CN112293787B - Atomized fuming material for heating non-combustion products - Google Patents

Atomized fuming material for heating non-combustion products Download PDF

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CN112293787B
CN112293787B CN202011298892.XA CN202011298892A CN112293787B CN 112293787 B CN112293787 B CN 112293787B CN 202011298892 A CN202011298892 A CN 202011298892A CN 112293787 B CN112293787 B CN 112293787B
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weight
parts
starch
atomized
acid
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CN112293787A (en
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黄亮
杨双艳
周瑾
杨紫刚
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Yunnan Chunxu Biotechnology Co ltd
Yunnan Nanzhong Technology Co ltd
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Yunnan Nanzhong Technology Co ltd
Yunnan Chunxu Biotechnology Co ltd
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    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00—Cigars; Cigarettes
    • A24D1/20—Cigarettes specially adapted for simulated smoking devices

Abstract

The invention relates to an atomized fuming material for heating non-combustible products, which is prepared from betel nut extract, herbal plant powder, starch, adhesive, acid-base regulator, fuming auxiliary agent and edible spice. The heating non-combustion product made of the atomized smoke material can provide similar physiological satisfaction and function as tobacco, so that the existing tobacco product is replaced to a certain extent. Compared with the nicotine content of the effective component of the existing tobacco products, the arecoline content of the effective component of the heating nonflammable product can be reduced by 10-20 times, so that the product safety and the manufacturing cost of the invention have obvious advantages.

Description

Atomized fuming material for heating non-combustion products
[ field of technology ]
The invention belongs to the technical field of production of heating non-combustible products. More particularly, the present invention relates to an atomized smoking material for heating a non-combustion article.
[ background Art ]
Heated nonflammable products are a new class of consumer products developed in recent years, which were originally developed as new tobacco products. Traditional tobacco products, such as cigarettes, pipes, cigars, etc., are lit and kept in a static burning state, and the heat generated by the burning of the materials evaporates, cracks the chemical components in the tobacco materials, and finally generates smoke which can be sucked. The temperature of the static combustion process of the tobacco reaches 600-900 ℃ and is in a local anoxic environment condition at the combustion cone position, so that smoke components released by the combustion of the tobacco are very complex and contain a large amount of components threatening health, wherein the generation of harmful components such as polycyclic aromatic hydrocarbon, micromolecular aldehyde ketone, benzene series, TSNA, CO and the like are directly related to the high temperature in the combustion process, and a large amount of research work shows that the release level of the components can be effectively reduced by reducing the temperature of the combustion cone of the cigarette.
In order to reduce the health hazard caused by smoking tobacco products, tobacco enterprises develop heating non-burning tobacco products first, and compared with traditional smoking grass, the heating non-burning tobacco uses an external heat source to heat tobacco materials, and the heating temperature is controlled within the range of 200-400 ℃, so that the tobacco can be heated and evaporated and release some smoke components, and the condition of triggering the burning of the tobacco materials is not reached. Meanwhile, in order to increase the smoke concentration and improve the atomization release effect of tobacco components, the smoke agent such as glycerol, propylene glycol, glycerol triacetate and the like is added into tobacco materials in order to heat the non-combustible tobacco products.
The currently marketed heating non-combustible products comprise two major types, namely chemical heating and electric heating, wherein the chemical heating is represented by ReVO pushed out by Reynolds tobacco, the products are obtained by heating tobacco materials by taking a static combustion carbon rod as a heat source through a heat conducting aluminum tube, and related patents of the products such as CN 201611055399, the invention name of the products are such as carbon heating smoking products and a preparation method thereof; the electric heating products adopt an external electric heating source to heat tobacco materials, so that the temperature control is more accurate, and the current products adopting the electric heating source comprise 'IQOS' of Feimo International, 'GLO' of Yimei tobacco, 'PLOOM' of Japanese tobacco, 'LIL' of Korean tobacco and the like, for example PCT/EP2018/054090 and the invention name 'AEROSOL-GENERATING DEVICE AND METHOD FOR USING A SHEET OF AEROSOL-FORMING SUBSTRATE IN AN AEROSOL-GENERATING DEVICE'; PCT/JP2016/069033, entitled "CARTRIDGE FOR AEROSOL INHALER, AEROSOL INHALER PROVIDED WITH SAME, AND HEAT-GENERATING SHEET FOR AEROSOL INHALER"; PCT/EP2017/083784, the name "AEROSOL GENERATING DEVICE AND ARTICLE", etc. The novel heated non-combustible tobacco product has significantly reduced levels of harmful ingredient release compared to conventional tobacco due to the significantly reduced heating temperature of the tobacco material, while the heated non-combustible tobacco product can also provide similar smoking quality and nicotine release levels as conventional cigarettes. Thus, new tobacco products represented by IQOS have achieved very desirable development results in recent years, and at present, market share approaching or exceeding 10% has been reached in japan, korea, and central european regions, and IQOS products passed the us FDA's Modified Risk Tobacco Product (MRTP) certification in 2019 and began to be marketed in the us. It is expected that heating non-combustible tobacco products will be the main stream of development in the market for some time in the future.
However, on the other hand, the heating non-combustion technique has outstanding utility value for some non-tobacco materials, except for tobacco. By utilizing the functions of heating by an external heat source and evaporating and carrying the fumigant, the smoke can be effectively generated, the components in the carried heated material are transferred and evaporated, and the smoke which can be pumped is generated. So that some herbal cartridges other than tobacco have also been developed in recent times. However, no literature report has been made so far on non-tobacco herbal cartridges using betel nuts.
Conventionally, the areca nut is chewed and eaten after alkaline substances such as lime are added into fresh areca nut, and the areca nut is usually chewed and eaten after being dried, marinated by heating and flavored and packaged. At present, alkaline substances added in betel nuts and betel nut fibers repeatedly stimulate oral mucosa, and the alkaline substances and betel nut fibers cause cancerogenic risks in the oral cavity and the digestive tract of betel nut consumers. In addition, the residue discharged by chewing betel nuts is inconvenient and has environmental protection problem.
Therefore, the present inventors have completed the present invention by a large number of experimental studies and analysis summaries on the basis of summarizing the prior art.
[ invention ]
[ problem to be solved ]
It is an object of the present invention to provide an atomized smoking material for heating a non-combustion article.
Technical scheme
The invention is realized by the following technical scheme.
The present invention relates to an atomized smoking material for heating a non-combustible article.
The atomization fuming material is prepared from 10 to 20 parts by weight of betel nut extract, 30 to 50 parts by weight of herb powder, 5 to 15 parts by weight of starch, 2 to 10 parts by weight of adhesive, 0.1 to 2.0 parts by weight of acid-base modifier, 5 to 20 parts by weight of fuming auxiliary agent and 0.2 to 2.0 parts by weight of edible spice.
