CN101705149A - Tobacco essence and preparation method thereof - Google Patents
Tobacco essence and preparation method thereof Download PDFInfo
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- CN101705149A CN101705149A CN200910110168A CN200910110168A CN101705149A CN 101705149 A CN101705149 A CN 101705149A CN 200910110168 A CN200910110168 A CN 200910110168A CN 200910110168 A CN200910110168 A CN 200910110168A CN 101705149 A CN101705149 A CN 101705149A
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Abstract
The invention belongs to the technical field of tobacco additive, and relates to tobacco essence and a preparation method thereof. The tobacco essence comprises the following components in percentage by weight: 4.5 to 7.5 percent of tamarind extract, 1.5 to 4.5 percent of mimetic citronella extract, 0.5 to 1.5 percent of dried plum extract, 16.5 to 19.5 percent of liquid glucose, 4.5 to 7.5 percent of Maillard reactant, 8.5 to 11.5 percent of xylitol (liquid), 5.5 to 8.5 percent of natural juice acid, 2.5 to 5.5 percent of hops tincture, 2.5 to 5.5 percent of tobacco B-type extract, 0.1 to 0.5 percent of vanilline, 16 to 20 percent of propanediol, 5 to 8 percent of alcohol, 4.5 to 7.5 percent of drug flavor aromatic base and the balance of water. The drug flavor aromatic base comprises 20 to 30 percent of sage clary oil, 20 to 30 percent of pineapple ketone, 20 to 30 percent of guaiacol and 10 to 40 percent of alcohol.
Description
[technical field]
The invention belongs to the tobacco additive agent technical field, relate to a kind of tobacco aromatics using and preparation method thereof.
[background technology]
Flavouring essence for tobacco is redeployed by multiple spices, has certain odor type, can be directly used in the mixture of tobacco flavoring.
Plant fruit flavour type essence occupies certain market share in flavouring essence for tobacco market, major customer crowd is the women smoker, but raising along with people's living standard, taste to cigarette has had higher requirement, the increasing male sex has produced interest to this kind of plant fruit flavour type cigarette, so the demand of plant fruit flavour type flavouring essence for tobacco on market constantly enlarges.
Traditional technology prepares plant fruit flavour type tobacco aromatics using and allocates with natural plant pefume and synthetics mostly, the spices that makes with this method, because technology is fairly simple, simultaneously because the restriction of perfume material, there is the fragrance dullness in the spices of gained, and fragrance is not true to nature, and is poor to the property improved of tobacco, fragrance time length while is short, and mouthfeel is not good after sucking.
[summary of the invention]
The present invention proposes prescription of a kind of tobacco aromatics using that has the plant fruital newly and preparation method thereof in order to solve the existing deficiency of present conventional art.Flavouring essence for tobacco fragrance with the compound fruital of plant provided by the invention is true to nature, and lasting fragrance, can give out pleasant delicate fragrance and sweet taste, and is good to the modification of tobacco, eliminated the assorted flavor of tobacco, and mouthfeel is better.
Concrete technical scheme of the present invention is as follows:
A kind of flavouring essence for tobacco, its component and each percentages of ingredients (weight percent) content are:
Tamarind medicinal extract 4.5%～7.5%;
Imitative Mao Xiang medicinal extract 1.5%～4.5%;
Smoked plum medicinal extract 0.5%～1.5%;
Liquid Glucose 16.5%～19.5%;
Maillard reaction thing 4.5%～7.5%;
Xylitol (liquid) 8.5%～11.5%;
Straight juice acid 5.5%～8.5%;
Hops tincture 2.5%～5.5%;
Tobacco Type B extract 2.5%～5.5%;
Vanillin food grade,1000.000000ine mesh 0.1%～0.5%;
Propylene glycol 16%～20%;
Alcohol 5%～8%;
Flavour of a drug perfume base 4.5%～7.5%;
Surplus is a water.
Preferably, each components contents of described essence is:
Tamarind medicinal extract 6.5%;
Imitative Mao Xiang medicinal extract 2.5%;
Smoked plum medicinal extract 1.5%;
Liquid Glucose 17.5%;
Maillard reaction thing 6.5%;
Xylitol (liquid) 9.5%;
Straight juice acid 7.5%;
Hops tincture 3.5%;
Tobacco Type B extract 4.5%;
Vanillin food grade,1000.000000ine mesh 0.3%;
Propylene glycol 18.5%;
Alcohol 6.2%;
Flavour of a drug perfume base 6.5%;
Water 9%.
