CN112826150A - Plant silk type binary structure heating non-combustible product - Google Patents

Plant silk type binary structure heating non-combustible product Download PDF

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Publication number
CN112826150A
CN112826150A CN202110247253.9A CN202110247253A CN112826150A CN 112826150 A CN112826150 A CN 112826150A CN 202110247253 A CN202110247253 A CN 202110247253A CN 112826150 A CN112826150 A CN 112826150A
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China
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smoke
section
tobacco
combustible
plant
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Inventor
杨紫刚
周瑾
黄亮
施庆珍
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Yunnan Chunxu Biotechnology Co ltd
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Yunnan Chunxu Biotechnology Co ltd
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/40Constructional details, e.g. connection of cartridges and battery parts
    • A24F40/46Shape or structure of electric heating means
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/40Constructional details, e.g. connection of cartridges and battery parts

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)

Abstract

The invention relates to a plant silk type heating non-combustible product with a binary structure, which is formed by wrapping a smoke generating section and a smoke binding section which are made of plant silk materials containing smoke generating agents through outer layer wrapping paper in sequence or by sequentially filling the smoke generating section and the smoke binding section into a tube made of silica gel, paper or high polymer materials with the temperature higher than 300 ℃; the smoke binding section is a suction end; the heating non-combustible product has the advantages of large smoke quantity, low smoke suction temperature and the like, is suitable for heaters for central heating, circumferential heating or central and circumferential heating, has a simple structure, is easy to industrialize, and has a very good industrial application prospect.

Description

Plant silk type binary structure heating non-combustible product
[ technical field ] A method for producing a semiconductor device
The invention belongs to the technical field of tobacco processing. More particularly, the present invention relates to a plant silk type binary structure heating non-combustible product.
[ background of the invention ]
With the development of the society and the continuous improvement of the living standard of people, people pay more and more attention to the health problem of people, the cigarette smoking safety is more and more important to smokers, and the cigarette smoking safety is also a technical problem which needs to be solved urgently in the tobacco industry. The heating non-combustible product is a novel product developed in recent years, and as the smoke is released by heating and baking through an external heat source, the release amount of harmful ingredients of the product is remarkably reduced, and compared with the traditional smoking tobacco, the safety of the product is remarkably improved, the product is approved in the market, and good market feedback is obtained.
The solution of smoking of heated non-combustible products is the technical solution of using a heat source to heat and release the fumes, in order to reduce the temperature of the fumes at the inlet, the multi-element structural unit is added in the structure of the cigarette bullet, but the temperature of the lip end is still higher, so that the experience defects of less smoke amount and lighter fragrance are caused, these drawbacks also limit the choice of more consumers to heat non-combustible products, and due to the structural limitations of the cigarettes of non-combustible products, the problem still cannot be solved effectively, meanwhile, the complicated filter stick structure causes difficult product manufacture and high production cost, for example, US20140305448A1 discloses a quaternary structure of a non-burning heating cigarette bomb, which is a smoking section, a supporting section, a cooling section and a filtering section, the production process is complex, the smoking experience is influenced by the melting phenomenon in the cooling section in the smoking process, and the defects of small smoke quantity, high smoke temperature and the like exist. At present, the flakes and the particles are used as fuming and aroma-producing materials, the plants need to be subjected to powdering treatment and then are subjected to recombination papermaking or granulation, the mechanical requirement is high, and the process is complex.
Therefore, in view of the technical defects of the prior art, the inventors summarized the analysis of the prior art and performed a great deal of tests and analysis, and finally completed the present invention.
[ summary of the invention ]
[ problem to be solved ]
The invention aims to provide a plant silk type binary structure heating non-combustible product.
[ solution ]
The invention is realized by the following technical scheme.
The invention relates to a plant silk type binary structure heating non-combustible product.
The plant silk type heating non-combustible product with the binary structure is formed by sequentially wrapping a smoke generation section and a smoke binding section which are made of plant silk materials containing smoke generating agents through outer-layer wrapping paper, or sequentially filling the smoke generation section and the smoke binding section into a tube made of silica gel, paper or high polymer materials which can resist the temperature higher than 300 ℃; the smoke binding section is a suction end.
