CN107236355A - A kind of novel non-toxic opaquing fluid and preparation method thereof - Google Patents
A kind of novel non-toxic opaquing fluid and preparation method thereof Download PDFInfo
- Publication number
- CN107236355A CN107236355A CN201710501317.7A CN201710501317A CN107236355A CN 107236355 A CN107236355 A CN 107236355A CN 201710501317 A CN201710501317 A CN 201710501317A CN 107236355 A CN107236355 A CN 107236355A
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- CN
- China
- Prior art keywords
- opaquing fluid
- preparation
- toxic
- novel non
- pul
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D10/00—Correcting fluids, e.g. fluid media for correction of typographical errors by coating
Abstract
The invention provides a kind of novel non-toxic opaquing fluid and preparation method thereof, described opaquing fluid is prepared from by main material Pul, solvent deionized water, pigment, surfactant glycerine, thickener and lemon oil, and described preparation method comprises the following steps:a)Prepare the Pul aqueous solution, b)Charging mixing, c)Preparing finished articles.It is with low cost present invention is disclosed a kind of novel non-toxic opaquing fluid and preparation method thereof, opaquing fluid production and using very convenient, non-environmental-pollution, the gun-ho performance for not only possessing existing opaquing fluid, and fragrant odour, beneficial health, production can be promoted on a large scale.
Description
Technical field
The present invention relates to a kind of office appliance, and in particular to a kind of novel non-toxic opaquing fluid and preparation method thereof, belongs to and does
Utility technical field.
Background technology
Office appliance is enterprise or individual assistant product used in during office.Office appliance industry is related to
Field widely, the species covered also widely, including:Archive files articles for use, desktop articles for use, office equipment, finance are used
A series of articles for use related to work such as product, consumptive material.Wherein, to be that people are engaged in routine office work activity essential for desktop articles for use
Standing article, desktop articles for use mainly include:Stapler, nail puller, card punch, scissors, cutter, hand papercutter, ticket-holder, nail pin system
Row, penknife, glue stick, glue, adhesive tape, Tape Dispenser, opaquing fluid, calculator, instrument chi, compasses, pen container, pen bag, calendar stand, meeting
Board and other items.
The fine chemical product of clerical error is corrected when opaquing fluid is for handling official business, writing, can be avoided using opaquing fluid
Because the repetition that accidental clerical error must be carried out is copied, and save the plenty of time.Opaquing fluid is the office appliance of consumption-type, demand
Amount is very big.At present, the key component of commercially available opaquing fluid has:1)Pigment, plays covering;2)Film forming matter, mainly resin
Or polymer, play adhesive attraction;3)Solvent, makes coating turn into liquid, easy to apply;4)Auxiliary agent, such as thickener, levelling agent, table
Face activating agent etc..The compositions such as film forming matter and solvent therein are organic matter, during use, and poisonous organic matter can be waved
Hair, causes to poison, and pollute environment to human body.The solvent of existing opaquing fluid is n-hexane, hexamethylene or trichloroethanes.
A large amount of contact n-hexanes or hexamethylene, can cause DPN, poisoner may occur in which myasthenia and trick sensory nerve by
The symptom of damage;And trichloroethanes has anesthetic effect, poisoner has the extremely symptom such as tired, pale and gastrointestinal tract disorder, seriously
Person has Liver and kidney function infringement.
The content of the invention
For the demand, the invention provides a kind of novel non-toxic opaquing fluid and preparation method thereof, opaquing fluid production
With using very convenient, with low cost, non-environmental-pollution, not only possess the gun-ho performance of existing opaquing fluid, and smell
Fragrance, beneficial health can promote production on a large scale.
The present invention is a kind of novel non-toxic opaquing fluid and preparation method thereof, and described opaquing fluid is mould more by the short stalk of main material
Sugar, solvent deionized water, pigment, surfactant glycerine, thickener and lemon oil are prepared from, and described preparation method includes
Following steps:a)Prepare the Pul aqueous solution, b)Charging mixing, c)Preparing finished articles.
In a preferred embodiment of the present invention, the raw material percentage formula of described opaquing fluid is:Short stalk is mould
Polysaccharide 37.5%~42.5%, pigment 47.5%~52.5%, surfactant glycerine 4%~5%, thickener 4.75%~5.25%, lemon
Lemon oil 0.25%~0.75%.
In a preferred embodiment of the present invention, described pigment is by titanium dioxide and ultrafine kaolin in mass ratio 1:1 mixing
Form.
In a preferred embodiment of the present invention, described thickener is nano inorganic water-based thickener aluminium-magnesium silicate, and it is used
The mass fraction that amount accounts for amount of pigment is 10%.
