CN105595404B - Tobacco buccal tablet and preparation method thereof - Google Patents
Tobacco buccal tablet and preparation method thereof Download PDFInfo
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Abstract
The invention relates to tobacco products, and particularly discloses a tobacco buccal tablet and a preparation method thereof. The tobacco buccal tablets select the special sun-cured tobacco in Guizhou area as the main tobacco raw material, and are subjected to aroma enhancement and/or nicotine reduction treatment, so that the tobacco buccal tablets are strong in aroma and moderate in strength, balance the physiological satisfaction and the taste comfort of the product, and have important significance for improving the taste quality and market adaptability of buccal smokeless tobacco products; maca is subjected to superfine grinding or composite extraction technology to prepare maca extract, and the maca extract is optimally compounded with other plant components, so that the spicy taste of maca is reduced, the utilization efficiency of active ingredients is improved, and the maca extract has synergistic effect with tobacco materials, can resist fatigue, improve the mental state of a human body, and reduce the nicotine dependence of smokers; the product based on the invention has comfortable taste and lasting fragrance, does not generate smoke, can be used in public places, is convenient to carry, and is a novel chemical smokeless tobacco product with comfortable taste, safety and environmental protection.
Description
Technical Field
The invention relates to a tobacco product, in particular to a tobacco buccal tablet and a preparation method thereof.
Background
The smoke produced by combustible smoking articles contains harmful components that are harmful to human health. China is the biggest tobacco producing country and consuming country in the world, and the harm of second-hand smoke is suffered by more than 3 hundred million of people smoking and about 7.4 hundred million of people not smoking in China, and the harmfulness of smoking becomes a serious public health problem. In 2006, 1 month, the tobacco control framework convention of the world health organization takes effect formally in China, the government is promoting the public places to forbid smoking comprehensively, and the traditional cigarettes are under more and more control in multiple links such as production, marketing, consumption and the like. Smokeless tobacco products provide a physiological satisfaction to consumers in a non-burning form similar to smoking traditional cigarettes, and mainly include buccal (no chewing, with residue), buccal (no chewing, without residue), gum-based (chewing, with residue) tobacco products, and the like. The smokeless tobacco product does not produce harmful components in the smoke of the combustible smoking tobacco product, avoids the harm of second-hand smoke, can be used as a supplementary substitute product of the traditional cigarette, and has important significance for protecting public health.
The tobacco fine powder or the tobacco extract is mixed with other additives and then pressed into a certain shape, when in use, the tobacco fine powder or the tobacco extract is disintegrated and dissolved in the oral cavity, so that the effective components such as nicotine and fragrant substances are released more stably to provide certain physiological satisfaction for consumers, no smoke is generated, the tobacco product is convenient to use and easy to accept by domestic consumers, and the tobacco product is a novel smoke-free tobacco product with good development prospect in the domestic market. The foreign buccal type smokeless tobacco product mainly provides physiological satisfaction by simply adding nicotine into the product, plays a certain role in substituting for smoking, cannot reduce the dependence of smokers on nicotine, and has the advantages of quick release of free nicotine and no tobacco fragrance of the product.
Disclosure of Invention
In order to solve the problems in the prior art, the invention aims to provide a tobacco buccal tablet and a preparation method thereof.
In order to realize the purpose of the invention, the invention firstly provides a tobacco buccal tablet which comprises the following components in parts by weight:
the nicotine content in the tobacco buccal tablet is 0.005-6 mg/g;
the tobacco material comprises tobacco powder and/or tobacco extract.
Preferably, the tobacco buccal tablet comprises the following raw materials in parts by weight:
further, the maca composition comprises maca powder or maca extract;
or the maca composition comprises maca powder or maca extract and one or more of bee pollen, moringa extract, gynostemma pentaphylla extract, medlar extract, inulin, assaya extract, camu extract, cola extract, guarana extract, custard extract, alfalfa extract, noni extract and damiana extract;
preferably, the maca composition is formulated as: 30-60 parts of maca extract, 20-40 parts of bee pollen, 10-30 parts of moringa oleifera extract and 5-15 parts of guarana extract;
or: 20-40 parts of maca extract, 20-40 parts of medlar extract, 10-30 parts of gynostemma pentaphylla extract and 10-30 parts of camu fruit extract;
or: 40-70 parts of maca extract, 10-30 parts of inulin, 5-20 parts of assai fruit extract and 5-20 parts of custard apple extract;
or: 40-60 parts of maca extract, 10-30 parts of cola nut extract, 5-15 parts of alfalfa extract, 5-15 parts of noni extract and 5-15 parts of damiana extract.
Maca is a cruciferous Lepidium plant native to the Andes mountain area of south America, and has rich nutritive value and health promotion effect. But the effective components in the plant cells cannot be completely released by direct eating or mechanical crushing. In order to improve the dissolution rate and the human body absorption rate of the active ingredients, the maca component used in the technical scheme of the invention is maca superfine powder or maca extract.
The maca has strong spicy and bitter mouthfeel, and the maca component and other preferable plant components are compounded in the technical scheme of the invention, so that the mouthfeel quality of the maca is effectively improved, and the use effect of the maca composition is improved.
Preferably, the preparation method of the maca powder comprises the following steps:
(1) cleaning fresh maca, cutting into slices with the thickness of 1-5mm, and drying the maca to the moisture content of less than 5% by utilizing a freeze drying or low-temperature drying technology. The freeze drying temperature is-20 deg.C to-45 deg.C, and the vacuum degree is 10-30 Pa. The low-temperature drying temperature is 30-60 ℃, and the vacuum degree is 100-200 Pa.