According to a preferred embodiment of the invention, the plant silk material is a flue-cured tobacco, tobacco stem, sun-cured tobacco or burley tobacco silk smoking material together with a mint, tea, betel nut or cocoa non-tobacco silk smoking material.
According to another preferred embodiment of the invention, the plant silk material is made by rolling tobacco or non-tobacco silk with the width of 0.5-3.0 mm, and the filling rate of the plant silk material in the smoking section is 40-80%.
According to another preferred embodiment of the invention, the smoking agent is one or more selected from the group consisting of glycerol, propylene glycol, glycerol diacetate and glycerol triacetate.
According to another preferred embodiment of the present invention, the content of the smoke agent is 10 to 50% by weight of the plant silk material.
According to another preferred embodiment of the invention, said fume-bounding section is a cylinder of silicone rubber, polyethylene, polypropylene, vinylidene chloride, polylactic acid, polyurethane, cellulose acetate or paper material, in which cylinder or between the cylinder and the outer paper is provided a through-going hole parallel to its longitudinal axis.
According to another preferred embodiment of the invention, the side of the cross section of the smoke binding section is circular, zigzag or wavy; the edge of the cross section of the through hole is circular, zigzag or wavy.
According to another preferred embodiment of the invention, when the through hole is positioned in the middle of the flue gas binding section, the distance between the wall of the through hole and the outer wall of the flue gas binding section is 1-3 mm.
According to another preferred embodiment of the present invention, in the cross section of the flue gas bound section, the ratio of the area of the through holes to the area of the non-through holes is 0.3 to 2.0.
According to another preferred embodiment of the invention, the water content of the flue gas bound section is 2.0 to 4.0% by weight.
The present invention will be described in more detail below.
The invention relates to a plant silk type binary structure heating non-combustible product.
The plant silk type heating non-combustible product with the binary structure is formed by wrapping a smoke generating section and a smoke binding section which are sequentially made of plant silk materials containing smoke agents through outer layer wrapping paper, and the specific structure is shown in figure 1, wherein 1-the smoke generating section is shown in the figure; 2-a flue gas binding section; 2-1-straight through hole; 3-wrapping paper; or the plant silk type binary structure heating non-combustible product is obtained by sequentially loading into a tube made of silica gel, paper or high molecular material with temperature resistance higher than 300 deg.C, and the specific structure is shown in figure 2, wherein figure 1-smoke generation section; 2-a flue gas binding section; 2-1-straight through hole; 3-1-tube; the smoke binding section is a suction end.
According to the invention, the main function of the plant silk material in the heat-not-burn product is to provide fragrance to the product, and the plant silk material is a flue-cured tobacco, tobacco stem, sun-cured tobacco or burley tobacco shred smoking material and a mint, tea, betel nut or cocoa non-tobacco shred smoking material.
The tobacco shred smoking materials are finished tobacco raw materials commonly used in the prior art, or expanded tobacco leaves or expanded tobacco stems processed by the prior expansion processing method, the processed tobacco raw materials have increased volume and increased pores, and can absorb more smoking agents and spice substances, and the specific situation is shown in document CN110638083A, the invention name of which is 'an efficient preparation method of expanded tobacco shreds', CN 103169150B, the invention name of which is 'a preparation method of expanded tobacco stems'.
Non-tobacco shredded smoking materials such as mint are currently marketed products which can be used as such or after the same expansion treatment.
According to the invention, the plant silk material is formed by rolling tobacco silk or non-tobacco silk with the width of 0.5-3.0 mm, and the filling rate of the plant silk material in a smoking section is 40-80%.
In the present invention, the filling rate is understood to be the ratio of the volume of the plant silk material to the volume of the smoking segment, expressed as a percentage.
When the filling rate is in the range, if the width of the filamentous smoking material is less than 0.5mm, broken filaments are easy to agglomerate in the rolling process, and the suction resistance is influenced; if the width of the filamentous smoking material is more than 3.0mm, the porosity of the rolled material is high, the heating is insufficient, and the smoking amount is influenced.
