CN105230940A - Functional hard candy and preparation method thereof - Google Patents
Functional hard candy and preparation method thereof Download PDFInfo
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- CN105230940A CN105230940A CN201510683038.8A CN201510683038A CN105230940A CN 105230940 A CN105230940 A CN 105230940A CN 201510683038 A CN201510683038 A CN 201510683038A CN 105230940 A CN105230940 A CN 105230940A
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Abstract
The invention relates to a tobacco product, in particular to a functional hard candy and a preparation method thereof. The functional hard candy adds tobacco materials and maca combinations into hard candy substrates, can slowly dissolve in oral cavities to steadily release nicotine and maca combination components, is low in content of the nicotine and irritation, supplies appropriate physical satisfaction and comfort feeling for consumers, has the effects of resisting fatigue and improving mental states, reduces dependency to nicotine, and can play the effect of improving smoking habits for long-term use. The functional hard candy is a novel no-smoke tobacco product which can be used in public places.
Description
Technical field
The present invention relates to tobacco product, specifically, relate to a kind of functional hard candy and preparation method thereof.
Background technology
Smoke-free tobacco product is in the process used, do not burn, smokeless produces, avoid the harm of harmful pyrolysis product and second-hand-cigarette, main implementation comprises the type of sucking and (does not chew, have residue), containing change type (not chewing, without residue), gum base type (chew, have residue) etc.At present, smoke-free tobacco product mainly in Europe, North America etc. area sell with the form of in bulk or packed buccal cigarette.But domestic consumer there is no the tradition using buccal cigarette, and packed buccal cigarette directly uses in the oral cavity with the form of tobacco leaf particle, nicotine release is unstable, and excitant is comparatively large, and comfortableness is poor, and the acceptance level of domestic consumer is low.That tobacco material is mixed with other additives containing change type smoke-free tobacco product, under the effects such as saliva, discharge the active ingredient such as nicotine, fragrance matter more reposefully, excitant is little, easy to use, domestic consumer is acceptant, is the Novel smokeless gas tobacco product that there is fine development prospect in a kind of market at home.
Hard candy is a kind of common leisure food, resistance toly to chew, entrance solution time is long, be suitable as the matrix of smoke-free tobacco product.Application number is in the patent " hard sugar containing tobacco component " of 200810049285.2, tobacco extract, nicotine and flavouring essence for tobacco is added in hard sugar matrix, the hard sugar of preparation containing tobacco component.But smoke-free tobacco product is different from the practical way of traditional cigarette, mainly rely on the absorption such as mucous membrane of mouth, stomach lining, therefore, in smoke-free tobacco product, directly use the security of nicotine and flavouring essence for tobacco still to wait to discuss.Existing smoke-free tobacco product to provide certain physiology satisfaction, just as the supplementary substitute of traditional cigarette, can not reduce the dependence feeling to nicotine, and excitement is stronger mainly through release nicotine.
Summary of the invention
In order to solve problems of the prior art, the object of this invention is to provide a kind of functional hard candy and preparation method thereof.
In order to realize the object of the invention, first the present invention provides a kind of functional hard candy, and its raw material by weight, comprises following component:
Nicotine content in described functional hard candy is 0.05 ~ 1mg/g;
The pH value of described functional hard candy is 6-8;
Described tobacco-containing material comprises tobacco powder and/or tobacco extract.
As preferably, its raw material by weight, comprises following component:
Further, described agate card composition comprises maca powder or agate card extract;
Or described agate card composition to comprise in maca powder or agate card extract and Bee Pollen, Moringa extract, Herb Gynostemmae Pentaphylli extract, wolfberry fruit extract, inulin, A Sayi berry extract, card nurse berry extract, kola extract, Guarana extract, Sakyamuni extract, extractive of alfalfa, Noni extract, damiana extract one or more combination;
Preferably, the formula of described agate card composition is: agate card extract 50-70 part, wolfberry fruit extract 10-30 part, Guarana extract 5-20 part, Moringa extract 5-20 part;
Or: agate card extract 30-50 part, A Sayi berry extract 10-30 part, card nurse berry extract 10-30 part, kola extract 10-30 part;
Or: maca powder 30-50 part, Bee Pollen 20-40 part, inulin 5-20 part, Herb Gynostemmae Pentaphylli extract 10-30 part;
Or: maca powder 40-60 part, extractive of alfalfa 10-30 part, Noni extract 5-20 part, damiana extract 5-20 part, Sakyamuni extract 5-20 part.
Agate card is a kind of Cruciferae separate row Vegetable spp plant originating in mountain area, South America Andean, has abundant nutritive value and health-care efficacy.But directly the active ingredient in plant cell cannot discharge by edible or mechanical crushing completely.In order to improve dissolution rate and the human absorptivity of active ingredient, the agate card component used in technical solution of the present invention is agate card Ultramicro-powder or agate card extract.
Agate card component and preferred other plant component, with comparatively strong pungent, pained mouthfeel, are carried out composite in technical solution of the present invention, are effectively improved the mouthfeel quality of agate card, and improve the result of use of agate card composition by agate card itself.
Preferably, the preparation method of described maca powder is:
(1) by after fresh agate card cleaning, be cut into the sheet of thickness 1-5mm, then utilize freeze drying or low temperature drying technology by agate card moisture drying extremely lower than 5%.Cryodesiccated temperature is-20 ~-45 DEG C, and vacuum is 10-30Pa.The temperature of low temperature drying is 30-60 DEG C, and vacuum is 100-200Pa.
(2) dried agate card section is pulverized, sieved, obtain 20-100 object meal.
(3) utilize low-temperature airflow micronizer that agate card meal is carried out separating twice, screening obtains agate card Ultramicro-powder.
More preferably, the granularity of described maca powder is greater than 200 orders.
