2016-02-25 | 2016-02-25 | Fragrant microcapsule for composite cigarettes and preparation method and application thereof |
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| CN105725258A true CN105725258A (en) | 2016-07-06 |
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| CN201610104050.3A Pending CN105725258A (en) | 2016-02-25 | 2016-02-25 | Fragrant microcapsule for composite cigarettes and preparation method and application thereof |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106565450A (en) * | 2016-10-14 | 2017-04-19 | 云南中烟工业有限责任公司 | Novel chalcone compound extracted from Campanumoea javanica, and preparation method and application thereof |
| CN106565449A (en) * | 2016-10-14 | 2017-04-19 | 云南中烟工业有限责任公司 | Preparation method and applications of chalcone compound capable of increasing cigarette smoking sweetness |
| CN106723299A (en) * | 2016-12-30 | 2017-05-31 | 中国烟草总公司广东省公司 | A kind of rose scent smears cigarette and preparation method thereof |
| CN107164090A (en) * | 2017-05-31 | 2017-09-15 | 东南大学 | A kind of cigarette perfume microcapsule and preparation method |
| CN107583575A (en) * | 2016-07-10 | 2018-01-16 | 青岛科技大学 | A kind of preparation of stable type flores aurantii flavor flavouring essence for tobacco and purposes |
| CN107581652A (en) * | 2016-07-10 | 2018-01-16 | 青岛科技大学 | A kind of preparation of stable type tobira flavor flavouring essence for tobacco and purposes |
| CN107594621A (en) * | 2017-09-25 | 2018-01-19 | 云南程耀生物科技有限公司 | A kind of fruity flavor composite particles and its preparation method and application |
| CN111035622A (en) * | 2019-11-20 | 2020-04-21 | 东莞波顿香料有限公司 | Angelica keiskei chalcone microcapsule and preparation method thereof |
| CN112813733A (en) * | 2021-01-19 | 2021-05-18 | 云南中烟工业有限责任公司 | Cigarette paper, preparation method thereof and application of cigarette paper in improving content of DGP in cigarette smoke |
| CN113679081A (en) * | 2021-09-08 | 2021-11-23 | 湖北中烟工业有限责任公司 | Spice essential oil for cigarettes and preparation method thereof |
| CN117089405A (en) * | 2023-08-23 | 2023-11-21 | 广州科百欣香料有限公司 | Rose-type essence microcapsule for cigarettes and preparation method and application thereof |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0464324A2 (en) * | 1990-07-06 | 1992-01-08 | Japan Tobacco Inc. | A preparation method of a flavoring granule for tobacco products |
| CN101203148A (en) * | 2005-06-21 | 2008-06-18 | 玛奈·菲尔萨公司 | Smoking device incorporating a breakable capsule, breakable capsule and process for manufacturing said capsule |
| CN101519417A (en) * | 2009-04-20 | 2009-09-02 | 中国科学技术大学 | Preparation method and application of effective ingredients of rose fragrance emitting agent for cigarettes |
| CN101928641A (en) * | 2010-09-29 | 2010-12-29 | 江南大学 | Essence microcapsule with long-term effectiveness and preparation method thereof |
| CN101972619A (en) * | 2010-09-01 | 2011-02-16 | 浙江中烟工业有限责任公司 | Preparation method of menthol microcapsules |
| WO2011116979A1 (en) * | 2010-03-26 | 2011-09-29 | Philip Morris Products S.A. | Method for making particle of a hydrophobic additive and a polysaccharide coating and tobacco products containing particle of a hydrophobic additive and a polysaccharide coating |
| CN102940307A (en) * | 2012-11-19 | 2013-02-27 | 湖南中烟工业有限责任公司 | Slow-release alkaline microcapsule for buccal tobacco product and preparation method and application thereof |
| CN103408620A (en) * | 2013-08-15 | 2013-11-27 | 西南化工研究设计院有限公司 | Neohesperidin synthesis technology |
| CN103706311A (en) * | 2012-10-09 | 2014-04-09 | 陈敏 | Microcapsule preparation technology for obviously improving overall performances of product |
-
2016
- 2016-02-25 CN CN201610104050.3A patent/CN105725258A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0464324A2 (en) * | 1990-07-06 | 1992-01-08 | Japan Tobacco Inc. | A preparation method of a flavoring granule for tobacco products |
| CN101203148A (en) * | 2005-06-21 | 2008-06-18 | 玛奈·菲尔萨公司 | Smoking device incorporating a breakable capsule, breakable capsule and process for manufacturing said capsule |
