CN112401292A - Atomized smoking material for heating non-combustible product - Google Patents
Atomized smoking material for heating non-combustible product Download PDFInfo
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- CN112401292A CN112401292A CN202011303071.0A CN202011303071A CN112401292A CN 112401292 A CN112401292 A CN 112401292A CN 202011303071 A CN202011303071 A CN 202011303071A CN 112401292 A CN112401292 A CN 112401292A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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Abstract
An atomized smoking material for heating non-combustible products is prepared from areca nut powder, starch, adhesive, pH regulator, smoking assistant and edible perfume through mixing, and thickening or sieving. The atomized smoking material for heating the non-combustible product releases the content of the betel nut in a heating mode, meets the requirement of consumers on the betel nut, and simultaneously can avoid the damage of crude fibers in the betel nut to the oral cavity and reduce the side effect caused by chewing the betel nut.
Description
[ technical field ] A method for producing a semiconductor device
The invention belongs to the technical field of production of heating non-combustible products. More particularly, the present invention relates to an atomized smoking material for heating a non-combustible article.
[ background of the invention ]
The heat non-combustible product is a novel consumer product developed on the basis of the traditional tobacco product, and the traditional tobacco product cracks chemical components in tobacco materials after being combusted, and finally generates smoke capable of being smoked. The components in the smoke are complex and various, such as nicotine, phenol, styrene, acetaldehyde, hydrogen acid salt, nitrate, sulfate, ammonium salt and the like which pose a threat to health.
In order to reduce the health hazard brought by smoking tobacco products, a heating non-combustion tobacco product is developed, compared with the traditional combustion type tobacco, the heating non-combustion tobacco releases some smoke components after being heated within the range of 200-400 ℃ in a low-temperature environment, and some smoke components do not reach the condition of initiating the combustion of tobacco materials, so that the harmful components in the smoke can be effectively reduced, but substances such as nicotine and the like which are addictive to people are still released.
The non-combustible heating product at the present stage is mainly electrically heated, the temperature controllability can be realized by adopting an electronic heater to heat the non-combustible heating product, the heat of the heater is absorbed by the smoking material, the fragrant substances and the like in the smoking material are released along with the smoke, and the smoke which can be sucked by consumers is formed. The tobacco product is made to be non-combustible by heating, although the release of harmful substances can be reduced, nicotine still exists, so that the application of the non-combustible by heating to non-tobacco raw materials is a new direction of non-combustible by heating and has outstanding use value. Some non-tobacco herbal type atomizing cores have therefore been developed in the recent past.
The areca nuts contain arecoline, which is alkaloid with the effect similar to that of nicotine, and can bring physiological strength to consumers while sucking, but the utilization of the areca nuts by people is limited to chewing. Research shows that the areca nut raw fruit contains 10.8% of crude fiber, and the crude fiber can damage the epithelial cells of the oral cavity of a human body when a person chews the areca nut, so that the mucosal layer of the oral cavity is damaged, and the canceration probability is increased. The chemical substances contained in betel nut form nitrosamine substances after chewing, and the teeth are seriously abraded after long-term chewing. Chewing the dry betel nut can also cause the symptoms of dizziness, palpitation, sweating, tremor, blood pressure drop, abdominal pain, constipation and other betel nut drunkenness. In addition, chewing betel nut to spit out residues also has the problems of inconvenience and environmental protection.
Aiming at the technical defects in the prior art, the inventor finally completes the invention through a large amount of experimental research and analytical summary.
[ summary of the invention ]
[ problem to be solved ]
It is an object of the present invention to provide an atomised smoking material for heating non-combustible articles.
[ solution ]
The invention is realized by the following technical scheme.
The present invention relates to an atomised smoking material for heating non-combustible articles.
The atomized fuming material is composed of 30-70 parts by weight of dry areca nut powder, 5-15 parts by weight of starch, 2-10 parts by weight of adhesive, 0.1-2.0 parts by weight of acid-base regulator, 5-20 parts by weight of fuming auxiliary agent and 0.2-2.0 parts by weight of edible spice.
According to a preferred embodiment of the invention, the atomized smoking material is composed of 40-60 parts by weight of dry areca nut powder, 8-12 parts by weight of starch, 4-8 parts by weight of adhesive, 0.6-1.4 parts by weight of acid-base regulator, 9-16 parts by weight of smoking assistant and 0.8-1.4 parts by weight of edible spice.
According to another preferred embodiment of the invention, the arecoline content of the dry powder of areca nuts is 0.05-1.0% by weight.
According to another preferred embodiment of the invention, the grain size of the betel nut dry fruit powder is 40-200 meshes.
According to another preferred embodiment of the invention, the starch is corn starch, potato starch, wheat starch, sorghum starch or sweet potato starch having a purity of more than 90% by weight.
According to another preferred embodiment of the invention, the adhesive is one or more adhesives selected from the group consisting of water-soluble starch, sodium carboxymethyl cellulose, guar gum, pectin, and chitosan.
