CN104783321A - Mouth containing type smokeless tobacco product containing hop ingredient and preparation method of mouth containing type smokeless tobacco product containing hop ingredient - Google Patents
Mouth containing type smokeless tobacco product containing hop ingredient and preparation method of mouth containing type smokeless tobacco product containing hop ingredient Download PDFInfo
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- CN104783321A CN104783321A CN201510071948.0A CN201510071948A CN104783321A CN 104783321 A CN104783321 A CN 104783321A CN 201510071948 A CN201510071948 A CN 201510071948A CN 104783321 A CN104783321 A CN 104783321A
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- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
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Abstract
The invention relates to a mouth containing type smokeless tobacco product containing the hop ingredient. The mouth containing type smokeless tobacco product comprises, by weight, 20-50 parts of tobacco materials, 1-30 parts of hops or hop products, 0.5-5 parts of salt substance, 1-30 parts of a sweetening agent, 0.5-15 parts of a natural flavoring agent, 1-5 parts of a humectant, 0-10 parts of polybutene, 0.005-1 part of an antioxidant, 30-60 parts of water and an appropriate amount of an acidity regulator. Tobacco materials used in the mouth containing type smokeless tobacco product are processed through nicotine reducing and aroma enhancement, excitement of the product to the oral cavity and the stomach is reduced, the added hop ingredient gives the unique hop fragrance to the product, the taste quality of mouth containing tobaccos is improved, and the mouth containing type smokeless tobacco product is small in irritation and comfortable in taste.
Description
Technical field
The present invention relates to a kind of buccal smokeless tobacco product containing hops constituents and preparation method thereof, belong to smokeless tobacco art.
Background technology
Smoke-free tobacco product provides mainly through sucking, containing modes such as changing, chew the physiology satisfaction being similar to and sucking traditional cigarette goods to consumer, because smoke-free tobacco product does not burn in the process used, therefore can not produce the harmful components in cigarette smoke, it also avoid " second-hand-cigarette " harm to environment and human body.Smoke-free tobacco product can be divided into mouth type and nose type two class, and wherein buccal smokeless tobacco product is the best mouth type smoke-free tobacco product of current commercialization.
Mainly rely on flue gas different at pulmonary absorption with traditional cigarette, buccal smokeless tobacco product directly uses in oral cavity, has stronger excitant, cause comfortable taste degree lower to oral cavity, throat, esophagus, stomach etc.At present, buccal smokeless tobacco product is mainly for European & American Market research and development and produce, and domestic consumer there is no the consumption habit of this kind of smoke-free tobacco product.Therefore; be necessary the component to existing buccal smokeless tobacco product and technique proposition improvement; the shortcoming that its excitant is large to improving, comfortableness is poor; the characteristic buccal smokeless tobacco product meeting domestic consumer's taste custom of exploitation low irritant, high degree of comfort is an important directions of domestic novel tobacco goods development, has important function for the health of Protection of consumer and the marketing of buccal smokeless tobacco product.
CN1101077217A discloses one and adds in cigarette by Chinese herbal medicine, reduce the irritating method of flue gas, wherein Chinese herbal medicine can be hops, is first extracted by hops and obtains medicinal extract or volatile oil, again medicinal extract or volatile oil are added cigarette in proportion, realize reducing the irritating effect of flue gas.But, the method complex process, extract productive rate is low, and is difficult to complete reservation hops constituents and local flavor by the mode extracted; Lupulus extract is added buccal smokeless tobacco product simultaneously and also there are some problems, such as, the service time of buccal smokeless tobacco product is 30 minutes, therefore require that the active ingredient release in buccal smokeless tobacco product is evenly lasting, and directly add the release uniformity of volatile oil and persistence effect poor; Moreover hops, with certain bitter taste, needs the coordination being realized hops and tobacco by formula Design, thus brings exquisiteness, soft mouthfeel.
Summary of the invention
The object of the present invention is to provide a kind of buccal smokeless tobacco product containing hops constituents and preparation method thereof, it is higher that it has comfortable taste degree, stimulates less feature, and have unique hops fragrance.
For achieving the above object, the present invention adopts following technical scheme:
Containing a buccal smokeless tobacco product for hops constituents, by weight, comprise following raw material: tobacco-containing material 20-50 part; Hops or hops goods 1-30 part; Savory agent 0.5-5 part; Sweetener 1-30 part; Natural flavours 0.5-15 part; Humectant 1-5 part; Excipients 0-10 part; Antioxidant 0.005-1 part; Water 30-60 part; Acidity regulator is appropriate.
