CN107118847A - A kind of essence for simulating the fragrant and sweet style of tobacco natural coal - Google Patents
A kind of essence for simulating the fragrant and sweet style of tobacco natural coal Download PDFInfo
- Publication number
- CN107118847A CN107118847A CN201710333817.4A CN201710333817A CN107118847A CN 107118847 A CN107118847 A CN 107118847A CN 201710333817 A CN201710333817 A CN 201710333817A CN 107118847 A CN107118847 A CN 107118847A
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- CN
- China
- Prior art keywords
- fragrant
- essence
- sweet
- tobacco
- cigarette
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
- C11B9/003—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing less than six carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0069—Heterocyclic compounds
- C11B9/0073—Heterocyclic compounds containing only O or S as heteroatoms
- C11B9/0076—Heterocyclic compounds containing only O or S as heteroatoms the hetero rings containing less than six atoms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0069—Heterocyclic compounds
- C11B9/0092—Heterocyclic compounds containing only N as heteroatom
Abstract
The invention discloses a kind of essence for simulating the fragrant and sweet style of tobacco natural coal, its composition is constituted and content is matched after basis is carefully studied to the flue gas fragrance component after cigarette burning and determined, selecting in cigarette mainstream flue gas has fragrant and sootiness fragrance the main aroma-producing substance of burnt fragrant and sweet, baking, preferably simulates natural burnt fragrant and sweet of cigarette smoke.The essence of the present invention can be used for tobacco and its product perfuming, modification and the natural burnt fragrant and sweet feature of enhancing tobacco itself.
Description
Technical field
The invention belongs to essence spice for cigarette technical field, specifically, tobacco natural coal is simulated the present invention relates to one kind
The composition of fragrant and sweet style.
Background technology
Cigarette style characteristic refers to the note impression that band gives people during cigarette smoking.Cigarette product generally have itself unique and
Stable aromatic style.The odor characteristic that tobacco business improves commonly using essence and flavoring agent and highlights tobacco.Fragrant and sweet Jiao is dense
One of typical note of odor type tobacco leaf, is also the style and features that high-end raw material of cigarette Zimbabwe tobacco leaf is protruded.How this is protruded
Advantageous burnt fragrant and sweet style simultaneously improves product quality, is the problem of tobacco company pays special attention to.Scientific research personnel it is also proposed
Number of ways tackles this problem.Such as screen and cultivate burnt fragrant and sweet tobacco variety, improve tobacco leaf formulation, exploitation with burnt fragrant and sweet
Essence and flavoring agent of feature etc..In recent years, when developing tobacco essence spices, scientific research personnel increasingly tends to simulate the sheet of tobacco
Perfume (or spice), the style and features natural to tobacco itself are modified and improved, and to improve product quality, meet consumer demand.
Cigarette product produces flue gas in suction by burning, the actual sensory experience of consumer come from main flume into
Point.Mainstream smoke constituents are only derived partly from the transfer of tobacco component, largely come from the high temperature pyrolysis of tobacco leaf, therefore
Its composition is constituted and sensory experience is complicated more than tobacco leaf.Want to simulate this perfume of cigarette, it is necessary to the fragrance of main flume into
Divide and main aroma-producing substance is studied, to instruct essence and flavoring agent to develop.
The content of the invention
By high-resolution comprehensive two dimensional gas chromatography-flight time mass spectrum and gas-chromatography-of the invention, which smells, debates instrument focusing sweet tea
The main flume of cigarette leaf is studied in detail can preferably simulate the burnt fragrant and sweet essence of cigarette smoke there is provided a kind of, be used to
Modification and the fragrant and sweet style of natural coal of enhancing tobacco.
Table 1, which is shown, is presented fragrant and sootiness fragrance the material of burnt fragrant and sweet, baking in the burnt fragrant and sweet main flow flue gas in tobacco of typical case.
Determine and calculate fragrance activity value (ratio of content and threshold value) to assess each aroma substance to entirety on the basis of threshold value
The contribution of fragrance.Wherein fragrance activity value is more than 1 and having 18 materials, have 11 materials more than 5, and these materials are main
Flow the burnt fragrant and sweet significant contributor of flue gas.Maximum preceding 11 materials of selection aroma strength configure burnt fragrant and sweet essence and pass through each thing
The scientific compatibility of matter content so that the best results of essence.
Each Ingredients Weight per distribution ratio of essence of the present invention simulation fragrant and sweet style of tobacco natural coal is：
Guaiacol 0.59-2.37%, pineapple ketone 3.51-14.03%, angelica lactone 0.92-3.68%, 4- vinyl are cured
Methyl-pyrazin 0.80-3.19%, the 4- methyl of wound wood phenol 1.17-4.69%, 2- acetylpyridine 0.57-2.30%, 2- ethyl -6 is cured
The wooden phenol 0.51-2.045%, gamma-valerolactone 0.04-0.17%, 4-ethyl guaiacol 0.12-0.49%, methyl cyclopentene of wound
Alcohol ketone 0.92-3.69%, ethylcyclopentenolone 0.84-3.35%, surplus is solvent.