Described flavour of a drug perfume base comprises Salvia Sclare L.oil, pineapple ketone, methyl catechol and alcohol, and wherein each components contents is respectively:
Salvia Sclare L.oil 20%～30%;
Pineapple ketone 20%～30%;
Methyl catechol 20%～30%;
Alcohol 10%～40%.
Preferably, each components contents in the described flavour of a drug perfume base is:
Salvia Sclare L.oil 21%;
Pineapple ketone 25%;
Methyl catechol 22%;
Alcohol 32%.
The present invention also provides a kind of preparation method of essence as mentioned above, and the concrete steps of method are as follows:
(1) it is standby accurately to take by weighing each component according to above-mentioned each percentages of ingredients content;
(2) propylene glycol the joining in the reactor that tobacco Type B extract is housed slowly under hand mixing that take a morsel, treat that tobacco Type B extract dissolves fully after, add vanillin food grade,1000.000000ine mesh again, stir;
(3) the Maillard reaction thing is heated to 95 ℃ after, treat after it fuses fully it to be joined in the reactant of above-mentioned steps (2), continue to stir;
(4) propylene glycol, water and the flavour of a drug perfume base with remainder mixes in the back reactant that adds in the above-mentioned steps (3), continues to stir;
(5) alcohol, Xylitol (liquid), Liquid Glucose and tamarind medicinal extract are mixed the back and add in the reactant of above-mentioned steps (4), continue to stir;
(6) under condition of stirring, will imitate in the reactant of Mao Xiang medicinal extract, smoked plum medicinal extract, straight juice acid and hops tincture adding above-mentioned steps (5), and continue heated and stirred then and refluxed 30 minutes;
(7) stop to reflux, continue to stir after 30 minutes, leave standstill and made finished product in 24 hours.
Wherein, it is as follows to produce the step of flavour of a drug essence:
(1) it is standby to take by weighing each component according to each percentages of ingredients content of flavour of a drug essence;
(2) Salvia Sclare L.oil, pineapple ketone, methyl catechol and alcohol are added in the proportion container in order one by one, the dissolving that stirs gets final product.
Flavour of a drug perfume base of the present invention adopts Salvia Sclare L.oil, pineapple ketone, methyl catechol and alcohol to mix.
Wherein, Salvia Sclare L.oil is colourless or weak yellow liquid, have medicinal herbs, delicate fragrance, the banksia rose, Xin Xiang and oranges and tangerines fragrance, main component is phanteine, phantol, Geraniol, Terpineol 350, nerolidyl acetate and sclareol, is used for tobacco and can obviously improves bitter taste in the tobacco;
Pineapple ketone is called for short furanone, is the main component of pineapple furans spices, and it has unique caramel fruital flavor and the effect of intensive flavouring, is the flavoring pineapple essence that is widely used in tobacco industry;
Methyl catechol is yellow to deep yellow liquid, has special fragrant and sweet fragrance, and phenol flavor slightly can be miscible with alcohol, is a kind of spices with Moschus, has the effect of antibiotic and sterilizing simultaneously.
Above-mentioned flavour of a drug perfume base is exactly obviously to reduce assorted flavors such as bilgy odour in the tobacco and bitter taste in the effect of this flavouring essence for tobacco, after having eliminated the various assorted flavor in the tobacco, be aided with following various spices, making essence of the present invention have the fragrant and sweet flavor of plant with plant fruital.
