CN110184122A - A kind of cigarette particle of quick sensing fragrance and its preparation method and application - Google Patents
A kind of cigarette particle of quick sensing fragrance and its preparation method and application Download PDFInfo
- Publication number
- CN110184122A CN110184122A CN201910550865.8A CN201910550865A CN110184122A CN 110184122 A CN110184122 A CN 110184122A CN 201910550865 A CN201910550865 A CN 201910550865A CN 110184122 A CN110184122 A CN 110184122A
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- CN
- China
- Prior art keywords
- cigarette
- particle
- agent
- parts
- inorganic salts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
Abstract
The present invention relates to a kind of cigarette particles of quick sensing fragrance, component including following parts by weight: 5-10 parts of solid, water soluble perfume (or spice) source material, 0.5-5 parts of sweetener, disintegrating agent are 2-5 parts, remaining as the mixture of inorganic salts alkaline agent and organic acid agent, total amount is 100 parts；Wherein, inorganic salts alkaline agent is mixed with organic acid agent 1:0.8~2.0 in mass ratio.The cigarette solves the problems, such as water-soluble fragrant source material to be introduced into cigarette filter rod and keeps flue gas moisture constant during the smoking process with particle, and the grain fraction is simple, simple process, and production energy consumption is small.
Description
Technical field
The present invention relates to a kind of cigarette particle, especially a kind of cigarette particle of quick sensing fragrance further relates to its preparation
Methods and applications.
Background technique
Being disintegrated particle is a kind of granule containing sodium bicarbonate and organic acid, tablet can be enable to be disintegrated rapidly, dissolve out medicine
Effective component in agent improves the dissolution rate and bioavilability of drug.When be disintegrated granule encounter water when, contained by carbon
The organic acids such as sour hydrogen sodium and citric acid, tartaric acid can chemically react rapidly, release carbon dioxide gas largely to produce
Anger is steeped, in aqueous solution visible vigorous reaction.
Addition has the material of absorption property in cigarette filter rod, is the main means of lowering harm and decreasing coking.However, due to tar reduction
The development of harm reduction technology is so that the flavor and taste of tobacco product substantially reduces, therefore tobacco business researcher passes through in filter stick simultaneously
Mend the important side that fragrant and flavouring technique or carrier are tobacco business concerns with the loss for supplementing cigarette smoke fragrance and study
To.
Now in common filter stick, glyceryl triacetate flavoring, gel, middle line form fragrance are not easy to keep, and diffusion rate is fast.
Although can also add the fragrant particle of load in filter stick easily reduces moisture when flue gas passes through because granular absorption is strong.In addition,
The prior art also has adds quick-fried pearl in filter stick, but fragrant source is currently only fat-soluble flavors and fragrances in quick-fried pearl content, so that
The water-soluble flavors and fragrances that good sense of taste improves in cigarette is limited in filter stick addition use.
Summary of the invention
In order to solve above-mentioned soluble perfume fragrance in filter stick addition using being limited, flue gas moisture easily drops after particle addition
The problems such as low, the purpose of the present invention is to provide cigarette particles of a kind of quick sensing fragrance and its preparation method and application.
Technical solution of the present invention is specific as follows:
A kind of cigarette particle of quick sensing fragrance, the component including following parts by weight:
Solid, water soluble perfume (or spice) source expect 5-10 part, 0.5-5 parts of sweetener, disintegrating agent be 2-5 parts, remaining as inorganic salts alkaline agent with it is organic
The mixture of sour agent, total amount are 100 parts；Wherein, inorganic salts alkaline agent is mixed with organic acid agent 1:0.8~2.0 in mass ratio.
Further, the solid, water soluble perfume (or spice) source material be crystal sugar orange freeze-dried powder, blueberry freeze-dried powder, dark plum freeze-dried powder or its
One of his Natural Food articles freeze-dried powder, solid, water soluble flavors and fragrances or a variety of combinations.
Further, the sweetener is one kind or more of xylitol, antierythrite, white granulated sugar and other type sweeteners
Kind combination.
Further, the disintegrating agent is low-substituted hydroxypropyl cellulose, carboxymethyl starch and crosslinked polyethylene pyrroles
One or more combinations of alkanone.
Further, the inorganic salts alkaline agent is that natrium carbonicum calcinatum, anhydrous sodium bicarbonate and other chance acid can produce CO2's
One of inorganic salts are a variety of.