According to a preferred embodiment of the invention, the atomized smoke generating material is prepared from 12-18 parts by weight of betel nut extract, 36-44 parts by weight of herb powder, 8-12 parts by weight of starch, 4-8 parts by weight of adhesive, 0.6-1.4 parts by weight of acid-base modifier, 9-16 parts by weight of smoke generating auxiliary agent and 0.8-1.4 parts by weight of edible spice.
According to another preferred embodiment of the present invention, the betel nut extract is water, ethanol, acetone, acidic aqueous solution extract or supercritical CO 2 An extract; the betulin content of the betel nut extract is 1-10% by weight.
According to another preferred embodiment of the present invention, the herbal plant powder is tea leaf, peppermint leaf, mugwort leaf, loquat leaf, cocoa, kudzu root, licorice or sugarcane plant powder, the particle size of which is 40-200 mesh.
According to another preferred embodiment of the invention, the starch is corn starch, potato starch, wheat starch or sweet potato starch having a purity of more than 90% by weight.
According to another preferred embodiment of the invention, the adhesive is one or more adhesives selected from the group consisting of water-soluble starch, sodium carboxymethyl cellulose, guar gum, cationic guar gum, pectin or chitosan.
According to another preferred embodiment of the present invention, the acid-base modifier is one or more acid-base modifiers selected from sodium carbonate, sodium bicarbonate, sodium lactate, potassium carbonate, dipotassium citrate, monopotassium citrate, potassium malate or monopotassium malate.
According to another preferred embodiment of the invention, the fuming aid is one or more fuming aids selected from glycerol, propylene glycol, triacetin, stearic acid or hexadecane.
According to another preferred embodiment of the present invention, the flavorant is one or more flavorants selected from menthol, vanillin, ethyl maltol, 1, 4-dimethyl pyrazine, coffee-flavored flavorants, blueberry-flavored flavorants, apple-flavored flavorants, orange juice-flavored flavorants, and like flavor products.
According to another preferred embodiment of the invention, the atomized smoking material is a sheet-like, 0.1-0.5 mm thick, 0.3-1.2 mm diameter particulate or 40-100 mesh powder smoking material.
The present invention will be described in more detail below.
The present invention relates to an atomized smoking material for heating a non-combustible article.
In the present invention, the term heated non-combustible product is understood to mean a tobacco substitute product which releases smoke upon heating by a heating means. The term "atomized smoking material" is understood to mean a smoking material for use in the heated non-combustible article described above.
The atomization fuming material is prepared from 10 to 20 parts by weight of betel nut extract, 30 to 50 parts by weight of herb powder, 5 to 15 parts by weight of starch, 2 to 10 parts by weight of adhesive, 0.1 to 2.0 parts by weight of acid-base modifier, 5 to 20 parts by weight of fuming auxiliary agent and 0.2 to 2.0 parts by weight of edible spice.
Betel nut is a plant with medicinal value and is a traditional Chinese medicinal material. Its main physiological function is to refresh brain, promote digestion and expel parasites. Betel (Arecoline) which is a main functional component contained in betel is a small molecular alkaloid, and the small molecular alkaloid has a health care function and pharmacological activity, and the betel can improve the sensitivity of sympathetic nerves and parasympathetic nerves of a person, so that the concentration and the reaction of the person can be assisted and improved; betulin can paralyze the nervous system of insect bodies, and further expel some insect bodies in the body such as cestode suis, niu Taochong, schistosoma mansoni, liver fluke, helminths and the like out of the body. Betulin delays atherosclerosis, reduces blood viscosity, and has auxiliary effect on controlling blood sugar. Thus, betel nuts are a widely used class of addictive consumer products. However, a great deal of clinical practice in modern medicine has shown that arecoline has a certain cytotoxicity and risk of pathogenicity. Therefore, the invention provides an atomized smoke material prepared from betel nuts, so as to change the traditional and existing betel alkali intake and absorption modes, thereby more effectively controlling the release level of betel alkali and reducing the harm of betel nuts taking.
According to the invention, the main function of the betel nut extract in the atomization fuming material is to provide betel nut aroma and betel nut alkali components.
According to the invention, the betel nut extract is water, ethanol, acetone, acidic aqueous solution extract or supercritical CO 2 An extract.
The betel nut extracts used in the invention are all extracts obtained by betel nut extraction according to the prior art documents, for example, the betel nut water extract is obtained by extracting betel nut by using water according to the method described in CN101461874A, the invention name of the method for simultaneously extracting betel nut alkaloid and pigment from betel nut by ultrasonic assisted method, zheng Yajun and the like, and the betel nut water extract has the characteristics of high betel nut alkali extraction recovery rate and easy water-soluble solution; according to Luo Shishu, the method described in pages 1-64 of the university of Hainan thesis entitled "extraction and separation of arecoline from Arecae semen and research on its activity", 2011, an ethanol extract of Arecae semen is obtained by extracting Arecae semen with ethanol, and has the characteristics of low extraction cost, and easy dissolution in aqueous solution and alcoholic solution due to the fragrance of Arecae semen;
according to the method described in Cheng Huan et al entitled "response surface method optimization of betel nut kernel polyphenol extraction process", "food research and development", 39 (4), 2018, pages 35-41 ", betel nut acetone extract is obtained by extracting betel nut with acetone, and has the characteristics of high enrichment of betel nut polyphenol components and easy dissolution in ester solution and alcohol solution;
According to the method described in CN 201010549811, the invention name of Li Faqing et al, namely a method for extracting arecoline from betel nuts, an acidic aqueous solution extract of betel nuts is obtained by extracting betel nuts from betel nuts by using an acidic aqueous solution, and the acidic aqueous solution extract of betel nuts has the characteristics of high purity of arecoline and high extraction efficiency. The acidic aqueous solution is an aqueous solution of one or more inorganic acid selected from sulfuric acid, hydrochloric acid, phosphoric acid or nitric acid, or an aqueous solution of one or more organic acid selected from acetic acid, propionic acid, n-butyric acid or oxalic acid;
according to Liu Gong et al entitled "supercritical CO 2 Process research on extraction of betel nut alkaloid (method described in China food industry, 2011, stage 1, pages 53-54), betel nut supercritical CO is obtained by extracting betel nut 2 Extract of betel nut critical CO 2 The extract has the characteristics of high betulin content, volatile aroma component retention number and easy dissolution in ester-soluble solution.
Betulin in betel is measured according to the method described in Ding Fanglin, peng Shu entitled "HPLC_ESI_MS method", journal of agricultural product processing, 2008, 4 th phase ", and the betulin content of the betel extract is usually 1-10% by weight. In the invention, if the arecoline content of the areca extract is lower than 1%, the arecoline content of cigarettes added with the areca extract is lower, so that the physiological strength feeling of the product is affected; if the arecoline content of the areca catechu extract is higher than 10%, the arecoline content in the cigarette product is too high, and the use is uncomfortable; therefore, betulin content of betulin extract is reasonable in the range of 1-10%, preferably 2-8%, more preferably 4-6%;
Of course, other betel nut extracts may be used in the present invention, except that they do not negatively affect the aerosol-generating material of the present invention and its articles, and are within the scope of the present invention.