(2) And (3) slicing and crushing the dried maca, and screening to obtain coarse powder of 20-100 meshes.
(3) And (3) carrying out secondary crushing on the maca coarse powder by using a low-temperature airflow ultrafine crusher, and screening to obtain maca ultrafine powder.
More preferably, the maca powder has a particle size of greater than 200 mesh.
Further preferably, the maca powder has a particle size of greater than 2000 mesh.
Preferably, the preparation method of the maca extract comprises the following steps:
(1) cleaning fresh maca, cutting into slices with the thickness of 1-5mm, and drying the maca to the moisture content of less than 5% by utilizing a freeze drying or low-temperature drying technology. And (3) slicing and crushing the dried maca, and screening to obtain coarse powder of 20-100 meshes.
(2) 95% ethanol is used as an extracting agent, and the proportion of the extracting agent to the maca powder is 10: 1-30: 1, extracting for 1-5 hours at 50-80 ℃, separating, and concentrating in vacuum to obtain maca alcohol extract.
(3) Adding 10-20 times of water into the filter residue extracted in the step (2), extracting for 0.5-3 hours at 80-100 ℃, separating, and concentrating in vacuum to obtain the maca water extract.
(4) Mixing maca alcohol extract and water extract according to the ratio of 1: 1-5: mixing at a ratio of 1 to obtain maca extract. Further freeze drying and spray drying to obtain powder maca extract.
More preferably, the alcohol extraction process and the water extraction process can be interchanged in sequence, or other treatment processes can be added before or after any process.
Further preferably, the extraction method comprises one or more of solvent extraction, ultrasound-assisted extraction, microwave-assisted extraction, distillation extraction, and the like.
Preferably, the other extract components in the maca composition are paste or powder extracts obtained by drying, crushing, extracting and concentrating.
The tobacco powder is prepared by cleaning and drying tobacco materials, mechanically crushing and screening to obtain coarse powder of 20-100 meshes; and (3) carrying out secondary crushing on the tobacco coarse powder by using a low-temperature airflow ultrafine crusher, and screening to obtain tobacco powder.
Preferably, the tobacco powder has a mesh size greater than 200 mesh;
more preferably, the mesh size of the tobacco powder is larger than 500 meshes;
further preferably, the mesh size of the tobacco powder is greater than 2000 mesh.
The tobacco extract is liquid tobacco extract or tobacco extract compound fine powder.
The liquid tobacco extract is a tobacco extract obtained by drying, crushing and screening tobacco and extracting, and the tobacco extract compound fine powder is prepared from the tobacco extract by means of molecular distillation, freeze drying, spray drying and the like under the action of an excipient. The extraction method is selected from one or more of supercritical extraction, solvent extraction, ultrasonic-assisted extraction, microwave-assisted extraction, distillation extraction and the like.
The tobacco is selected from one or more of flue-cured tobacco, sun-cured tobacco, air-cured tobacco, burley tobacco, aromatic tobacco and yellow flower tobacco.
More preferably, the sun-cured tobacco is selected from one or more of red-cured tobacco, yellow-cured tobacco and other local sun-cured tobacco, and the sun-cured tobacco is selected from one or more of maryland tobacco, cigar tobacco and other local sun-cured tobacco.
Further preferably, the tobacco is sun-cured tobacco produced in Guizhou area, or a combination of the sun-cured tobacco and other tobacco.
Preferably, the tobacco is one or more of regular tobacco leaf and organic ecological tobacco leaf.
Preferably, the tobacco is subjected to natural fermentation, aging (in one embodiment of the present invention, the aging time is one year), stem extraction, washing, dehydration, and flavoring.
The flavoring treatment is to soak or soak the tobacco material with the flavoring liquid, or to spray the flavoring liquid on the tobacco powder or the tobacco extract. The flavoring liquid can be prepared by decocting flavoring material with water or flavoring agent.
