CN104479873A - Formula of smoky flavor module for electronic cigarette - Google Patents

Formula of smoky flavor module for electronic cigarette Download PDF

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Publication number
CN104479873A
CN104479873A CN201410825492.8A CN201410825492A CN104479873A CN 104479873 A CN104479873 A CN 104479873A CN 201410825492 A CN201410825492 A CN 201410825492A CN 104479873 A CN104479873 A CN 104479873A
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CN
China
Prior art keywords
electronic cigarette
smoke
cigarette
formula
smoky
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Application number
CN201410825492.8A
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Chinese (zh)
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CN104479873B (en
Inventor
张启东
刘俊辉
柴国璧
王丁众
孙世豪
屈展
宗永立
张建勋
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Zhengzhou Tobacco Research Institute of CNTC
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Zhengzhou Tobacco Research Institute of CNTC
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Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06Use of materials for tobacco smoke filters
    • A24D3/14Use of materials for tobacco smoke filters of organic materials as additive

Abstract

The invention discloses a formula of a smoky spice module for an electronic cigarette. The formula of the smoky spice module is characterized by comprising the followingcomponents: guaiacol, 2,6-dimethoxyphenol, 4-ethyl guaiacol, eugenol, iso-eugenol, 3,4-dimethylcyclopentenolone, 4-hydroxy-2,5-dimethyl-3(2H)furanone and a solvent. The components of the smoky spice module all exist in cigarette smoke, the smoky smell of the smoke of the electronic cigarette can be improved greatly when the formula is applied to an electronic cigarette core, the smoky smell moreapproximates the aroma of cigarette smoke, and the requirements of an electronic cigarette consumer for pursuing sensory characteristics of cigarettes are met.