The feature of other spices that the present invention adds is as follows:
Tamarind medicinal extract is natural monomer perfume, has the mixing breath of camerlsed and sour-sweet perfume (or spice), can strengthen fragrant and sweet note with this spices as the prescription of this essence, improves mouthfeel and the pleasant impression of tobacco simultaneously;
Imitative Mao Xiang medicinal extract is mainly used in and improves cigarette odor-absorbing, regulates and swashs property, alleviates assorted gas, and can enrich flue gas, promotes pure and fresh and natural flavor;
Smoked plum medicinal extract has sour-sweet flavor, can increase the sour-sweet interest sense of tobacco;
Glucose and Xylitol all are the sweeting agents in the foodstuff additive, and Xylitol also has cooling taste, are added in the cigarette with these two kinds of spices, can obviously improve the mouthfeel of tobacco;
Straight juice acid has the foodstuff additive of sour-sweet flavor, can make the sweet tart flavour of essence of the present invention denseer;
Hops tincture is a yellow liquid, and main component has humulone, lupulone etc., and it has simple and elegant hops perfume (or spice), can be used for the fragrant coordination of cigarette, relaxes the sharp flavor of tobacco;
Tobacco Type B extract has the natural style of tobacco, adds tobacco Type B extract component in the present invention in described perfume formulation and can replenish tobacco inherent feature natural style, and can justify and cigarette perfume (or spice);
Vanillin food grade,1000.000000ine mesh is a synthon spices, has the dense fragrant and sweet and slight butterfat perfume (or spice) of the blue beans of tangible similar folder, uses in this prescription and can produce slighter sweet creamy;
Propylene glycol and alcohol are as the thinner and the solvent of monomer perfume, and simultaneously, alcohol is volatile solvent, is composition common in the perfume formulation, and fragrance is evaporated.
The present invention with the flavour of a drug perfume base as the fragrance basis, on the basis, increase other and multiplely have the spices of diverse fragrant flavour and sweet taste as auxiliary material, various component according to above-mentioned specific mixed together, formed a spice mixt with specific fragrance, it can be coordinated with this perfume of tobacco preferably, and fragrance gracefulness, plentiful.
The proportioning of above-mentioned various spices is the more satisfactory situations that obtain in through test of many times and allocation process, select for use above-mentioned multiple raw material monomer to coordinate mutually simultaneously, can form and have multiple compound fragrance, delicate fragrance with cream perfume (or spice), the fragrance of a flower and fruital, have compound tastes such as tart flavour, sweet taste and cooling taste simultaneously, such essence can obviously improve the mouthfeel of tobacco, has removed the bitter taste in the tobacco.
The present invention has adopted the Maillard reaction thing in the process of producing essence, the Maillard reaction thing is the reacted product of carbohydrate and amino acid, have fragrance and sweet taste, in this prescription, this Maillard reaction owner will play catalyzer and function of stabilizer, make the fragrance precipitation and the slaking of essence, fragrance is lasting and true to nature more.
After stirring is finished, left standstill 24 hours simultaneously, make the fragrance intermingling precipitation and the slaking of multiple spices, make fragrance more mellow and fuller, fragrance is more lasting.
[embodiment]
The invention provides a kind of flavouring essence for tobacco and preparation method thereof, the invention will be further elaborated and explanation below in conjunction with embodiment:
Embodiment 1
A kind of flavouring essence for tobacco makes by following steps:
(1) preparation 18g flavour of a drug perfume base is standby, the preparation method of this flavour of a drug perfume base is as follows: accurate weighing Salvia Sclare L.oil 3.6g, pineapple ketone 3.6g, methyl catechol 3.6g and 7.2g alcohol, then above-mentioned each component is added in the proportion container in order one by one and stir, get final product stand for standby use up to the whole dissolvings of each component.
(2) it is standby accurately to take by weighing each component according to following each components contents;
Tamarind medicinal extract 18g;
Imitative Mao Xiang medicinal extract 18g;
Smoked plum medicinal extract 2g;
Liquid Glucose 78g;
Maillard reaction thing 18g;
Xylitol (liquid) 46g;
Straight juice acid 22g;
Hops tincture 22g;
Tobacco Type B extract 10g;
Vanillin food grade,1000.000000ine mesh 2g;
Propylene glycol 64g;
Alcohol 32g;
Water 50g.