Further, the sugar group is selected from fructose, glucose, sucrose, maltose, hydrogenated starch hydrolysate, corn syrup, maple syrup, aspartame, licorice powder, glycyrrhetate, stevioside, mogroside, thaumatin, honey, mannose, D-mannitol, lactose, lactitol, xylitol, acesulfame potassium, neotame, aspartame, maltitol, sorbitol, saccharin sodium, cyclamate, calcium cyclamate, sucralose, alitame, isomaltulose, erythritol, isomaltooligosaccharide, galactooligosaccharide, lactulose, fructooligosaccharide, raffinose, soybean oligosaccharide, lactulose, xylooligosaccharide, inulin oligosaccharide, sucralose, glycyrrhizin, neohesperidin dihydrochalcone, curculin, miraculin, tetrandrine, diosmetin, bistame, disaccharide, sucrose, and sucrose, One or more of L-arabinose;
the flavoring agent is selected from one or more of fruit extract, aloe extract, honeysuckle extract, tincture of Momordica grosvenori, tincture of hawthorn, tincture of jujube, bergamot oil, tincture of fenugreek, tincture of hops, tincture of cacao, tincture of smoked plum, tincture of black tea, tincture of green tea, lemon oil, coffee oil, leaf oil of brussels-fruit, clove leaf oil, basil oil, sweet orange oil, native kanggeke oil, brandy oil, grapefruit oil, chrysanthemum morifolium oil, coffee powder, plum powder, red date powder, cocoa powder, green tea powder, and rum;
the filler is selected from one or more of talcum powder, calcium hydrophosphate, calcium carbonate, magnesium carbonate, calcium phosphate, corn starch, cyclodextrin, maltodextrin, D-mannitol, lactose, lactitol, xylitol, maltitol and sorbitol;
the binder is selected from one or more of starch, phosphorylated distarch phosphate, sodium carboxymethyl starch, sodium starch phosphate, maltodextrin, cyclodextrin, microcrystalline cellulose, sodium carboxymethyl cellulose, hydroxypropyl cellulose, methyl cellulose, ethyl cellulose, hydroxypropyl methyl cellulose, gelatin, gum arabic, casein, chitin, chitosan and derivatives thereof, chitosan oligosaccharide and derivatives thereof, sodium alginate, ammonium alginate, propylene glycol alginate, tara gum, mannitol, sorbitol, lactitol, guar gum, pectin, gloiopeltis gum, fenugreek gum, locust bean gum, tragacanth gum, xanthan gum, peach gum, shellac, cassia gum, tragacanth gum, carrageenin, curdlan, soluble soybean polysaccharide, tamarind gum, pullulan polysaccharide, flaxseed gum;
the emulsifier is selected from one or more of mono-fatty acid glyceride, di-fatty acid glyceride, tri-fatty acid glyceride, lecithin, soybean phospholipid, defatted cocoa powder, acetylated mono-fatty acid glyceride, polyglycerol fatty acid ester, polyethylene glycol, polyethylene sorbitan ester, poloxamer, and sucrose fatty acid ester;
the disintegrating agent is selected from one or more of starch, pregelatinized starch, microcrystalline cellulose, cross-linked polyvinylpyrrolidone, sodium carboxymethyl starch, low-substituted hydroxypropyl cellulose, cross-linked sodium carboxymethyl cellulose, gellan gum and xanthan gum;
the cooling agent is selected from one or more of menthol, peppermint oil, Asian mint oil, Asian peppermint oil, natural menthol, N-p-phenylethano menthyl formamide, N- (2- (pyridine-2-yl) ethyl) menthyl formamide and menthone;
the antioxidant is selected from one or more of tea polyphenol, butyl hydroxy anisole, sodium benzoate, dibutyl hydroxy toluene, propyl gallate, sorbic acid and potassium salt thereof, dl-alpha-tocopherol, D-alpha-tocopherol, vitamin C, calcium ascorbate, ascorbyl palmitate, D-isoascorbic acid and sodium salt thereof, carnosic acid, licorice antioxidant, bamboo leaf antioxidant, gingko biloba extract, tea extract and grape seed extract;
the lubricant is selected from one or more of stearic acid, calcium stearate, magnesium stearate, sodium stearate, potassium stearate, talcum powder, carnauba wax, beeswax, polyethylene wax, polyethylene glycol, paraffin, petroleum paraffin, microcrystalline paraffin, candelilla wax, sucrose fatty acid ester and hydrogenated vegetable oil.
The invention also provides a preparation method of the tobacco buccal tablet, which is a granulation and tabletting method and specifically comprises the following steps:
(1) mixing tobacco powder and/or tobacco extract, maca composition, sugar base, flavoring agent, filler, binder, and emulsifier uniformly, adjusting pH to 6-8, and wet granulating with granulator to obtain 14-50 mesh granule;
(2) drying the composition granules obtained by granulating in the step (1) in an oven for 0.5-2 hours, and sieving by a sieve with 14-50 meshes for finishing;
(3) mixing the obtained granule with antioxidant, refreshing agent, disintegrating agent, and lubricant, and tabletting;
or, the method is a direct compression method, comprising the following steps:
(1) mixing tobacco powder and/or tobacco extract, maca composition, sugar base, flavoring agent, filler, binder, emulsifier, antioxidant, algefacient, disintegrating agent, and lubricant uniformly, adjusting pH to 6-8, pressing into tablet in a tablet press,
(2) drying the tablets obtained in the step (1) in an oven to obtain the tablet;
wherein the pH regulator is selected from one or more of sodium carbonate, sodium bicarbonate, potassium carbonate, potassium bicarbonate, sodium citrate, potassium citrate and sodium gluconate.
The invention also provides application of the tobacco buccal tablet in the aspect of serving as a tobacco supplementary substitute.
The invention has the beneficial effects that:
according to the tobacco buccal tablet, the special sun-cured tobacco in Guizhou area is selected as the main tobacco raw material, and is subjected to aroma enhancement and/or nicotine reduction treatment, so that the tobacco buccal tablet is strong in aroma and moderate in strength, the physiological satisfaction and the taste comfort degree of the product are balanced, and the tobacco buccal tablet has important significance for improving the taste quality and market adaptability of buccal smokeless tobacco products; maca is subjected to superfine grinding or composite extraction technology to prepare maca extract, and the maca extract is optimally compounded with other plant components, so that the spicy taste of maca is reduced, the utilization efficiency of active ingredients is improved, and the maca extract has synergistic effect with tobacco materials, can resist fatigue, improve the mental state of a human body, and reduce the nicotine dependence of smokers; the product based on the invention has comfortable taste and lasting fragrance, does not generate smoke, can be used in public places, is convenient to carry, and is a novel chemical smokeless tobacco product with comfortable taste, safety and environmental protection.
Detailed Description
The following examples are intended to illustrate the invention but are not intended to limit the scope of the invention.
Example 1
The weight ratio of each component is as follows:
the maca composition comprises the following components in parts by weight: 40 parts of maca extract, 30 parts of wall-broken bee pollen, 20 parts of moringa oleifera extract and 10 parts of guarana extract.