When the width of the filamentous smoking material is within the range, if the filling rate is lower than 40%, the cut tobacco falls off to influence the product quality; if the filling rate is higher than 80%, the filling amount is too large, which causes too high suction resistance and affects the suction experience.
The primary function of the smoke agent in the heated non-combustible article is to provide the smoke required when smoking the heated non-combustible article of the invention.
According to the invention, the said smoke agent is one or more smoke agents selected from glycerol, propylene glycol, glycerol diacetate or glycerol triacetate, all of which are currently marketed products, such as glycerol diacetate sold under the name diacetate by Hubei Hengheng technology Co., Ltd, glycerol triacetate sold under the name triacetate by Jiangsu Caesalpe Biotech Co., Ltd.
According to the invention, the content of the smoke agent is 10-50% of the weight of the plant silk material. If the addition amount of the smoke agent is less than 10%, the smoke amount of people in smoking is less, and smoking experience is influenced; if the addition amount of the smoke agent is more than 50 percent, the mobility of the tobacco shreds and the non-tobacco shreds is poor in the processing process, and the tobacco shreds and the non-tobacco shreds are difficult to process to obtain products meeting quality requirements.
According to the invention, the main function of the smoke binding section in the non-combustible heating product is that the smoke binding section has enough area for heat exchange with smoke and enough heat capacity, and has the functions of cooling and guiding, so as to reduce the temperature of the smoke and guide the smoke for being sucked by consumers.
According to the invention, the smoke binding section is a cylinder made of silicon rubber, polyethylene, polypropylene, vinylidene chloride, polylactic acid, polyurethane, cellulose acetate or paper material, and a through hole parallel to the longitudinal axis of the cylinder is arranged in the cylinder or between the cylinder and the outer layer wrapping paper.
The silicone, polyethylene, polypropylene, vinylidene chloride, polylactic acid, polyurethane, cellulose acetate or paper materials used in the present invention are all commonly used in the art and are currently marketed products, such as silicone sold under the trade name silicone rubber by Balginia Yunnanensis Biotech, Inc., vinylidene chloride sold under the trade name PVDC by Guangzhou Xin porcelain environmental protection materials, Inc., cellulose acetate sold under the trade name cellulose acetate by Shaoxing-like textile technology, Inc.
According to the invention, the water content of the flue gas binding section is 2.0-4.0% by weight. If the water content of the smoke binding section is lower than 2.0%, the cooling effect is not ideal, and the suction experience is influenced; if the water content of the smoke binding section is higher than 4.0%, the smoking material of the smoking section is easy to absorb moisture, and the product quality is affected, so that the water content of the smoke binding section is suitable to be 2.0-4.0%. In the present invention, the water content is measured according to GB/T23357-2009 Karl Fischer method for measuring the moisture of tobacco and tobacco products.
In the invention, the side of the cross section of the smoke binding section is circular, zigzag or wavy; the edge of the cross section of the through hole is circular, zigzag or wavy. Of course, the cross section of the flue gas confinement section and the cross section of the through hole can be in other regular shapes or irregular shapes, and one can select the shape according to actual conditions, which will not cause any difficulty for the person skilled in the art.
In the invention, when the through hole is positioned in the middle of the flue gas binding section, the distance between the wall of the through hole and the outer wall of the flue gas binding section is 1-3 mm. In the present invention, when the edge of the through hole cross section is non-circular, this distance is understood to be the shortest distance between the wall of the through hole and the outer wall of the flue gas confinement section.
According to the invention, on the cross section of the smoke binding section, the ratio of the area of the through holes to the area of the non-through holes is 0.3-2.0. If the ratio of the area of the straight-through hole to the area of the non-straight-through hole is less than 0.3, the area of the straight-through hole is smaller, the suction resistance is large in the suction process, and the smoke concentration is insufficient; if the ratio of the area of the straight through hole to the area of the non-straight through hole is larger than 2.0, the area of the straight through hole is too large, the material amount of a smoke bounding section is small, and the heat capacity of the smoke bounding section is insufficient, so that the smoke temperature and the temperature of a lip end of a smoke bomb are higher, and the smoking experience of people is influenced. Preferably, the ratio of the area of the through holes to the area of the non-through holes is 0.5 to 1.8, and more preferably, the ratio of the area of the through holes to the area of the non-through holes is 0.8 to 1.6.