Further preferably, the granularity of described maca powder is for being greater than 2000 orders.
Preferably, the preparation method of described agate card extract is:
(1) by after fresh agate card cleaning, be cut into the sheet of thickness 1-5mm, then utilize freeze drying or low temperature drying technology by agate card moisture drying extremely lower than 5%.Dried agate card section is pulverized, sieved, obtains 20-100 object meal.
(2) utilize 95% ethanol as extractant, the ratio of extractant and maca powder is 10:1-30:1, at 50-80 DEG C, extract 1-5 hour, and separation, Vacuum Concentration obtain agate card alcohol extract.
(3) filter residue after extraction in (2) is added 10-20 times of water, at 80-100 DEG C, extract 0.5-3 hour, separation, Vacuum Concentration obtain agate card water extract.
(4) be get Ma Ka extract after agate card alcohol extract and water extract being mixed according to 1:1-5:1 ratio.Powdery agate card extract can be prepared through further freeze drying, spraying dry.
More preferably, the order of alcohol extraction process and extraction process by water can exchange, or adds other treatment process before, during and after arbitrary operation
Further preferably, described extracting method comprises one or more the combination in extraction, ultrasound on extracting, microwave auxiliary extraction, distillation extraction etc.
Preferably, other extract components in described agate card composition are through drying, pulverizing, extraction, concentrate the paste or powdered extract that obtain.
Described tobacco powder after cleaning, drying, carries out mechanical crushing by tobacco-containing material, screening obtains 20-100 object meal; Utilize low-temperature airflow micronizer that tobacco meal is carried out separating twice, screening obtains tobacco powder.
Preferably, the order granularity of described tobacco powder is greater than 200 orders;
More have choosing, the order granularity of described tobacco powder is greater than 500 orders;
Further preferably, the order granularity of described tobacco powder is greater than 2000 orders.
Described tobacco extract is liquid tobacco extract or tobacco extract compound fine powder.
Described liquid tobacco extract refers to that tobacco is after super-dry, pulverizing, screening, through extracting the tobacco extract obtained, described tobacco extract compound fine powder be tobacco extract through means such as molecular clock, freeze drying, spraying dry, the tobacco extract compound fine powder made under the effect of excipient.Described extracting method be selected from supercritical extract, extraction, ultrasound on extracting, microwave auxiliary extraction, distillation extraction etc. one or more.
Described tobacco be selected from flue-cured tobacco, suncured tabacco, air-curing of tobacco leaves, burley tobaccos, Turkish tobaccos, Nicotiniana rustica one or more.
More preferably, described suncured tabacco be selected from Dark sun-cured and Sun cured tobacco and other region suncured tabacco one or more, described air-curing of tobacco leaves be selected from Maryland, cigar and other region air-curing of tobacco leaves one or more.
Further preferably, described tobacco is the airing cigarette originating from Guizhou province, or the combination of this airing cigarette and other tobaccos.
Preferably, described tobacco is one or more in conventional tobacco leaf and ecological organic tobacco leaf.
Preferably, described tobacco through spontaneous fermentation, ageing (in an embodiment of the invention, digestion time is a year), take out stalk, cleaning, dehydration after carry out flavouring process.
Described flavouring process refers to spice liquid immersion or infiltrates tobacco-containing material, or is sprayed onto on tobacco powder or tobacco extract by spice liquid.Spice liquid decocts water by spices material or flavouring agent is formulated.
Further, described glycosyl is selected from sucrose, fructose, glucose (slurry), HFCS, maltose, hydrogenated starch hydrolysate, corn syrup, Maple Syrup, honey, steviol glycoside, mogroside, xylitol, lactitol, maltitol (slurry), D-sorbite (slurry), mannose, D-mannital, isomaltoketose, isomalt, isomalto-oligosaccharide, antierythrite, milk ketose, gossypose, soyabean oligosaccharides, lactosucrose, xylo-oligosaccharide, galactooligosaccharide, FOS, inulooligosaccharide, lactose, protein sugar, licorice powder, glycyrrhetate, Africa arrowroot glucin, acesulfame potassium, knob is sweet, Aspartame, saccharin sodium, honey element, calcium cyclamate, Sucralose, alitame, Sucralose, glycyrrhizin, NHDC, curculin, miracle fruit thaumatin T, potato root of fangji glucin, two sweet, one or more in Arabinose and other food glycosyls,
Described flavouring agent is selected from licorice powder, ground coffee, plum powder, red date powder, cocoa power, green tea powder, fruit extract, aloe extract, Honegsukle flower P.E, arhat fruit tincture, hawthorn fruit tincture, red date tincture, faenum graecum tincture, hop tincture, cocoa tincture, dark plum tincture, black tea tincture, green tea tincture, hergamot oil, lemon oil, caffeol, buchu leaves oil, clove leaf oil, basil, orange oil, natural cognac, Michelia oil, peppermint oil, grapefruit oil, FLOS CHRYSANTHEMI ALBA from Haizhou of China oil, one or more combination in Rum, fruit extract can be one or more in apple, apricot, banana, blackberry, blueberry, cherry, jujube, fig, sweet orange, peach, pear, plum, plum, grape, prune and other fruit extracts,
Described acid be selected from citric acid, gluconic acid, L MALIC ACID, lactic acid, tartaric acid and other food acid taste agent one or more;
Described freshener is selected from menthol, mentha piperita oil, asia peppermint oil, asia peppermint vegetable oil, penner oil, Natural menthol, N-to one or more in benzene acetonitrile base peppermint alkyl formamides, N-(2-(pyridine-2-base) ethyl) peppermint alkyl formamides, menthalactone and other mint extract or derivative etc.;