The preparation steps are as follows:
(1) and raw material treatment
Air-cured tobacco in Guizhou area is naturally fermented and aged for one year, and then stem extraction, cleaning and dehydration treatment are carried out. According to the weight ratio of liquorice: water 1: 10, decocting the liquorice for 1 hour at 90-100 ℃, cooling, filtering, adding 5 weight percent of honey into the filtrate to prepare spice liquid, soaking the sun-cured tobacco for 24-72 hours by the spice liquid, and performing aroma enhancement treatment. Taking out the sun-cured tobacco, and drying at the temperature of 120-140 ℃ until the water content is less than 3 wt%. And crushing the dried tobacco material, and sieving the crushed tobacco material with a 80-mesh sieve to obtain tobacco coarse powder. Then carrying out secondary superfine grinding and sieving to obtain the sun-cured tobacco powder with the granularity of 500-4000 meshes.
The maca composition is obtained by compounding maca extract with wall-broken bee pollen, moringa extract, guarana extract and the like in proportion.
(2) And granulating
Dispersing xanthan gum, maca composition, fructus momordicae tincture, blueberry extract, menthol, poloxamer and the like in deionized water to prepare a binder solution for later use; after the raw and auxiliary materials are sieved by a 100-mesh sieve, the sun-cured tobacco powder, the xylitol, the sorbitol, the maltodextrin, the microcrystalline cellulose and the sodium carbonate are weighed according to the formula and fully mixed, and then wet granulation is carried out on a granulator by a 20-mesh sieve by utilizing a binder solution. Putting the wet material into a box type dryer, and drying at 50-80 ℃ until the water content of the material is 3-6 wt%. And then, granulating the dried material by using a 18-mesh sieve and storing for later use.
(3) And tabletting
Adding potassium sorbate and magnesium stearate into the dry material, uniformly mixing, feeding into a tabletting machine, and tabletting according to the specification of 1.0g of each tablet to obtain the tobacco buccal tablet. The shape of the tablet can be round, oval, diamond, cone, leaf, flower, fruit, drop, etc., and the surface of the product can be embossed with shade or shade, such as enterprise name, enterprise logo, letter abbreviation, etc.
(4) Coating and polishing
Or making sugar coating with shellac ethanol solution, syrup, acacia and pulvis Talci, performing surface polishing with edible carnauba wax, and packaging to obtain buccal tablet.
Example 2
The weight ratio of each component is as follows:
the maca composition comprises the following components in parts by weight: 30 parts of maca extract, 30 parts of medlar extract, 20 parts of gynostemma pentaphylla extract and 20 parts of kamu fruit extract.
The preparation steps are as follows:
(1) and raw material treatment
Air-cured tobacco in Guizhou area is naturally fermented and aged for one year, and then stem extraction, cleaning and dehydration treatment are carried out. According to the weight percentage of honeysuckle: water 1: 15 at 80-90 deg.c for 1-3 hr, filtering, adding corn syrup in 10 wt% into the filtrate to compound perfume liquid, and cooling. Spraying the essence solution onto sun-cured tobacco, soaking at 30-60 deg.C for 8-24 hr, and flavoring. Taking out tobacco material from the spice liquid, removing water by a rotary cage, and drying at 50-60 ℃ until the water content is less than 3 wt%. And crushing the dried tobacco material, and sieving the crushed tobacco material with a 80-mesh sieve to obtain tobacco coarse powder. Then carrying out secondary superfine grinding and sieving to obtain the mixed tobacco powder with the granularity of 300-2000 meshes.
And compounding the maca extract with the wolfberry extract, the gynostemma pentaphylla extract, the camu fruit extract and the like according to a proportion to obtain the maca composition.
(2) And tabletting
Dispersing sodium alginate in deionized water to prepare a binder solution for later use; after the raw and auxiliary materials are sieved by a 100-mesh sieve, the mixed tobacco powder, the maca composition, the isomaltitol, the isomaltooligosaccharide, the green tea powder, the green tea tincture, the corn starch, the menthol, the sodium carboxymethyl starch, the D-sodium erythorbate and the carnauba wax are weighed according to the formula, are uniformly stirred and fed into a tablet machine, and the tabletting is carried out according to the specification of 1.0g of each tablet, so that the tobacco buccal tablet is obtained. The shape of the tablet can be round, oval, diamond, cone, leaf, flower, fruit, drop, etc., and the surface of the product can be embossed with shade or shade, such as enterprise name, enterprise logo, letter abbreviation, etc. Drying the tablets in an oven to obtain the tobacco buccal tablet.
(3) Coating and polishing
The raw materials of gelatin, syrup, talcum powder, green tea tincture and the like are used as plain tablets to prepare sugar coatings, and the sugar coatings are subjected to surface polishing treatment by using Chinese wax and then packaged to obtain the tobacco buccal tablets with green tea flavor.
Example 3
The weight ratio of each component is as follows:
the maca composition comprises the following components in parts by weight: 60 parts of maca extract, 20 parts of inulin, 10 parts of assai fruit extract and 10 parts of cusaia cusaiba extract.
The preparation steps are as follows:
(1) and raw material treatment
Air-cured tobacco in Guizhou area is naturally fermented and aged for one year, subjected to stem extraction, cleaning and dehydration treatment, then subjected to heat treatment in water at the temperature of 80-90 ℃ for 1-2 hours, taken out, subjected to water removal in a rotating cage, and dried at the temperature of 40-60 ℃. According to the steps of sun-drying the tobacco: aromatic tobacco 4: 1, and sieving by a sieve of 80 meshes to obtain tobacco coarse powder. Then carrying out secondary superfine grinding and sieving to obtain the mixed tobacco powder with the granularity of 400-3000 meshes.