Preferably, described tobacco product, by weight, comprises following raw material: tobacco-containing material 20-30 part; Hops or hops goods 1-15 part; Savory agent 1-2 part; Sweetener 5-15 part; Natural flavours 1.5-5 part; Humectant 1-2 part; Excipients 1-3 part; Antioxidant 0.005-0.05 part; Water 35-55 part; Acidity regulator is appropriate.
Preferably, described hops to comprise in bitter type, odor type, bitter fragrant inclusive type hops the combination of one or more.Hops refers to the female inflorescence of Moraceae humulus plants hops, can be fresh hops or squeezing hops.Hops goods refer to the goods processed further by hops and obtain, and as hops powder, pellet hop, hop extract, hop tincture, hops wet goods, the cone of hops also can be used for making hops goods after drying.
Tobacco-containing material of the present invention is selected from the combination of one or more in flue-cured tobacco, air-curing of tobacco leaves, suncured tabacco; Wherein air-curing of tobacco leaves comprises the combination of one or more in burley tobaccos, Maryland, cigar etc.; The combination of one or more that suncured tabacco comprises in Dark sun-cured, Sun cured tobacco, Turkish tobaccos, makhorka etc.Different from the modulator approach of flue-cured tobacco, air-curing of tobacco leaves and suncured tabacco are processed mainly through the mode of airing, in the present invention, unless specified otherwise, air-curing of tobacco leaves and suncured tabacco are referred to as airing cigarette.Tobacco-containing material of the present invention is selected from the positions such as leaf, flower, stem, seed, products obtained therefrom after tobacco processing.
Preferably, described tobacco-containing material is at least containing the airing cigarette that Guizhou province produces.
Preferably, described savory agent is by regulating saline taste, cover and improve the bitter taste of tobacco material and hops, improve mouthfeel quality, comprise top grade table salt, Exposure to Sunlight fine salt, iodizedsalt, Cardia Salt, add selenium salt, add zinc salt, salt of enriching blood, the combination of one or more added in calcium salt, preventing decayed tooth salt, dimension B2 salt, nutritive salt.
Preferably, described sweetener is sugar or sugar-free sweetener, and by regulating sweet taste, balanced saline taste, covers and improve the bitter taste of tobacco material and hops, improves mouthfeel quality, comprises fructose, glucose, sucrose, maltose, hydrogenated starch hydrolysate, licorice powder, ammonium glycyrrhetate, glycyrrhizic acid one potassium and tripotassium, steviol glycoside, mogroside, Africa arrowroot glucin, honey, mannose, D-mannital, lactose, lactitol, xylitol, acesulfame potassium, knob is sweet, Aspartame, maltitol, D-sorbite, saccharin sodium, honey element, calcium cyclamate, Sucralose, alitame, isomaltoketose, antierythrite, isomalto-oligosaccharide, isomalt, galactooligosaccharide, milk ketose, FOS, gossypose, soyabean oligosaccharides, lactosucrose, xylo-oligosaccharide, inulooligosaccharide, Sucralose, glycyrrhizin, NHDC, curculin, miracle fruit thaumatin T, potato root of fangji glucin, two sweet, the combination of one or more in Arabinose.
Preferably, described acidity regulator is mainly used to the pH value regulating goods, control the release of nicotine and improve the mouthfeel of goods, comprising the combination of one or more in sodium carbonate, potash, sodium acid carbonate, saleratus, sodium pyrophosphate, dipotassium hydrogen phosphate, sodium hydrogen phosphate, calcium monohydrogen phosphate, tripotassium phosphate, tertiary sodium phosphate, potassium metapbosphate, natrium citricum, potassium citrate, gluconic acid sodium salt, diammonium hydrogen phosphate.
Preferably, described natural flavours is used for improving the fragrance mouthfeel of goods, comprise bergamot oil, currant absolute oil, buchu leaves oil, cassie absolute, ginger oil, absolute of jasmine, lavender oil, lemon oil, peppermint oil, menthol, orange oil, neroli oil, red date tincture, clove bud tincture, clove leaf oil, basil, tea perfume oil, patchouli oil, tagetes oil, hawthorn fruit tincture, cocoa tincture, dark plum tincture, black tea tincture, coffee tincture, FLOS CHRYSANTHEMI ALBA from Haizhou of China oil, cognac, mace oil, ground coffee, plum powder, red date powder, cocoa power, green tea powder, Herba Menthae powder, aloe extract, Honegsukle flower P.E, Lotus Leafextract, fruit extract or inspissated juice, the combination of one or more in Rum.