According to another preferred embodiment of the present invention, the pH regulator is one or more pH regulators selected from the group consisting of sodium carbonate, sodium bicarbonate, sodium lactate, potassium carbonate, dipotassium citrate, monopotassium citrate, potassium malate and monopotassium malate.
According to another preferred embodiment of the invention, the smoking aid is one or more smoking aids selected from glycerol, propylene glycol, triacetin, stearic acid or hexadecane.
According to another preferred embodiment of the present invention, the flavorant is one or more flavorants selected from the group consisting of menthol, vanillin, ethyl maltol, 1, 4-dimethylpyrazine, coffee flavor, blueberry flavor, apple flavor, orange juice flavor, and similar flavor products.
According to another preferred embodiment of the invention, the atomized smoking material is a sheet-like smoking material with a thickness of 0.1 to 0.5mm, a granular material with a diameter of 0.3 to 1.2mm or a powdery smoking material with a particle size of 40 to 100 meshes.
The present invention will be described more specifically below.
The invention relates to an atomized smoking material for heating non-combustible products, which consists of 30-70 parts by weight of dry areca nut powder, 5-15 parts by weight of starch, 2-10 parts by weight of adhesive, 0.1-2.0 parts by weight of acid-base regulator, 5-20 parts by weight of smoking aid and 0.2-2.0 parts by weight of edible spice.
The existing research results show that the arecoline content of the arecoline dry fruit powder is greater than 50mg/mL, the arecoline content is greater than 10mg/mL, the arecoline powder can inhibit cell growth and DNA synthesis, excessive consumption of the arecoline can cause the phenomena of vomiting, diuresis, lethargy, convulsion and the like, but the appropriate consumption of the arecoline has the effects of promoting gastrointestinal digestion, promoting blood flow and the like.
In the invention, the main function of the areca nut dry fruit powder in the atomized smoking material is to provide areca nut taste and provide physiological satisfaction for consumers. As the arecoline contained in the areca is an M-like receptor agonist, is easy to permeate blood brain barrier and is a main active substance which influences the nervous system, a certain amount of arecoline can cause the body to be excited, and a certain anti-fatigue and anti-depression effect can be achieved.
The arecoline content of the areca nut dry fruit powder is 0.05-1.0% by weight. If the arecoline content of the areca nut dry fruit powder is less than 0.05%, the physiological satisfaction of consumers cannot be met; if the arecoline content of the dry powder of areca nuts is higher than 1.0%, an overstimulation reaction can be generated, such as dizziness, palpitation, sweating, tremor, blood pressure reduction and other areca nut intoxication manifestations can be caused. Accordingly, the arecoline content of the dry powder of areca nuts is suitably 0.05-1.0%, preferably 0.08-0.8%. More preferably 0.12 to 0.5%.
The granularity of the betel nut dry fruit powder used in the invention is 40-200 meshes. Experimental research shows that if the grain size of the areca nut dry fruit powder is below 40 meshes, the distribution of the areca nut dry fruit powder grains in the atomized smoking material is uneven, so that the balance of smoking taste is influenced. The non-combustible heating product is mainly characterized in that the heating sheet of the electronic heating equipment is used for heating the smoking material, the heating sheet is dispersed in a circumferential shape after heat is produced, if the areca powder is not uniformly distributed, the positions with high content of the areca powder can cause strong taste, and the positions with low content of the areca powder do not have the areca taste; if the particle size of the areca nut dry fruit powder is more than 200 meshes, the prepared atomized smoking material has high compactness, low overall bulkiness and small pore diameter, and is not beneficial to releasing fragrant substances in the smoking process. Therefore, the granularity of the betel nut dry fruit powder is reasonable to be 40-200 meshes, preferably 70-180 meshes, and more preferably 100-160 meshes.
The dry powder of areca nuts used in the present invention is a product currently sold in the market, for example, sold under the name of olive areca nut by valia, soursa, ma.
Starch is a high molecular carbohydrate, a polysaccharide composed of a single type of sugar unit. The starch is divided into straight-chain molecules and branched-chain molecules, wherein the straight-chain molecules are formed by alpha-1, 4-glycosidic bonds of D-hexacyclic glucose, the branched-chain molecules are alpha-1, 6-glycosidic bonds at the branch positions, and the rest are alpha-1, 4-glycosidic bonds. Amylose contains several hundred glucose units and amylopectin contains several thousand glucose units.
In the present invention, the primary function of starch in the atomized smoking material is to act as a thickener to adjust the consistency of the atomized smoking material slurry. The starch used in the present invention is corn starch, potato starch, wheat starch, sorghum starch or sweet potato starch having a purity of 90% by weight or more.
Starches having a purity of 90% or more are used mainly because if the starch purity is below 90% by weight, the viscosity control of the slurry is affected and excessive foreign impurities are introduced.
Wherein the corn starch (corn starch) is prepared by soaking corn in 0.3% sulfurous acid, crushing, sieving, precipitating, drying, and grinding. The corn contains fat, phosphorus element and vitamin B2, and contains linoleic acid, vitamin E, glutathione, selenium and dietary fiber. The corn starch used in the present invention is a product currently marketed, for example, by Shanghai Kaolingjian under the trade name edible corn starch.