The smoke binding section is prepared by adopting an extrusion method or an injection molding method, and concretely, the extrusion method refers to CN 102642291B and the invention name of 'preparation process of large-diameter silicone tube'; for example, CN 107639787 a, entitled "a process for forming a silicone layer on the surface of a glass bottle by injection molding" is referred to as an injection molding method.
In the present invention, the outer-layer wrapping paper used is a common forming paper generally used in the art; the tube is made of silica gel, paper or high polymer material which can resist the temperature higher than 300 ℃, and the paper is cellulose paper, kraft paper, laminating paper and coated paper, for example; the polymer material is, for example, polyphenylene, polyimide, graphene polymer, or the like; these are commercially available products, for example, cellulose paper sold under the trade name of molding paper by the development ltd of the science and technology industry of engineth, yun, a coated paper sold under the trade name of water-and oil-barrier paper by the ltd of the paper industry of xu, polyphenylene sold under the trade name of PPSU by the ltd of majeri, and a graphene polymer sold under the trade name of graphene composite material by the cely leixi colloidal graphite factory.
The average smoke temperature, smoke concentration and sensory evaluation method are specifically described below.
The original-flavor cigarette cartridges produced in Feimo International and heated non-burning HHETs are selected as comparison cigarette cartridges, and according to the standards of GBT 19609-.
The average smoke concentration is measured by using the device by adopting a light transmission method under the conditions that the wavelength lambda of a laser light source is 630 mu m and the detection optical path is 4 cm;
and (3) pumping procedure: selecting iQOS smoking set produced by Felmo International, wherein the smoking program is that the equipment enters a smoking state after the heater finishes preheating, the smoking capacity of each port is 35ml, the smoking time is 2s, the flow rate of the smoking air flow is 17.5ml/s, the smoking interval is 13s, the total number of the smoking ports is 16, and the total smoking working time is 240 s;
and (3) temperature measurement: measuring the mainstream smoke temperature and the lip end temperature of the smoke cartridge by using a K-type thermocouple temperature detector;
smoke concentration index determination: the light transmission method for measuring the smoke concentration is a non-contact measuring method, when a light source passes through an aerosol medium, light beams and aerosol particle spherical surfaces generate scattering and refraction and the absorption effect of particles on the light, so that the transmission light intensity of a laser light source penetrating through aerosol smoke can be attenuated, when the aerosol concentration is higher, the transmission light intensity attenuation effect is more obvious, and when the aerosol concentration is lower, the transmission light intensity attenuation effect is weaker. The ratio of the intensity of the incident light to the intensity of the absorbed light under the specified detection conditions is called the extinction ratio, which is the measured smoke density index expressed in%.
[ advantageous effects ]
The invention has the beneficial effects that:
the plant silk type binary structure heating non-combustible product has the advantages of easy insertion, simple plant silk material processing, no falling and dropping of the silk material, large smoke generation amount, low smoke suction temperature and the like, is suitable for a heater for central heating, circumferential heating or central and circumferential heating, has simple structure, is easy to industrialize, and has very good industrial application prospect.
[ description of the drawings ]
FIG. 1 is a schematic structural view of a filament-type binary-heating non-combustible product of the present invention;
FIG. 2 is a schematic structural view of a filament-type binary-heating non-combustible product according to the present invention;
in the figure:
1-a smoke generation section; 2-a flue gas binding section; 2-1-straight through hole; 3-wrapping paper; 3-1-tube.
[ detailed description ] embodiments
The invention will be better understood from the following examples.
Example 1: the invention relates to a plant silk type binary structure heating non-combustible product
The implementation of this example is as follows:
the plant silk type heating non-combustible product with the binary structure is formed by sequentially wrapping a smoke generation section and a smoke binding section which are made of plant silk materials containing glycerol smoke agents through outer-layer wrapping paper kraft paper, wherein the smoke binding section is a suction end.