| CN101519417A (en) * | 2009-04-20 | 2009-09-02 | 中国科学技术大学 | Preparation method and application of effective ingredients of rose fragrance emitting agent for cigarettes |
| WO2011116979A1 (en) * | 2010-03-26 | 2011-09-29 | Philip Morris Products S.A. | Method for making particle of a hydrophobic additive and a polysaccharide coating and tobacco products containing particle of a hydrophobic additive and a polysaccharide coating |
| CN101972619A (en) * | 2010-09-01 | 2011-02-16 | 浙江中烟工业有限责任公司 | Preparation method of menthol microcapsules |
| CN101928641A (en) * | 2010-09-29 | 2010-12-29 | 江南大学 | Essence microcapsule with long-term effectiveness and preparation method thereof |
| CN103706311A (en) * | 2012-10-09 | 2014-04-09 | 陈敏 | Microcapsule preparation technology for obviously improving overall performances of product |
| CN102940307A (en) * | 2012-11-19 | 2013-02-27 | 湖南中烟工业有限责任公司 | Slow-release alkaline microcapsule for buccal tobacco product and preparation method and application thereof |
| CN103408620A (en) * | 2013-08-15 | 2013-11-27 | 西南化工研究设计院有限公司 | Neohesperidin synthesis technology |
Non-Patent Citations (2)
| Title |
|---|
| 金平正、金闻博: "《卷烟烟气安全性与危害防范》", 30 September 2009, 中国轻工业出版社 * |
| 雷声等: "玫瑰醇-β-D-吡喃葡萄糖苷键合态香料前体的合成及结构表征", 《现代食品科技》 * |
Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107583575A (en) * | 2016-07-10 | 2018-01-16 | 青岛科技大学 | A kind of preparation of stable type flores aurantii flavor flavouring essence for tobacco and purposes |
| CN107581652B (en) * | 2016-07-10 | 2021-07-13 | 青岛科技大学 | Preparation and application of stable erythrina indica flavor tobacco essence |
| CN107581652A (en) * | 2016-07-10 | 2018-01-16 | 青岛科技大学 | A kind of preparation of stable type tobira flavor flavouring essence for tobacco and purposes |
| CN106565450B (en) * | 2016-10-14 | 2019-02-19 | 云南中烟工业有限责任公司 | A kind of novel Chalcone Compounds, preparation method and the usage extracted from Bai Yun Shen |
| CN106565449B (en) * | 2016-10-14 | 2019-02-19 | 云南中烟工业有限责任公司 | A kind of preparation method and application for the chalcone compounds can increase cigarette smoking sweet tea sense |
| CN106565450A (en) * | 2016-10-14 | 2017-04-19 | 云南中烟工业有限责任公司 | Novel chalcone compound extracted from Campanumoea javanica, and preparation method and application thereof |
| CN106565449A (en) * | 2016-10-14 | 2017-04-19 | 云南中烟工业有限责任公司 | Preparation method and applications of chalcone compound capable of increasing cigarette smoking sweetness |
| CN106723299A (en) * | 2016-12-30 | 2017-05-31 | 中国烟草总公司广东省公司 | A kind of rose scent smears cigarette and preparation method thereof |
| CN107164090A (en) * | 2017-05-31 | 2017-09-15 | 东南大学 | A kind of cigarette perfume microcapsule and preparation method |
| CN107594621A (en) * | 2017-09-25 | 2018-01-19 | 云南程耀生物科技有限公司 | A kind of fruity flavor composite particles and its preparation method and application |
| CN111035622B (en) * | 2019-11-20 | 2021-11-09 | 东莞波顿香料有限公司 | Angelica keiskei chalcone microcapsule and preparation method thereof |
| CN111035622A (en) * | 2019-11-20 | 2020-04-21 | 东莞波顿香料有限公司 | Angelica keiskei chalcone microcapsule and preparation method thereof |
| CN112813733A (en) * | 2021-01-19 | 2021-05-18 | 云南中烟工业有限责任公司 | Cigarette paper, preparation method thereof and application of cigarette paper in improving content of DGP in cigarette smoke |
| CN113679081A (en) * | 2021-09-08 | 2021-11-23 | 湖北中烟工业有限责任公司 | Spice essential oil for cigarettes and preparation method thereof |
| CN113679081B (en) * | 2021-09-08 | 2023-03-21 | 湖北中烟工业有限责任公司 | Spice essential oil for cigarettes and preparation method thereof |
| CN117089405A (en) * | 2023-08-23 | 2023-11-21 | 广州科百欣香料有限公司 | Rose-type essence microcapsule for cigarettes and preparation method and application thereof |
| CN117089405B (en) * | 2023-08-23 | 2024-03-12 | 广州科百欣香料有限公司 | Rose-type essence microcapsule for cigarettes and preparation method and application thereof |
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Application publication date: 20160706 |