Further, the organic acid agent is one of citric acid, tartaric acid and malic acid or a variety of combinations.
The invention further relates to cigarette particle preparation method, include the following steps:
Step (1), raw material preparation
Prepare raw material by following parts by weight:
Solid, water soluble perfume (or spice) source expect 5-10 part, 0.5-5 parts of sweetener, disintegrating agent be 2-5 parts, remaining as inorganic salts alkaline agent with it is organic
The mixture of sour agent, total amount are 100 parts；Wherein, inorganic salts alkaline agent is mixed with organic acid agent 1:0.8~2.0 in mass ratio；
Step (2) is granulated
The mixture of step (1) is put into dry granulating machine to be granulated；Particle is crossed 50~80 meshes and is disintegrated to get to cigarette
Particle.
The invention further relates to application of the cigarette particle in cigarette, the particle is being filtered with the additive amount of 1 ~ 3mg/mm
Stick uniformly adds when forming；Or compound addition is carried out with a composite module and filter stick, specific additive amount should be with cigarette product
Subject to design.
Compared with prior art, the invention has the following advantages that
(1) water-soluble solid perfume (or spice) source is expected to use effervesce disintegration technical tie-up by the present invention for the first time, during the smoking process, cigarette
Water environment provided by air water point can be such that disintegrating agent, organic acid agent, inorganic salts alkaline agent reacts rapidly, the CO of generation2Gas is rapid
Solid perfume (or spice) source material strip is entered into flue gas, making smoking property of cigarette, person perceives rapidly individual features fragrance, reacts while the water generated maintains
Flue gas moisture balance, avoids flue gas from generating dry sensation and excitement.
(2) preparation method supplementary material of the present invention is simple, cheap, and disintegration dry method granulation processes are easy, strong operability,
Preparation time is short, and production energy consumption is small.
(3) cigarette arrived of the invention with disintegration particle there are also the effect of apparent reducing tar and reducing harm, relative to blank sample,
H value is obviously reduced, and under the premise of quick sensing fragrance, also helps health.
Detailed description of the invention
Fig. 1 is the XRD diagram of example reaction front and back, fragrant source object.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical solution in the present embodiment is clearly and completely described, is shown
So, described embodiment is only rather than whole example to a part of example of the present invention.Based on the implementation in the present invention
Example, those of ordinary skill in the art's every other embodiment obtained under that premise of not paying creative labor, belongs to
The scope of protection of the invention.
Embodiment 1
The preparation method of the cigarette particle of the quick sensing fragrance of the present embodiment, includes the following steps:
Step (1), raw material preparation
The cigarette particle for producing 100kg prepares raw material by following parts by weight:
Crystal sugar orange freeze-dried powder 10kg, xylitol 0.5kg, hydroxymethyl starch 3kg, sodium bicarbonate 45kg, citric acid 41.5kg are weighed,
It is uniformly mixed；
Step (2) is granulated
The mixture of step (1) is put into dry granulating machine to be granulated；Particle crosses 60 meshes to get cigarette disintegration is arrived
Grain.
Embodiment 2
The preparation method of the cigarette particle of the quick sensing fragrance of the present embodiment, includes the following steps:
Step (1), raw material preparation
The cigarette particle for producing 100kg prepares raw material by following parts by weight:
Weigh blueberry freeze-dried powder 5kg, white granulated sugar 4kg, low-substituted hydroxypropyl cellulose 5kg, natrium carbonicum calcinatum 35kg, tartaric acid
51kg is uniformly mixed；
Step (2) is granulated
The mixture of step (1) is put into dry granulating machine to be granulated；Particle crosses 50 meshes to get cigarette disintegration is arrived
Grain.
Embodiment 3
The preparation method of the cigarette particle of the quick sensing fragrance of the present embodiment, includes the following steps:
Step (1), raw material preparation
The cigarette particle for producing 100kg prepares raw material by following parts by weight:
Weigh crystal sugar orange freeze-dried powder 8kg, antierythrite 2kg, crosslinked polyvinylpyrrolidone 2kg, sodium bicarbonate 30kg, malic acid
58kg is uniformly mixed；
Step (2) is granulated
The mixture of step (1) is put into dry granulating machine to be granulated；Particle crosses 60 meshes to get cigarette disintegration is arrived
Grain.