Dispersing 1% of bergamot oil and 5% of beta-cyclodextrin in ethanol, strongly stirring, uniformly mixing to prepare a spice liquid, uniformly spraying the spice liquid in tobacco fine powder, uniformly stirring until no agglomeration exists, and balancing moisture to obtain the aroma-enhancing mixed tobacco powder.
The maca composition is obtained by compounding the maca extract with inulin, an assai fruit extract, an custard extract and the like according to a proportion.
(2) And granulating
Dispersing arabic gum, gellan gum, fructus mume tincture, and soybean phospholipid in deionized water to obtain binder solution; after the raw and auxiliary materials are sieved by a 100-mesh sieve, the mixed tobacco powder, the maca composition, the sodium bicarbonate, the xylitol, the stevioside, the D-mannitol and the like are weighed according to the formula and are fully mixed, and wet granulation is carried out on the binder solution on a granulator by a 18-mesh sieve. And (3) putting the wet material into a box type dryer, and drying at 50-60 ℃ until the water content of the material is less than 3 wt%. And then, granulating the dried material by using a 16-mesh sieve and storing for later use.
(3) And tabletting
Adding vitamin C, magnesium stearate and the like into the dry material, feeding the mixture into a tabletting machine after uniformly stirring, and tabletting according to the specification of 0.5g of each tablet to obtain the tobacco buccal tablet. The shape of the tablet can be round, oval, diamond, cone, leaf, flower, fruit, drop, etc., and the surface of the product can be embossed with shade or shade, such as enterprise name, enterprise logo, letter abbreviation, etc.
(4) Coating and polishing
The sugar coating is prepared by using the raw materials of maltitol, gelatin, dark plum tincture and the like as plain tablets, and the tobacco buccal tablets with plum flavor are obtained by performing surface polishing treatment on candelilla wax and carnauba wax and then packaging.
Example 4
The weight ratio of each component is as follows:
the maca composition comprises the following components in parts by weight: 50 parts of maca extract, 20 parts of cola nut extract, 10 parts of alfalfa extract, 10 parts of noni extract and 10 parts of damiana extract.
The preparation steps are as follows:
(1) and raw material treatment
Air-cured tobacco in Guizhou area is naturally fermented and aged for one year, cured and aged for one year, subjected to stem extraction, cleaning and dehydration treatment, and dried at 40-60 ℃. Drying the aromatic tobacco at 40-60 deg.C. According to the flue-cured tobacco: sun-drying the tobacco: aromatic tobacco 5: 3: 2, and preparing the mixed tobacco extract by using a solvent extraction method or a supercritical extraction method.
Extracting tobacco: gum arabic: β -cyclodextrin ═ 1: 2: 3 dispersing in deionized water according to the weight ratio, stirring strongly to form uniform emulsion, and spray drying to form the tobacco extract compound.
And compounding the maca extract with a cola extract, an alfalfa extract, a noni extract, a damiana extract and the like in proportion to obtain the maca composition.
(2) And granulating
Dispersing pullulan polysaccharide, natural kang' ke oil, hops tincture, lecithin and half weight of cross-linked polyvinylpyrrolidone in deionized water to prepare a binder solution for later use; after the raw and auxiliary materials are sieved by a 100-mesh sieve, the tobacco extract compound, the maca composition, the sodium carbonate, the isomaltulose, the maple syrup, the cyclodextrin and the like are weighed according to the formula and are fully mixed, and wet granulation is carried out on a granulator by a 20-mesh sieve by utilizing a binder solution. And (3) putting the wet material into a box type dryer, and drying at 50-60 ℃ until the water content of the material is less than 3 wt%. And then, granulating the dried material by using a 20-mesh sieve and storing for later use.
(3) And tabletting
Adding potassium sorbate, peppermint oil, the other half weight of crosslinked polyvinylpyrrolidone, microcrystalline wax and the like into the dry materials, feeding the mixture into a tablet press after uniformly stirring, and tabletting according to the specification of 0.5g of each tablet to obtain the tobacco buccal tablet. The shape of the tablet can be round, oval, diamond, cone, leaf, flower, fruit, drop, etc., and the surface of the product can be embossed with shade or shade, such as enterprise name, enterprise logo, letter abbreviation, etc.
(4) Coating and polishing
The preparation method comprises the steps of preparing a sugar coating by using raw materials such as isomaltulose, corn syrup, menthol, pullulan and the like as plain tablets, polishing the surface of the plain tablets by using polyethylene glycol and beeswax, and packaging the plain tablets to obtain the tobacco buccal tablets with the bouquet flavor.
Comparative example 1
The weight ratio of each component is as follows:
the maca composition comprises the following components in parts by weight: 40 parts of maca extract, 30 parts of wall-broken bee pollen, 20 parts of moringa oleifera extract and 10 parts of guarana extract.
The procedure was as in example 1.
Comparative example 2
The weight ratio of each component is as follows:
the procedure was as in example 4.
Comparative example 3
The weight ratio of each component is as follows:
the procedure was as in example 2.
Comparative example 4
The weight ratio of each component is as follows:
the maca composition comprises the following components in parts by weight: 60 parts of maca extract, 20 parts of inulin, 10 parts of assai fruit extract and 10 parts of cusaia cusaiba extract.
The procedure was as in example 3.