Preferably, described humectant is used for keeping the moisture in goods, comprises the combination of one or more in propane diols, glycerine, water-soluble plant polysaccharide, honey, polydextrose, maltitol pulp, sorbitol syrup.
Preferably, described excipients passes through thickening, the effect of cohering keeps the Stability Analysis of Structures of goods and sticky profit mouthfeel, comprise calcium carbonate, starch, phosphorylation PASELLI EASYGEL, sodium carboxymethyl starch, starch phosphate sodium, maltodextrin, cyclodextrin, microcrystalline cellulose, sodium carboxymethylcellulose, hydroxypropyl cellulose, methylcellulose, ethyl cellulose, HPMC, gelatin, Arabic gum, casein, chitin, chitosan, chitosan oligosaccharide and derivative, sodium alginate, propylene glycol alginate, tara gum, mannitol, D-sorbite, lactitol, guar gum, pectin, gloiopeltis glue, trigonella bean gum, locust bean gum, Sunset Abelmoschus Root glue, xanthans, cassia gum, carragheen, curdlan, soluble soybean polysaccharide, tamarind seed polysaccharide glue, pulullan polysaccharide, the combination of one or more in flaxseed gum.
Preferably, described antioxidant is used for preventing the oxidation deterioration of goods, improve the property stability of goods, comprise Tea Polyphenols, butylated hydroxy anisole, dibutyl hydroxy toluene, potassium metabisulfite, sodium pyrosulfite, sodium sulfite, sodium hydrogensulfite, vitamin C, vitamin E, Calcium Ascorbate, ascorbyl palmitate, D-araboascorbic acid and sodium salt thereof, n-propyl gallate, calcium lactate, sodium lactate, sorbic acid and sylvite thereof, disodium ethylene diamine tetraacetate, phytic acid and sodium salt, Licorice root antioxidant, AOB, ginkgo biloba extract, tea extract, the combination of one or more in grape seed extract.
Second aspect present invention provides a kind of preparation method of the buccal smokeless tobacco product containing hops constituents, comprises the steps:
1. sieve after drying tobacco material, pulverizing, obtain 20-100 object tobacco powder;
Or tobacco powder is made tobacco extract, tobacco extract composite powder.
2. be dissolved in deionized water by savory agent, sweetener, mix, at 60-100 DEG C, carry out steam treatment 2-24 hour with tobacco powder, tobacco extract or tobacco extract composite powder, cooling, equilibrium water conten to water content is 20-45%; Preferred steaming temperature is 70-90 DEG C;
3. by hops or hops goods with 2. in gained mixture mix, add acidity regulator, be adjusted to pH=5-9;
4. continue to add natural flavours, antioxidant, humectant, excipients, mix, control moisture in material and make it keep non-caking state;
5., after the process of material sterilization, packaging, two-stage sterilization process, packs and gets product.
Wherein, step 1. in, described tobacco extract is prepared from by following steps: by tobacco material after super-dry, pulverizing, by means such as supercritical extract, ultrasound on extracting, microwave auxiliary extraction or Simultaneous distillation-extraction, obtain the tobacco extract that solid content is greater than 35%.Gained tobacco extract mixes according to weight ratio 1:5-15 with capsule material, and in deionized water, strong stirring is dispersion liquid uniformly, is spray dried to tobacco extract composite powder in dispersion.
Step 1. in, also comprise and pretreatment carried out to tobacco-containing material, thus improve product mouthfeel and improve odor characteristic; Described pretreatment comprises one or more in the process of reduction nicotine, flavouring process or heat treatment.
The process of described reduction nicotine is specially: tobacco material is immersed in 10-50 doubly in 30-90 DEG C of water of raw material volume, be the citric acid of 0.5-2% or citrate etc. containing mass percent in described water, soak after 10-60 minute, filter moisture, dry at 40-150 DEG C to moisture be 3-10%.
Described flavouring process refers to that adopting conventional spice berry to decoct water is mixed with spice liquid or is mixed with spice liquid with flavouring agent, utilizes spice liquid to soak or infiltrates tobacco-containing material, or spice liquid is evenly sprayed at tobacco material surface.
Described heat treatment refers to carries out the processing procedures such as frying, baking/oven heat, infrared heating, heating using microwave by tobacco material.