Described thickener is selected from starch, phosphorylation PASELLI EASYGEL, sodium carboxymethyl starch, starch phosphate sodium, maltodextrin, cyclodextrin, microcrystalline cellulose, sodium carboxymethylcellulose, hydroxypropyl cellulose, methylcellulose, ethyl cellulose, HPMC, gelatin, Arabic gum, casein, chitin, Chitosan-phospholipid complex, chitosan oligosaccharide and derivative thereof, sodium alginate, ammonium alginate, propylene glycol alginate, tara gum, mannitol, D-sorbite, lactitol, guar gum, pectin, gloiopeltis glue, trigonella bean gum, locust bean gum, Sunset Abelmoschus Root glue, xanthans, peach gum, lac, cassia gum, bassora gum, carragheen, curdlan, soluble soybean polysaccharide, tamarind seed polysaccharide glue, pulullan polysaccharide, one or more in flaxseed gum and other food grade thickener,
Described emulsifying agent be selected from single, double, triglyceride, lecithin, soybean lecithin, degreased cocoa powder, acetylation list bis-fatty acid glyceride, polyglyceryl fatty acid ester, polyethylene glycol, polyethylene sorbitan ester, poloxamer, sucrose fatty ester and other food emulsifying agents one or more;
Described edible coloring agent is selected from titanium dioxide, erythrosine, light blue, monascus yellow pigment, tea uranidin, Tea Green Pigment, Ipomoea batatas(L.)Lam, β-A Piao-8 '-carotenal, copper chlorophyll, indigo, Pasania cuspidata palm fibre, lycopene, citrus is yellow, black soya bean is red, blackcurrant is red, safflower yellow, red rice is red, Monascus color, turmeric, burnt sugar coloring, fruit of Cherokee rose palm fibre, coreopsis yellow extract, cacao pigment, chilli orange, radish red, peanut-skin red, the certain herbaceous plants with big flowers that falls is red, roselle is red, Grape Skin is red, mulberries are red, wild jujube look, natural amaranth, alkermes, red bayberry is red, lutein, algae is blue, one or more in beta carotene and other edible coloring agents,
Described antioxidant is selected from one or more in Tea Polyphenols, butylated hydroxy anisole, Sodium Benzoate, dibutyl hydroxy toluene, n-propyl gallate, sorbic acid and sylvite thereof, dl-alpha-tocopherol, d-alpha-tocopherol, vitamin C, Calcium Ascorbate, ascorbyl palmitate, D-araboascorbic acid and sodium salt, carnosic acid, Licorice root antioxidant, AOB, ginkgo biloba extract, tea extract and grape seed extract and other food antioxidants.
Present invention also offers the preparation method of described functional hard candy, described method comprises the steps:
(1) glycosyl added dissolving in hot water, filter to obtain syrup;
(2) step (2) gained syrup is proceeded to the infusion of vacuum sugar boiling machine, control steam pressure is 0.5-0.95atm, and sugar cook temperature is 140-210 DEG C, and infusion is to syrup homogeneous transparent, and moisture is less than 2wt%;
(3) step (2) gained syrup is cooled to 100-140 DEG C, tobacco powder and/or tobacco extract, agate card composition, flavouring agent, acid, freshener, emulsifying agent, thickener, edible coloring agent, antioxidant etc. is added by proportioning, stir, adjustment pH is 6-8;
(4) by step (3) gained syrup injection moulding mould, cool rapidly, make syrup solidify sizing to mould disks, demoulding when being cooled to 30-40 DEG C, dressing, packaging obtain;
Wherein, pH adjusting agent is selected from one or more in sodium carbonate, sodium acid carbonate, potash, saleratus, natrium citricum, potassium citrate, gluconic acid sodium salt.
Present invention also offers described functional hard candy and supplement the application in substitute as tobacco.
Beneficial effect of the present invention is:
The functional hard candy provided of the present invention, directly do not add nicotine and chemical synthesis essence and flavoring agent, and in hard sugar matrix, with the addition of Guizhou airing tobacco powder end, tobacco extract, agate card composition and natural flavours, can slowly dissolve in the oral cavity, Stable Release nicotine and agate card composition components, nicotine content is low, and excitant is low, characteristic perfume is obvious, is supplied to the suitable physiology satisfaction of consumer and comfort; And have antifatigue, improve the effect of the state of mind, reduce the dependence to nicotine, Long-Time Service can play the effect improving smoking habit.Product of the present invention is a kind of Novel smokeless gas tobacco product that can use in public places.
Detailed description of the invention
Following examples for illustration of the present invention, but are not used for limiting the scope of the invention.
The composition used in the embodiment of the present invention is principal component, and wherein maca powder, agate card extract, tobacco powder and tobacco extract can be prepared by method disclosed in description.
The shape of functional hard candy provided by the invention can be the shapes such as spherical, elliposoidal, taper, cylindrical, prismatic, regular polygon shape, platform turriform, capsule shape, leaf, flower-shape, fruit shape, product surface can carry out characters cut in intaglio or characters cut in relief embossing, such as enterprise name, corporate identify, letter, leaf, flower, fruit etc.
Below by way of specific instantiation, embodiments of the present invention are described, those skilled in the art the content disclosed by this description can understand other advantages of the present invention and effect easily.The present invention can also be implemented or be applied by detailed description of the invention different in addition, and the every details in this description also can based on different viewpoints and application, carries out various modification or change not deviating under spirit of the present invention.
Notice, in the following example, the concrete process equipment that indicates or device all adopt conventional equipment in this area or device; All force value and scope all refer to absolute pressure.
Embodiment 1
Weight ratio shared by each component is as follows:
Wherein, in the formula of agate card composition, the weight ratio of each component is as follows: agate card extract 60 parts, wolfberry fruit extract 20 parts, Guarana extract 10 parts, Moringa extract 10 parts.