Wherein the plant silk material is formed by rolling flue-cured tobacco silk with the width of 0.8mm, and the filling rate of the flue-cured tobacco silk in a smoking section is 67 percent; the content of the glycerin smoke agent is 32 percent of the weight of the plant filamentous material;
the smoke binding section is a cylinder made of silicon rubber by adopting an extrusion method, and the water content of the smoke binding section is 2.4 percent by weight when the smoke binding section is detected by adopting the method described in the specification; a through-bore is provided in the cylinder parallel to its longitudinal axis. The side of the cross section of the smoke binding section is in a sawtooth shape; the edge of the cross section of the through hole is circular.
The distance between the wall of the through hole and the outer wall of the smoke binding section is 2.3 mm. The ratio of the area of the through holes to the area of the non-through holes in the cross section of the flue gas confinement section was 0.7.
The mean mainstream smoke temperature, mean lip end temperature, mean smoke concentration and sensory evaluation of the example of the heated non-combustible cartridges were measured according to the methods described in the specification of the present application, and the measurement results are shown in table 1.
Meanwhile, the mainstream average smoke temperature, the average lip temperature, the average smoke concentration and the sensory evaluation were also carried out using the heat non-burning HEETs original flavor cartridge produced by Feimo as a control cartridge, and the test results thereof are also shown in Table 1.
Example 2: the invention relates to a plant silk type binary structure heating non-combustible product
The implementation of this example is as follows:
the plant filamentous type binary structure heating non-combustible product is formed by sequentially wrapping a smoke generating section and a smoke binding section, wherein the smoke generating section is composed of plant silk materials containing a smoke generating agent of a mixture (weight ratio is 1:1) of glycerin and propylene glycol, the smoke binding section is wrapped by outer layer wrapping paper cellulose paper, and the smoke binding section is a suction end.
Wherein the plant silk material is formed by rolling burley tobacco shreds with the width of 1.2mm, and the filling rate of the burley tobacco shreds in the smoking section is 72 percent; the content of the smoke agent in the mixture of glycerin and propylene glycol (weight ratio 1:1) is 37% of the weight of the plant silk material;
the smoke binding section is a cylinder made of polyethylene by adopting an extrusion method, and the water content of the smoke binding section is 3.1 percent by weight when the smoke binding section is detected by adopting the method described in the specification; a through-bore is provided in the cylinder parallel to its longitudinal axis. The side of the cross section of the smoke binding section is wavy; the edge of the cross section of the through hole is in a sawtooth shape.
The distance between the wall of the through hole and the outer wall of the smoke binding section is 1.2 mm. The ratio of the area of the through holes to the area of the non-through holes in the cross section of the flue gas confinement section was 1.1.
The mean smoke temperature of the mainstream, mean lip temperature, mean smoke concentration and sensory evaluation of the example heated non-burning cartridges were measured according to the methods described in the specification of the present application, and the results of the measurements are shown in table 1.
Example 3: the invention relates to a plant silk type binary structure heating non-combustible product
The implementation of this example is as follows:
the plant silk type heating non-combustible product with the binary structure is formed by sequentially wrapping a smoke generation section and a smoke binding section, wherein the smoke generation section is composed of plant silk materials containing a smoke generating agent of a mixture (weight ratio is 2:1) of glycerol and glycerol diacetate, the smoke binding section is wrapped by outer-layer wrapping paper laminating paper, and the smoke binding section is a suction end.
Wherein the plant silk material is formed by rolling a mixture (weight ratio is 3:1) of flue-cured tobacco and tea leaf silk with the width of 1.4mm, and the filling rate of the mixture of the flue-cured tobacco and the tea leaf silk in a smoking section is 59%; the content of the smoke agent of the mixture of glycerol and glycerol diacetate (weight ratio 2:1) is 42 percent of the weight of the plant filamentous material;
the smoke binding section is a cylinder made of polypropylene by adopting an extrusion method, and the water content of the smoke binding section is 2.9 percent by weight when the smoke binding section is detected by adopting the method described in the specification; a through-bore is provided in the cylinder parallel to its longitudinal axis. The side of the cross section of the smoke binding section is wavy; the edge of the cross section of the through hole is wavy.