The tobacco buccal tablets prepared in the examples 1 to 4 and the comparative examples 1 to 4 are subjected to sensory evaluation test, and the sensory quality evaluation method specifically comprises the following steps:
(1) sensory quality evaluation index
The sensory quality evaluation method comprises setting 9 evaluation indexes including taste, physiological strength, characteristic fragrance, tobacco fragrance, irritation, comfort, release uniformity, release persistence and oral aftertaste. The mouth feel refers to the initial comprehensive feelings of smell, taste, touch and the like of a user after the smokeless tobacco product is put into the mouth. The physiological strength refers to the physiological satisfaction felt by a user in the using process, namely the strength. The characteristic fragrance refers to the quantity and quality of the characteristic fragrance felt by a user during use. The tobacco fragrance refers to the quantity and quality of the tobacco fragrance felt by a user in the using process. The stimulation is uncomfortable feelings such as pungency, dryness and the like felt by the oral cavity, the nasal cavity, the throat, the esophagus and the like of a user in the using process. The comfortable feeling refers to the pleasant feeling that a user feels like fragrance coordination, a soft feeling, a feeling of no residue or foreign matter, and the like during use. The release uniformity refers to the release stability with time of the fragrance, physiological strength, etc. sensed by the user during use. The release duration refers to the duration of the fragrance and the physiological intensity sensed by a user in the using process. The aftertaste of the oral cavity refers to the comprehensive feeling of smell, taste and touch left in the oral cavity of a user after the use process.
(2) Sensory quality evaluation scoring rules
The sensory quality evaluation scoring rule adopts a percentile scoring method. The percentage rating method is characterized in that different weights, namely different scores, are given to all the sensory quality evaluation indexes according to the influence degree of all the sensory quality evaluation indexes on the sensory quality of the smokeless tobacco product, 9 sensory quality evaluation indexes are respectively graded according to 5 grades, 10 grades or 20 grades, and the highest score values of the 9 sensory quality evaluation indexes are added to be one hundred.
The scoring rules of the 9 sensory quality evaluation indexes are as follows: the sensory quality evaluation indexes are divided into 6 grades, the weight, the grading scale and the grading interval of each grade are shown in table 1, and the minimum scoring unit is 0.5.
The sensory quality evaluation index weight refers to the highest score value of the sensory quality evaluation index obtained in the sensory quality evaluation process. The sensory quality evaluation index scoring interval refers to a score interval corresponding to a certain evaluation scale in the sensory quality evaluation process of the sensory quality evaluation index, wherein a higher score is contained in the score interval, and a lower score is not contained in the score interval.
The stronger the sensory quality evaluation index 'irritation' is, the lower the score is; the better the sensory quality evaluation indexes of 'mouth feel' and 'aftertaste in the oral cavity' and the higher the score is; the higher the feeling of the sensory quality evaluation indexes of physiological strength, characteristic fragrance, tobacco fragrance, comfort, release uniformity and release persistence is, the higher the score is;
the total sensory quality evaluation score is obtained by arithmetically adding scores of all the sub-sensory quality evaluation indexes. The higher the total score, the better the sensory quality evaluation of the smokeless tobacco product.
TABLE 1 evaluation scoring rules for sensory quality of smokeless tobacco products
(3) Sensory quality evaluation implementation method
a. Evaluator settings
Preferably, an evaluation team is provided that contains 9 evaluators.
b. Evaluation of implementation Process
Blinding a batch of smokeless tobacco product samples to be evaluated by 3-digit digital codes (if the number of the samples is more than 999, the digital codes can be upgraded to 4 digits, and the like), and randomly processing the samples in sequence; carrying out sensory quality evaluation according to the sequence of the processed samples, distributing each sample to each person of an evaluation team before the evaluation of each sample is started, and carrying out sensory evaluation on the smokeless tobacco products; according to the weights, evaluation scales and scoring intervals of 9 sensory quality evaluation indexes in the table 1, an evaluator performs sensory quality evaluation on each evaluation index, records evaluation results in a sensory evaluation recording table, summarizes all sensory quality evaluations of an evaluation team into a single-sample sensory quality evaluation summary table, and performs evaluation result statistical processing; and after finishing the sensory quality evaluation of all the samples in sequence, summarizing the sensory quality evaluation of all the samples into a batch sample sensory quality evaluation summary table.
c. Statistical analysis of evaluation results
Preferably, the method for calculating the individual sensory quality evaluation index score is as follows: removing a lowest score and a highest score from all scores of the 9 evaluators participating in the sensory quality evaluation on the sensory quality evaluation index, wherein the remaining 7 scores are effective scores, the arithmetic mean value of the effective scores is the score of the sensory quality evaluation index, and two decimal places are reserved in the result;
and the sum of the arithmetic mean values of the scores of the single sensory quality evaluation indexes is the total score of sensory quality evaluation of the smokeless tobacco product, and two decimal places are reserved for the result. The higher the total score value, the better the sensory evaluation of the smokeless tobacco product. The specific results are shown in table 2:
TABLE 2 sensory quality evaluation statistical table for tobacco buccal tablets
As can be seen from table 2, the tobacco buccal tablet of the present invention uses the Guizhou sun-cured tobacco as the main tobacco raw material, the added maca component is processed by a special process, and is compounded with the preferred plant component to form the maca composition, the product has the characteristics of obvious characteristic aroma, small irritation, comfortable taste, stable release, good aftertaste, etc., and the same effect cannot be achieved by only using the flue-cured tobacco as the tobacco raw material or directly using the maca powder as the added component.