According to the present invention, herbaceous plants are understood to be a class of plants with underdeveloped xylem in the stem, few lignified cells and weak supportability, such as tea leaves, peppermint, etc. The herbal plant powder has the main function of adsorbing the betel nut extract component in the atomization fuming material, is used as a betel nut extract component carrier, and supplements a plurality of plant aroma components for the atomization fuming material.
The herbal plant powder used in the invention is tea leaf, peppermint leaf, mugwort leaf, loquat leaf, cocoa, kudzuvine root, liquorice or sugarcane plant powder, and the granularity of the herbal plant powder is 40-200 meshes.
Tea (Camellia sinensis (L.) O.Ktze.) has effects of reducing cardiovascular disease and cerebrovascular disease risk and death risk, reducing cholesterol and blood pressure, and enhancing immunity.
The tea leaves used in the invention are green tea, black tea, oolong tea, white tea, yellow tea or black tea, which are all products sold on the market at present, such as green tea sold under the trade name of super green tea by Yunnan Jing Gu Chaan company, black tea sold under the trade name of first grade Yunnan red by Yunnan Jing Gu tea factory company, oolong tea sold under the trade name of super oolong tea by Yunnan Jing Gu tea factory company, white tea sold under the trade name of super white tea by Yunnan Jing Gu Chaan company, yellow tea sold under the trade name of first grade yellow tea by Yunnan Jing Gu tea factory company, and black tea sold under the trade name of super black tea by Yunnan Jing Gu tea factory company.
The invention adopts a common mechanical grinding method to grind the tea into the tea dust with the granularity of 40-200 meshes.
Peppermint (Mentha haplocalyx briq.) is a commonly used traditional Chinese medicine. It is a pungent and cool drug for inducing sweat and relieving fever, and can be used for treating influenza, headache, conjunctival congestion, fever, laryngopharynx swelling and pain, etc. Peppermint is used for replacing tea in common practice, and is used for clearing heart fire and improving eyesight.
From the plant classification, peppermint is classified into purple-stem purple vein and green-stem.
The mint used in the present invention is a product currently marketed, for example, spearmint sold under the trade name spearmint by the company of post-mPacific camellia garden, mPacific, and spearmint sold under the trade name high quality dry spearmint by the company of post-mPacific camellia garden.
The invention adopts a conventional mechanical grinding method to process the mint into the mint powder with the granularity of 40-200 meshes.
Artemisia argyi Levl. Et Van has effects of warming channel, eliminating dampness, dispelling cold, stopping bleeding, relieving inflammation and asthma, relieving cough, preventing miscarriage, and resisting allergy.
The moxa used in the present invention is a product currently sold in the market.
The invention adopts a conventional mechanical grinding method to process the mugwort leaves into mugwort leaf powder with the granularity of 40-200 meshes.
Loquat (Eriobotrya japonica) contains amygdalin in both leaves, fruits and cores, contains various fructose, glucose, potassium, phosphorus, iron, calcium, VA, VB, VC and the like, and has the effects of clearing lung-heat, relieving cough, harmonizing stomach, promoting urination and quenching thirst.
The loquat leaves used in the present invention are currently commercially available products, such as those sold under the trade name dry loquat leaves by the wholesale company of Chinese herbal medicine in Huimin, bozhou.
The invention adopts a conventional mechanical grinding method to process the loquat leaves into the loquat powder with the granularity of 40 to 200 meshes.
The flavanol and procyanidine contained in cocoa (Theobroma cacao L.) have positive promotion effects in protecting cardiovascular system, regulating blood pressure, increasing nitric oxide production, oxidation defense, and immune system.
The cocoa used in the present invention may be a product currently on the market, such as that sold under the trade name pure cocoa beans by the company of tin-free okang foods.
The invention adopts a conventional mechanical grinding method to process the cocoa into the cocoa powder with the granularity of 40-200 meshes.
Radix Puerariae has effects of relieving muscle and fever, promoting eruption, promoting salivation, quenching thirst, and invigorating yang and relieving diarrhea, and is commonly used for treating exterior syndrome fever, pain in neck and back, measles, pyretic disease, thirst, yin deficiency, diabetes, heat diarrhea, spleen deficiency diarrhea.
The kudzuvine root used in the invention is a product sold in the market at present, for example, a product sold under the trade name sulfur-free kudzuvine root butyl by the company limited of the pharmaceutical industry of the Gao Zhou Yuan Shengtang.
The invention adopts a conventional mechanical grinding method to process the radix puerariae into the radix puerariae powder with the granularity of 40-200 meshes.
Glycyrrhrizae radix has effects of invigorating spleen and replenishing qi, clearing heat and detoxicating, eliminating phlegm and relieving cough, relieving spasm and pain, and harmonizing various drugs, and is commonly used for spleen and stomach weakness, listlessness debilitation, cardiopalmus short breath, cough with excessive phlegm, gastric and abdominal, limb spasm and pain.
The licorice used in the present invention is a product currently marketed, for example, by the company limited by the pharmaceutical industry, the Ming Yuan Shengtang, bo.
The invention adopts a conventional mechanical grinding method to process the liquorice into the liquorice powder with the granularity of 40-200 meshes.
Sugarcane contains rich sugar and water, and also contains various vitamins, fat, protein, organic acid, calcium, iron and other substances which are very beneficial to human metabolism. It has effects of clearing away heat and toxic materials, promoting salivation, quenching thirst, regulating stomach function, relieving vomit, and nourishing yin.
The sugarcane used in the present invention is a product currently marketed, such as sugarcane from Yunnan de Hongjia, a production place.
The invention adopts a conventional mechanical grinding method to process the sugarcane into the sugarcane powder with the granularity of 40-200 meshes.
In the present invention, it is not preferable that the particle size of all the herbal powders exceeds the range because the uniformity of the distribution of the particle size of the herbal powders is poor when the particle size is smaller than 40 mesh and the powder size is too fine when the particle size is larger than 200 mesh, so that the flavor is not easily released from the prepared smoking material.
Of course, any other herbal powders having the above-described herbal powder effect can be used in the present invention, except that they do not adversely affect the atomized smoking material of the present invention and its products, and such herbal powders are also within the scope of the present invention.
Starch is a high molecular carbohydrate, a polysaccharide consisting of a single type of sugar unit. Starch is divided into a linear chain molecule and a branched chain molecule, wherein the linear chain molecule is formed by alpha-1, 4-glycosidic bond of D-hexacyclic glucose, the branching position of the branched chain molecule is alpha-1, 6-glycosidic bond, and the rest is alpha-1, 4 glycosidic bond. Amylose contains hundreds of glucose units and amylopectin contains thousands of glucose units.
According to the invention, the primary function of the starch in the atomized smoking material of the invention is the thickener function to regulate the consistency of the atomized smoking material slurry.
The starch used in the invention is corn starch, potato starch, wheat starch or sweet potato starch with the purity of more than 90% by weight.