The present invention the 3rd object is to provide a kind of purposes of the buccal smokeless tobacco product containing hops constituents.
The present invention by adding hops or hops goods in buccal smokeless tobacco product, be equipped with the components such as sweetener, savory agent, flavouring agent, make to act synergistically between each component, certain physiology satisfaction and comfortable mouthfeel are provided, also there is antibacterial anti-oxidant, tranquilizing and allaying excitement, stomach strengthening and digestion promoting, the effects such as preventing phlegm from forming and stopping coughing, can also bring unique hops fragrance to product simultaneously.The excitement of this product to mucous membrane of mouth, throat, esophagus, stomach lining significantly reduces, and not containing anticorrisive agent, is the novel buccal smokeless tobacco product of a kind of applicable domestic consumer.
Detailed description of the invention
Below by way of specific instantiation, embodiments of the present invention are described, those skilled in the art the content disclosed by this description can understand other advantages of the present invention and effect easily.The present invention can also be implemented or be applied by detailed description of the invention different in addition, and the every details in this description also can based on different viewpoints and application, carries out various modification or change not deviating under spirit of the present invention.
Notice, in the following example, the concrete process equipment that indicates or device all adopt conventional equipment in this area or device.
In addition should be understood that the one or more method steps mentioned in the present invention do not repel and can also to there is additive method step or can also insert additive method step before and after described combination step between these steps clearly mentioned, except as otherwise noted.In the present invention, airing cigarette is air-curing of tobacco leaves, suncured tabacco or the two mixing, and the two can arbitrary proportion combination.
Described in the present invention, each raw material is except specified otherwise, is existing disclosing and sells product.
Embodiment 1:
Weight ratio shared by each component is as follows: airing cigarette (produce by Guizhou, lower with) 20 parts, bitter type hops 5 parts, aroma hop 3 parts, table salt 1.5 parts, maltitol 10 parts, 2 parts, sodium carbonate, cherry fruit juice 1.5 parts, propane diols 1 part, potassium sorbate 0.02 part, Arabic gum 2 parts, water is 53.98 parts.
Implementation step is as follows:
1., the preparation of spice liquid: according to gardenia: after the ratio mixing of water weight ratio 1:30, fried 30 minutes, be cooled to 40-60 DEG C, add 5% honey and be modulated into spice liquid;
After utilizing spice liquid that airing cigarette is infiltrated 5-10 hour, put into baking oven, under 110 DEG C of conditions, be dried to moisture is 3-10%, and after pulverizing, screening, obtaining granularity is 30-50 object airing tobacco powder end.
2., by table salt, maltitol dissolve in deionized water, be sprayed onto on airing tobacco powder end, mix, steam treatment 15-20 hour at 70 DEG C, cooling, equilibrium water conten is to 20-45%.
3., by after aroma hop and bitter type hops removing impurity, room temperature air-flow dries, obtaining granularity after pulverizing, screening is 60-80 object hops powder, first bitter type hops powder is added step 2. in gained mixture, steam treatment 1 hour at 90 DEG C, then add aroma hop powder, continue steam treatment 30 minutes, cooling, adds aqueous sodium carbonate in material, regulates pH=5-9.
4. the cherry fruit juice, by concentrated, propane diols, potassium sorbate, Arabic gum are dispersed in 50 DEG C of deionized waters, are added in material, mix in agitator, and equilibrium water conten makes material keep non-caking state.
5., by after the process of material sterilization, pack by the specification of poisture-penetrability pouch according to every bag of 0.5g, two-stage sterilization, pack product.
Embodiment 2:
Weight ratio shared by each component is as follows: flue-cured tobacco 22.5 parts, airing cigarette 7.5 parts, 6 parts, fresh hops, add zinc salt 1 part, 5 parts, fructose, sodium acid carbonate 1 part, 2 parts, green tea powder, propane diols 2 parts, Tea Polyphenols 0.05 part, cyclodextrin 3 parts, and water is 49.95 parts.The content adding zinc gluconate in zinc salt is 20mg/kg.
Implementation step is as follows:
1., the preparation of spice liquid: be 0.5% buchu leaves oil by mass percent, 0.5% cassie absolute, 2% beta-schardinger dextrin-be dispersed in water, strong stirring 1-3 hour, makes spice liquid at 55 DEG C;
The aqueous citric acid solution of preparation mass percent 1%, flue-cured tobacco, airing cigarette are immersed in the citric acid solution of 50 times of volumes, soak 1 hour at 80 DEG C, remove soak with drier, putting into baking oven, under 110 DEG C of conditions, be dried to moisture be 3-10%, pulverizes, screening, obtaining order granularity is 50-70 object tobacco powder, spice liquid is evenly sprayed in tobacco powder, is as the criterion not lump, equilibrium water conten.