(3) get 10g propylene glycol joining in the reactor that tobacco Type B extract is housed slowly under hand mixing, treat that tobacco Type B extract dissolves fully after, add vanillin food grade,1000.000000ine mesh again, stir;
(4) the Maillard reaction thing is heated to 95 ℃ after, treat after it fuses fully it to be joined in the reactant of above-mentioned steps (3), continue to stir;
(5) propylene glycol, water and the flavour of a drug perfume base with remainder mixes in the back reactant that adds in the above-mentioned steps (4), continues to stir;
(6) alcohol, Xylitol (liquid), Liquid Glucose and tamarind medicinal extract are mixed the back and add in the reactant of above-mentioned steps (5), continue to stir;
(7) under condition of stirring, will imitate in the reactant of Mao Xiang medicinal extract, smoked plum medicinal extract, straight juice acid and hops tincture adding above-mentioned steps (6), continue heated and stirred then 15 minutes;
(8) stop to reflux, continue to stir after 30 minutes, leave standstill and made finished product in 24 hours.
Prepare the 400g flavouring essence for tobacco by above-mentioned steps, wherein in this essence, each percentages of ingredients content is as follows:
Tamarind medicinal extract 4.5%;
Imitative Mao Xiang medicinal extract 4.5%;
Smoked plum medicinal extract 0.5%;
Liquid Glucose 19.5%;
Maillard reaction thing 4.5%;
Xylitol (liquid) 11.5%;
Straight juice acid 5.5%;
Hops tincture 5.5%;
Tobacco Type B extract 2.5%;
Vanillin food grade,1000.000000ine mesh 0.5%;
Propylene glycol 16%;
Alcohol 8%;
Flavour of a drug perfume base 4.5%;
Water 12.5%.
Each the percentages of ingredients content that wherein is used to prepare the flavour of a drug perfume base is respectively:
Salvia Sclare L.oil 20%;
Pineapple ketone 20%;
Methyl catechol 20%;
Alcohol 40%.
Embodiment 2
A kind of flavouring essence for tobacco makes by following steps:
(1) preparation 30g flavour of a drug perfume base is standby, the preparation method of this flavour of a drug perfume base is as follows: accurate weighing Salvia Sclare L.oil 9g, pineapple ketone 9g, methyl catechol 9g and 3g alcohol, then above-mentioned each component is added in the proportion container in order one by one and stir, get final product stand for standby use up to the whole dissolvings of each component.
(2) it is standby accurately to take by weighing each component according to following each components contents;
Tamarind medicinal extract 30g;
Imitative Mao Xiang medicinal extract 6g;
Smoked plum medicinal extract 6g;
Liquid Glucose 66g;
Maillard reaction thing 30g;
Xylitol (liquid) 34g;
Straight juice acid 34g;
Hops tincture 10g;
Tobacco Type B extract 22g;
Vanillin food grade,1000.000000ine mesh 0.4g;
Propylene glycol 80g;
Alcohol 20g;
Water 31.6g.
(3) get 15g propylene glycol joining in the reactor that tobacco Type B extract is housed slowly under hand mixing, treat that tobacco Type B extract dissolves fully after, add vanillin food grade,1000.000000ine mesh again, stir;
(4) the Maillard reaction thing is heated to 95 ℃ after, treat after it fuses fully it to be joined in the reactant of above-mentioned steps (3), continue to stir;
(5) propylene glycol, water and the flavour of a drug perfume base with remainder mixes in the back reactant that adds in the above-mentioned steps (4), continues to stir;
(6) alcohol, Xylitol (liquid), Liquid Glucose and tamarind medicinal extract are mixed the back and add in the reactant of above-mentioned steps (5), continue to stir;
(7) under condition of stirring, will imitate in the reactant of Mao Xiang medicinal extract, smoked plum medicinal extract, straight juice acid and hops tincture adding above-mentioned steps (6), continue heated and stirred then 15 minutes;
(8) stop to reflux, continue to stir after 30 minutes, leave standstill and made finished product in 24 hours.
Prepare the 400g flavouring essence for tobacco by above-mentioned steps, wherein in this essence, each percentages of ingredients content is as follows:
Tamarind medicinal extract 7.5%;
Imitative Mao Xiang medicinal extract 1.5%;
Smoked plum medicinal extract 1.5%;
Liquid Glucose 16.5%;
Maillard reaction thing 7.5%;
Xylitol (liquid) 8.5%;
Straight juice acid 8.5%;
Hops tincture 2.5%;
Tobacco Type B extract 5.5%;
Vanillin food grade,1000.000000ine mesh 0.1%;
Propylene glycol 20%;
Alcohol 5%;
Flavour of a drug perfume base 7.5%;
Water 7.9%.