In the present invention, if the starch purity is less than 90% by weight, slurry viscosity control is affected and foreign impurities are excessively introduced.
Wherein corn starch (corn starch) is prepared by soaking corn with 0.3% sulfurous acid, crushing, sieving, precipitating, drying, and grinding. The corn contains fat, phosphorus element and vitamin B2 in cereal food, and contains linoleic acid, vitamin E, glutathione, trace element selenium and dietary fiber.
The corn starch used in the present invention is a product currently on the market, such as corn starch sold under the trade name food grade corn starch by the Guangzhou chemical Co., ltd.
Potato Starch (Potato Starch) is a product obtained from washed potatoes by crushing, filtering, precipitating, and drying, and can be used as a thickener. The potato starch used in the present invention is a product currently on the market, such as potato starch sold under the trade name food grade potato starch by the deep-wound chemical company, inc.
Wheat starch is mainly used in food thickeners, gelatinizers, binders or stabilizers, etc. The wheat starch used in the present invention is a product currently on the market, for example, a wheat starch sold under the trade name of food grade wheat starch by the deep-wound chemical industry Co., guangzhou.
Sweet potato is rich in nutrition and contains a large amount of sugar, protein, fat and various vitamins and minerals. Sweet potato starch is heated to be pasty, so that the vitamin C which is thermolabile and water-soluble is well protected, and mineral matters in the sweet potato starch play an important role in maintaining and regulating human body functions. The sweet potato starch used in the invention is a product sold in the market at present, for example, sweet potato starch sold by Guangzhou, deep-wound chemical industry Co., ltd under the trade name of food-grade sweet potato.
Of course, all other starches having the above-described effect may be used in the present invention, except that they do not adversely affect the atomized smoking material of the present invention and its articles, and are within the scope of the present invention.
In the present invention, an adhesive is understood to be a type of organic or inorganic natural substance or organic or inorganic synthetic substance that is capable of bonding together one or more different materials and has sufficient strength after curing.
According to the invention, the adhesive has the main function of bonding plant powder and fiber together in the atomization fuming material so as to form the atomization fuming material.
The adhesive used in the present invention is one or more adhesives selected from the group consisting of water-soluble starch, sodium carboxymethyl cellulose, guar gum, cationic guar gum, pectin, or chitosan.
The water-soluble starch is a low-degree hydrolysis product formed by controlling between starch and starch sugar, has strong hydration force, can be dissolved at normal temperature, has good viscosity and carrier effect, strong heat resistance, difficult browning, good emulsification effect and thickening effect, small hygroscopicity, difficult agglomeration, good film forming property and the like. The water-soluble starch used in the present invention is a product currently marketed, for example, by the company of Yunfeng starch, inc. in Nanto under the trade name food-grade water-soluble starch.
Sodium carboxymethyl cellulose has the functions of adhesion, thickening, strengthening, emulsifying, water retention, suspending and the like, and is generally used as a thickening agent, a drug carrier, an adhesive and an anti-redeposition agent. The sodium carboxymethyl cellulose used in the present invention is a product currently commercially available, for example, sodium carboxymethyl cellulose sold under the trade name of food-grade sodium carboxymethyl cellulose by the company of the chemical industry, division of the family of the yoku, city.
Guar gum is a macromolecular natural hydrocolloid, belongs to natural galactomannan, is a natural thickener, is free-flowing powder from white to yellowish, can be dissolved in cold water or hot water, and forms a gelatinous substance when meeting water, thereby achieving the effect of rapid thickening. Guar gum used in the present invention is a product currently marketed, for example guar gum sold under the trade name food grade guar gum by Zhejiang Kangxing biotechnology Co.
Cationic guar gum is a water-soluble high molecular food gum/hydrocolloid, the chemical name of which is guar hydroxypropyl trimethyl ammonium chloride, and has satisfactory foaming and foam stabilizing efficacy in foaming products. The cationic guar used in the present invention is a product currently marketed, for example, by the company Guangzhou Hongchang biotechnology limited under the trade name food grade cationic guar.
Pectin is a class of heteropolysaccharides widely present in the primary wall and cell intermediate sheets of plant cell walls, and pectin is specified as an emulsifier, stabilizer, thickener according to food additive food sanitation standards (GB 2760-2014). The pectin used in the present invention is a product currently marketed, for example, by Shandong huge bioengineering Inc. under the trade name food grade pectin.
The chitosan is a product of removing partial acetyl of natural polysaccharide chitin, has multiple physiological functions of biodegradability, biocompatibility, no toxicity, bacteriostasis, anticancer, lipid reduction, immunity enhancement and the like, and is widely applied to food additives, textiles, agriculture, environmental protection, antibacterial agents, biomedical fields and other daily chemical industries. The chitosan used in the invention is a product sold in the market at present, for example, the chitosan sold by Shenzhen rubbing biotechnology Co., ltd under the trade name of food-grade chitosan.
Of course, any other adhesive that has the above-described effect may be used in the present invention, except that it does not adversely affect the atomized smoking material of the present invention and its articles, and such adhesives are within the scope of the present invention.
According to the invention, the main function of the acid-base regulator in the atomization fuming material is to regulate the smoke taste and the smoke irritation.
The acid-base modifier used in the invention is one or more acid-base modifiers selected from sodium carbonate, sodium bicarbonate, sodium lactate, potassium carbonate, dipotassium citrate, monopotassium citrate, potassium malate or monopotassium malate. All of them are products currently marketed, such as sodium bicarbonate sold under the trade name of food-grade sodium bicarbonate by Shandong Jiuqiujin, sodium lactate sold under the trade name of food-grade sodium lactate by Shandong Jiuqiujin, potassium carbonate sold under the trade name of food-grade potassium carbonate by Shandong Jiuqiujin, dipotassium citrate sold under the trade name of food-grade dipotassium citrate by Shandong Jiujiujin, monopotassium citrate sold under the trade name of food-grade monopotassium citrate by Shandong Jiujin, monopotassium malate sold under the trade name of food-grade potassium malate by Shandong Jiujin, monopotassium malate sold under the trade name of food-grade monopotassium malate by Shandong Jiujin.
Of course, any other acid-base modifier having the above-mentioned effects can be used in the present invention, but they do not adversely affect the atomized smoking material and its products of the present invention, and these acid-base modifiers are also within the scope of the present invention.
According to the invention, the primary function of the smoke generating aid in the aerosol-generating smoking material of the invention is that it volatilizes smoke carrying the flavour substances when heated.
The fuming aid used in the present invention is one or more fuming aids selected from glycerol, propylene glycol, glyceryl triacetate, stearic acid or hexadecane. They are all products that are currently on the market, examples are glycerol sold under the trade name of food-grade glycerol by Guangzhou Brilliant chemical Co., ltd, propylene glycol sold under the trade name of food-grade propylene glycol by Guangzhou Brilliant chemical Co., ltd, glyceryl triacetate sold under the trade name of food-grade glyceryl triacetate by Guangzhou Brilliant chemical Co., ltd, stearic acid sold under the trade name of food-grade stearic acid by Guangzhou Qianliang fine chemical Co., ltd, and hexadecane sold under the trade name of food-grade hexadecane by Guangzhou Qianliang fine chemical Co., ltd.