Preparation process is as follows:
(1) Feedstock treating
By the spontaneous fermentation of Guizhou airing cigarette, ageing 1 year, flue-cured tobacco baking, ageing 1 year, carried out taking out stalk, cleaning, processed, dry at 40-60 DEG C.Turkish tobaccos are dried at 40-60 DEG C.According to airing cigarette: flue-cured tobacco: the weight ratio mixing of Turkish tobaccos=6:3:1, to pulverize, solvent extraction method or supercritical extraction is utilized to obtain smoking mixture extract.
By tobacco extract: Arabic gum: by weight dispersion in deionized water, strong stirring is emulsion uniformly for beta-schardinger dextrin-=1:2:3, and spraying dry forms tobacco extract compound.
Agate card composition is obtained after agate card extract and wolfberry fruit extract, Guarana extract, Moringa extract etc. is composite in proportion.
(2) candy preparation
In jacketed pan, add enough water, be heated to boiling, take sucrose, fructose, glucose etc., add in hot water and fully dissolve by formula, 80 eye mesh screens proceed to holding vessel and store after filtering.The syrup changed is proceeded to the infusion of vacuum sugar boiling machine, control steam pressure is 0.85-0.9atm, and sugar cook temperature is 140-170 DEG C, and infusion is to syrup homogeneous transparent, and moisture is less than 2wt%.
The syrup concentrated is cooled to 130-140 DEG C, add tobacco extract compound, agate card composition, orange oil, dark plum tincture, lecithin, citric acid, Arabic gum, sodium alginate, menthol, sodium acid carbonate, Ipomoea batatas(L.)Lam, potassium sorbate etc., be stirred to and mix.By the quantitative injection moulding mould of syrup be in harmonious proportion, whole mould disks is cooled rapidly, makes syrup solidify sizing.Demoulding when being cooled to 30-40 DEG C, utilizes isomalt to carry out dressing, packaging and functional hard candy.The specification of functional hard candy is every 5.0 ± 0.1g.
Embodiment 2
Weight ratio shared by each component is as follows:
Wherein, in the formula of agate card composition, the weight ratio of each component is as follows: agate card extract 40 parts, A Sayi berry extract 20 parts, card nurse berry extract 20 parts, kola extract 20 parts.Preparation process is as follows:
(1) Feedstock treating
By the spontaneous fermentation of Guizhou airing cigarette, ageing 1 year, carry out taking out stalk, cleaning, processed.According to Radix Glycyrrhizae: the ratio of water=1:10-20 was by Radix Glycyrrhizae at 90-100 DEG C fried 1 hour, and cooling, after filtration, adding weight ratio in filtrate is that 5% honey is mixed with spice liquid, with spice liquid, airing cigarette is infiltrated 24-72 hour, carries out flavouring process.After airing cigarette is taken out, dry under 120-140 DEG C of condition to moisture and be less than 3wt%.Dried tobacco-containing material is pulverized, crosses 80 mesh sieves and obtain tobacco meal.Then carry out secondary ultramicro grinding, sieving obtains order granularity and is greater than 500 object tobacco powders.Prepare order granularity according to identical method after tea-drying and be greater than 500 object green tea powders.
Agate card composition is obtained after agate card extract and A Sayi berry extract, card nurse berry extract, kola extract etc. is composite in proportion.
(2) candy preparation
In jacketed pan, add enough water, be heated to boiling, take sucrose, maltitol, isomalt, add in hot water and fully dissolve by formula, 80 eye mesh screens proceed to holding vessel and store after filtering.The syrup changed is proceeded to the infusion of vacuum sugar boiling machine, control steam pressure is 0.85-0.9atm, and sugar cook temperature is 140-160 DEG C, and infusion is to syrup homogeneous transparent, and moisture is less than 2wt%.
The syrup concentrated is cooled to 120-130 DEG C, adds that tobacco powder, agate card composition, peach gum, natural cognac, Rum, hop tincture, glyceryl triacetate, blackcurrant are red, D-araboascorbic acid sodium etc., be stirred to and mix.By the quantitative injection moulding mould of syrup be in harmonious proportion, whole mould disks is cooled rapidly, makes syrup solidify sizing.Demoulding when being cooled to 30-40 DEG C, utilizes isomalt to carry out dressing, packaging and functional hard candy.The specification of functional hard candy is every 5.0 ± 0.1g.
Embodiment 3
Weight ratio shared by each component is as follows:
Wherein, in the formula of agate card composition, the weight ratio of each component is as follows: maca powder 40 parts, broker wall bee pollen 30 parts, inulin 10 parts, Herb Gynostemmae Pentaphylli extract 20 parts.
Preparation process is as follows:
(1) Feedstock treating
By the spontaneous fermentation of Guizhou airing cigarette, ageing 1 year, carry out taking out stalk, cleaning, processed, then heat treatment 1 hour in 80-90 DEG C of water, after taking out, rotating cage removes moisture, dries at 40-60 DEG C.According to airing cigarette: the weight ratio mixing of Turkish tobaccos=4:1, pulverizing, cross 80 mesh sieves and obtain tobacco meal.Then carry out secondary ultramicro grinding, sieving obtains order granularity and is greater than 500 object tobacco powders.
By weight ratio be 1% buchu leaves oil, 5% beta-schardinger dextrin-dispersion in ethanol, strong stirring, mix and make spice liquid, be evenly sprayed in tobacco powder, be as the criterion not lump, after balance, namely obtain flavouring tobacco powder.
Agate card composition is obtained after maca powder and broker wall bee pollen, inulin, Herb Gynostemmae Pentaphylli extract etc. is composite in proportion.
(2) candy preparation
Enough water in jacketed pan, is heated to boiling, takes isomalt, isomalto-oligosaccharide, add in hot water and fully dissolve by formula, and 80 eye mesh screens proceed to holding vessel and store after filtering.The syrup changed is proceeded to the infusion of vacuum sugar boiling machine, control steam pressure is 0.6-0.8atm, and sugar cook temperature is 140-160 DEG C, and infusion is to syrup homogeneous transparent, and moisture is less than 2wt%.