Wherein, the percentage by weight composition of each component of the composition solvent is：Ethanol 30-70%, propane diols 10-
40%, glycerine 10-40%.
The essence of the present invention can be used for tobacco and its product perfuming, modification and the natural burnt fragrant and sweet spy of enhancing tobacco itself
Levy.
Beneficial effects of the present invention are embodied in：
The essence of the present invention is obtained on the basis of the main aroma-producing substance of Accurate Analysis cigarette mainstream flue gas, preferably
The natural burnt sweet tea of tobacco, roasting characteristics fragrance are simulated, this perfume is coordinated naturally with tobacco, can modify and improve tobacco natural coal sweet tea
Fragrant breeze lattice.
Burnt fragrant and sweet Related Component and its fragrance energy value in the burnt fragrant and sweet tobacco leaf main flume of the typical case of table 1
Embodiment
With reference to embodiment, the invention will be further described.
Embodiment 1
The weight percent of each composition of the essence of the present embodiment simulation fragrant and sweet style of tobacco natural coal, which is matched, is：Guaiacol
1.18%, pineapple ketone 7.01%, angelica lactone 1.84%, 4- vinyl guaiacols 2.34%, 2- acetylpyridines 1.15%, 2-
The Methyl-pyrazin of ethyl -6 1.60%, 4- methyl guaiacol and 4s 1.02%, gamma-valerolactone 0.09%, 4-ethyl guaiacol
0.25%, methyl cyclopentenyl ketone 1.84%, ethylcyclopentenolone 1.68%, solvent 80%.
Wherein, the percentage by weight composition of each component of composition solvent is：Ethanol 60%, propane diols 20%, glycerine 20%.
The index of correlation parameter of essence is as shown in table 2 obtained by the present embodiment：
The essence physical and chemical index of table 2
The essence is used for perfuming cigarette, addition is 5/10000ths, by specialty evaluation person progress sensory evaluating smoking, and with
Non- perfuming cigarette is contrasted, as a result as shown in table 3.It can be seen that, compared with control group, cigarette product aroma quality after perfuming,
The basic indexs such as perfume quantity, roundness degree have larger improvement, at the same flue-cured tobacco is fragrant, burnt fragrant and sweet and the fragrant note of baking there has also been it is larger
Improve.Illustrate that the essence product can effectively improve the organoleptic quality of cigarette, and the prominent burnt fragrant and sweet note of enhancing.
The cigarette sensory evaluating smoking attribute of table 3 and result
Embodiment 2
The essence of the fragrant and sweet style of simulation tobacco natural coal in the present embodiment is configured to by mass percentage：Guaiacol
1.77%, pineapple ketone 10.52%, angelica lactone 2.76%, 4- vinyl guaiacols 3.52%, 2- acetylpyridines 1.72%,
The Methyl-pyrazin 2.40% of 2- ethyls -6,4- methyl guaiacol and 4s 1.53%, gamma-valerolactone 0.13%, 4-ethyl guaiacol
0.37%, methyl cyclopentenyl ketone 2.77%, ethylcyclopentenolone 2.51%, solvent 70%.
Wherein, the percentage by weight composition of each component of composition solvent is：Ethanol 70%, propane diols 10%, glycerine 20%.
The index of correlation of essence product is as shown in table 4 obtained by the present embodiment.
The essence physical and chemical index of table 4
The essence is used for perfuming cigarette, addition is 8/10000ths, by specialty evaluation person progress sensory evaluating smoking, and with
Non- perfuming cigarette is contrasted, as a result as shown in table 5.Compared with control group, cigarette product aroma quality, fragrance after perfuming
The basic indexs such as amount, roundness degree have larger improvement, while flue-cured tobacco is fragrant, the fragrant note of burnt fragrant and sweet and baking there has also been larger carry
It is high.Illustrate that the essence product can effectively improve the organoleptic quality of cigarette, and the prominent burnt fragrant and sweet note of enhancing.
The cigarette sensory evaluating smoking attribute of table 5 and result
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
Any modifications, equivalent substitutions and improvements made within refreshing and principle etc., should be included in the scope of the protection.
Claims (2)
1. a kind of essence for simulating the fragrant and sweet style of tobacco natural coal, it is characterised in that：The weight percent of each composition of the essence
Match and be：
Guaiacol 0.59-2.37%, pineapple ketone 3.51-14.03%, angelica lactone 0.92-3.68%, 4- vinyl guaiaci lignum
Methyl-pyrazin 0.80-3.19%, 4- the methyl guaiaci lignum of phenol 1.17-4.69%, 2- acetylpyridine 0.57-2.30%, 2- ethyl -6
Phenol 0.51-2.045%, gamma-valerolactone 0.04-0.17%, 4-ethyl guaiacol 0.12-0.49%, methyl cyclopentenyl ketone
0.92-3.69%, ethylcyclopentenolone 0.84-3.35%, surplus is solvent.