Of course, any other smoke generating aids having the above-described effect may be used in the present invention, except that they do not adversely affect the atomized smoke generating material of the present invention and its articles, and such smoke generating aids are within the scope of the present invention.
According to the invention, the main function of the edible spice in the atomized smoke material is to provide the atomized smoke material with fragrance, change the smoke style and improve the smoke taste.
The flavorant used in the present invention is one or more flavorants selected from menthol, vanillin, ethyl maltol, 1, 4-dimethyl pyrazine, coffee flavor, blueberry flavor, apple flavor, orange juice flavor, and like flavor products.
Wherein menthol is the main component in peppermint and peppermint essential oil, exists in free and ester state, can be used as the perfuming agent of toothpaste, perfume, beverage and candy, etc., menthol used in the invention is the product sold by Hunan national biotechnology Co., ltd.
The vanillin has the chemical name of 3-methoxy-4-hydroxybenzaldehyde, has the fragrance of vanilla beans and rich milk fragrance, plays roles of flavoring and fixing fragrance, and is widely applied to industries of cosmetics, tobacco, cakes, candies, baked foods and the like. The vanillin used in the invention is, for example, a product sold under the trade name of food grade vanillin by the pharmaceutical chemical company of marchanna white.
Ethyl maltol is a safe, reliable, low-dosage and remarkable-effect food additive, and has a molecular formula of C 7 H 8 O 3 Is a good flavor synergist for tobacco, food, beverage, essence, fruit wine, daily cosmetics and the like. The ethyl maltol used in the present invention is, for example, a product sold by the pharmaceutical chemical company of marchanna white under the trade name of food grade ethyl maltol.
1, 4-dimethyl pyrazine is a food flavor additive having the flavor of nut, mould, roast, nut and roast foods. The 1, 4-dimethylpyrazine used in the present invention is, for example, a product sold under the trade name 1, 4-dimethylpyrazine by Shanghai Zhongxin perfumery Co.
The coffee flavor, the blueberry flavor, the apple flavor and the orange juice flavor used in the invention are all products sold in the market at present, such as coffee flavor sold by Yunnan Balanophora biotechnology Co., under the trade name of mellow coffee, blueberry flavor sold by Yunnan Balanophora biotechnology Co., under the trade name of blueberry essence, apple flavor sold by Yunnan Balana biotechnology Co., under the trade name of green apple essence, and orange juice flavor sold by Yunnan Balana biotechnology Co., under the trade name of orange juice essence.
Of course, any other flavorant having the above-described effect can be used in the present invention, except that it does not adversely affect the atomized smoking material of the present invention and its articles, and such flavorants are within the scope of the present invention.
According to the invention, when the contents of the herbal plant powder, the starch, the adhesive, the acid-base regulator, the fuming auxiliary agent and the edible spice are in the ranges, if the content of the betel nut extract is lower than 10 parts by weight, the betel nut alkali content of the atomized fuming material is lower, the betel nut aroma is insufficient, and the satisfaction is weak; if the content of the betel nut extract is more than 20 parts by weight, the betel nut alkali content is too high, which causes uncomfortable sucking of the aspirator and also the cost is too high; therefore, the content of the betel nut extract is reasonable in 10 to 20 parts by weight, preferably 12 to 18 parts by weight, more preferably 14 to 16 parts by weight;
When the content of the betel nut extract, the starch, the adhesive, the acid-base regulator, the fuming auxiliary agent and the edible spice are in the range, if the content of the herbal plant powder is lower than 30 parts by weight, the amount of the betel nut extract adsorbed by the herbal plant powder is lower, so that the plant aroma characteristic of the atomized fuming material is not obvious; if the content of the herbal plant powder is higher than 50 parts by weight, the amount of the areca catechu extract adsorbed by the herbal plant powder is excessive, the flavoring is not easy to coordinate, the plant aroma is too intense, and the product cost is too high; accordingly, the content of the herb powder is suitably 30 to 50 parts by weight, preferably 36 to 44 parts by weight, more preferably 38 to 42 parts by weight;
when the content of the betel nut extract, the herbal plant powder, the adhesive, the acid-base regulator, the fuming auxiliary agent and the edible spice is in the range, if the content of the starch is lower than 5 parts by weight, the atomized fuming material of the invention can not be thickened effectively, and the use effect is poor; if the starch content is higher than 15 parts by weight, the atomized smoke material of the invention is too viscous, and bad smell is brought after the starch is gelatinized; accordingly, a starch content of 5 to 15 parts by weight is appropriate, preferably 8 to 12 parts by weight, more preferably 9 to 11 parts by weight;
When the content of the betel nut extract, the herbal plant powder, the starch, the acid-base regulator, the fuming auxiliary agent and the edible spice are in the range, if the content of the adhesive is lower than 2 parts by weight, the adhesiveness between the raw materials of the atomized fuming material is insufficient, and the atomized fuming material is difficult to form or is poor to form; if the content of the adhesive is higher than 10 parts by weight, the atomized smoke material is too viscous, and the raw material taste of the adhesive is too heavy, so that peculiar smell is brought; therefore, the content of the adhesive is preferably 2 to 10 parts by weight, preferably 4 to 8 parts by weight, more preferably 5 to 7 parts by weight;
when the content of the betel nut extract, the herbal plant powder, the starch, the adhesive, the fumigant and the edible spice are in the range, if the content of the acid-base regulator is lower than 0.1 weight part, the capability of regulating the smoke taste and the smoke irritation is insufficient, the smoke fragrance is not obvious to disperse, and the physiological intensity is too strong; if the content of the acid-base regulator is higher than 2.0 parts by weight, the smoke is too strong in stimulation, and the smoke comfort level is reduced along with a certain degree of peculiar smell; accordingly, the content of the acid-base modifier is preferably 0.1 to 2.0 parts by weight, more preferably 0.6 to 1.4 parts by weight, still more preferably 0.8 to 1.2 parts by weight;
When the content of the betel nut extract, the herbal plant powder, the starch, the adhesive, the acid-base regulator and the edible spice is in the range, if the content of the fuming auxiliary agent is lower than 5 parts by weight, the capability of volatilizing the aromatic substances to form smoke by heating is obviously insufficient; if the content of the fuming auxiliary agent is higher than 20 parts by weight, the atomized fuming material of the invention can generate too thick smoke, so that the experience of a smoker is affected, and the fuming auxiliary agent is easy to absorb moisture and is very unfavorable for preserving cigarette products; thus, a fuming aid content of 5 to 20 parts by weight is feasible, preferably 9 to 16 parts by weight, more preferably 10 to 14 parts by weight;
when the content of the betel nut extract, the herbal plant powder, the starch, the adhesive, the acid-base regulator and the fuming auxiliary agent are in the range, if the content of the edible spice is less than 0.2 weight part, the smoke style cannot be fully changed, and the smoke taste can be improved; if the content of the edible spice is more than 2.0 parts by weight, the aroma of the edible spice presses the characteristic aroma of the plant raw material; thus, a flavorant content of 0.2 to 2.0 parts by weight is suitable, preferably 0.8 to 1.4 parts by weight, more preferably 1.0 to 1.2 parts by weight.