The syrup concentrated is cooled to 130-140 DEG C, adds tobacco powder, agate card composition, steviol glycoside, caffeol, cocoa tincture, faenum graecum tincture, soybean lecithin, gelatin, carnosic acid etc., be stirred to and mix, dewater to moisture and be less than 2wt%.By the quantitative injection moulding mould of syrup be in harmonious proportion, whole mould disks is cooled rapidly, makes syrup solidify sizing.Demoulding when being cooled to 30-40 DEG C, utilizes D-mannital to carry out dressing, packaging and functional hard candy.The specification of functional hard candy is every 3.0 ± 0.1g.
Embodiment 4
Weight ratio shared by each component is as follows:
Wherein, in the formula of agate card composition, the weight ratio of each component is as follows: maca powder 50 parts, extractive of alfalfa 20 parts, Noni extract 10 parts, damiana extract 10 parts, Sakyamuni extract 10 parts.
Preparation process is as follows:
(1) Feedstock treating
By the spontaneous fermentation of Guizhou airing cigarette, ageing 1 year, flue-cured tobacco baking, ageing 1 year, carried out taking out stalk, cleaning, processed, dry at 40-60 DEG C.Turkish tobaccos are dried at 40-60 DEG C.According to airing cigarette: flue-cured tobacco: the weight ratio mixing of Turkish tobaccos=6:3:1, to pulverize, solvent extraction method or supercritical extraction is utilized to obtain smoking mixture extract.
Agate card composition is obtained after maca powder and extractive of alfalfa, Noni extract, damiana extract, Sakyamuni extract etc. is composite in proportion.
(2) candy preparation
In jacketed pan, add suitable quantity of water, be heated to boiling, take inulooligosaccharide, FOS, hydrogenated starch hydrolysate, add in hot water and fully dissolve by formula, 80 eye mesh screens proceed to holding vessel and store after filtering.The syrup changed is proceeded to the infusion of vacuum sugar boiling machine, control steam pressure is 0.6-0.8atm, and sugar cook temperature is 170-200 DEG C, and infusion is to syrup homogeneous transparent, and moisture is less than 2wt%.
The syrup concentrated is cooled to 140-160 DEG C, adds tobacco extract, agate card composition, green tea powder, green tea tincture, glyceryl triacetate, Arabic gum, sodium carbonate, menthol, vitamin C etc., be stirred to and mix.By the quantitative injection moulding mould of syrup be in harmonious proportion, whole mould disks is cooled rapidly, makes syrup solidify sizing.Demoulding when being cooled to 30-40 DEG C, utilizes antierythrite etc. to carry out dressing, packaging and functional hard candy.The specification of functional hard candy is every 3.0 ± 0.1g.
Comparative example 1
Weight ratio shared by each component is as follows:
Wherein, the composition of agate card composition is: agate card extract 40 parts, A Sayi berry extract 20 parts, card nurse berry extract 20 parts, kola extract 20 parts.
By flue-cured tobacco spontaneous fermentation, ageing 1 year, carry out taking out stalk, cleaning, processed.3wt% is less than at 120-140 DEG C of oven dry to moisture.Pulverized by dried tobacco-containing material, screening obtains order granularity and is greater than 300 object flue-cured tobacco powder.Preparation process is with reference to embodiment 2.
Comparative example 2
Weight ratio shared by each component is as follows:
Wherein, agate card composition is maca powder.
Preparation process is with reference to embodiment 4.
Comparative example 3
Weight ratio shared by each component is as follows:
Preparation process is with reference to embodiment 1.
Comparative example 4
Weight ratio shared by each component is as follows:
Wherein, in the formula of agate card composition, the weight ratio of each component is as follows: maca powder 40 parts, Bee Pollen 30 parts, inulin 10 parts, Herb Gynostemmae Pentaphylli extract 20 parts.
Preparation process is with reference to embodiment 3.
Functional hard candy prepared by embodiment 1-4 and comparative example 1-4 is carried out sensory evaluation test, sensory quality assessment method, specific as follows:
(1) sensory quality assessment index
This sensory quality assessment method arranges 9 evaluation indexes altogether, comprise entrance mouthfeel, physiological strength, feature be fragrant, tobacco is fragrant, excitement, comfort, release uniformity, release persistence and oral cavity pleasant impression.After described entrance mouthfeel refers to that smoke-free tobacco product puts into oral cavity, the initial synthetic impressions such as the sense of smell of user, the sense of taste and sense of touch.Described physiological strength refers in use, the physiology satisfaction that user experiences, i.e. strength.Described feature perfume (or spice) refers in use, the amount of the characteristic perfume that user experiences and matter.Described tobacco perfume (or spice) refers in use, the amount of this perfume (or spice) of tobacco that user experiences and matter.Described excitement refers in use, and the positions such as user oral cavity, nasal cavity, throat, esophagus are experienced the discomfort such as pungent, dry and are subject to.Described comfort refers in use, smell coordination that user experiences, soft and moist sense, without the impression of the fragrance such as residue foreign body sensation.Described release uniformity refers in use, user experience the release stability in time such as fragrance, physiological strength.Described release persistence refers to that in use, user experiences the duration such as fragrance, physiological strength length.Described oral cavity pleasant impression refers to after use procedure, the comprehensive impression of the remaining sense of smell in user oral cavity, the sense of taste and sense of touch.
(2) sensory quality assessment scoring rule
Described sensory quality assessment scoring rule adopts hundred-mark system point system.Described hundred-mark system point system refers to according to every sensory quality assessment index the influence degree of smoke-free tobacco product aesthetic quality, give the weight that each sensory quality assessment index is different, i.e. different score value, 9 sensory quality assessment indexs are marked by 5 points, 10 points or twenty point system respectively, and the highest score value of 9 sensory quality assessment indexs adds and be a percentage.