The tobacco buccal tablets added with the maca composition and the tobacco buccal tablets not added with the maca composition prepared by the invention are handed to people with smoking habit for evaluation. The number of participated people is 100, and the age is between 25 and 55. Dividing the persons participating in use evaluation into two groups, wherein the age and smoking years of each group of persons are equivalent, and respectively using the tobacco buccal tablets added with or not added with the maca composition for 3 months; then, the use feeling evaluation tables were filled at the time points of one week, one month, and three months, respectively, and the results are shown in table 3.
TABLE 3 usage feeling evaluation Table for tobacco buccal tablets
From the results in table 3, it can be found that the tobacco buccal tablets added with the maca composition have more effective effect of reducing nicotine dependence compared with the tobacco buccal tablets not added with the maca composition; with the prolonging of the service time, a part of evaluators also feel the effects of relieving fatigue, enhancing physical strength and the like; the buccal tobacco tablet added with the maca composition basically has no obvious oral discomfort, respiratory tract discomfort, digestive tract discomfort or other adverse feelings after being used, and has good human body tolerance.
In conclusion, the present invention effectively overcomes various disadvantages of the prior art and has high industrial utilization value.
Although the invention has been described in detail hereinabove with respect to a general description and specific embodiments thereof, it will be apparent to those skilled in the art that modifications or improvements may be made thereto based on the invention. Accordingly, such modifications and improvements are intended to be within the scope of the invention as claimed.
Claims (5)
1. The tobacco buccal tablet is characterized by comprising the following raw materials in parts by weight:
the nicotine content in the tobacco buccal tablet is 0.005-6 mg/g;
the tobacco material comprises tobacco powder and/or tobacco extract; the raw materials of the tobacco powder and the tobacco extract are tobaccos, and the tobaccos are sun-cured tobaccos produced in Guizhou areas or the combination of the sun-cured tobaccos and other tobaccos; performing natural fermentation, aging, stem extraction, cleaning and dehydration on the tobacco, and then performing aroma enhancement treatment, wherein the aroma enhancement treatment refers to soaking or infiltrating the tobacco material with spice liquid; the mesh size of the tobacco powder is larger than 2000 meshes;
the maca composition comprises the following components in parts by weight: 30-60 parts of maca extract, 20-40 parts of bee pollen, 10-30 parts of moringa oleifera extract and 5-15 parts of guarana extract;
or: 20-40 parts of maca extract, 20-40 parts of medlar extract, 10-30 parts of gynostemma pentaphylla extract and 10-30 parts of camu fruit extract;
or: 40-70 parts of maca extract, 10-30 parts of inulin, 5-20 parts of assai fruit extract and 5-20 parts of custard apple extract;
or: 40-60 parts of maca extract, 10-30 parts of cola nut extract, 5-15 parts of alfalfa extract, 5-15 parts of noni extract and 5-15 parts of damiana extract;
the preparation method of the maca extract comprises the following steps:
(1) cleaning fresh maca, cutting into slices with the thickness of 1-5mm, and drying the maca to the moisture content of less than 5% by using a low-temperature drying technology; cutting the dried maca into pieces, crushing and screening to obtain coarse powder of 20-100 meshes;
(2) 95% ethanol is used as an extracting agent, and the proportion of the extracting agent to the maca powder is 10: 1-30: 1, extracting for 1-5 hours at 50-80 ℃, separating, and concentrating in vacuum to obtain maca alcohol extract;
(3) adding 10-20 times of water into the filter residue extracted in the step (2), extracting for 0.5-3 hours at 80-100 ℃, separating, and concentrating in vacuum to obtain maca water extract;
(4) mixing maca alcohol extract and water extract according to the ratio of 1: 1-5: mixing at a ratio of 1 to obtain maca extract.
2. The tobacco-containing tablet according to claim 1, wherein the sugar group is selected from the group consisting of fructose, glucose, sucrose, maltose, hydrogenated starch hydrolysate, corn syrup, maple syrup, aspartame, licorice powder, glycyrrhetate, stevioside, mogroside, thaumatin, honey, mannose, D-mannitol, lactose, lactitol, xylitol, acesulfame potassium, neotame, aspartame, maltitol, sorbitol, saccharin sodium, cyclamate, calcium cyclamate, sucralose, alitame, isomaltulose, erythritol, isomaltooligosaccharide, galactooligosaccharide, lactulose, fructooligosaccharide, raffinose, soy oligosaccharide, lactulose, xylooligosaccharide, inulin oligosaccharide, sucralose, glycyrrhizin, neohesperidin dihydrochalcone, curculin protein, fructooligosaccharide, sucrose, fructooligosaccharide, neohesperidin dihydrochalcone, and fructooligosaccharide, One or more of miracle fruit sweet protein, Stephania tuberosa Stephania, double sweet and L-arabinose;
the flavoring agent is selected from one or more of Aloe extract, flos Lonicerae extract, fructus Siraitiae Grosvenorii tincture, fructus crataegi tincture, fructus Jujubae tincture, Foshou oil, semen Trigonellae tincture, flos Lupuli tincture, cacao tincture, mume fructus tincture, black tea tincture, green tea tincture, lemon oil, coffee oil, Bukuzu leaf oil, folium Caryophylli oil, basil oil, sweet orange oil, native Congcke oil, flos Magnoliae oil, fructus Citri Grandis oil, flos Chrysanthemi oil, coffee powder, mume fructus powder, fructus Jujubae powder, cocoa powder, green tea powder, and rum;