Potato Starch (Potato Starch) is a product obtained by washing potatoes, pulverizing, filtering, precipitating, and oven drying, and can be used as a thickener. The potato starch used in the present invention is a product currently marketed, for example, by deep-invasive chemical company, Inc. in Guangzhou under the trade name food-grade potato starch.
The wheat starch is mainly applied to food thickeners, gelling agents, adhesives or stabilizers and the like. The wheat starch used in the present invention is a product currently marketed, for example, by deep-invasive chemical company, Guangzhou, under the trade name food-grade wheat starch.
The sorghum starch used in the present invention is a product currently on the market, for example, sorghum starch sold under the trade name sorghum flour by Shandong Kezhen Xiang Liou.
Sweet potato is rich in nutrition, and contains a large amount of sugar, protein, fat and various vitamins and minerals. The sweet potato starch is heated into paste, so that the heat-labile and water-soluble vitamin C is well protected, and the mineral substances in the vitamin C play an important role in maintaining and regulating the functions of a human body. The sweet potato starch used in the present invention is a product sold in the market at present, for example, a sweet potato starch sold by deep-creative chemical company ltd, guangzhou, under the trade name of food-grade sweet potato.
Of course, all other starches which have the above-mentioned effects may be used in the present invention, except that they do not adversely affect the atomized smoking material and its articles of manufacture, and are within the scope of the present invention.
In the context of the present invention, an adhesive is understood to be a type of organic or inorganic natural substance or organic or inorganic synthetic substance which is capable of bonding together one or more different materials and which, after curing, has sufficient strength.
According to the invention, the main function of the adhesive in the atomized smoking material is a sticking effect, i.e. the adhesive is an organic or inorganic natural or synthetic substance which has sufficient strength after being solidified, namely, the adhesive is used for sticking dispersed substances such as fragrant substances, plant herbal powder, fibers and the like together.
The adhesive used in the invention is one or more adhesives selected from water-soluble starch, sodium carboxymethyl cellulose, guar gum, pectin or chitosan.
The water-soluble starch is a controlled low-degree hydrolysis product between starch and starch sugar, has strong hydration, can be dissolved at normal temperature, has good viscosity and carrier effect, strong heat resistance, difficult browning, good emulsification effect and thickening effect, small hygroscopicity, difficult agglomeration, good film forming property and the like. The water-soluble starch used in the present invention is a product currently marketed, for example, by Yunfeng starch Co., Ltd, of Nantong under the trade name of food grade water-soluble starch.
Sodium carboxymethylcellulose has binding, thickening, reinforcing, emulsifying, water-retaining, suspending, and other effects, and is commonly used as a thickener, a drug carrier, an adhesive, and an anti-redeposition agent. The sodium carboxymethylcellulose used in the present invention is a product currently marketed, for example, by the Kovar chemical Co., Ltd., Nichtu, under the trade name of food grade sodium carboxymethylcellulose.
Guar gum is a macromolecular natural hydrophilic colloid, belongs to natural galactomannan, is a natural thickener, is white to yellowish free flowing powder, can be dissolved in cold water or hot water, and can form a colloidal substance when meeting water, thereby achieving the effect of rapid thickening. The guar gum used in the present invention is a product currently marketed, for example, by Zhejiang Kangxing Biotech Limited under the trade name food grade guar.
Pectin is a heteropolysaccharide widely existing in the primary wall and the cell intermediate sheet layer of plant cell walls, and can be used as an emulsifier, a stabilizer and a thickener according to the food additive edible health standard (GB 2760-2014). The pectin used in the present invention is a product currently marketed, for example, by Shandong McRong bioengineering, Inc. under the trade name food grade pectin.
The chitosan is a product of natural polysaccharide chitin with partial acetyl removed, has multiple physiological functions of biodegradability, biocompatibility, nontoxicity, bacteriostasis, cancer resistance, lipid reduction, immunity enhancement and the like, and is widely applied to the fields of food additives, textiles, agriculture, environmental protection, antibacterial agents, biomedicine and other daily chemical industries. The chitosan used in the present invention is a product currently sold in the market, for example, chitosan sold under the trade name of food grade chitosan by Shenzhen topology Biotech Limited.
Of course, any other adhesive that performs the above-described function may be used in the present invention, provided that they do not adversely affect the atomized smoking material and its articles of manufacture, and such adhesives are within the scope of the present invention.
In the invention, the main function of the acid-base regulator in the atomized smoking material is to regulate the taste and irritation of smoke.
The acid-base modifier used in the present invention is one or more acid-base modifiers selected from sodium carbonate, sodium bicarbonate, sodium lactate, potassium carbonate, dipotassium citrate, monopotassium citrate, potassium malate, and monopotassium malate, which are currently commercially available products, such as sodium lactate sold under the trade name food-grade sodium lactate by Shandong Jiu chemical Co., Ltd, dipotassium citrate sold under the trade name dipotassium citrate by Shandong Jiu chemical Co., Ltd, monopotassium citrate sold under the trade name monopotassium citrate by Shandong Jiu chemical Co., Ltd, potassium malate sold under the trade name potassium malate by Shandong Jiu chemical Co., Ltd, monopotassium malate sold under the trade name monopotassium malate by Shandong Jiu chemical Co., Ltd, and sodium bicarbonate sold under the trade name sodium bicarbonate by Suzhou Kenshi chemical Co., Ltd.
