CN111449272A - Novel atomized solid matrix and preparation process thereof - Google Patents

Novel atomized solid matrix and preparation process thereof Download PDF

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Publication number
CN111449272A
CN111449272A CN202010313518.6A CN202010313518A CN111449272A CN 111449272 A CN111449272 A CN 111449272A CN 202010313518 A CN202010313518 A CN 202010313518A CN 111449272 A CN111449272 A CN 111449272A
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solid matrix
edible
agent
weight
novel atomized
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桂方晋
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Medicinal Preparation (AREA)

Abstract

The invention relates to a novel atomized solid substrate and a preparation process thereof, the novel atomized solid substrate comprises the following components, by weight, 0-40% of traditional Chinese medicine or vitamin C for reducing phlegm, relieving cough and asthma, 10-60% of filler, 0-10% of sweetening agent, 0-5% of sour agent, 10-30% of atomizing agent, 0-10% of edible essence, 3-10% of edible adhesive and 10-30% of water, and the preparation steps are as follows: s1, preparing the traditional Chinese medicines for eliminating phlegm, relieving cough and asthma or vitamin C, a filler, a sweetener and an acidulant into a powdery mixture according to the weight percentage; s2, mixing and stirring the atomizing agent, the edible essence, the edible adhesive and the water uniformly according to the weight percentage; s3, uniformly mixing the mixture prepared in the two previous steps to prepare a solid matrix with a geometrical shape; s4, drying the solid matrix obtained in the step S3 to make the moisture content of the solid matrix less than 15%. The product is made of non-tobacco materials, is healthier for human bodies, has better taste and smell and stronger experience.