the filler is selected from one or more of talcum powder, calcium hydrophosphate, calcium carbonate, magnesium carbonate, calcium phosphate, corn starch, cyclodextrin, maltodextrin, D-mannitol, lactose, lactitol, xylitol, maltitol and sorbitol;
the binder is selected from one or more of starch, phosphorylated distarch phosphate, sodium carboxymethyl starch, sodium starch phosphate, maltodextrin, cyclodextrin, microcrystalline cellulose, sodium carboxymethyl cellulose, hydroxypropyl cellulose, methyl cellulose, ethyl cellulose, hydroxypropyl methyl cellulose, gelatin, gum arabic, casein, chitin, chitosan and derivatives thereof, chitosan oligosaccharide and derivatives thereof, sodium alginate, ammonium alginate, propylene glycol alginate, tara gum, mannitol, sorbitol, lactitol, guar gum, pectin, gloiopeltis gum, fenugreek gum, locust bean gum, tragacanth gum, xanthan gum, peach gum, shellac, cassia gum, tragacanth gum, carrageenin, curdlan, soluble soybean polysaccharide, tamarind gum, pullulan polysaccharide, flaxseed gum;
the emulsifier is selected from one or more of fatty acid monoglyceride, fatty acid diglyceride, fatty acid triglyceride, lecithin, soybean phospholipid, defatted cocoa powder, acetylated fatty acid monoglyceride, polyglycerol fatty acid ester, polyethylene glycol, polyethylene sorbitan ester, poloxamer, and sucrose fatty acid ester;
the disintegrating agent is selected from one or more of starch, pregelatinized starch, microcrystalline cellulose, cross-linked polyvinylpyrrolidone, sodium carboxymethyl starch, low-substituted hydroxypropyl cellulose, cross-linked sodium carboxymethyl cellulose, gellan gum and xanthan gum;
the cooling agent is selected from one or more of menthol, peppermint oil, Asian mint oil, Asian peppermint oil, natural menthol, N-p-phenylethano menthyl formamide, N- (2- (pyridine-2-yl) ethyl) menthyl formamide and menthone;
the antioxidant is selected from one or more of tea polyphenol, butyl hydroxy anisole, sodium benzoate, dibutyl hydroxy toluene, propyl gallate, sorbic acid and potassium salt thereof, dl-alpha-tocopherol, D-alpha-tocopherol, vitamin C, calcium ascorbate, ascorbyl palmitate, D-isoascorbic acid and sodium salt thereof, carnosic acid, licorice antioxidant, bamboo leaf antioxidant, gingko biloba extract, tea extract and grape seed extract;
the lubricant is selected from one or more of stearic acid, calcium stearate, magnesium stearate, sodium stearate, potassium stearate, talcum powder, carnauba wax, beeswax, polyethylene wax, polyethylene glycol, paraffin, petroleum paraffin, microcrystalline paraffin, candelilla wax, sucrose fatty acid ester and hydrogenated vegetable oil.
3. The tobacco-containing tablet according to claim 2, wherein the sugar group is selected from one or more of xylitol, sorbitol, isomalt, isomaltooligosaccharides, steviol glycosides, isomaltulose, maple syrup; the flavoring agent is selected from one or more of fructus Siraitiae Grosvenorii tincture, fructus Myrtilli extract, green tea powder, green tea tincture, mume fructus tincture, native KANGJIAOKE oil, and flos Lupuli tincture; the filler is selected from one or more of maltodextrin, corn starch, D-mannitol and cyclodextrin; the adhesive is selected from one or more of xanthan gum, sodium alginate, Arabic gum and pullulan; the emulsifier is one or more selected from poloxamer, soybean phospholipid and lecithin; the disintegrating agent is selected from one or more of microcrystalline cellulose, sodium carboxymethyl starch, gellan gum and cross-linked polyvinylpyrrolidone; the cooling agent is selected from one or more of menthol and peppermint oil; the antioxidant is selected from one or more of potassium sorbate, D-sodium erythorbate and vitamin C; the lubricant is selected from one or more of magnesium stearate, carnauba wax and microcrystalline paraffin.
4. The method for preparing the tobacco buccal tablet as claimed in any one of claims 1 to 3, wherein the preparation method is a granulation and tabletting method, and specifically comprises the following steps:
(1) mixing tobacco powder and/or tobacco extract, maca composition, sugar base, flavoring agent, filler, binder, and emulsifier uniformly, adjusting pH to 6-8, and wet granulating with granulator to obtain 14-50 mesh granule;
(2) drying the composition granules obtained by granulating in the step (1) in an oven for 0.5-2 hours, and sieving by a sieve with 14-50 meshes for finishing;
(3) mixing the obtained granule with antioxidant, refreshing agent, disintegrating agent, and lubricant, and tabletting;
or, the preparation method is a direct compression method, and comprises the following steps:
(1) mixing tobacco powder and/or tobacco extract, maca composition, sugar base, flavoring agent, filler, binder, emulsifier, antioxidant, algefacient, disintegrating agent, and lubricant uniformly, adjusting pH to 6-8, pressing into tablet in a tablet press,
(2) drying the tablets obtained in the step (1) in an oven to obtain the tablet;
in the granulation and tabletting method and the direct tabletting method, the pH regulator is selected from one or more of sodium carbonate, sodium bicarbonate, potassium carbonate, potassium bicarbonate, sodium citrate, potassium citrate and sodium gluconate.
5. Use of the tobacco-containing sheet of any one of claims 1 to 3 as a supplemental substitute for tobacco.
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