Of course, any other pH modifying agents which have the above-described effects may be used in the present invention, provided that they do not adversely affect the atomized smoking material and its articles of manufacture, and are within the scope of the present invention.
In the present invention, the primary function of the smoking aid in the atomized smoking material is that the smoking material, when heated, volatilizes a smoke carrying flavour material to provide consumer smoking.
The smoking aid used in the present invention is one or more selected from the group consisting of glycerol, propylene glycol, triacetin, stearic acid and hexadecane, which are currently commercially available products such as propylene glycol sold under the trade name food grade propylene glycol by Guangzhou Brilliant alliance chemical Co., Ltd, triacetin sold under the trade name food grade triacetin by Guangzhou Brilliant alliance chemical Co., Ltd, stearic acid sold under the trade name food grade stearic acid by Guangzhou Qianjiaojian Fine chemical Co., Ltd, and hexadecane sold under the trade name food grade hexadecane by Guangzhou Qianjiaojian Fine chemical Co., Ltd.
Of course, all other smoking aids having the above-described functions may be used in the present invention, provided they do not adversely affect the atomized smoking material of the present invention and its articles, and are within the scope of the present invention.
In the invention, the edible spice has the main functions of providing fragrance for the atomized smoking material, changing the style of smoke and improving the smoke taste.
The flavorant used in the present invention is one or more flavorants selected from the group consisting of menthol, vanillin, ethyl maltol, 1, 4-dimethylpyrazine, coffee flavor, blueberry flavor, apple flavor, orange juice flavor, and similar flavor products.
Among them, menthol is a main component of peppermint and peppermint essential oils, exists in a free and ester state, and is useful as an aromatizing agent for toothpaste, perfume, beverage, candy, etc., and menthol used in the present invention is, for example, a product sold under the trade name food grade menthol by south Hunan China Biotechnology Co., Ltd.
The vanillin has a chemical name of 3-methoxy-4-hydroxybenzaldehyde, has vanilla bean fragrance and strong milk fragrance, has functions of increasing and fixing fragrance, and is widely used in industries of cosmetics, tobacco, cakes, candies, baked foods and the like. The vanillin used in the present invention is, for example, a product sold under the trade name food grade vanillin by Wuhananabai pharmaceutical chemical Co.
The ethyl maltol is a safe and reliable food additive with low dosage and remarkable effect, and the molecular formula is C7H8O3It is a good fragrance synergist for tobacco, food, beverage, essence, fruit wine, daily cosmetics, etc. The ethyl maltol used in the present invention is, for example, a product sold under the trade name food grade ethyl maltol by wuhananea pharmaceutical chemical limited.
1, 4-dimethylpyrazine is a food flavor additive having the flavor of nut, mildew, roasted, nut and roasted foods. The 1, 4-dimethylpyrazine used in the present invention is, for example, a product sold under the trade name of 1, 4-dimethylpyrazine by Shanghai Haoxin spices Ltd.
The coffee-flavored flavor, the blueberry-flavored flavor, the apple-flavored flavor, and the orange-flavored flavor used in the present invention are all currently marketed products, such as coffee-flavored flavor sold under the trade name mellow coffee by Balaophora yunnanensis Biotech Co., Ltd, blueberry-flavored flavor sold under the trade name blueberry essence by Balaophora yunnanensis Biotech Co., Ltd, apple-flavored flavor sold under the trade name green apple essence by Balaophora yunnanensis Biotech Co., Ltd, and orange-flavored flavor sold under the trade name orange juice essence by Balaophora yunnanensis Biotech Co., Ltd.
Of course, all other flavorants having the above-described effects may be used in the present invention, provided they do not adversely affect the atomized smoking material and articles thereof of the present invention, and are within the scope of the invention.
In the invention, when the contents of the starch, the adhesive, the pH regulator, the fuming auxiliary agent and the edible spice are in the range, if the content of the betel nut dry fruit powder is lower than 30 parts by weight, the aroma of the betel nut is insufficient and the satisfaction of the betel nut is weak; if the content of the areca nut dry fruit powder is higher than 70 parts by weight, the arecoline content is too high, which causes suction discomfort and high cost; therefore, the content of the areca nut dry fruit powder is preferably 30 to 70 parts by weight, more preferably 40 to 60 parts by weight, and still more preferably 46 to 54 parts by weight.
Similarly, when the content of the areca nut dry fruit powder, the adhesive, the pH regulator, the smoking aid and the edible spice is in the range, if the content of the starch is lower than 5 parts by weight, the atomized smoking material cannot be effectively thickened, and the using effect is poor; if the starch content is higher than 15 parts by weight, the atomized smoking material of the invention is too viscous, and can cause bad smell after starch gelatinization; therefore, the content of starch is preferably 5 to 15 parts by weight, more preferably 8 to 12 parts by weight, and still more preferably 8.8 to 11.2 parts by weight.