2., will add zinc salt, fructose liquid dissolve in deionized water, be sprayed on tobacco powder, after mixing at 75 DEG C steam treatment 10-15 hour, coolant seal, equilibrium water conten is to 20-45%.
3., by draft beer flower through freeze drying, pulverize, sieve, obtaining granularity is 60-80 object draft beer pollen end, fully mixes with the mixture after steam treatment, adds sodium acid carbonate and regulates pH=5-9.
4., by green tea powder, propane diols, Tea Polyphenols, cyclodextrin be dispersed in 45 DEG C of deionized waters, stir, to add in material and to mix, control moisture in material and make it keep non-caking state.
5., by after the process of material sterilization, pack by the specification of poisture-penetrability pouch according to every bag of 0.5g, two-stage sterilization, pack product.
Embodiment 3:
Weight ratio shared by each component is as follows: flue-cured tobacco 15 parts, airing cigarette 5 parts, Turkish tobaccos 5 parts, pellet hop 15 parts, iodizedsalt 1 part, xylitol 10 parts, steviol glycoside 0.02 part, natrium citricum 1 part, red date powder 3 parts, glycerine 1 part, Licorice root antioxidant 0.01 part, sodium alginate 1 part, water is 42.97 parts.The content of determination of iodine in salt adding iodine acid potassium is 30mg/kg.
Implementation step is as follows:
1., by 15-30 minute in flue-cured tobacco, airing cigarette mixing immersion 50 times of volumes, 90-100 DEG C deionized water, drier is utilized to remove moisture, put into baking oven, under 60-100 DEG C of condition, be dried to moisture is 3-10%, and taking granularity after crushing and screening is 60-80 object tobacco powder; Tobacco powder is put into baking box, heat treatment 1-2 hour at 110-160 DEG C;
Turkish tobaccos being put into baking oven, under 40 DEG C of conditions, be dried to moisture be 3-10%, and crushing and screening granularity is 60-80 object tobacco powder, puts into baking oven, and heat treatment 30-60 minute at 90-120 DEG C, obtains Turkish tobaccos powder;
By the step 1. each tobacco powder mixing of gained.
2., by iodizedsalt, xylitol, steviol glycoside dissolve in deionized water, be sprayed at step 1. on gained tobacco powder, after mixing at 80 DEG C steam treatment 8-10 hour, then take out coolant seal, equilibrium water conten is to 20-45%.
3., pellet hop is pulverized after, mix with tobacco powder, add natrium citricum, mix in agitator regulate pH=5-9.
4., by red date powder, glycerine, Licorice root antioxidant, sodium alginate be dispersed in 40 DEG C of deionized waters, stir, add in material, mix, control moisture in material and make it keep non-caking state.
5., by after the process of material sterilization, pack by the specification of poisture-penetrability pouch according to every bag of 0.8g, two-stage sterilization, pack product.
Embodiment 4:
Weight ratio shared by each component is as follows: tobacco extract composite powder 28 parts, pellet hop 10 parts, hop tincture 1 part, Cardia Salt 1 part, isomalt 6 parts, isomalto-oligosaccharide 4 parts, Momordia grosvenori aglycone 0.01 part, gluconic acid sodium salt 2 parts, coffee tincture 2 parts, glycerine 1 part, AOB 0.005 part, sodium carboxymethylcellulose 2 parts, water is 42.985 parts.Potassium chloride containing 20% weight ratio in Cardia Salt.
Implementation step is as follows:
1., by flue-cured tobacco, Turkish tobaccos dry at 40-60 DEG C respectively, according to flue-cured tobacco: Turkish tobaccos weight ratio 9:1 mixes, pulverizing, utilizes ultrasonic wave added solvent extraction method to obtain tobacco extract; Add in deionized water by tobacco extract, beta-schardinger dextrin-, gelatin by weight 1:5:2 again, strong stirring is dispersion liquid uniformly, and namely spraying dry obtains tobacco extract composite powder.