Embodiment 4
The preparation method of the cigarette particle of the quick sensing fragrance of the present embodiment, includes the following steps:
Step (1), raw material preparation
The cigarette particle for producing 100kg prepares raw material by following parts by weight:
Dark plum freeze-dried powder 10kg, xylitol 4kg, hydroxymethyl starch 4kg, sodium bicarbonate 44kg, citric acid 38kg are weighed, mixing is equal
It is even；
Step (2) is granulated
The mixture of step (1) is put into dry granulating machine to be granulated；Particle crosses 80 meshes to get cigarette disintegration is arrived
Grain.
Embodiment 5
The preparation method of the cigarette particle of the quick sensing fragrance of the present embodiment, includes the following steps:
Step (1), raw material preparation
The cigarette particle for producing 100kg prepares raw material by following parts by weight:
Weigh dark plum freeze-dried powder and each 5kg of blueberry freeze-dried powder, xylitol and white granulated sugar each 2kg, hydroxymethyl starch 4kg, bicarbonate
Sodium and natrium carbonicum calcinatum each 20kg, tartaric acid 42kg are uniformly mixed；
Step (2) is granulated
The mixture of step (1) is put into dry granulating machine to be granulated；Particle crosses 80 meshes to get cigarette disintegration is arrived
Grain.
Embodiment 6
The preparation method of the cigarette particle of the quick sensing fragrance of the present embodiment, includes the following steps:
Step (1), raw material preparation
The cigarette particle for producing 100kg prepares raw material by following parts by weight:
Weigh dark plum freeze-dried powder 8kg, each 5kg of white granulated sugar, hydroxymethyl starch and crosslinked polyvinylpyrrolidone each 2.5kg are anhydrous
Sodium carbonate 42kg, tartaric acid and malic acid 20kg are uniformly mixed；
Step (2) is granulated
The mixture of step (1) is put into dry granulating machine to be granulated；Particle crosses 80 meshes to get cigarette disintegration is arrived
Grain.
For verifying flue gas moisture balance, the application is by the cigarette of embodiment 1 with disintegration particle respectively with 1mg/mm, 2mg/mm
Additive amount uniformly added in filter stick formation, the filter stick sample of addition is for rolling into cigarette sample 1,2, in addition to being not added with this
Particle, blank sample coiling process and sample 1,2 are consistent.
Flue gas moisture analysis, detection are carried out to sample cigarette according to GB/T 19609-2004, GB/T 23203.1-2013
It the results are shown in Table 1.
1 particulate samples cigarette smoke moisture testing result of table
As can be known from Table 1, sample 1,2 flue gas moistures are not reduced compared with blank sample, wherein sample 1 or even slightly above blank
Sample；The total granules content of sample 1,2 is below blank sample.
In addition, the application is used as fragrance matter source using solid, water soluble perfume (or spice) source material (crystal sugar orange freeze-dried powder), when anhydrous
Tap touching, fragrant source does not discharge；It when there is contact with moisture, is reacted, when generating bubble, fragrant source substance is discharged with bubble.
For the holding and release for verifying fragrant source substance, we are disintegrated particle and perfume (or spice) to forward and backward cigarette is reacted in embodiment 1
Source object has carried out X-ray diffraction (XRD) analysis, as a result as shown in Figure 1.
Cigarette disintegration particle and fragrant source object, fragrant source object have apparent characteristic peak at 10 ° or so before comparison is reacted, this feature
Peak also has in particle before the reaction to be shown, because auxiliary material peak shape has certain overlapping, and fragrant source object content phase in this particle in sample
To lower, therefore fragrant source object characteristic peak is opposite weakens；Comparison reaction front and back cigarette disintegration particle, fragrant source object characteristic peak disappear,
Show that fragrant source object is discharged with bubble during the reaction.As it can be seen that the application can be very good to solve the problems, such as that fragrance is not easy to keep.
Finally, we are according to YQ/T 17-2012, YC/T 254-2008, YC/T 253-2008, YC/T 255-2008,
GB/T 21130-2007, YC/T 377-2017 detects the harmful components of above-mentioned sample 1,2, and testing result is shown in Table 2.