When the content of the betel nut dry fruit powder, the starch, the pH regulator, the smoking assistant and the edible spice is in the range, if the content of the adhesive is lower than 2 parts by weight, the adhesion degree between the raw materials of the atomized smoking material is insufficient, and the atomized smoking material is difficult to mold or is not easy to mold; if the content of the adhesive is higher than 10 parts by weight, the atomized smoking material of the invention is too viscous, and the raw material of the adhesive is too heavy to cause peculiar smell; therefore, the content of the adhesive is reasonably 2 to 10 parts by weight, preferably 4 to 8 parts by weight, and more preferably 5 to 7 parts by weight.
When the contents of the areca nut dry fruit powder, the starch, the adhesive, the fuming auxiliary agent and the edible spice are in the range, if the content of the acid-base regulator is lower than 0.1 part by weight, the capacity of regulating the taste and the irritation of smoke is insufficient, the smoke fragrance is not obviously diffused, and the physiological strength is too strong; if the content of the acid-base regulator is higher than 2.0 parts by weight, the smoke stimulation is too strong, and the smoke comfort is reduced along with a certain degree of peculiar smell; therefore, the content of the pH adjusting agent is feasible to be 0.1 to 2.0 parts by weight, preferably 0.6 to 1.4 parts by weight, and more preferably 0.8 to 1.2 parts by weight.
When the content of the betel nut dry fruit powder, the starch, the adhesive, the acid-base regulator and the edible spice is in the range, if the content of the fuming auxiliary agent is lower than 5 parts by weight, the capacity of volatilizing the fragrant substances by heating to form smoke is obviously insufficient; if the content of the smoking assistant is higher than 20 parts by weight, the atomized smoking material of the invention generates too dense smoke, which affects the experience of smokers, and is easy to absorb moisture, thus being very unfavorable for the storage of cigarette products; therefore, it is feasible that the content of the smoke generating aid is 5 to 20 parts by weight, preferably 9 to 16 parts by weight, more preferably 11 to 14 parts by weight.
When the content of the betel nut dry fruit powder, the starch, the adhesive, the acid-base regulator and the smoking aid is in the range, if the content of the edible spice is lower than 0.2 part by weight, the style of smoke cannot be fully changed, and the smoke taste cannot be improved; if the content of the edible spice is higher than 2.0 parts by weight, the aroma of the edible spice suppresses the characteristic aroma of the plant raw materials; therefore, the content of the flavorant is preferably 0.2 to 2.0 parts by weight, more preferably 0.8 to 1.4 parts by weight, and still more preferably 1.0 to 1.2 parts by weight.
Preferably, the atomized smoking material consists of 40-60 parts by weight of dry areca nut powder, 8-12 parts by weight of starch, 4-8 parts by weight of adhesive, 0.6-1.4 parts by weight of acid-base regulator, 9-16 parts by weight of smoking aid and 0.8-1.4 parts by weight of edible spice.
More preferably, the atomized smoking material consists of 46-54 parts by weight of dry areca nut powder, 8.8-11.2 parts by weight of starch, 5-7 parts by weight of adhesive, 0.8-1.2 parts by weight of acid-base regulator, 11-14 parts by weight of smoking aid and 1.0-1.2 parts by weight of edible spice.
According to the invention, the atomized smoking material is a flaky smoking material with the thickness of 0.1-0.5 mm and the diameter of 0.3-1.2 mm, or a powdery smoking material with the granularity of 40-100 meshes.
The atomized smoking material of the present invention was produced into a sheet-like smoking material having a thickness of 0.1 to 0.5mm by the processing method described in the conventional sheet processing method (CN106714590A, entitled "method for producing homogenized tobacco material"), into a granular atomized smoking material having a diameter of 0.3 to 1.2mm by the conventional powder granulation processing method (CN111000282A, entitled "alkaloid smoking particles for low-temperature heating non-combustible product and method for producing the same"), or into a powdery smoking material having a particle size of 40 to 100mm by the conventional grinding processing method (CN201910787685, entitled "a heating non-combustible smoking product and method for producing the same") using a grinder commonly used in the present technical field.
According to the standard of smoking evaluation of the sensory technical requirements of GB5606.4-2005, a small group of smoking evaluation experts organized to consist of 7 smoking evaluation experts smoked cigarettes on sale using the atomized smoking material (powder, sheet and particle) of the invention, and the smoking evaluation results are listed in Table 1.
According to the No. 4 of the GB5606.4-2005 cigarette, sensory quality evaluation in sensory technical requirements is mainly composed of indexes such as smoke temperature, smoke amount, number of suction openings, physiological strength, fragrance, style characteristics, comfortableness and peculiar smell. The sensory quality evaluation score is made in percentage, the highest score is 100, and each item is divided into score units by 0.5.
Wherein, the smoke temperature is the heat of the smoke temperature sensed in the suction inlet cavity when a smoker smokes the cigarette. Therefore, when sensory quality evaluation is performed, the models of the heaters are required to be consistent, the heaters need to be calibrated first, and each heater is ensured to have the same heating temperature and heating time.