Description

A kind of electronic cigarette smoke flavour spices module is filled a prescription
Technical field
The invention belongs to tobacco product meat flavor formulating technology field, specifically a kind of electronic cigarette smoke flavour spices module formula.
Background technology
Spices module refers to and to be similar to by odour characteristics and the good multiple perfume material of Harmony allocates formed feature odor type unit in proportion.According to the actual requirements, different spices modules is carried out combining the blending mode obtaining essence and can be described as modularization blending.Because spices module has clear and definite feature odor type, effectively can improve the specific aim of use, make blending process more convenient; Meanwhile, the spices module of plurality of raw materials composition remains certain rich, avoids the shortcoming that the single synthetic perfume fragrance of composition is dull, stiff.
Along with countries in the world are to fulfiling of " Framework Convention on Tobacco Control " and deepening continuously of smoking and health research, electronic cigarette, as a kind of substitute products of cigarette, obtains the attention in market gradually.Although at present remain in dispute to the security of electronic cigarette, contrast traditional cigarette, the objectionable constituent kind of electronic cigarette or content all have and reduces significantly (Z. Cahn and M. Siegel, journal of Public Health Policy, 2011, vol. 32,1,16 – 31).But existing market electronic cigarette fragrance style on sale is more dull, the mainly product of the odor type such as peppermint, cocoa, fruit, the fragrance characteristic abundant with cigarette smoke is far apart.Mixing the electronic cigarette that fragrance characteristic is similar to cigarette smoke, is that current electronic cigarette product attracts one of effective way of more human consumers.
Owing to there is not the process of cigarette burning, the smoke perfume that electronic cigarette human consumer experiences, mainly from the spices in its cigarette core segment electronic cigarette liquid.In cigarette smoke containing many flavour ingredients (A. Rodgman and T. A. Perfetti, beitr ge zur Tabakforschung International, 2009, vol. 23,5,277 – 333), these compositions are basic substances of cigarette fragrance characteristic.Utilize flavour ingredient intrinsic in cigarette smoke, mix the various spices module with cigarette different characteristics fragrance, produce positive pushing effect by electronic cigarette simulation cigarette fragrance characteristic, the more human consumers of attraction.
Summary of the invention
The object of the invention is to utilize the smoke flavour composition existed in cigarette smoke, a kind of electronic cigarette smoke flavour spices module formula is provided.Perfumer for smoke flavour feature, can use this spices module easily in electronic cigarette liquid, strengthens the rich of electronic cigarette fragrance and the similarity with cigarette fragrance characteristic.
Above-mentioned purpose of the present invention is achieved by the following technical programs:
An electronic cigarette smoke flavour spices module formula, is made up of by mass percentage following component: methyl catechol 1-5%; 2,6-syringol 1-5%; 4-ethyl guaiacol 1-6%; Eugenol 0-4%; Isoeugenol 0-5%; 3,4-dimethylcyclopentene alcohol ketone 1-5%; 4-hydroxyl-2,5-dimethyl-3 (2H) furanone 0-5%; Solvent 70-95%.Said components sum is 100%.
Wherein, solvent can be any one or the two or more mixing in water, glycerine, propylene glycol, ethanol.
Formula relates generally to the composition of three class aromatic styles: methyl catechol, 2,6-syringol and 4-ethyl guaiacol all have typical smoke flavour feature, and are cigarette smoke proper constituent, sootiness sensillary base can be provided to adjust for electronic cigarette; 3,4-dimethylcyclopentene alcohol ketone and 4-hydroxyl-2,5-dimethyl-3 (2H) furanone has caramel breath, and be the proper constituent of cigarette smoke, burnt fragrant and sweet gas can be provided for electronic cigarette, and burnt fragrant and sweet gas be cigarette burning produce except tangy flavour, very important odour characteristics, has good compatibleness with smoke flavour; Eugenol and isoeugenol are the compositions with pungent fragrance, are also the proper constituents of cigarette smoke, can play the effect strengthening this electronic cigarette spices total tune.
In electronic cigarette smoke flavour spices module formula of the present invention raw materials used be commercially available; Preparation process is the mix and blend dissolution process of blending field routine, without the need to specific installation.
The present invention has following beneficial effect:
(1) composition of electronic cigarette smoke flavour spices module formula of the present invention is all present in cigarette smoke, can significantly improve the smoke flavour impression of electronic cigarette, make it more close to the organoleptic feature of cigarette smoke.
(2) electronic cigarette smoke flavour spices module formula odour characteristics of the present invention is clearly stable, uses with strong points, can be used in tobacco juice for electronic smoke allocation process very easily.
(3) the raw materials used easy acquisition of electronic cigarette smoke flavour spices module formula of the present invention, production technique is simple.
Embodiment
Below in conjunction with examples of implementation, the present invention is described further, but and limits the scope of the invention never in any form.
embodiment 1
Smoke flavour spices module composition (mass percentage)
Methyl catechol 3%; 2,6-syringol 3%; 4-ethyl guaiacol 2%; Eugenol 1%; 3,4-dimethylcyclopentene alcohol ketone 1%; Glycerine 30%; Propylene glycol 60%.
Smoke flavour spices module solution 0.1 mL of above-mentioned composition is added in tobacco juice for electronic smoke 10 mL of this laboratory development, gets 4 mL after Homogeneous phase mixing and add in electronic cigarette core, after leaving standstill 2h, carry out suction evaluation by 7 electronic cigarette sensory evaluation personnel.All evaluation personnel all experience, and with the addition of the electronic cigarette of smoke flavour spices module, and smoke flavour impression obviously strengthens, and slightly pungent perfume (or spice) and caramel sample fragrance, add the rich of electronic cigarette fragrance.
embodiment 2
Smoke flavour spices module composition (mass percentage)
Methyl catechol 5%; 2,6-syringol 5%; 4-ethyl guaiacol 4%; 3,4-dimethylcyclopentene alcohol ketone 1%; Water 10%; Glycerine 75%.
Smoke flavour spices module solution 0.1 mL of above-mentioned composition is added in tobacco juice for electronic smoke 10 mL of this laboratory development, gets 4 mL after Homogeneous phase mixing and add in electronic cigarette core, after leaving standstill 2h, carry out suction evaluation by 7 electronic cigarette sensory evaluation personnel.All evaluation personnel all experience, and with the addition of the electronic cigarette of smoke flavour spices module, and smoke flavour impression is strong, and smoke flavour odour characteristics is true cigarette smoke relatively; Meanwhile, slightly caramel sample fragrance, oral cavity and throat produce slight excitement and are subject to.
embodiment 3
Smoke flavour spices module composition (mass percentage)
Methyl catechol 2%; 2,6-syringol 2%; 4-ethyl guaiacol 2%; Eugenol 2%; Isoeugenol 1%; 3,4-dimethylcyclopentene alcohol ketone 2%; 4-hydroxyl-2,5-dimethyl-3 (2H) furanone 1%; Water 8%; Propylene glycol 80%.
Smoke flavour spices module solution 0.1 mL of above-mentioned composition is added in commercially available tobacco juice for electronic smoke 10 mL, gets 4 mL after Homogeneous phase mixing and add in electronic cigarette core, after leaving standstill 2h, carry out suction evaluation by 7 electronic cigarette sensory evaluation personnel.All evaluation personnel all experience, and with the addition of the electronic cigarette of smoke flavour spices module, occur soft stacte feature; Meanwhile, experience the burnt fragrant and sweet feature of good pungent fragrant characteristic sum with smoke flavour fragrance Harmony, oral cavity and throat's comfortableness better.
embodiment 4
Smoke flavour spices module composition (mass percentage)
Methyl catechol 4%; 2,6-syringol 4%; 4-ethyl guaiacol 2%; Eugenol 4%; Isoeugenol 2%; 3,4-dimethylcyclopentene alcohol ketone 2%; 4-hydroxyl-2,5-dimethyl-3 (2H) furanone 2%; Propylene glycol 80%.
Smoke flavour spices module solution 0.1 mL of above-mentioned composition is added in commercially available tobacco juice for electronic smoke 10 mL, gets 4 mL after Homogeneous phase mixing and add in electronic cigarette core, after leaving standstill 2h, carry out suction evaluation by 7 electronic cigarette sensory evaluation personnel.All evaluation personnel all experience, and with the addition of the electronic cigarette of smoke flavour spices module, occur obvious stacte feature; Burnt fragrant and sweet and pungent fragrant feature is also obvious, and with the commercially available electronic cigarette of stacte characteristic sum overall fragrance keynote Harmony better, meanwhile, oral cavity and throat's comfortableness good.