2., by Cardia Salt, isomalt, isomalto-oligosaccharide, Momordia grosvenori aglycone, gluconic acid sodium salt dissolve in deionized water, fully mix with smoking mixture extract composite powder,
3. after, by pellet hop grinding to form 60-80 order powder, by pellet hop powder, hop tincture and step 2. gained mixture mix, add acidity regulator to pH=5-9;
4., by coffee tincture, glycerine, AOB, sodium carboxymethylcellulose dispersion in deionized water, be sprayed onto on material, mix, control moisture in material and make it keep non-caking state;
5., by after the process of material sterilization, pack by the specification of poisture-penetrability pouch according to every bag of 0.8g, two-stage sterilization, pack product.
Comparative example 1:
Adopt the method identical with embodiment 1 to prepare tobacco product, difference is only:
(1) tobacco-containing material is replaced with flue-cured tobacco, addition is 28 parts;
(2) hops or hops goods are not added;
(3) 1. step does not carry out flavouring process;
(4) flue-cured tobacco is put into baking oven, under 110-140 DEG C of condition, be dried to moisture is 3-10%.Pulverized by dried tobacco-containing material, screening obtains 30-50 object tobacco powder.
Sensory quality assessment
Buccal smokeless tobacco product prepared by embodiment 1-4 and comparative example is carried out sensory quality assessment, and method is as follows.
(1) evaluation index
This sensory quality assessment method arranges 9 evaluation indexes altogether, comprise entrance mouthfeel, physiological strength, feature be fragrant, tobacco is fragrant, excitement, comfort, release uniformity, release persistence and oral cavity pleasant impression.
The particular content of every evaluation index is as follows:
Entrance mouthfeel refers to: after buccal smokeless tobacco product puts into oral cavity, the initial synthetic impression of the taste and smell of user.
Physiological strength refers to: in use, the physiology satisfaction that user experiences, i.e. strength.
Feature perfume (or spice) refers to: in use, the amount of the characteristic perfume that user experiences and matter.
Tobacco perfume (or spice) refers to: in use, the amount of this perfume (or spice) of tobacco that user experiences and matter.
Excitement refers to: in use, and the positions such as user oral cavity, nasal cavity, throat, esophagus are experienced the discomfort such as pungent, dry and are subject to.
Comfort refers to: in use, smell coordination that user experiences, soft and moist sense, without the impression of the fragrance such as residue foreign body sensation.
Release uniformity refer to: in use, user experience the release stability in time such as fragrance, physiological strength.
Release persistence refers to: in use, user experiences the duration such as fragrance, physiological strength length.
Oral cavity pleasant impression refers to: after use procedure, the comprehensive impression of the taste and smell that user oral cavity is remaining.
(2) score principle
The score principle of indices is: evaluation index is divided into 6 grades, every shared weight and code of points as shown in table 1, minimum score unit is 0.5 point.Lower point of each score interval is not included in this section of score.Excitement is stronger, and score is lower; The impression of entrance mouthfeel, oral cavity pleasant impression is better, and score is higher; Sundry item experiences stronger, and score is higher; Final score is added by the arithmetic of each subitem score and is obtained.Total score score is higher, then represent that the sensory quality assessment effect of this buccal smokeless tobacco product is better.
Score value and the score of table 1 buccal smokeless tobacco product sensory quality assessment index are interval
(3) evaluation method
The team of smokeing panel test comprising at least 7 members of smoking is set, everyone a buccal smokeless tobacco product sensory quality assessment table, adopt the marking mode secretly commented, sensory evaluation is carried out to buccal smokeless tobacco product, according to weight and the code of points of 9 sensory quality assessment indexs in table 1, member of smoking tackles every evaluation index and carries out sensory quality assessment, and records its evaluation result.
In the score of every sensory quality assessment index, remove one minimum point and a best result, remain be divided into effective point, calculate the arithmetic mean of instantaneous value effectively divided and be single item evaluation index score, result reservation two-decimal; The arithmetic mean of instantaneous value of each single index scoring adds the sensory quality assessment integrate score being buccal smokeless tobacco product with total score, and result retains two-decimal.Total score score value is higher, then represent that the sensory evaluation effect of this buccal smokeless tobacco product is better.
Concrete outcome is as shown in table 2:
Table 2 is containing the sensory evaluation index comparing result of the buccal smokeless tobacco product of hops constituents
Found by sensory evaluation, contain the buccal smokeless tobacco product of hops constituents in above-described embodiment compared with comparative example, improve oral cavity comfort level, excitant is little, and has unique hops fragrance, and fragrance release is lasting, with embodiment 1 best results.