The distance between the wall of the through hole and the outer wall of the smoke binding section is 2.1 mm. On the cross section of the smoke binding section, the ratio of the area of the straight through hole to the area of the non-straight through hole is 1.3.
The mean smoke temperature of the mainstream, mean lip temperature, mean smoke concentration and sensory evaluation of the example heated non-burning cartridges were measured according to the methods described in the specification of the present application, and the results of the measurements are shown in table 1.
Example 4: the invention relates to a plant silk type binary structure heating non-combustible product
The implementation of this example is as follows:
the plant silk type heating non-combustible product with the binary structure is formed by sequentially wrapping a smoke generation section and a smoke binding section which are made of plant silk materials containing glycerin smoke agents through polyimide of outer-layer wrapping paper, wherein the smoke binding section is a suction end.
Wherein the plant shred material is formed by rolling a mixture (weight ratio is 1:1) of expanded cut tobacco and expanded cut stem with the width of 2.1mm, and the filling rate of the mixture of the expanded cut tobacco and the expanded cut stem in a smoking section is 53 percent; the content of the glycerin smoke agent is 36 percent of the weight of the plant filamentous material;
the smoke binding section is a cylinder made of vinylidene chloride by adopting an extrusion method, and the water content of the smoke binding section is 2.2 percent by weight when the smoke binding section is detected by adopting the method described in the specification; a through-bore is provided in the cylinder parallel to its longitudinal axis. The side of the cross section of the smoke binding section is circular; the edge of the cross section of the through hole is wavy.
The distance between the wall of the through hole and the outer wall of the smoke binding section is 1.4 mm. On the cross section of the smoke binding section, the ratio of the area of the straight through hole to the area of the non-straight through hole is 1.6.
The mean smoke temperature of the mainstream, mean lip temperature, mean smoke concentration and sensory evaluation of the example heated non-burning cartridges were measured according to the methods described in the specification of the present application, and the results of the measurements are shown in table 1.
Example 5: the invention relates to a plant silk type binary structure heating non-combustible product
The implementation of this example is as follows:
the plant silk type heating non-combustible product with the binary structure is formed by sequentially wrapping a smoke generation section and a smoke binding section, wherein the smoke generation section is composed of plant silk materials containing a smoke generating agent of a mixture (weight ratio is 1:3) of glycerol and glycerol triacetate, and the smoke binding section is a suction end.
Wherein the plant silk material is formed by rolling 2.4 mm-wide betel nut shreds, and the filling rate of the betel nut shreds in the smoking section is 66%; the content of the mixture of glycerin and triacetyl glycerine as the smoke agent is 12% of the weight of the plant filamentous material;
the smoke binding section is a cylinder made of polylactic acid by adopting an extrusion method, and the water content of the smoke binding section is 3.2 percent by weight when the smoke binding section is detected by adopting the method described in the specification; a through-bore is provided in the cylinder parallel to its longitudinal axis. The side of the cross section of the smoke binding section is circular; the edge of the cross section of the through hole is in a sawtooth shape.
The distance between the wall of the through hole and the outer wall of the smoke binding section is 2.8 mm. On the cross section of the smoke binding section, the ratio of the area of the straight through hole to the area of the non-straight through hole is 0.8.
The mean smoke temperature of the mainstream, mean lip temperature, mean smoke concentration and sensory evaluation of the example heated non-burning cartridges were measured according to the methods described in the specification of the present application, and the results of the measurements are shown in table 1.
Example 6: the invention relates to a plant silk type binary structure heating non-combustible product
The implementation of this example is as follows:
the plant silk type heating non-combustible product with the binary structure is obtained by sequentially filling a smoke generation section and a smoke binding section, which are made of plant silk materials containing a smoke generating agent of a mixture (weight ratio is 2:1) of glycerol and glycerol diacetate, into a tube made of a silica gel material with the temperature resistance higher than 300 ℃; the smoke binding section is a suction end.