Preferably, the atomization fuming material is prepared from 12-18 parts by weight of betel nut extract, 36-44 parts by weight of herb powder, 8-12 parts by weight of starch, 4-8 parts by weight of adhesive, 0.6-1.4 parts by weight of acid-base modifier, 9-16 parts by weight of fuming auxiliary agent and 0.8-1.4 parts by weight of edible spice.
More preferably, the atomized fuming material is prepared from 14-16 parts by weight of betel nut extract, 38-42 parts by weight of herb powder, 9-11 parts by weight of starch, 5-7 parts by weight of adhesive, 0.8-1.2 parts by weight of acid-base modifier, 10-14 parts by weight of fuming auxiliary agent and 1.0-1.2 parts by weight of edible spice.
According to the invention, the atomized fuming material is a sheet-shaped material with the thickness of 0.1-0.5 mm, a granular material with the diameter of 0.3-1.2 mm or a powdery fuming material with the granularity of 40-100 meshes.
The atomized smoke material of the present invention is formed into a sheet-like smoke material having a thickness of 0.1 to 0.5mm by a processing method described in a conventional sheet processing method (CN 106714590a, the invention name "a method for producing homogenized tobacco material"), and the atomized smoke material of the present invention is formed into a particulate atomized smoke material having a diameter of 0.3 to 1.2mm by a conventional powder granulation processing method (CN 111000282a, the invention name "alkaloid smoke particles for low-temperature heating nonflammable products and a preparation method thereof") using a granulator commonly used in the art, or the atomized smoke material of the present invention is mixed and ground into a powder smoke material having a particle size of 40 to 100mm by a conventional grinding processing method (CN 201910787685, the invention name "a heating nonflammable smoke product and a preparation method thereof") using a grinder commonly used in the art.
According to the sensory requirements of GB5606.4-2005 cigarettes, a group of 7 panelists rated the cigarettes on sale using the atomized smoking materials (powder, flakes, granules) of the invention, with the results shown in Table 1.
According to GB5606.4-2005 part 4 of cigarette, the sensory quality assessment in sensory technical requirements mainly comprises indexes such as smoke temperature, smoke quantity, suction quantity, physiological intensity, fragrance, style characteristics, comfort, peculiar smell and the like. The sensory quality evaluation score was a percent, divided up to 100 points, and each item was a score unit of 0.5 points.
Wherein the smoke temperature is the smoke temperature heat sensed in the mouth of a smoker when smoking a cigarette. Therefore, the consistency of the heater types is ensured when the sensory quality evaluation is carried out, and the heaters are required to be calibrated first, so that each heater has the same heating temperature and heating duration.
The smoke volume is how much smoke is exhaled from the mouth when a smoker draws on a cigarette.
The number of suction ports is the number of ports sucked when the smoke amount decreases obviously when a smoker sucks cigarettes according to a certain suction mode.
Irritation refers to the slight and obvious uncomfortable feeling of smoke on the sense, such as abnormal irritation to nasal cavity, oral cavity, throat, etc.
The aroma refers to aroma and aftertaste, namely inherent aroma of tobacco special for heating non-combustible cigarette smoke and taste feeling left after the smoke exhales from oral cavity and nasal cavity.
The style characteristics are the essential smell of the fragrance style of the heated non-combustible cigarettes, and the change of the fragrance can be obviously felt.
The comfort consists of two parts, namely, the uncomfortable feeling of smoke on sense organs during suction, such as sprint of nasal cavity, oral cavity and throat, mao Jihuo burn and the like; secondly, sensory discomfort is felt when the cigarette bullet is inserted into or pulled out of the smoking set before and after the smoking, such as laborious insertion, bending, head dropping during pulling out, and the like.
The peculiar smell is a peculiar smell (except for added aroma) which is obviously different from the natural smell of the heated non-combustible cigarette, so that the cigarette loses the smoking value.
In the section 4 of GB5606.4-2005 cigarettes, the lowest evaluation results of the sensory quality evaluation of cigarettes of different classes in sensory technical requirements are different, and the class I is more than or equal to 85, the class II and the class III are more than or equal to 75, the class IV and the class V are more than or equal to 60, so that the difference between the standard evaluation of the heated non-combustible products and the traditional cigarettes is normal. The invention is modified based on the traditional cigarette grading standard so as to be more in line with the evaluation of heating incombustibility. The highest gloss and smoothness of the traditional cigarettes are divided into 5 minutes; the highest evaluation of fragrance fullness and fineness is divided into 32 minutes; the highest harmonic assessment is divided into 6; the highest evaluation of no miscellaneous gas is 12; the non-irritation assessment was rated as 20 points at maximum; the highest score for purity and comfort was 25. Compared with the traditional cigarettes, the method has the advantages that the heating is performed by using an external heat source without burning, the heating temperature is controlled within the range of 200-400 ℃, so that the herbal powder can be heated, evaporated and released, and the condition of triggering the burning of materials is not reached, therefore, the evaluation standard of the herbal powder is different from the evaluation standard of the traditional cigarettes.
The invention has the advantages of heating and non-combustion scoring standard smoke temperature of 20 minutes, smoke quantity of 20 minutes, suction mouth number of 20 minutes, physiological intensity of 8 minutes, fragrance of 8 minutes, style of 8 minutes, comfort of 8 minutes and peculiar smell of 8 minutes.
Meanwhile, cigarettes identical to the above cigarettes using the conventional sheet-like atomized smoking material (CN 106714590a, inventive name "method for producing homogenized tobacco material") were also subjected to the same evaluation as the control sample 1, and cigarettes identical to the above cigarettes using the conventional particulate atomized smoking material (CN 111000282a, inventive name "alkaloid smoking particles for low-temperature heating non-combustible products and method for producing same") were also subjected to the same evaluation as the control sample 2, and the evaluation results thereof are also shown in table 1.
As can be seen from the foregoing, the atomized smoking material of the present invention has the following technical characteristics:
the heating non-combustion product made of the atomized smoke material can provide physiological satisfaction and function similar to tobacco, and can replace the existing tobacco product to a certain extent; compared with the nicotine content of the effective component of the existing tobacco products, the arecoline content of the effective component of the heating nonflammable product can be reduced by 10-20 times, so that the product safety and the manufacturing cost of the invention have obvious advantages.