Although above the present invention is described in detail with a general description of the specific embodiments, on basis of the present invention, can make some modifications or improvements it, this will be apparent to those skilled in the art.Therefore, these modifications or improvements without departing from theon the basis of the spirit of the present invention, all belong to the scope of protection of present invention.
Claims (10)
1., containing a buccal smokeless tobacco product for hops constituents, it is characterized in that, by weight, comprise following raw material: tobacco-containing material 20-50 part; Hops or hops goods 1-30 part; Savory agent 0.5-5 part; Sweetener 1-30 part; Natural flavours 0.5-15 part; Humectant 1-5 part; Excipients 0-10 part; Antioxidant 0.005-1 part; Water 30-60 part; Acidity regulator is appropriate.
2. buccal smokeless tobacco product according to claim 1, is characterized in that, by weight, comprises following raw material: tobacco-containing material 20-30 part; Hops or hops goods 1-15 part; Savory agent 1-2 part; Sweetener 5-15 part; Natural flavours 1.5-5 part; Humectant 1-2 part; Excipients 1-3 part; Antioxidant 0.005-0.05 part; Water 35-55 part; Acidity regulator is appropriate.
3. buccal smokeless tobacco product according to claim 1 and 2, is characterized in that, described hops be selected from bitter type, odor type, bitter fragrant inclusive type hops one or more.
4. buccal smokeless tobacco product according to claim 1 and 2, is characterized in that, described hops refers to the female inflorescence of Moraceae humulus plants hops, comprises fresh hops and squeezing hops.
5. buccal smokeless tobacco product according to claim 1 and 2, it is characterized in that, described hops goods refer to be processed into further by the cone of hops or hops hops powder, pellet hop, hop extract, hop tincture, the combination of one or more in hop oil.
6. buccal smokeless tobacco product according to claim 1, is characterized in that, described tobacco-containing material is selected from the combination of one or more in flue-cured tobacco, air-curing of tobacco leaves, suncured tabacco;
Preferably, described air-curing of tobacco leaves is selected from the combination of one or more in burley tobaccos, Maryland, cigar; The one or more combination that suncured tabacco is selected from Dark sun-cured, Sun cured tobacco, Turkish tobaccos, makhorka;
Described tobacco-containing material is selected from leaf, flower, stem, seed position, and through tobacco processing after products obtained therefrom;
Further preferably, described tobacco-containing material is at least containing the airing cigarette that Guizhou province produces.
7. the buccal smokeless tobacco product according to any one of claim 1-6, it is characterized in that, described savory agent is selected from table salt, Exposure to Sunlight fine salt, iodizedsalt, Cardia Salt, adds selenium salt, adds zinc salt, salt of enriching blood, the combination of one or more added in calcium salt, preventing decayed tooth salt, dimension B2 salt, nutritive salt;
Described sweetener is selected from fructose, glucose, sucrose, maltose, hydrogenated starch hydrolysate, licorice powder, ammonium glycyrrhetate, glycyrrhizic acid one potassium and tripotassium, steviol glycoside, mogroside, Africa arrowroot glucin, honey, mannose, D-mannital, lactose, lactitol, xylitol, acesulfame potassium, knob is sweet, Aspartame, maltitol, D-sorbite, saccharin sodium, honey element, calcium cyclamate, Sucralose, alitame, isomaltoketose, antierythrite, isomalto-oligosaccharide, isomalt, galactooligosaccharide, milk ketose, FOS, gossypose, soyabean oligosaccharides, lactosucrose, xylo-oligosaccharide, inulooligosaccharide, Sucralose, glycyrrhizin, NHDC, curculin, miracle fruit thaumatin T, potato root of fangji glucin, two sweet, the combination of one or more in Arabinose,
Described flavouring agent is selected from bergamot oil, currant absolute oil, buchu leaves oil, cassie absolute, ginger oil, absolute of jasmine, lavender oil, lemon oil, peppermint oil, menthol, orange oil, neroli oil, red date tincture, clove bud tincture, clove leaf oil, basil, tea perfume oil, patchouli oil, tagetes oil, hawthorn fruit tincture, cocoa tincture, dark plum tincture, black tea tincture, coffee tincture, FLOS CHRYSANTHEMI ALBA from Haizhou of China oil, cognac, mace oil, ground coffee, plum powder, red date powder, cocoa power, green tea powder, Herba Menthae powder, aloe extract, Honegsukle flower P.E, Lotus Leafextract, fruit extract or inspissated juice, the combination of one or more in Rum,