Wherein the plant silk material is formed by rolling a mixture (weight ratio is 1:1) of expanded cut tobacco stems and shredded mint with the width of 0.9mm, the filling rate of the mixture of the expanded cut tobacco stems and the shredded mint in a smoking section is 49%, and the content of the mixture of glycerol and glycerol diacetate in the smoking agent is 25% of the weight of the plant silk material;
the smoke binding section is a paper material cylinder, and the water content of the smoke binding section is 2.0% by weight by detection by the method described in the specification; a through-bore is provided in the cylinder parallel to its longitudinal axis. The side of the cross section of the smoke binding section is circular; the edge of the cross section of the through hole is wavy.
The distance between the wall of the through hole and the outer wall of the smoke binding section is 1.9 mm. On the cross section of the smoke binding section, the ratio of the area of the straight through hole to the area of the non-straight through hole is 0.6.
The mean smoke temperature of the mainstream, mean lip temperature, mean smoke concentration and sensory evaluation of the example heated non-burning cartridges were measured according to the methods described in the specification of the present application, and the results of the measurements are shown in table 1.
Table 1: the invention relates to a detection result of a plant silk type binary structure heating non-combustible product
Figure BDA0002964534240000101
Figure BDA0002964534240000111
The results listed in table 1 clearly show that the average temperature of the mainstream smoke of the non-combustible product heated by the plant silk binary structure is reduced by 6-8 ℃, the temperature of the smoke at the lip end is reduced by 5-7 ℃ and the difference of the smoke concentration is at least 19.9% compared with that of the HEETs sample of the control sample, and sensory evaluation results show that the smoke of the control sample is hot during smoking and is accompanied by a bit of stinging, the temperature at the lip end is also higher, the phenomenon does not exist in examples 1-6, the smoke temperature is generally lower than that of the smoke of the control sample, the smoke concentration is higher, and the smoking comfort is better than that of the control sample.

Claims (10)

1. A plant silk type heating non-combustible product with a binary structure is characterized in that the product is formed by wrapping a smoke generating section and a smoke binding section which are made of plant silk materials containing smoke generating agents through outer wrapping paper in sequence, or is obtained by sequentially filling the smoke generating section and the smoke binding section into a tube made of silica gel, paper or high polymer materials with the temperature higher than 300 ℃; the smoke binding section is a suction end.
2. A heated non-combustible article according to claim 1 characterised in that the plant thread material is a cured tobacco, tobacco stem, sun-cured tobacco or burley tobacco thread smoking material together with a mint, tea, areca or cocoa non-tobacco thread smoking material.
3. A heat-incombustible article according to claim 1 or 2, wherein the plant silk material is formed by rolling tobacco or non-tobacco silk having a width of 0.5 to 3.0mm, and has a filling rate of 40 to 80% in the smoking section.
4. A heat not burn article according to claim 1 characterised in that the smoke generating agent is one or more smoke generating agents selected from glycerol, propylene glycol, glycerol diacetate or glycerol triacetate.
5. A heated non-combustible article according to claim 4 characterised in that the smoke agent is present in an amount of 10 to 50% by weight of the plant silk material.
6. A heated non-combustible article according to claim 1 characterised in that the smoke-binding section is a cylinder of silicone rubber, polyethylene, polypropylene, vinylidene chloride, polylactic acid, polyurethane, cellulose acetate or paper material with through holes parallel to its longitudinal axis provided in the cylinder or between the cylinder and the outer paper wrapper.
7. A heated non-combustible article according to claim 1 characterised in that the sides of the cross-section of said flue gas confinement section are circular, serrated or wavy; the edge of the cross section of the through hole is circular, zigzag or wavy.
8. The non-combustible heated product according to claim 1, wherein when the through hole is located in the middle of the flue gas bound section, the distance between the wall of the through hole and the outer wall of the flue gas bound section is 1-3 mm.
9. A heated non-combustible article according to claim 1, characterised in that the ratio of the area of said through holes to the area of non-through holes is 0.3 to 2.0 in the cross section of said flue gas bound section.
10. A heated non-combustible article according to claim 1 characterised in that the water content of the flue gas bound stage is 2.0 to 4.0% by weight.
CN202110247253.9A 2021-03-05 2021-03-05 Plant silk type binary structure heating non-combustible product Pending CN112826150A (en)

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