[ advantageous effects ]
The beneficial effects of the application are as follows:
the application relates to an atomized smoke material containing betel nut extract. The heating non-combustion product made of the atomized smoke material can provide similar physiological satisfaction and function as tobacco, so that the existing tobacco product is replaced to a certain extent. Compared with the nicotine content of the effective component of the existing tobacco products, the arecoline content of the effective component of the heating nonflammable product can be reduced by 10-20 times, so that the product safety and the manufacturing cost cannot be obviously improved.
Compared with the traditional chewing betel nut, the heating non-burning product containing betel nut components can achieve similar physiological satisfaction with lower betel nut component content, avoid the stimulation of the fiber in the addition of strong alkali and betel nut to the oral cavity and digestive tract, and improve the health risk of the product.
[ detailed description ] of the application
The application will be better understood by the following examples.
Example 1: the application discloses an atomized fuming material
The implementation of this example is as follows:
10 parts by weight of a water betel nut extract with betulin content of 1% by weight, 30 parts by weight of green tea leaf herbal plant powder with granularity of 40 meshes sold by Yunnan Jinggu tea factory company under the trade name of superfine green tea, 8 parts by weight of corn starch with purity of 90.8% by weight sold by Guangzhou deep-wound chemical Co Ltd under the trade name of food grade corn starch, 5 parts by weight of a water-soluble starch adhesive sold by Nantong Yunfeng starch Co Ltd under the trade name of food grade water-soluble starch, 0.8 part by weight of a sodium bicarbonate acid-base regulator sold by Shandong Jiuyuanjie chemical Co Ltd under the trade name of food grade sodium bicarbonate, 10 parts by weight of a glycerol fuming aid sold by Guangshi Lian chemical Co Ltd under the trade name of food grade glycerol, and 0.8 parts by Hunan biological technology Co Ltd under the trade name of food grade menthol are uniformly mixed, and the obtained mixture is manufactured into a sheet material with thickness of 0.170mm by adopting the processing method described in the specification.
The sheet-like smoking material prepared using this example was subjected to a puff evaluation according to the method described in the present specification, the evaluation results of which are shown in table 1.
Meanwhile, the same cigarettes as those described above using the conventional sheet-like atomized smoking material (CN 106714590a, entitled "method for producing homogenized tobacco material") were also subjected to the same evaluation as the control sample 1, and the evaluation results thereof are also shown in table 1.
Example 2: the application discloses an atomized fuming material
The implementation of this example is as follows:
the method comprises the steps of uniformly mixing 12 parts by weight of an ethanol betel nut extract with a betulin content of 4% by weight, 36 parts by weight of a propylene glycol fuming additive sold by Kagaku Kogyo Co Ltd in the trade name of Zigaku, 12 parts by weight of potato starch sold by Kagaku Kogyo Co Ltd in the trade name of food-grade potato starch with a purity of 92.1% by weight, 7 parts by weight of a sodium carboxymethyl cellulose adhesive sold by Kiku Kogyo Co Ltd in the trade name of food-grade sodium carboxymethyl cellulose, 1.2 parts by weight of a sodium bicarbonate acid-base modifier sold by Shandong Jiuyaku Kogyo Co Ltd in the trade name of food-grade sodium bicarbonate, 14 parts by weight of a propylene glycol fuming additive sold by Guangshi Kogyo Co Ltd in the trade name of food-grade propylene glycol, and 1.4 parts by Wuhan Lagena Kogyo Co Ltd in the trade name of food-grade vanillin, and preparing the obtained mixture into a granular material with a diameter of 0.3-0.5mm by adopting a processing method described in the specification.
The particulate smoking material prepared using this example was subjected to a smoking evaluation according to the method described in the specification of the present application, the evaluation results of which are shown in table 1.
Meanwhile, cigarettes identical to the cigarettes described above using the conventional particulate atomized smoking material (CN 201811285170, entitled "a heating non-combustible cigarette smoking particulate material and method for producing the same") were also subjected to the same evaluation as control sample 2, and the evaluation results are also shown in table 1.
Example 3: the application discloses an atomized fuming material
The implementation of this example is as follows:
18 parts by weight of an acetone betel nut extract with 10% arecoline content by weight, 44 parts by weight of mugwort herb powder with the granularity of 120 meshes sold by the company of Katsuji in milliy under the trade name mugwort leaf, 5 parts by weight of wheat starch with the purity of 94.8% by weight sold by the company of Guangzhou deep-wound chemical industry Co under the trade name of food-grade wheat starch, 2 parts by weight of guar gum adhesive sold by the company of Zhejiang Kangxing biotechnology Co under the trade name of food-grade guar gum, 0.1 part by weight of sodium lactate regulator sold by the company of Shandong Jiuji chemical industry Co under the trade name of food-grade sodium lactate, 5 parts by weight of glycerol triacetate fuming aid sold by the company of Guangzhou Brilliant chemical industry Co under the trade name of food-grade glycerol triacetate, and 1.0 part by the company of Wuhan Katsuji chemical industry Co under the trade name of food-grade ethyl maltol are uniformly mixed, and the obtained mixture is sieved by a sieve with 40 meshes, so that the powdery material with the granularity of 40 meshes is prepared.
The powdery smoking material prepared using this example was subjected to a smoking evaluation according to the method described in the present specification, and the evaluation results are shown in table 1.
Example 4: the application discloses an atomized fuming material
The implementation of this example is as follows:
14 parts by weight of a betel nut extract of a sulfuric acid aqueous solution with betel nut alkali content of 3% by weight, 50 parts by weight of a dry loquat leaf herbal powder sold by Huimin Chinese medicine wholesale company of the city of Bo, 15 parts by weight of corn starch sold by deep-wound chemical Co., ltd. In Guangzhou with purity of 90.8% by weight under the trade name of food-grade corn starch, 10 parts by weight of a cationic guar gum sold by red-Chang biotechnology Co., ltd. In Guangzhou under the trade name of food-grade cationic guar gum, 2.0 parts by weight of a potassium carbonate alkali regulator sold by Jiulong chemical Co., ltd. In Shandong under the trade name of food-grade potassium carbonate, 9 parts by weight of a stearic acid fuming aid sold by Qianli chemical Co., ltd. In Guangzhou under the trade name of food-grade stearic acid, and 1.2 parts by Shanghai Zhenchen flavor Co., ltd. Under the trade name of 1, 4-dimethyl pyrazine are uniformly mixed, and the obtained mixture is made into a sheet material with a thickness of 0.2mm by adopting the processing method described in the specification.
The sheet-like smoking material prepared using this example was subjected to a puff evaluation according to the method described in the present specification, the results of which are shown in table 1.