The amount of smoke is the amount of smoke exhaled from the mouth of a smoker when smoking a cigarette.
The number of the suction openings is the number of the openings sucked when a smoker sucks the cigarette according to a certain suction mode and the smoke quantity is obviously reduced.
Irritation refers to a slight and noticeable unpleasant sensation caused by smoke to the senses, such as abnormal irritation of the nasal cavity, oral cavity, throat, etc.
The aroma refers to aroma and aftertaste, namely the special tobacco aroma of cigarette smoke which is heated and not burnt and the taste feeling left by the smoke after being exhaled from oral cavity and nasal cavity.
The style characteristic means that the cigarette has the aroma style and the essential smell of the cigarette which is not burnt when being heated, and the change of the aroma can be obviously sensed.
The comfort is composed of two parts, firstly, the smoke gas can not feel comfortable on sense organs during suction, such as spurting on nasal cavity, oral cavity and throat, and singeing with a spike; secondly, the cigarette bullet is inserted into or pulled out of the smoking set before and after smoking, and the feeling of discomfort in sense is caused, such as labor waste during insertion, bending, head dropping during pulling out and the like.
The peculiar smell is a strange smell (except for additional fragrance) which is obviously different from the intrinsic smell of the cigarette which is not combusted by heating, so that the cigarette loses the smoking value.
In the No. 4 of the GB5606.4-2005 cigarette, the evaluation results of the lowest evaluation of the sensory quality of different types of cigarettes in the sensory technical requirements are different, wherein one type is more than or equal to 85, the second type and the third type are more than or equal to 75, and the fourth type and the fifth type are more than or equal to 60, so that the difference between the standard evaluation of the non-combustible product and the traditional cigarette is normal. The invention is modified on the basis of the traditional cigarette scoring standard so as to better accord with the evaluation of the heating non-combustible product. The highest gloss and oil lubrication in the traditional cigarette is divided into 5 points; the highest evaluation of rich and fine fragrance is 32 points; the concordance rating was a maximum of 6; the maximum rating of the miscellaneous gas-free is 12; the highest non-irritation evaluation is 20 points; the highest evaluation of purity and comfort is 25 points. Compared with the traditional cigarette, the non-combustible product is heated by an external heat source, the heating temperature is controlled within the range of 200-400 ℃, so that the herbal powder can be heated to evaporate and release some components, and the condition of initiating material combustion is not met, so that the evaluation standard of the non-combustible product is different from the evaluation standard of the traditional cigarette.
The invention has the heating non-combustion scoring standard smoke temperature highest score of 20, the smoke amount highest score of 20, the suction port number highest score of 20, the physiological strength highest score of 8, the fragrance highest score of 8, the style characteristic highest score of 8, the comfort highest score of 8 and the peculiar smell highest score of 8.
Meanwhile, the same cigarette as the above cigarette using the existing sheet-like atomized smoking material (CN106714590A, the name of the invention "method for producing homogenized tobacco material") as a control sample 1, the same cigarette as the above cigarette using the existing granular atomized smoking material (CN111000282A, the name of the invention "alkaloid smoking particles for low-temperature heating non-combustible smoking article and preparation method thereof") as a control sample 2, and the same cigarette as the above cigarette using the existing powdery smoking material (CN201910787685, the name of the invention "a heating non-combustible smoking article and preparation method thereof") as a control sample 3 were also subjected to the same smoke evaluation, and the results of the smoke evaluation are also shown in table 1.
From the foregoing, it will be appreciated that the atomized smoking material of the present invention has the following technical characteristics: the atomized smoking material has large smoking amount, low smoke temperature, certain physiological strength, namely physiological satisfaction, lasting fragrance, full fragrance and obvious areca fragrance style
[ advantageous effects ]
The invention has the beneficial effects that: the atomized smoking material for heating the non-combustible product releases the content of the betel nut in a heating mode, meets the requirement of consumers on the betel nut, and simultaneously can avoid the damage of crude fibers in the betel nut to the oral cavity and reduce the side effect caused by chewing the betel nut.
The atomized smoking material has the function of replacing cigarettes, the arecoline is a substance well replacing nicotine, the arecoline can be burnt when being taken in the mouth, and eating the arecoline can stimulate sensory nerves of people to enable the people to be in an excited state and has the function of relieving fatigue.
[ detailed description ] embodiments
The invention will be better understood from the following examples.
Example 1: the invention relates to an atomized smoking material
The implementation of this example is as follows:
62 parts by weight of dry areca fruit powder with a particle size of 180 meshes sold under the trade name of olive areca nut by West pharmaceutical industry, bold, West, 9 parts by weight of corn starch sold under the trade name of edible corn starch by Shanghai financial food, Inc., 2 parts by weight of sodium carboxymethyl cellulose adhesive sold under the trade name of food grade sodium carboxymethyl cellulose by Reticulture chemical, Inc., Nguchi, 0.1 part by weight of sodium lactate pH regulator sold under the trade name of food grade sodium lactate by Shandong Jiu chemical, Inc., 10 parts by weight of hexadecane fuming auxiliary sold under the trade name of hexadecane by Qianzhou Qianyujin refinement chemical, 1.2 parts by weight of menthol flavor sold under the trade name of food grade menthol by Hunan south China biotechnology, Inc., the resulting mixture was formed into a sheet smoking material having a thickness of 0.170mm using the processing methods described in the specification.