The scoring rule of described 9 sensory quality assessment indexs is as follows: described sensory quality assessment index is divided into 6 grades, and every shared weight, scoring scale and scoring are interval as shown in table 1, and minimum score unit is 0.5 point.
Described sensory quality assessment index weights refers to this sensory quality assessment index the highest getable score value in sensory quality assessment process.Described sensory quality assessment index score is interval refers to that the score value of this sensory quality assessment index in sensory quality assessment process corresponding to a certain evaluation scale is interval, and wherein comparatively high score is included in this section of score, and lower point is not included in this section of score.
Described sensory quality assessment index " excitement " impression is stronger, and score is lower; Described sensory quality assessment index " entrance mouthfeel ", " oral cavity pleasant impression " experience better, and score is higher; Described sensory quality assessment index " physiological strength ", " feature is fragrant ", " tobacco is fragrant ", " comfort ", " release uniformity ", " release persistence " experience stronger, and score is higher;
Described sensory quality assessment total score is added by the arithmetic of each subitem sensory quality assessment index score and is obtained.Total score score is higher, then represent that the sensory quality assessment effect of this smoke-free tobacco product is better.
Table 1 smoke-free tobacco product sensory quality assessment scoring rule
(3) sensory quality assessment implementation method
Valuation officer is arranged
Preferably, the evaluation team comprising 7 valuation officers is set.
Evaluation operation process
A collection of smoke-free tobacco product sample to be evaluated is carried out blind mark (if sample number is greater than 999, then digital code can be upgraded to 4, the rest may be inferred) with 3 digit numerical code, and by sampfe order random process; Carry out sensory quality assessment according to the sampfe order after process, before each sample starts evaluation, be distributed to and evaluate everyone a smoke-free tobacco product sensory quality assessment record sheet of team, sensory evaluation is carried out to smoke-free tobacco product; According to weight, evaluation scale and the interval of scoring of 9 sensory quality assessment indexs in table 1, valuation officer tackles every evaluation index and carries out sensory quality assessment, and in sensory evaluation record sheet records appraisal result, then all sensory quality assessments evaluating team are aggregated in monocyte sample sensory quality assessment summary sheet, and carry out evaluation result statistical disposition; After completing the sensory quality assessment of all samples successively, the sensory quality assessment of all samples is aggregated in batch sample sensory quality assessment summary sheet.
Evaluation result statistical analysis
Preferably, the computational methods of individual event sensory quality assessment index score are: 7 participate in the valuation officer of sensory quality assessments to all scorings of this sensory quality assessment index in remove one minimum point and a best result, remain 5 scorings for effective score, the arithmetic mean of instantaneous value of effective score is this sensory quality assessment index score, and result retains two-decimal;
The arithmetic mean of instantaneous value of each individual event sensory quality assessment index score adds and is the sensory quality assessment total score of smoke-free tobacco product, and result retains two-decimal.Total score score value is higher, then represent that the sensory evaluation effect of this smoke-free tobacco product is better.Concrete outcome is as shown in table 2:
The sensory quality assessment statistical form of the functional hard candy of table 2
From table 2, provided by the present invention is main tobacco material with Guizhou airing cigarette, and the hard candy adding agate card composition has entrance comfortable taste, characteristic perfume is obvious, the feature such as comfortable taste, good after-taste.The effect of adding agate card extract in agate card composition is better than maca powder, because agate card extract is enriched the agate card active ingredient of more high-load.Be only tobacco material with flue-cured tobacco or directly do not reach same effect using maca powder as addO-on therapy.
Evaluate after the personage that the hard candy of interpolation agate card composition the present invention prepared and the hard candy not adding agate card composition meet at smoking habit uses.Participation number is totally 100 people, and the age is between 25-55.The personnel participating in in-service evaluation are divided into two groups, and age and the years of smoking of often organizing personnel are suitable, and use the hard candy adding and do not add agate card composition respectively, service time is 3 months; Then one week, one month, trimestral time point fills in use sense respectively by evaluation table, summarized results lists table 3 in.
The use sense of the functional hard candy of table 3 is by evaluation table
Can be found by table 3 result, compared with not adding the hard candy of agate card composition, the hard candy adding agate card composition has the effect of more effective minimizing Nicotine Dependence sense, and along with the prolongation of service time, also has evaluation personnel to experience fatigue-relieving, improve the effects such as the state of mind; The hard candy adding agate card composition uses rear substantially without obvious oral cavity sense of discomfort, respiratory tract sense of discomfort, alimentary canal sense of discomfort or other bad impressions, and human tolerance is good.
In sum, the present invention effectively overcomes various shortcoming of the prior art and tool high industrial utilization.
Although above the present invention is described in detail with a general description of the specific embodiments, on basis of the present invention, can make some modifications or improvements it, this will be apparent to those skilled in the art.Therefore, these modifications or improvements without departing from theon the basis of the spirit of the present invention, all belong to the scope of protection of present invention.
Claims (10)
1. a functional hard candy, is characterized in that, its raw material by weight, comprises following component:
Nicotine content in described functional hard candy is 0.05 ~ 1mg/g;
The pH value of described functional hard candy is 6-8;
Described tobacco-containing material comprises tobacco powder and/or tobacco extract.