In a preferred embodiment of the present invention, described step a)In, the Pul aqueous solution is existed by Pul
Dissolved solution is made in a certain amount of deionized water, and its concentration is 0.5g/mL.
In a preferred embodiment of the present invention, described step b)In, charging mixing temperature is 60 DEG C, and mixing speed is
800r/min, mixing time is 20min.
In a preferred embodiment of the present invention, described step c)In, preparing finished articles include milled processed and filtered and packaged,
Wherein, grinding technics condition is:Drum's speed of rotation rate 60%, 35 DEG C of operating temperature, milling time 6h.
Present invention is disclosed a kind of novel non-toxic opaquing fluid and preparation method thereof, opaquing fluid production and using very square
Just, it is with low cost, non-environmental-pollution, the gun-ho performance for not only possessing existing opaquing fluid, and fragrant odour, beneficial human body
Health, production can be promoted on a large scale.
Brief description of the drawings
The present invention is further detailed explanation with reference to the accompanying drawings and detailed description:
Fig. 1 is the process step diagram of novel non-toxic amendment liquid and preparation method thereof of the embodiment of the present invention.
Embodiment
Presently preferred embodiments of the present invention is described in detail below in conjunction with the accompanying drawings, so that advantages and features of the invention energy
It is easier to be readily appreciated by one skilled in the art, apparent is clearly defined so as to be made to protection scope of the present invention.
Fig. 1 is the process step diagram of novel non-toxic amendment liquid and preparation method thereof of the embodiment of the present invention;The opaquing fluid is by main material
Pul, solvent deionized water, pigment, surfactant glycerine, thickener and lemon oil are prepared from, described preparation
Method comprises the following steps:a)Prepare the Pul aqueous solution, b)Charging mixing, c)Preparing finished articles.
The novel non-toxic opaquing fluid that the present invention is referred to, using deionized water as solvent, passes through using Pul as main material
It is prepared by addition composite pigment, surfactant glycerine, nano inorganic water-based thickener aluminium-magnesium silicate and lemon oil;Wherein,
Pul is a kind of using starch or carbohydrate as raw material, the extracellular pure natural macromolecule polysaccharide produced through microbial fermentation,
The Pul is soluble in water, safety non-toxic, edible;The Pul aqueous solution of water preparation is dissolved in Pul
With good adhesivity, coating and film forming, so as to replace poisonous organic matter that opaquing fluid is made, and it can protect
Demonstrate,proving the opaquing fluid being made has preferable writing quality again.Composite pigment is by titanium dioxide and ultrafine kaolin in mass ratio 1:1 mixes
Conjunction is formed, and the composite pigment can effectively improve the covering power of opaquing fluid.The consumption of nano inorganic water-based thickener aluminium-magnesium silicate is accounted for
The mass fraction of composite pigment consumption is 10%, and it has preferable thickening effect, is remarkably improved the viscosity of batch mixing.Live on surface
Property agent glycerine can increase the brightness on film forming caudacoria surface, and make film soft, smooth.The addition of lemon oil can not only make what is be made
Opaquing fluid distributes strong citris aromas, and can play a part of refreshing the mind, and can eliminate clerical workforce because of long-term work
The fatigue of generation.
Embodiment 1
Specific preparation method is as follows:
a)The Pul aqueous solution is prepared, specific preparation process is:By weight percentage, first take 37.5% short stalk mould many
Sugar is put into stirring container, then adds deionized water solvent by a certain percentage, at normal temperatures uniform stirring, and concentration is made and is
The 0.5g/mL Pul aqueous solution.
b)Charging is mixed, and specific preparation process is:First by a certain amount of titanium dioxide and ultrafine kaolin in mass ratio 1:1 mixes
Close, composite pigment is made;Then by weight percentage, 52.5% composite pigment, 4% surfactant glycerine, 5.25% thickening are taken
Agent and 0.75% lemon oil, are added sequentially to step a)In the Pul aqueous solution of preparation, heating response solution temperature to 60
DEG C, 20min is stirred with 800r/min mixing speed, batch mixing is made.
c)Preparing finished articles, specific preparation process is:First by step b)The batch mixing produced is transferred in ball mill, and in rotating speed
6h is ground under the conditions of rate 60%, the ball-milling technology that 35 DEG C of operating temperature;Then filtration treatment is carried out, you can opaquing fluid finished product is made;
Finally packed.