The sheet smoking material prepared using this example was evaluated for smoking according to the method described in the specification of the application, and the results are shown in table 1.
Meanwhile, the same cigarettes as the above cigarettes using the conventional sheet-like atomized smoking material (CN106714590A, entitled "method for producing homogenized tobacco material") were also subjected to the same evaluation as in control sample 1, and the evaluation results are also shown in table 1.
Example 2: the invention relates to an atomized smoking material
The implementation of this example is as follows:
mixing dry fruit powder of Arecae semen (70 wt. parts) with particle size of 40 mesh and sold as semen Canarii albi by Wenzhou, Sasa, 11 wt. parts of potato starch sold as food grade potato starch by Guangzhou deep creative chemical company, 10 wt. parts of pectin adhesive sold as food grade pectin by Shandong Jurong bioengineering, Inc., 2.0 wt. parts of dipotassium citrate regulator sold as food grade sodium lactate by Shandong Jiu, chemical engineering, Inc., 14 wt. parts of propylene glycol fuming adjuvant sold as food grade propylene glycol by Guangzhou Brilliant union, and 0.2 wt. parts of edible flavor of blueberry flavor sold as blueberry flavor by Yunnan Balaozi Biotech, Inc., the resulting mixture was formed into a particulate smoking material having a diameter of 0.5mm using the processing methods described in the specification.
The particulate smoking material prepared using this example was evaluated for smoking according to the methods described in the specification of the application and the results are shown in table 1.
Meanwhile, the same cigarettes as the above cigarettes using the existing particulate atomized smoking material (CN111000282A, entitled "alkaloid smoking particles for low-temperature heating of non-combustible articles and method for producing the same") were also subjected to the same evaluation as in control sample 2, and the evaluation results are also shown in table 1.
Example 3: the invention relates to an atomized smoking material
The implementation of this example is as follows:
42 parts by weight of areca nut dry fruit powder with the granularity of 200 meshes sold by Wenzhou, pharmaceutical industry and chemical industry Limited, 15 parts by weight of sweet potato starch sold by Guangzhou, deep creative chemical industry Limited, 4 parts by weight of water-soluble starch adhesive sold by Nantong, Yunfeng starch Limited, 4 parts by weight of water-soluble starch sold by Nantong, 0.8 part by weight of potassium malate pH regulator sold by Shandong, Jiuhuai chemical industry Limited, 20 parts by weight of glycerol triacetate fuming auxiliary sold by Guangzhou, British chemical industry Limited, 0.8 part by weight of vanillin food flavor sold by Wuhana white pharmaceutical industry Limited, and sold by food grade vanillin are uniformly mixed, the resulting mixture was processed into a powdered smoking material having a particle size of 100 mesh using the processing methods described in the specification.
The powdered smoking material prepared using this example was evaluated for smoking according to the method described in the specification of the application, and the results are shown in table 1.
Meanwhile, a cigarette identical to the above cigarette using the existing powdery atomized smoking material (CN201910787685, entitled "a smoking article which is non-combustible by heating and a method for producing the same") was also subjected to the same evaluation as the control sample 3, and the evaluation results are also shown in table 1.
Example 4: the invention relates to an atomized smoking material
The implementation of this example is as follows:
uniformly mixing 30 parts by weight of dry areca fruit powder with the granularity of 80 meshes sold by Wenzhou, Sasa, pharmaceutical industry and company Limited, 8 parts by weight of wheat starch sold by Guangzhou, deep creative chemical company and company Limited, 8 parts by weight of wheat starch sold by food grade wheat starch, 5 parts by weight of chitosan adhesive sold by Shenzhen development Biotech company and company Limited, 1.2 parts by weight of monopotassium malate modifier sold by Shandong, Jiu, chemical industry and company Limited, 1.4 parts by weight of stearic acid fuming aid sold by Guangzhou Qianjiaojian refining chemical company and company Limited, 16 parts by weight of apple flavor edible flavor sold by Yunnan Balaozi, biological technology and company Limited, and trade name of green apple flavor, the resulting mixture was formed into a sheet smoking material having a thickness of 0.40mm using the processing methods described in the specification.
The sheet smoking material prepared using this example was evaluated for smoking according to the method described in the specification of the application, and the results are shown in table 1.
Example 5: the invention relates to an atomized smoking material
The implementation of this example is as follows:
mixing 36 weight parts of dry fruit powder of Areca catechu with particle size of 120 meshes sold as green fruit Areca catechu by Wenzhou, 12 weight parts of sorghum starch sold as sorghum flour by Shandong Binzhen sweet oil Co., Ltd, 7 weight parts of guar gum adhesive sold as food grade guar gum by Zhejiang Kangxing Biotech Co., Ltd, 0.6 weight parts of sodium bicarbonate acid-base modifier sold as food grade sodium lactate by Shandong Jiu chemical Co., Ltd, 5 weight parts of glycerol fuming auxiliary sold as glycerol food grade by Guangzhou Britain Ling chemical Co., Ltd, 1.0 weight parts of 1, 4-dimethylpyrazine edible flavor sold as 1, 4-dimethylpyrazine by Shanghai Xin flavor Co., Ltd, the resulting mixture was formed into a particulate smoking material having a diameter of 1.2mm using the processing methods described in the specification.