2. functional hard candy according to claim 1, is characterized in that, its raw material by weight, comprises following component:
3. functional hard candy according to claim 1 and 2, is characterized in that, described agate card composition comprises maca powder or agate card extract;
Or described agate card composition to comprise in maca powder or agate card extract and Bee Pollen, Moringa extract, Herb Gynostemmae Pentaphylli extract, wolfberry fruit extract, inulin, A Sayi berry extract, card nurse berry extract, kola extract, Guarana extract, Sakyamuni extract, extractive of alfalfa, Noni extract, damiana extract one or more combination;
Preferably, the formula of described agate card composition is: agate card extract 50-70 part, wolfberry fruit extract 10-30 part, Guarana extract 5-20 part, Moringa extract 5-20 part;
Or: agate card extract 30-50 part, A Sayi berry extract 10-30 part, card nurse berry extract 10-30 part, kola extract 10-30 part;
Or: maca powder 30-50 part, Bee Pollen 20-40 part, inulin 5-20 part, Herb Gynostemmae Pentaphylli extract 10-30 part;
Or: maca powder 40-60 part, extractive of alfalfa 10-30 part, Noni extract 5-20 part, damiana extract 5-20 part, Sakyamuni extract 5-20 part.
4. functional hard candy according to claim 3, is characterized in that, the order granularity of tobacco powder and maca powder is greater than 200 orders; Be preferably greater than 2000 orders.
5. the functional hard candy according to any one of claim 1,2,4, it is characterized in that, the raw material of described tobacco powder and tobacco extract is tobacco, and described tobacco is one or more in flue-cured tobacco, air-curing of tobacco leaves, suncured tabacco, burley tobaccos, Turkish tobaccos, Nicotiniana rustica;
Preferably, described tobacco is the airing cigarette originating from Guizhou province, or the combination of this airing cigarette and other tobaccos.
6. functional hard candy according to claim 5, it is characterized in that, described tobacco through spontaneous fermentation, ageing, take out stalk, cleaning, dehydration after carry out flavouring process, described flavouring process refers to spice liquid immersion or infiltrates tobacco-containing material, or is sprayed onto on tobacco powder or tobacco extract by spice liquid.
7. functional hard candy according to claim 1 and 2, is characterized in that,
Described glycosyl is selected from sucrose, fructose, glucose (slurry), HFCS, maltose, hydrogenated starch hydrolysate, corn syrup, Maple Syrup, honey, steviol glycoside, mogroside, xylitol, lactitol, maltitol (slurry), D-sorbite (slurry), mannose, D-mannital, isomaltoketose, isomalt, isomalto-oligosaccharide, antierythrite, milk ketose, gossypose, soyabean oligosaccharides, lactosucrose, xylo-oligosaccharide, galactooligosaccharide, FOS, inulooligosaccharide, lactose, protein sugar, licorice powder, glycyrrhetate, Africa arrowroot glucin, acesulfame potassium, knob is sweet, Aspartame, saccharin sodium, honey element, calcium cyclamate, Sucralose, alitame, Sucralose, glycyrrhizin, NHDC, curculin, miracle fruit thaumatin T, potato root of fangji glucin, two sweet, one or more in Arabinose and other food glycosyls,
Described flavouring agent is selected from licorice powder, ground coffee, plum powder, red date powder, cocoa power, green tea powder, fruit extract, aloe extract, Honegsukle flower P.E, arhat fruit tincture, hawthorn fruit tincture, red date tincture, faenum graecum tincture, hop tincture, cocoa tincture, dark plum tincture, black tea tincture, green tea tincture, hergamot oil, lemon oil, caffeol, buchu leaves oil, clove leaf oil, basil, orange oil, natural cognac, Michelia oil, peppermint oil, grapefruit oil, FLOS CHRYSANTHEMI ALBA from Haizhou of China oil, one or more combination in Rum, fruit extract can be one or more in apple, apricot, banana, blackberry, blueberry, cherry, jujube, fig, sweet orange, peach, pear, plum, plum, grape, prune and other fruit extracts,
Described acid be selected from citric acid, gluconic acid, L MALIC ACID, lactic acid, tartaric acid and other food acid taste agent one or more;
Described freshener is selected from menthol, mentha piperita oil, asia peppermint oil, asia peppermint vegetable oil, penner oil, Natural menthol, N-to one or more in benzene acetonitrile base peppermint alkyl formamides, N-(2-(pyridine-2-base) ethyl) peppermint alkyl formamides, menthalactone and other mint extract or derivative etc.;
Described thickener is selected from starch, phosphorylation PASELLI EASYGEL, sodium carboxymethyl starch, starch phosphate sodium, maltodextrin, cyclodextrin, microcrystalline cellulose, sodium carboxymethylcellulose, hydroxypropyl cellulose, methylcellulose, ethyl cellulose, HPMC, gelatin, Arabic gum, casein, chitin, Chitosan-phospholipid complex, chitosan oligosaccharide and derivative thereof, sodium alginate, ammonium alginate, propylene glycol alginate, tara gum, mannitol, D-sorbite, lactitol, guar gum, pectin, gloiopeltis glue, trigonella bean gum, locust bean gum, Sunset Abelmoschus Root glue, xanthans, peach gum, lac, cassia gum, bassora gum, carragheen, curdlan, soluble soybean polysaccharide, tamarind seed polysaccharide glue, pulullan polysaccharide, one or more in flaxseed gum and other food grade thickener,
Described emulsifying agent be selected from single, double, triglyceride, lecithin, soybean lecithin, degreased cocoa powder, acetylation list bis-fatty acid glyceride, polyglyceryl fatty acid ester, polyethylene glycol, polyethylene sorbitan ester, poloxamer, sucrose fatty ester and other food emulsifying agents one or more;
Described edible coloring agent is selected from titanium dioxide, erythrosine, light blue, monascus yellow pigment, tea uranidin, Tea Green Pigment, Ipomoea batatas(L.)Lam, β-A Piao-8 '-carotenal, copper chlorophyll, indigo, Pasania cuspidata palm fibre, lycopene, citrus is yellow, black soya bean is red, blackcurrant is red, safflower yellow, red rice is red, Monascus color, turmeric, burnt sugar coloring, fruit of Cherokee rose palm fibre, coreopsis yellow extract, cacao pigment, chilli orange, radish red, peanut-skin red, the certain herbaceous plants with big flowers that falls is red, roselle is red, Grape Skin is red, mulberries are red, wild jujube look, natural amaranth, alkermes, red bayberry is red, lutein, algae is blue, one or more in beta carotene and other edible coloring agents,
Described antioxidant is selected from one or more in Tea Polyphenols, butylated hydroxy anisole, Sodium Benzoate, dibutyl hydroxy toluene, n-propyl gallate, sorbic acid and sylvite thereof, dl-alpha-tocopherol, d-alpha-tocopherol, vitamin C, Calcium Ascorbate, ascorbyl palmitate, D-araboascorbic acid and sodium salt, carnosic acid, Licorice root antioxidant, AOB, ginkgo biloba extract, tea extract and grape seed extract and other food antioxidants.