Described acidity regulator is selected from the combination of one or more in sodium carbonate, potash, sodium acid carbonate, saleratus, sodium pyrophosphate, dipotassium hydrogen phosphate, sodium hydrogen phosphate, calcium monohydrogen phosphate, tripotassium phosphate, tertiary sodium phosphate, potassium metapbosphate, natrium citricum, potassium citrate, gluconic acid sodium salt, diammonium hydrogen phosphate;
Described humectant is selected from the combination of one or more in propane diols, glycerine, water-soluble plant polysaccharide, honey, polydextrose, maltitol pulp, sorbitol syrup;
Described antioxidant is selected from Tea Polyphenols, butylated hydroxy anisole, dibutyl hydroxy toluene, potassium metabisulfite, sodium pyrosulfite, sodium sulfite, sodium hydrogensulfite, vitamin C, vitamin E, Calcium Ascorbate, ascorbyl palmitate, D-araboascorbic acid and sodium salt thereof, n-propyl gallate, calcium lactate, sodium lactate, sorbic acid and sylvite thereof, disodium ethylene diamine tetraacetate, phytic acid and sodium salt, Licorice root antioxidant, AOB, ginkgo biloba extract, tea extract, the combination of one or more in grape seed extract,
Described excipients is selected from calcium carbonate, starch, phosphorylation PASELLI EASYGEL, sodium carboxymethyl starch, starch phosphate sodium, maltodextrin, cyclodextrin, microcrystalline cellulose, sodium carboxymethylcellulose, hydroxypropyl cellulose, methylcellulose, ethyl cellulose, HPMC, gelatin, Arabic gum, casein, chitin, chitosan, chitosan oligosaccharide and derivative, sodium alginate, propylene glycol alginate, tara gum, mannitol, D-sorbite, lactitol, guar gum, pectin, gloiopeltis glue, trigonella bean gum, locust bean gum, Sunset Abelmoschus Root glue, xanthans, cassia gum, carragheen, curdlan, soluble soybean polysaccharide, tamarind seed polysaccharide glue, pulullan polysaccharide, one or more combination in flaxseed gum.
8. the preparation method of the tobacco product described in any one of claim 1-7, is characterized in that, comprises the steps:
1. sieve after drying tobacco material, pulverizing, obtain 20-100 object tobacco powder;
Or tobacco powder is made tobacco extract, tobacco extract composite powder further;
2. be dissolved in deionized water by savory agent, sweetener, mix, at 60-100 DEG C, carry out steam treatment 2-24 hour with tobacco powder, tobacco extract or tobacco extract composite powder, cooling, equilibrium water conten to water content is 20-45%; Preferred steaming temperature is 70-90 DEG C;
3. by hops or hops goods with 2. in gained mixture mix, add acidity regulator, be adjusted to pH=5-9;
4. continue to add natural flavours, antioxidant, humectant, excipients, mix, control moisture in material and make it keep non-caking state;
5., after the process of material sterilization, packaging, two-stage sterilization process, packs and gets product.
9. preparation method according to claim 8, it is characterized in that, step 1. in, described tobacco extract be by tobacco material through super-dry, pulverize after, by supercritical extract, ultrasound on extracting, microwave auxiliary extraction or Simultaneous distillation-extraction means, obtain the tobacco extract that solid content is greater than 35%;
Gained tobacco extract mixes according to weight ratio 1:5-15 with capsule material, and in deionized water, strong stirring is dispersion liquid uniformly, is spray dried to tobacco extract composite powder in dispersion.
10. preparation method according to claim 8, is characterized in that, step 1. in also comprise pretreatment carried out to tobacco-containing material, described pretreatment comprises one or more that reduce in nicotine process, flavouring process or heat treatment;
Wherein, the process of described reduction nicotine is specially: tobacco material is immersed in 10-50 doubly in 30-90 DEG C of water of raw material volume, be the citric acid of 0.5-2% or citrate etc. containing mass percent in described water, soak after 10-60 minute, filter moisture, dry at 40-150 DEG C to moisture be 3-10%;
Described flavouring process refers to that adopting conventional spice berry to decoct water is mixed with spice liquid or is mixed with spice liquid with flavouring agent, utilizes spice liquid to soak or infiltrates tobacco-containing material, or spice liquid is evenly sprayed at tobacco material surface;
Described heat treatment refers to carries out the processing procedures such as frying, baking/oven heat, infrared heating, heating using microwave by tobacco material.
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