Each the percentages of ingredients content that wherein is used to prepare the flavour of a drug perfume base is respectively:
Salvia Sclare L.oil 30%;
Pineapple ketone 30%;
Methyl catechol 30%;
Alcohol 10%.
Embodiment 3
A kind of flavouring essence for tobacco makes by following steps:
(1) preparation 2600g flavour of a drug perfume base is standby, the preparation method of this flavour of a drug perfume base is as follows: accurate weighing Salvia Sclare L.oil 546g, pineapple ketone 650g, methyl catechol 572g and 832g alcohol, then above-mentioned each component is added in the proportion container in order one by one and stir, get final product stand for standby use up to the whole dissolvings of each component.
(2) it is standby accurately to take by weighing each component according to following each components contents;
Tamarind medicinal extract 2600;
Imitative Mao Xiang medicinal extract 1000;
Smoked plum medicinal extract 600;
Liquid Glucose 7000;
Maillard reaction thing 2600;
Xylitol (liquid) 3800;
Straight juice acid 3000;
Hops tincture 1400;
Tobacco Type B extract 1800;
Vanillin food grade,1000.000000ine mesh 120;
Propylene glycol 7400;
Alcohol 2480;
Water 3600.
(3) get 1300g propylene glycol joining in the reactor that tobacco Type B extract is housed slowly under hand mixing, treat that tobacco Type B extract dissolves fully after, add vanillin food grade,1000.000000ine mesh again, stir;
(4) the Maillard reaction thing is heated to 95 ℃ after, treat after it fuses fully it to be joined in the reactant of above-mentioned steps (3), continue to stir;
(5) propylene glycol, water and the flavour of a drug perfume base with remainder mixes in the back reactant that adds in the above-mentioned steps (4), continues to stir;
(6) alcohol, Xylitol (liquid), Liquid Glucose and tamarind medicinal extract are mixed the back and add in the reactant of above-mentioned steps (5), continue to stir;
(7) under condition of stirring, will imitate in the reactant of Mao Xiang medicinal extract, smoked plum medicinal extract, straight juice acid and hops tincture adding above-mentioned steps (6), continue heated and stirred then 15 minutes;
(8) stop to reflux, continue to stir after 30 minutes, leave standstill and made finished product in 24 hours.
Prepare the 40kg flavouring essence for tobacco by above-mentioned steps, wherein in this essence, each percentages of ingredients content is as follows:
Tamarind medicinal extract 6.5%;
Imitative Mao Xiang medicinal extract 2.5%;
Smoked plum medicinal extract 1.5%;
Liquid Glucose 17.5%;
Maillard reaction thing 6.5%;
Xylitol (liquid) 9.5%;
Straight juice acid 7.5%;
Hops tincture 3.5%;
Tobacco Type B extract 4.5%;
Vanillin food grade,1000.000000ine mesh 0.3%;
Propylene glycol 18.5%;
Alcohol 6.2%;
Flavour of a drug perfume base 6.5%;
Water 9%.
Each the percentages of ingredients content that wherein is used to prepare the flavour of a drug perfume base is respectively:
Salvia Sclare L.oil 21%;
Pineapple ketone 25%;
Methyl catechol 22%;
Alcohol 32%.
Need to prove; the above embodiments are the explanation to design of the present invention; rather than restriction; those of ordinary skill in the art can also make other proportioning according to above-mentioned design and principle; the given embodiment of these proportionings and the present invention belongs to the technical scheme that is equal to; as long as in the ratio range that the present invention gave, all should be within protection scope of the present invention.
Claims (8)
1. flavouring essence for tobacco, its component and each percentages of ingredients (weight percent) content are:
Tamarind medicinal extract 4.5%～7.5%;
Imitative Mao Xiang medicinal extract 1.5%～4.5%;
Smoked plum medicinal extract 0.5%～1.5%;
Liquid Glucose 16.5%～19.5%;
Maillard reaction thing 4.5%～7.5%;
Xylitol (liquid) 8.5%～11.5%;
Straight juice acid 5.5%～8.5%;
Hops tincture 2.5%～5.5%;
Tobacco Type B extract 2.5%～5.5%;
Vanillin food grade,1000.000000ine mesh 0.1%～0.5%;
Propylene glycol 16%～20%;
Alcohol 5%～8%;
Flavour of a drug perfume base 4.5%～7.5%;
Surplus is a water.