8. functional hard candy according to claim 7, it is characterized in that, described glycosyl is selected from sucrose, fructose, glucose, maltitol, isomaltoketose, isomalt, isomalto-oligosaccharide, steviol glycoside, inulooligosaccharide, FOS, hydrogenated starch hydrolysate etc.; Described flavouring agent is selected from orange oil, natural cognac, caffeol, dark plum tincture, hop tincture, cocoa tincture, faenum graecum tincture, green tea tincture, green tea powder, Rum etc.; Described acid is selected from citric acid etc.; Described thickener is selected from Arabic gum, peach gum, gelatin etc.; Described emulsifying agent is selected from lecithin, glyceryl triacetate, soybean lecithin etc.; Described freshener is selected from menthol etc.; Described colouring agent is selected from that blackcurrant is red, Ipomoea batatas(L.)Lam etc.; Described antioxidant is selected from potassium sorbate, D-araboascorbic acid sodium, carnosic acid, vitamin C etc.
9. the preparation method of the functional hard candy described in any one of claim 1 ~ 8, is characterized in that, described method comprises the steps:
(1) glycosyl added dissolving in hot water, filter to obtain syrup;
(2) step (2) gained syrup is proceeded to the infusion of vacuum sugar boiling machine, control steam pressure is 0.5-0.95atm, and sugar cook temperature is 140-210 DEG C, and infusion is to syrup homogeneous transparent, and moisture is less than 2wt%;
(3) step (2) gained syrup is cooled to 100-140 DEG C, add tobacco powder and/or tobacco extract, agate card composition, flavouring agent, acid, freshener, emulsifying agent, thickener, edible coloring agent, antioxidant etc. by proportioning, stir;
(4) by step (3) gained syrup injection moulding mould, cool rapidly, make syrup solidify sizing to mould disks, demoulding when being cooled to 30-40 DEG C, dressing, packaging obtain.
10. the functional hard candy described in any one of claim 1 ~ 8 is supplementing the application in substitute as tobacco.
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101233890A (en) * | 2008-02-29 | 2008-08-06 | 中国烟草总公司郑州烟草研究院 | Hard sugar containing tobacco component |
| CN101795710A (en) * | 2007-05-16 | 2010-08-04 | 麦克内尔股份公司 | Oral nicotine formulation buffered with amino acid |
| CN104068465A (en) * | 2014-07-08 | 2014-10-01 | 川渝中烟工业有限责任公司 | Method for making strong-flavor buccal cigarette |
| CN104130863A (en) * | 2014-07-15 | 2014-11-05 | 江西中烟工业有限责任公司 | Maca extract as well as preparation method thereof and application thereof to cigarettes |
| CN104770861A (en) * | 2015-02-11 | 2015-07-15 | 贵州中烟工业有限责任公司 | Mouth-holding type smokeless tobacco product and preparing method thereof |
| CN104770859A (en) * | 2015-02-11 | 2015-07-15 | 贵州中烟工业有限责任公司 | Mouth-keeping smokeless tobacco product containing fagopyrum particles |
-
2015
- 2015-10-20 CN CN201510683038.8A patent/CN105230940B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101795710A (en) * | 2007-05-16 | 2010-08-04 | 麦克内尔股份公司 | Oral nicotine formulation buffered with amino acid |
| CN101233890A (en) * | 2008-02-29 | 2008-08-06 | 中国烟草总公司郑州烟草研究院 | Hard sugar containing tobacco component |
| CN104068465A (en) * | 2014-07-08 | 2014-10-01 | 川渝中烟工业有限责任公司 | Method for making strong-flavor buccal cigarette |
| CN104130863A (en) * | 2014-07-15 | 2014-11-05 | 江西中烟工业有限责任公司 | Maca extract as well as preparation method thereof and application thereof to cigarettes |
| CN104770861A (en) * | 2015-02-11 | 2015-07-15 | 贵州中烟工业有限责任公司 | Mouth-holding type smokeless tobacco product and preparing method thereof |
| CN104770859A (en) * | 2015-02-11 | 2015-07-15 | 贵州中烟工业有限责任公司 | Mouth-keeping smokeless tobacco product containing fagopyrum particles |
Cited By (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US11612183B2 (en) * | 2015-12-10 | 2023-03-28 | R.J. Reynolds Tobacco Company | Protein-enriched tobacco composition |
| US20170164651A1 (en) * | 2015-12-10 | 2017-06-15 | R.J. Reynolds Tobacco Company | Protein-enriched tobacco composition |
| CN105852188A (en) * | 2016-03-30 | 2016-08-17 | 宁波艾克威特智能科技有限公司 | Coating composition for improving bulkiness of tobacco sheets |
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| CN106509979A (en) * | 2016-12-26 | 2017-03-22 | 福建中烟工业有限责任公司 | Composition and method for preparing tobacco extract by using composition |
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