The particulate smoking material prepared using this example was evaluated for smoking according to the methods described in the specification of the application and the results are shown in table 1.
Example 6: the invention relates to an atomized smoking material
The implementation of this example is as follows:
54 parts by weight of dry areca fruit powder having a particle size of 160 meshes and sold as olive areca by Wenzhou, pharmaceutical industry, Sasa, 5 parts by weight of corn starch sold as edible corn starch by Shanghai, financial food, Inc., 8 parts by weight of sodium carboxymethyl cellulose adhesive sold as food grade sodium carboxymethyl cellulose by Nuchho, vitamin, Inc., 1.4 parts by weight of monopotassium citrate as food grade sodium lactate, 9 parts by weight of glyceryl triacetate fuming adjuvant sold as food grade glyceryl triacetate by Guangzhou, Brilliant Union, Inc., 2.0 parts by weight of coffee flavor flavorant sold as mellow coffee by Yunnan Balaozi, Biotech, Inc., were mixed uniformly by the processing method described in the present specification, the resulting mixture was made into a powdered smoking material having a particle size of 50 mesh.
The powdered smoking material prepared using this example was evaluated for smoking according to the method described in the specification of the application, and the results are shown in table 1.
Table 1: the atomized smoking material prepared by the invention has sensory evaluation result
Note: the highest smoke temperature is 20 minutes; the highest smoke amount is 20 minutes; the highest fraction of the suction ports is 20 minutes; the highest physiological intensity is 8 points; the highest fragrance is 8 points; the highest score of style characteristics is 8; the highest comfort is 8 points; the highest peculiar smell is 8 points.
The results listed in table 1 clearly show that the atomized smoking material prepared by the invention has the advantages of large smoking amount, low smoke temperature, certain physiological strength, namely physiological satisfaction, lasting fragrance, full fragrance and obvious areca fragrance style.
Claims (10)
1. An atomized smoking material for heating non-combustible products is characterized by comprising 30-70 parts by weight of dry areca nut powder, 5-15 parts by weight of starch, 2-10 parts by weight of adhesive, 0.1-2.0 parts by weight of acid-base regulator, 5-20 parts by weight of smoking aid and 0.2-2.0 parts by weight of edible spice.
2. An atomized smoking material according to claim 1, wherein the atomized smoking material comprises 40 to 60 parts by weight of dry areca nut powder, 8 to 12 parts by weight of starch, 4 to 8 parts by weight of adhesive, 0.6 to 1.4 parts by weight of pH regulator, 9 to 16 parts by weight of smoking aid and 0.8 to 1.4 parts by weight of flavorant.
3. An atomized smoking material according to claim 1 or 2, wherein the arecoline content of the dry powder of areca catechu is 0.05-1.0% by weight.
4. An atomised smoking material according to claim 1 or 2, wherein the particle size of the areca nut dry fruit powder is 40-200 mesh.
5. An atomised smoking material according to claim 1 or 2, wherein the starch is maize, potato, wheat, sorghum or sweet potato starch having a purity of greater than 90% by weight.
6. An atomised smoking material according to claim 1 or 2, wherein the binder is one or more binders selected from water soluble starch, sodium carboxymethyl cellulose, guar gum, pectin or chitosan.
7. An atomised smoking material according to claim 1 or 2, wherein the pH modifying agent is one or more acid modifying agents selected from sodium carbonate, sodium bicarbonate, sodium lactate, potassium carbonate, dipotassium citrate, monopotassium citrate, potassium malate or monopotassium malate.
8. An atomised smoking material according to claim 1 or 2, wherein the smoking aid is one or more smoking aids selected from glycerol, propylene glycol, triacetin, stearic acid or hexadecane.
9. An atomised smoking material according to claim 1 or 2, characterised in that the flavourant is one or more flavourants selected from menthol, vanillin, ethyl maltol, 1, 4-dimethylpyrazine, coffee flavourants, blueberry flavourants, apple flavourants, orange juice flavourants and similar flavour products.
10. An atomized smoking material according to claim 1 or 2, wherein the atomized smoking material is a sheet-like smoking material having a thickness of 0.1 to 0.5mm, a particle-like smoking material having a diameter of 0.3 to 1.2mm, or a powdery smoking material having a particle size of 40 to 100 mesh.
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| CN113462030A (en) * | 2021-06-23 | 2021-10-01 | 深圳市华诚达精密工业有限公司 | Fiber elastic atomizing core and preparation method thereof |
| CN113679084A (en) * | 2021-08-19 | 2021-11-23 | 湖南伍子醉食品有限公司 | Method for preparing paper-making reconstituted tobacco by using betel nut flower base fibers |
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