Claims (2)

1. an electronic cigarette smoke flavour spices module formula, is characterized in that: be made up of by mass percentage following component: methyl catechol 1-5%; 2,6-syringol 1-5%; 4-ethyl guaiacol 1-6%; Eugenol 0-4%; Isoeugenol 0-5%; 3,4-dimethylcyclopentene alcohol ketone 1-5%; 4-hydroxyl-2,5-dimethyl-3 (2H) furanone 0-5%; Solvent 70-95%.
2. electronic cigarette smoke flavour spices module according to claim 1 formula, is characterized in that: described solvent is any one or two or more mixing in water, glycerine, propylene glycol, ethanol.
CN201410825492.8A 2014-12-28 2014-12-28 A kind of electronic cigarette smoke flavour spices module formula Active CN104479873B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410825492.8A CN104479873B (en) 2014-12-28 2014-12-28 A kind of electronic cigarette smoke flavour spices module formula

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Application Number Priority Date Filing Date Title
CN201410825492.8A CN104479873B (en) 2014-12-28 2014-12-28 A kind of electronic cigarette smoke flavour spices module formula

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CN104479873A true CN104479873A (en) 2015-04-01
CN104479873B CN104479873B (en) 2018-03-09

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107432496A (en) * 2016-05-25 2017-12-05 浙江中烟工业有限责任公司 One kind is applied to heating non-combustion-type tobacco product and its perfuming method
CN107432497A (en) * 2016-05-25 2017-12-05 浙江中烟工业有限责任公司 A kind of function essence for being applied to heating non-combustion-type tobacco product
CN114062528A (en) * 2020-07-29 2022-02-18 丘比株式会社 Vinegar, food and drink, method for imparting smoke aroma, and method for masking unpleasant odor

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102293438A (en) * 2011-05-27 2011-12-28 南京农业大学 Color, flavor and safety three-effect food fumeol and its preparation method
CN102304428A (en) * 2011-03-17 2012-01-04 广州市澳键丰泽生物科技有限公司 Formula of tobacco flavoring essence with sweet fragrance
CN103284323A (en) * 2013-06-19 2013-09-11 江苏中烟工业有限责任公司徐州卷烟厂 Tobacco sweetening agent for cigarettes and application method of tobacco sweetening agent
CN103704659A (en) * 2013-12-05 2014-04-09 杭州艾菲曼普香精香料有限公司 Maple flavor formula

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102304428A (en) * 2011-03-17 2012-01-04 广州市澳键丰泽生物科技有限公司 Formula of tobacco flavoring essence with sweet fragrance
CN102293438A (en) * 2011-05-27 2011-12-28 南京农业大学 Color, flavor and safety three-effect food fumeol and its preparation method
CN103284323A (en) * 2013-06-19 2013-09-11 江苏中烟工业有限责任公司徐州卷烟厂 Tobacco sweetening agent for cigarettes and application method of tobacco sweetening agent
CN103704659A (en) * 2013-12-05 2014-04-09 杭州艾菲曼普香精香料有限公司 Maple flavor formula

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107432496A (en) * 2016-05-25 2017-12-05 浙江中烟工业有限责任公司 One kind is applied to heating non-combustion-type tobacco product and its perfuming method
CN107432497A (en) * 2016-05-25 2017-12-05 浙江中烟工业有限责任公司 A kind of function essence for being applied to heating non-combustion-type tobacco product
CN107432496B (en) * 2016-05-25 2021-01-19 浙江中烟工业有限责任公司 Non-combustion tobacco product suitable for heating and flavoring method thereof
CN114062528A (en) * 2020-07-29 2022-02-18 丘比株式会社 Vinegar, food and drink, method for imparting smoke aroma, and method for masking unpleasant odor
CN114062528B (en) * 2020-07-29 2023-10-20 丘比株式会社 Vinegar, food and drink, method for giving fumigated aroma, and method for masking unpleasant odor

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