Example 5: the application discloses an atomized fuming material
The implementation of this example is as follows:
16 parts by weight of supercritical CO with arecoline content of 6% by weight 2 The betel nut extract, 38 parts by weight of cocoa herb powder sold by the company of tin-free okang food, with the granularity of 200 meshes, with the trade name of pure cocoa powder, 9 parts by weight of sweet potato starch sold by the company of Guangzhou deep-wound chemical industry, with the purity of 90.6% by weight, with the trade name of food-grade sweet potato, 4 parts by weight of pectin adhesive sold by the company of Shandong Kyoho bioengineering, with the trade name of food-grade pectin, 0.6 part by weight of dipotassium citrate alkali regulator sold by the company of Shandong Jiujin, with the granularity of food-grade dipotassium citrate, 16 parts by weight of hexadecane smoke-generating auxiliary agent sold by the company of Guangyi fine chemical industry, with the trade name of food-grade hexadecane, with the purity of 90.2 parts by weight, with the trade name of coffee-flavor edible flavor sold by the company of KappaUK, with the company of Yunnan Baku biological technology, with the trade name of mellow coffee, are uniformly mixed, and the obtained mixture is sieved by a 50 mesh sieve to prepare a powdery material with the granularity of 50 meshes.
The powdery smoking material prepared using this example was subjected to a smoking evaluation according to the method described in the present specification, and the evaluation results are shown in table 1.
Example 6: the application discloses an atomized fuming material
The implementation of this example is as follows:
uniformly mixing 20 parts by weight of an ethanol betel extract with arecoline content of 8% by weight, 42 parts by weight of kudzuvine root herbal powder with particle size of 180 meshes sold by the company limited by the pharmaceutical industry of the origin of the city, the salt of kudzuvine root, 11 parts by weight of corn starch with purity of 94.0% by weight sold by the company limited by the deep-wound chemical industry of Guangzhou, the product name of food-grade corn starch, 8 parts by weight of a chitosan adhesive sold by the company limited by the biological science and technology of Shenzhen, 1.4 parts by weight of a citric acid monopotassium salt regulator sold by the company limited by the Shandong, the product name of food-grade citric acid monopotassium salt, 20 parts by weight of a mixture (weight ratio 1:1) of fuming auxiliary agent sold by the company limited by the Guangdong, the company limited by the company, the product name of food-grade propylene glycol, and 2.0 parts by weight of blueberry flavor edible essence sold by the company limited by the company of Yunnan Balanophora, the resulting mixture was formed into a particulate smoking material having a diameter of 0.4 to 0.6mm using the processing methods described herein.
The particulate smoking material prepared using this example was subjected to a puff evaluation according to the method described in the present specification, the results of which are shown in table 1.
Example 7: the application discloses an atomized fuming material
The implementation of this example is as follows:
mixing 20 parts by weight of arecoline extract with 5% by weight, 38 parts by weight of a guar gum mixture (weight ratio 2:3) adhesive with granularity of 150 mesh sold by the company of the Ming's medicine of the origin of Zhejiang, 15 parts by weight of licorice herbal powder with purity of 92.1% by weight sold by the company of the Guangzhou deep-wound chemical industry, 2 parts by weight of potato starch sold by the company of the Uygur-chemical industry, 2 parts by weight of a stearic acid mixture (weight ratio 3:1) auxiliary agent sold by the company of the Kikumi chemical industry, 2 parts by weight of guar gum sold by the company of the Zhejiang Kangxing biotechnology, 1.2 parts by weight of a potassium malate alkali regulator sold by the company of the Shandong Jiuyuanjie chemical industry, 10 parts by weight of a triglycerin sold by the company of the Guangdong, and a food grade triglycerin by the company of the food grade, and 2.0 parts by weight of a stearic acid mixture (weight ratio 3:1) auxiliary agent sold by the company of the Qianli fine chemical industry, brand stearic acid and apple essence sold by the company of the biological flavor of the Guangdong, and apple essence by weight of the biological flavor, which are uniformly mixed by weight of apple flavor, the resulting mixture was formed into a sheet-like smoking material having a thickness of 0.20mm using the processing methods described in this specification.
The sheet-like smoking material prepared using this example was subjected to a puff evaluation according to the method described in the specification of the present application, and the evaluation results are shown in table 1.
Table 1: sensory evaluation result of atomized smoke material prepared by the application
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Note that: * The highest flue gas temperature is 20 minutes; the highest smoke amount is 20 minutes; the highest number of the suction ports is 20 minutes; the highest physiological intensity is divided into 8 minutes; the highest fragrance is 8 minutes; the highest score of style characteristics is 8; the highest comfort is 8 points; the highest odor is 8 minutes.
The sensory evaluation results listed in table 1 clearly show that: the atomized smoke material prepared by the application has the advantages of large smoke quantity, low smoke temperature, certain physiological strength, namely physiological satisfaction, obvious fragrance plump style and higher comfort.

Claims (6)

1. An atomized smoke generating material for heating non-combustible products, which is characterized by comprising 10-20 parts by weight of betel nutsThe smoke generating agent is prepared from 30 to 50 parts by weight of extract, 5 to 15 parts by weight of herb powder, 2 to 10 parts by weight of starch, 0.1 to 2.0 parts by weight of adhesive, 5 to 20 parts by weight of acid-base modifier, and 0.2 to 2.0 parts by weight of smoke generating auxiliary agent; the betel nut extract is water, ethanol, acetone, inorganic acid aqueous solution, organic acid aqueous solution extract or supercritical CO 2 An extract; the betulin content of the betel nut extract is 1-10% by weight; the herbal plant powder is tea leaf, peppermint leaf, mugwort leaf, loquat leaf, cocoa, kudzuvine root, liquorice or sugarcane plant powder, and the granularity of the herbal plant powder is 40-200 meshes; the starch is corn starch, potato starch, wheat starch or sweet potato starch with the purity of more than 90% by weight; the adhesive is one or more adhesives selected from sodium carboxymethyl cellulose, guar gum, cationic guar gum, pectin or chitosan.
2. An atomized smoking material according to claim 1, characterized in that it is made of 12-18 parts by weight of betel nut extract, 36-44 parts by weight of herb powder, 8-12 parts by weight of starch, 4-8 parts by weight of adhesive, 0.6-1.4 parts by weight of acid-base modifier, 9-16 parts by weight of smoking aid and 0.8-1.4 parts by weight of edible flavor.
3. An aerosol-generating smoking material according to claim 1 or claim 2, wherein the acid-base modifier is one or more acid-base modifiers selected from sodium carbonate, sodium bicarbonate, sodium lactate, potassium carbonate, dipotassium citrate, monopotassium citrate or potassium malate.
4. An aerosol-generating smoking material according to claim 1 or claim 2, wherein the smoking aid is one or more smoking aids selected from glycerol, propylene glycol, glyceryl triacetate, stearic acid or hexadecane.
5. An aerosol-generating smoking material according to claim 1 or 2, wherein the flavour is one or more flavours selected from menthol, vanillin, ethyl maltol, 1, 4-dimethyl pyrazine, coffee flavours, blueberry flavours, apple flavours or orange juice flavours.
6. An atomized smoking material according to claim 1 or 2, wherein the atomized smoking material is a sheet-like, 0.1-0.5 mm thick, 0.3-1.2 mm diameter particulate or 40-100 mesh powder smoking material.
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