Description

Novel atomized solid matrix and preparation process thereof
Technical Field
The invention relates to the field of electronic cigarettes, in particular to a novel atomized solid substrate which is healthier and has better taste, smell and experience and a manufacturing process thereof.
Background
In recent years, along with the gradual progress of global smoking control work, the health consciousness of the majority of smokers is continuously enhanced, and novel tobacco with relative health and low harm is gradually welcomed, and particularly, electronic cigarettes and non-combustible tobacco are more popular in the world. The electronic cigarette is popular because it accords with the smoking behavior habit of smokers and can also meet the smoking addiction of the smokers, namely nicotine. The existing electronic cigarette is changed into mist after liquid tobacco tar is heated and atomized, so that a user can suck the electronic cigarette. However, the smoking oil is easy to be sucked into the mouth, which causes serious discomfort of the mouth of a smoker, and meanwhile, the mouth feel and the smell are poor, and the user experience is not good. In 2015, after IQOS of Philips Moris on the market, atomized solid matrix appears, but some existing atomized solid matrix also contains tobacco powder, which is not good for health of smokers, but does not contain tobacco, so that the experience feeling is deficient, wood gas and scorched gas are too heavy, and the smokers are difficult to find resonance points similar to tobacco
Disclosure of Invention
Aiming at the existing defects, the invention provides a novel atomized solid matrix which is healthier and has better taste, smell and experience and a preparation process thereof.
The technical scheme adopted by the invention for solving the technical problems is as follows:
a novel atomized solid matrix comprises, by weight, 0-40% of traditional Chinese medicine or vitamin C for eliminating phlegm, relieving cough and asthma, 10-60% of filler, 0-10% of sweetener, 0-5% of sour agent, 10-30% of atomizing agent, 0-10% of edible essence, 3-10% of edible adhesive and 10-30% of water.
Preferably, the traditional Chinese medicine for reducing phlegm, relieving cough and relieving asthma comprises any one or a mixture of more of loquat leaves or loquat leaves, momordica grosvenori, olive, sterculia lychnophora, platycodon grandiflorum, bitter apricot seeds, perilla seeds, radix stemonae, ginkgo seeds, aster, tussilago farfarfarfara, Japanese ardisia, datura flower, physochlaina, aristolochia debilis, white mulberry root-bark, semen lepidii, rhododendron dauricum, peucedanum root, fritillaria cirrhosa, trichosanthes kirilowii maxim, fritillaria thunbergii, seaweed.
Preferably, the filling agent is a mixture of any one or more of red date, medlar, sorghum, wheat, corn, glutinous rice, coffee, cocoa, vanilla bean and black tonka bean.
Preferably, the sweetener comprises one or more of sucrose, maltose, xylitol, sorbitol, aspartame, thaumatin, stevioside, xylose and glycyrrhizin.
Preferably, the sour agent comprises a mixture of any one or more of malic acid, citric acid, tartaric acid, gluconic acid, lactic acid, fumaric acid, acetic acid and phosphoric acid.
Preferably, the atomizing agent comprises a mixture of any one or more of edible propylene glycol, edible glycerin, food-grade ester compounds and polyethylene glycol.
Preferably, the binding agent comprises a mixture of any one or more of modified starch, dextrin, guar gum, sodium alginate, gelatin, xanthan gum, agar, chitosan, pectin and peach gum.
A novel manufacturing process of an atomized solid matrix comprises the following processing and preparation steps:
s1, preparing a powdery mixture from 0-40% by weight of traditional Chinese medicines for eliminating phlegm, relieving cough and asthma or vitamin C, 10-60% by weight of a filling agent, 0-10% by weight of a sweetening agent and 0-5% by weight of a sour agent;
s2, mixing the following components in percentage by weight: mixing atomizing agent 10-30%, edible essence 0-10%, edible adhesive 3-10%, and water 10-30% at 60-80 deg.C, and stirring;
s3, uniformly mixing the mixture prepared in the S1 and S2 steps at 60-80 ℃, and cooling to prepare a solid matrix with a geometrical shape;
s4, drying the solid matrix obtained in the step S3 at 40-60 ℃ until the water content is lower than 15%.
Preferably, the powdery mixture is prepared by firstly crushing the components into dry powder and then stirring the dry powder of the components in a ball mill at the speed of 200-2000rpm for 0.5-3h at room temperature; the mixture prepared in the steps S1 and S2 is uniformly mixed by ultrasonic dispersion for 2-3 hours and stirring at the speed of 100-300 rpm.
Preferably, the solid substrate is in the shape of a sheet or cylinder.
The invention has the beneficial effects that: the raw materials used in the invention are non-tobacco materials, the traditional Chinese medicines in the non-tobacco materials are all beneficial to the respiratory system of people and are more beneficial to the health of human bodies, the wood gas and the scorched gas carried by the existing solid matrix are removed through the interaction among the components, the obtained fragrance is full and mellow, the non-tobacco substrate is more suitable for healthy smokers, the health of the smokers can be effectively protected, the taste and the smell are better, and the experience feeling is stronger. The manufactured product is convenient to store and process, can be processed into different shapes according to requirements, and is more beneficial to use.
Detailed Description
To more clearly illustrate the objects, technical solutions and advantages of the embodiments of the present invention, the present invention will be further described with reference to the following embodiments, which are clearly and completely described, and it is obvious that the described embodiments are some, but not all embodiments of the present invention. All other embodiments, which can be derived by a person skilled in the art from the embodiments of the present invention without inventive step, are within the scope of the present invention.
The embodiment of the invention provides a novel atomized solid matrix and a manufacturing process thereof, which comprises the following steps:
s1, preparing a powdery mixture from 0-40% by weight of traditional Chinese medicines for eliminating phlegm, relieving cough and asthma or vitamin C, 10-60% by weight of a filling agent, 0-10% by weight of a sweetening agent and 0-5% by weight of a sour agent; as the conventional forms of the traditional Chinese medicines are not powdery basically, the traditional Chinese medicines are mixed with other substances to form powdery substances, the components are firstly crushed into dry powder, and then the dry powder of the components is stirred in a ball mill at the room temperature at the speed of 200-2000rpm for 0.5-3h to prepare the traditional Chinese medicine, so that the particle aggregates are crushed, and the components can be mixed more uniformly; the traditional Chinese medicines for reducing phlegm, relieving cough and relieving asthma comprise any one or a mixture of more of loquat leaves or loquats, momordica grosvenori, olives, sterculia lychnophora, platycodon grandiflorum, bitter almonds, perilla seeds, radix stemonae, ginkgo seeds, aster, tussilago farfarfarfara, Japanese ardisia herb, datura flower, radix physochlainae, fructus aristolochiae, cortex mori, semen lepidii, dahurian rhododendron leaf, radix peucedani, bulbus fritillariae cirrhosae, fructus trichosanthis, thunberg fritillary bulb, seaweed and kelp, and can help the respiratory system, and the traditional Chinese medicines can be used as effective components to solve the respiratory system hair disease caused by smoking, and protect the health of; the filler is a mixture consisting of any one or more of red dates, medlar, sorghum, wheat, corn, glutinous rice, coffee, cocoa, vanilla beans and black beans, the natural plants have certain water absorption capacity, and the water absorption ensures that the product can always keep a certain water content without cracking and forming due to over-drying, and meanwhile, the fragrance of the product can be locked through certain water, and under the condition that the product is heated and is not combusted, the water is evaporated and the odor generated along with various substances of the product is emitted into smoke; the sweetener comprises one or more of sucrose, maltose, xylitol, sorbitol, aspartame, sweetener, steviosin, xylose, and glycyrrhizin; the sour agent comprises a mixture consisting of one or more of malic acid, citric acid, tartaric acid, gluconic acid, lactic acid, fumaric acid, acetic acid and phosphoric acid, and wood gas and scorched gas generated by the existing atomized solid matrix are removed through the interaction of the malic acid, the citric acid, the tartaric acid, the gluconic acid, the lactic acid, the fumaric acid, the acetic acid and the phosphoric acid, so that the taste and the smell of the product are more fragrant and better.
S2, mixing the following components in percentage by weight: mixing atomizing agent 10-30%, edible essence 0-10%, edible adhesive 3-10%, and water 10-30% at 60-80 deg.C, and stirring; the atomizing agent comprises a mixture consisting of one or more of edible propylene glycol, edible glycerin, a food-grade ester compound and food-grade polyethylene glycol, and can generate aerosol by atomization when being heated, so that the smoke quantity is increased, the situation of smoking cigarettes is better reached, the use experience of people is enhanced, and the edible raw materials are safer and harmless to human bodies; the addition of the edible essence can tune the tobacco fragrance and enhance the smell of the product on the basis of the product, so that the product has full and mellow fragrance, is more suitable for healthy smokers, and protects the health of the smokers while satisfying the smoking experience; the adhesive comprises any one or a mixture of more of modified starch, dextrin, guar gum, sodium alginate, gelatin, xanthan gum, agar, chitosan, pectin and peach gum, can be used in daily food, is harmless to human bodies, has good solubility in water, can form good viscosity after being dissolved, and is beneficial to product forming.
S3, uniformly mixing the mixture prepared in the S1 and S2 steps at 60-80 ℃, and cooling to prepare a solid matrix with a geometrical shape; in this case, the two preceding steps produce respective mixed semi-finished products which, when mixed, the particles are uniformly mixed by ultrasonic dispersion for 2 to 3 hours and stirring at the speed of 100 plus 300rpm, the particle aggregates are dispersed by the ultrasonic dispersion, the two semi-finished products are mixed more uniformly without generating agglomeration, in the case of a solid substrate of geometric shape, which can be used in different processes according to different requirements, the solid substrate is preferably in the form of a sheet or cylinder, for example, a rolled sheet for use in subsequent shredding, or cast directly into a mold of a corresponding form, such as a cylinder, thus, whether the cigarette is cut into threads or the cylindrical structure is adopted, the cigarette can be made by utilizing the existing equipment or the cigarette can be filled in a paper tube to be made into a shape similar to a real cigarette.
S4, drying the solid substrate obtained in the step S3 at 40-60 ℃ to ensure that the moisture content is lower than 15%, keeping the moisture content of the product at a certain level by drying, better keeping the shape and the fragrance of the product, avoiding the problem that the shape is not easy to keep or the product is damp and mildewed due to excessive moisture content of the product, keeping certain moisture content, being more beneficial to the use of the product, the fragrance emission and the fragrance maintenance in use, and drying can be carried out by a blowing or vacuum drying mode.
The specific case is as follows:
example 1:
weighing 15g of dried momordica grosvenori powder, 30g of dried red date powder, 15g of cocoa powder, 5g of sorbitol and 1g of malic acid, uniformly mixing for later use, weighing 15g of glycerol, 5g of edible essence, 15g of deionized water and 5g of modified starch, heating to 65 ℃, and uniformly stirring for later use. Mixing the above two mixed products at 65 deg.C, rolling into 0.2-0.3mm thick sheet with rolling device, and drying at 50 deg.C with vacuum drying oven until the water content is less than 10%. Cutting the sheet into 1.0-1.5mm thread with shredding device, and rolling into cigarette shape or filling into empty paper tube.
Example 2:
weighing 5g of olive dry powder, 40g of glutinous rice dry powder, 20g of vanilla bean powder and 5g of sorbitol, uniformly mixing for later use, weighing 15g of glycerol, 5g of edible essence, 15g of deionized water and 5g of guar gum, heating to 70 ℃, and uniformly stirring for later use. Mixing the above two mixed products at 70 deg.C, pouring into cylindrical mold with diameter of 7.4mm and depth of 12.5mm, cooling, molding, drying at 50 deg.C with vacuum drying oven until water content is less than 15%, and rolling into cigarette shape or filling into hollow paper tube.
It will be understood that modifications and variations can be made by persons skilled in the art in light of the above teachings and all such modifications and variations are intended to be included within the scope of the invention as defined in the appended claims.