Embodiment 2
Specific preparation method is as follows:
a)The Pul aqueous solution is prepared, specific preparation process is:By weight percentage, first take 42.5% short stalk mould many
Sugar is put into stirring container, then adds deionized water solvent by a certain percentage, at normal temperatures uniform stirring, and concentration is made and is
The 0.5g/mL Pul aqueous solution.
b)Charging is mixed, and specific preparation process is:First by a certain amount of titanium dioxide and ultrafine kaolin in mass ratio 1:1 mixes
Close, composite pigment is made;Then by weight percentage, 47.5% composite pigment, 5% surfactant glycerine, 4.75% thickening are taken
Agent and 0.25% lemon oil, are added sequentially to step a)In the Pul aqueous solution of preparation, heating response solution temperature to 60
DEG C, 20min is stirred with 800r/min mixing speed, batch mixing is made.
c)Preparing finished articles, specific preparation process is:First by step b)The batch mixing produced is transferred in ball mill, and in rotating speed
6h is ground under the conditions of rate 60%, the ball-milling technology that 35 DEG C of operating temperature;Then filtration treatment is carried out, you can opaquing fluid finished product is made;
Finally packed.
Present invention is disclosed a kind of novel non-toxic opaquing fluid and preparation method thereof, opaquing fluid production and using very square
Just, it is with low cost, non-environmental-pollution, the gun-ho performance for not only possessing existing opaquing fluid, and fragrant odour, beneficial human body
Health, production can be promoted on a large scale.
The foregoing is only a specific embodiment of the invention, but protection scope of the present invention is not limited thereto, any
Those skilled in the art disclosed herein technical scope in, the change that can expect without creative work or
Replace, should all be included within the scope of the present invention.Therefore, protection scope of the present invention should be limited with claims
Fixed protection domain is defined.
Claims (7)
1. a kind of novel non-toxic opaquing fluid and preparation method thereof, it is characterised in that described opaquing fluid is mould more by the short stalk of main material
Sugar, solvent deionized water, pigment, surfactant glycerine, thickener and lemon oil are prepared from, and described preparation method includes
Following steps:a)Prepare the Pul aqueous solution, b)Charging mixing, c)Preparing finished articles.
2. novel non-toxic opaquing fluid according to claim 1 and preparation method thereof, it is characterised in that described opaquing fluid
Raw material percentage formula is:Pul 37.5%~42.5%, pigment 47.5%~52.5%, surfactant are sweet
Oil 4%~5%, thickener 4.75%~5.25%, lemon oil 0.25%~0.75%.
3. novel non-toxic opaquing fluid according to claim 1 and preparation method thereof, it is characterised in that described pigment is by titanium
White powder and ultrafine kaolin in mass ratio 1:1 mixes.
4. novel non-toxic opaquing fluid according to claim 1 and preparation method thereof, it is characterised in that described thickener is
Nano inorganic water-based thickener aluminium-magnesium silicate, the mass fraction that its consumption accounts for amount of pigment is 10%.
5. novel non-toxic opaquing fluid according to claim 1 and preparation method thereof, it is characterised in that described step a)
In, the Pul aqueous solution is dissolved in a certain amount of deionized water and is made at normal temperatures by Pul, and its concentration is
0.5g/mL。
6. novel non-toxic opaquing fluid according to claim 1 and preparation method thereof, it is characterised in that described step b)
In, charging mixing temperature is 60 DEG C, and mixing speed is 800r/min, and mixing time is 20min.
7. novel non-toxic opaquing fluid according to claim 1 and preparation method thereof, it is characterised in that described step c)
In, preparing finished articles include milled processed and filtered and packaged, wherein, grinding technics condition is:Drum's speed of rotation rate 60%, work temperature
35 DEG C of degree, milling time 6h.
Priority Applications (1)
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CN201710501317.7A CN107236355A (en) | 2017-06-27 | 2017-06-27 | A kind of novel non-toxic opaquing fluid and preparation method thereof |
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CN201710501317.7A CN107236355A (en) | 2017-06-27 | 2017-06-27 | A kind of novel non-toxic opaquing fluid and preparation method thereof |
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CN201710501317.7A Pending CN107236355A (en) | 2017-06-27 | 2017-06-27 | A kind of novel non-toxic opaquing fluid and preparation method thereof |
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Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105230940A (en) * | 2015-10-20 | 2016-01-13 | 贵州中烟工业有限责任公司 | Functional hard candy and preparation method thereof |
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2017
- 2017-06-27 CN CN201710501317.7A patent/CN107236355A/en active Pending
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105230940A (en) * | 2015-10-20 | 2016-01-13 | 贵州中烟工业有限责任公司 | Functional hard candy and preparation method thereof |
Non-Patent Citations (1)
Title |
---|
马静等: "用正交试验法选择新型无毒涂改液配方", 《长春工业大学学报(自然科学版)》 * |
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