2. flavouring essence for tobacco according to claim 1 is characterized in that, preferred, each components contents of described essence is:
Tamarind medicinal extract 6.5%;
Imitative Mao Xiang medicinal extract 2.5%;
Smoked plum medicinal extract 1.5%;
Liquid Glucose 17.5%;
Maillard reaction thing 6.5%;
Xylitol (liquid) 9.5%;
Straight juice acid 7.5%;
Hops tincture 3.5%;
Tobacco Type B extract 4.5%;
Vanillin food grade,1000.000000ine mesh 0.3%;
Propylene glycol 18.5%;
Alcohol 6.2%;
Flavour of a drug perfume base 6.5%;
Water 9%.
3. flavouring essence for tobacco according to claim 1 and 2 is characterized in that, described flavour of a drug perfume base comprises Salvia Sclare L.oil, pineapple ketone, methyl catechol and alcohol, and wherein each components contents is respectively:
Salvia Sclare L.oil 20%～30%;
Pineapple ketone 20%～30%;
Methyl catechol 20%～30%;
Alcohol 10%～40%.
4. flavouring essence for tobacco according to claim 3 is characterized in that, preferred, each components contents in the described flavour of a drug perfume base is:
Salvia Sclare L.oil 21%;
Pineapple ketone 25%;
Methyl catechol 22%;
Alcohol 32%.
5. preparation method of essence as claimed in claim 1 or 2, the concrete steps of method are as follows:
(1) it is standby accurately to take by weighing each component according to claim 1 or 2 each percentages of ingredients content;
(2) propylene glycol the joining in the reactor that tobacco Type B extract is housed slowly under hand mixing that take a morsel, treat that tobacco Type B extract dissolves fully after, add vanillin food grade,1000.000000ine mesh again, stir;
(3) the Maillard reaction thing is heated to 95 ℃ after, treat after it fuses fully it to be joined in the reactant of above-mentioned steps (2), continue to stir;
(4) propylene glycol, water and the flavour of a drug perfume base with remainder mixes in the back reactant that adds in the above-mentioned steps (3), continues to stir;
(5) alcohol, Xylitol (liquid), Liquid Glucose and tamarind medicinal extract are mixed the back and add in the reactant of above-mentioned steps (4), continue to stir;
(6) under condition of stirring, will imitate in the reactant of Mao Xiang medicinal extract, smoked plum medicinal extract, straight juice acid and hops tincture adding above-mentioned steps (5), continue heated and stirred then 15 minutes;
(7) stop to reflux, continue to stir after 30 minutes, leave standstill and made finished product in 24 hours.
6. flavouring essence for tobacco according to claim 5 is characterized in that, described flavour of a drug perfume base comprises Salvia Sclare L.oil, pineapple ketone, methyl catechol and alcohol, and wherein each components contents is respectively:
Salvia Sclare L.oil 20%～30%;
Pineapple ketone 20%～30%;
Methyl catechol 20%～30%;
Alcohol 10%～40%.
7. flavouring essence for tobacco according to claim 6 is characterized in that, preferred, each components contents in the described flavour of a drug perfume base is:
Salvia Sclare L.oil 21%;
Pineapple ketone 25%;
Methyl catechol 22%;
Alcohol 32%.
8. according to claim 6 or 7 described flavouring essence for tobaccos, it is characterized in that the step of producing flavour of a drug essence is as follows:
(1) it is standby to take by weighing each component according to each percentages of ingredients content of flavour of a drug essence;
(2) Salvia Sclare L.oil, pineapple ketone, methyl catechol and alcohol are added in the proportion container in order one by one, the dissolving that stirs gets final product.
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| CN107118847A (en) * | 2017-05-12 | 2017-09-01 | 安徽中烟工业有限责任公司 | A kind of essence for simulating the fragrant and sweet style of tobacco natural coal |
| CN109207258A (en) * | 2017-07-05 | 2019-01-15 | 湖北中烟工业有限责任公司 | A kind of flavouring essence for tobacco modulator approach and its application with medicinal herbs, baking note |
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