Claims (10)

1. A novel atomized solid matrix characterized by: comprises the following components, by weight, 0-40% of traditional Chinese medicine or vitamin C for eliminating phlegm, relieving cough and asthma, 10-60% of filler, 0-10% of sweetener, 0-5% of sour agent, 10-30% of atomizing agent, 0-10% of edible essence, 3-10% of edible adhesive and 10-30% of water.
2. The novel atomized solid matrix according to claim 1, characterized in that: the traditional Chinese medicine for eliminating phlegm, relieving cough and relieving asthma comprises any one or a mixture of more of loquat leaves or loquat, fructus momordicae, olive, sterculia seed, platycodon grandiflorum, bitter apricot seed, perilla seed, radix stemonae, ginkgo seed, aster, tussilago, Japanese ardisia, datura flower, radix physochlainae, aristolochia debilis, white mulberry root-bark, semen lepidii, dahurian rhododendron leaf, radix peucedani, bulbus fritillariae cirrhosae, fructus trichosanthis, thunberg fritillary bulb, seaweed and kelp.
3. The novel atomized solid matrix according to claim 1, characterized in that: the filler is one or more of fructus Jujubae, fructus Lycii, jowar, semen Tritici Aestivi, semen Maydis, Oryza Glutinosa, coffee, cacao, vanilla bean, and black bean.
4. The novel atomized solid matrix according to claim 1, characterized in that: the sweetener comprises one or more of sucrose, maltose, xylitol, sorbitol, aspartame, thaumatin, stevioside, xylose, and glycyrrhizin.
5. The novel atomized solid matrix according to claim 1, characterized in that: the sour agent comprises one or more of malic acid, citric acid, tartaric acid, gluconic acid, lactic acid, fumaric acid, acetic acid, and phosphoric acid.
6. The novel atomized solid matrix according to claim 1, characterized in that: the atomizing agent comprises any one or a mixture of more of edible propylene glycol, edible glycerin, food-grade ester compounds and polyethylene glycol.
7. The novel atomized solid matrix according to claim 1, characterized in that: the adhesive comprises any one or a mixture of more of modified starch, dextrin, guar gum, sodium alginate, gelatin, xanthan gum, agar, chitosan, pectin and peach gum.
8. A novel manufacturing process of an atomized solid matrix is characterized in that: the processing and preparation steps are as follows:
s1, preparing a powdery mixture from 0-40% by weight of traditional Chinese medicines for eliminating phlegm, relieving cough and asthma or vitamin C, 10-60% by weight of a filling agent, 0-10% by weight of a sweetening agent and 0-5% by weight of a sour agent;
s2, mixing the following components in percentage by weight: mixing atomizing agent 10-30%, edible essence 0-10%, edible adhesive 3-10%, and water 10-30% at 60-80 deg.C, and stirring;
s3, uniformly mixing the mixture prepared in the S1 and S2 steps at 60-80 ℃, and cooling to prepare a solid matrix with a geometrical shape;
s4, drying the solid matrix obtained in the step S3 at 40-60 ℃ until the water content is lower than 15%.
9. The process for the preparation of the novel atomized solid matrix according to claim 8, characterized in that: the powdery mixture is prepared by firstly crushing each component into dry powder, and then stirring the dry powder of each component in a ball mill at the speed of 200-2000rpm for 0.5-3h at room temperature; the mixture prepared in the steps S1 and S2 is uniformly mixed by ultrasonic dispersion for 2-3 hours and stirring at the speed of 100-300 rpm.
10. The process for the preparation of the novel atomized solid matrix according to claim 8, characterized in that: the solid substrate is in the shape of a sheet or cylinder.
CN202010313518.6A 2020-04-20 2020-04-20 Novel atomized solid matrix and preparation process thereof Pending CN111449272A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111493069A (en) * 2020-04-21 2020-08-07 桂方晋 Solid chlorine dioxide sustained release agent and preparation method thereof
CN115500540A (en) * 2022-09-27 2022-12-23 南京诚达汇智新材料科技有限公司 Preparation method of Chinese herbal medicine atomization slice

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CN110477438A (en) * 2019-08-26 2019-11-22 广东神农烟科技术有限公司 It is a kind of to heat incombustible smoking article and preparation method thereof
CN110537718A (en) * 2019-08-13 2019-12-06 云南中烟工业有限责任公司 Method for improving aroma richness and aroma harmony of non-burning heated cigarette

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CN101124958A (en) * 2007-09-03 2008-02-20 闵祥梅 Health-care granada sucking product and its preparing process
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111493069A (en) * 2020-04-21 2020-08-07 桂方晋 Solid chlorine dioxide sustained release agent and preparation method thereof
CN115500540A (en) * 2022-09-27 2022-12-23 南京诚达汇智新材料科技有限公司 Preparation method of Chinese herbal medicine atomization slice

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