2. the essence of the simulation fragrant and sweet style of tobacco natural coal according to claim 1, it is characterised in that：Constitute the solvent
Each component percentage by weight composition be：Ethanol 30-70%, propane diols 10-40%, glycerine 10-40%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710333817.4A CN107118847A (en) | 2017-05-12 | 2017-05-12 | A kind of essence for simulating the fragrant and sweet style of tobacco natural coal |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710333817.4A CN107118847A (en) | 2017-05-12 | 2017-05-12 | A kind of essence for simulating the fragrant and sweet style of tobacco natural coal |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107118847A true CN107118847A (en) | 2017-09-01 |
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|---|---|---|---|
| CN201710333817.4A Pending CN107118847A (en) | 2017-05-12 | 2017-05-12 | A kind of essence for simulating the fragrant and sweet style of tobacco natural coal |
Country Status (1)
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| CN (1) | CN107118847A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111227297A (en) * | 2020-03-25 | 2020-06-05 | 中国烟草总公司郑州烟草研究院 | Spice composition for blasting beads capable of highlighting baking aroma characteristics of cigarettes, blasting bead aroma base module, blasting beads and cigarettes |
| CN111406970A (en) * | 2020-03-27 | 2020-07-14 | 四川中烟工业有限责任公司 | Sweet-burning base for cigarettes |
| CN113197331A (en) * | 2021-05-18 | 2021-08-03 | 云南中烟工业有限责任公司 | Tobacco leaf obtained by fermenting tobacco leaf with medicinal white starter, fermentation method and application |
| CN115806857A (en) * | 2022-09-16 | 2023-03-17 | 中国烟草总公司郑州烟草研究院 | Preparation method of tobacco extract special flavor group |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0110362B1 (en) * | 1982-12-06 | 1988-04-20 | L. GIVAUDAN & CIE Société Anonyme | Fragrance and flavour compositions |
| CN101705149A (en) * | 2009-11-13 | 2010-05-12 | 飞嘉创业添加剂(深圳)有限公司 | Tobacco essence and preparation method thereof |
| CN104522875A (en) * | 2014-12-28 | 2015-04-22 | 中国烟草总公司郑州烟草研究院 | Cigarette sweet aroma spice module formula |
| CN106398866A (en) * | 2016-06-15 | 2017-02-15 | 河南中烟工业有限责任公司 | Flavor threshold-based essence for flue-cured, sweet and fragrant cigarette and blending method thereof |
-
2017
- 2017-05-12 CN CN201710333817.4A patent/CN107118847A/en active Pending
Patent Citations (4)
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|---|---|---|---|---|
| EP0110362B1 (en) * | 1982-12-06 | 1988-04-20 | L. GIVAUDAN & CIE Société Anonyme | Fragrance and flavour compositions |
| CN101705149A (en) * | 2009-11-13 | 2010-05-12 | 飞嘉创业添加剂(深圳)有限公司 | Tobacco essence and preparation method thereof |
| CN104522875A (en) * | 2014-12-28 | 2015-04-22 | 中国烟草总公司郑州烟草研究院 | Cigarette sweet aroma spice module formula |
| CN106398866A (en) * | 2016-06-15 | 2017-02-15 | 河南中烟工业有限责任公司 | Flavor threshold-based essence for flue-cured, sweet and fragrant cigarette and blending method thereof |
Non-Patent Citations (3)
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|---|
| 毛多斌 等: "《卷烟香味化学》", 31 January 1994, 河南科学技术出版社 * |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111227297A (en) * | 2020-03-25 | 2020-06-05 | 中国烟草总公司郑州烟草研究院 | Spice composition for blasting beads capable of highlighting baking aroma characteristics of cigarettes, blasting bead aroma base module, blasting beads and cigarettes |
| CN111227297B (en) * | 2020-03-25 | 2021-11-26 | 中国烟草总公司郑州烟草研究院 | Spice composition for blasting beads capable of highlighting baking aroma characteristics of cigarettes, blasting bead aroma base module, blasting beads and cigarettes |
| CN111406970A (en) * | 2020-03-27 | 2020-07-14 | 四川中烟工业有限责任公司 | Sweet-burning base for cigarettes |
| CN111406970B (en) * | 2020-03-27 | 2022-03-01 | 四川中烟工业有限责任公司 | Sweet-burning base for cigarettes |
| CN113197331A (en) * | 2021-05-18 | 2021-08-03 | 云南中烟工业有限责任公司 | Tobacco leaf obtained by fermenting tobacco leaf with medicinal white starter, fermentation method and application |
| CN113197331B (en) * | 2021-05-18 | 2023-06-13 | 云南中烟工业有限责任公司 | Tobacco leaf obtained by fermenting tobacco leaf with medicinal white yeast, fermentation method and application |
| CN115806857A (en) * | 2022-09-16 | 2023-03-17 | 中国烟草总公司郑州烟草研究院 | Preparation method of tobacco extract special flavor group |
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| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170901 |
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| RJ01 | Rejection of invention patent application after publication |