Wherein H value (cigarette Evaluation of Harmfulness index) is by CO, HCN, NNK, NH3, benzo [a] pyrene, 7 phenol, crotonaldehyde subitem groups
At each subitem value is the ratio between measured value and reference value of a certain cigarette, and the sum of 7 subitem values are that the harmfulness of the cigarette is commented
Valence index value.Value is bigger, then harmfulness is bigger, and value is smaller, then harmfulness is smaller.
2 particulate samples cigarette smoke harmful components testing result of table
As can be seen from Table 2, the H value for being added to the sample of disintegration particle is effectively reduced, and such effect is for I
It is not expected that, the disintegrating agent of above-mentioned dosage, organic acid agent, in the rapid reaction process of inorganic salts alkaline agent may be also to upper
It states harmful components to be adsorbed, has achieved the effect that certain reducing tar and reducing harm.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (8)
1. a kind of cigarette particle of quick sensing fragrance, it is characterised in that: the component including following parts by weight:
Solid, water soluble perfume (or spice) source expect 5-10 part, 0.5-5 parts of sweetener, disintegrating agent be 2-5 parts, remaining as inorganic salts alkaline agent with it is organic
The mixture of sour agent, total amount are 100 parts；Wherein, inorganic salts alkaline agent is mixed with organic acid agent 1:0.8~2.0 in mass ratio.
2. the cigarette particle of quick sensing fragrance according to claim 1, it is characterised in that: solid, water soluble perfume (or spice) source
Material is crystal sugar orange freeze-dried powder, blueberry freeze-dried powder, dark plum freeze-dried powder or other Natural Food articles freeze-dried powders, solid, water soluble essence perfume
One of material or a variety of combinations.
3. the cigarette particle of quick sensing fragrance according to claim 1, it is characterised in that: the sweetener is xylose
One or more combinations of alcohol, antierythrite, white granulated sugar and other type sweeteners.
4. the cigarette particle of quick sensing fragrance according to claim 1, it is characterised in that: the disintegrating agent is low takes
For one or more combinations of hydroxypropyl cellulose, carboxymethyl starch and crosslinked polyvinylpyrrolidone.
5. the cigarette particle of quick sensing fragrance according to claim 1, it is characterised in that: the inorganic salts alkaline agent is nothing
Aqueous sodium carbonate, anhydrous sodium bicarbonate and other chance acid can produce CO2One of inorganic salts or a variety of.
6. the cigarette particle of quick sensing fragrance according to claim 1, it is characterised in that: the organic acid agent is lemon
One of acid, tartaric acid and malic acid or a variety of combinations.
7. the preparation method of the cigarette particle of one of claim 1-6, characterized by the following steps:
Step (1), raw material preparation
Prepare raw material by following parts by weight:
Solid, water soluble perfume (or spice) source expect 5-10 part, 0.5-5 parts of sweetener, disintegrating agent be 2-5 parts, remaining as inorganic salts alkaline agent with it is organic
The mixture of sour agent, total amount are 100 parts；Wherein, inorganic salts alkaline agent is mixed with organic acid agent 1:0.8~2.0 in mass ratio；
Step (2) is granulated
The mixture of step (1) is put into dry granulating machine to be granulated；Particle is crossed 50~80 meshes and is disintegrated to get to cigarette
Particle.
8. application of the cigarette particle of one of claim 1-6 in cigarette, it is characterised in that: by the particle with 1 ~ 3mg/mm
Additive amount uniformly added in filter stick formation；Or compound addition, specific additive amount are carried out with a composite module and filter stick
The cigarette product that should be subject to designs.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910550865.8A CN110184122A (en) | 2019-06-24 | 2019-06-24 | A kind of cigarette particle of quick sensing fragrance and its preparation method and application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910550865.8A CN110184122A (en) | 2019-06-24 | 2019-06-24 | A kind of cigarette particle of quick sensing fragrance and its preparation method and application |
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| Publication Number | Publication Date |
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| CN110184122A true CN110184122A (en) | 2019-08-30 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910550865.8A Pending CN110184122A (en) | 2019-06-24 | 2019-06-24 | A kind of cigarette particle of quick sensing fragrance and its preparation method and application |
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| CN (1) | CN110184122A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111466613A (en) * | 2020-04-09 | 2020-07-31 | 上海华宝生物科技有限公司 | Flavoring particle for filter stick, preparation method thereof and filter stick |
| CN114621818A (en) * | 2022-03-09 | 2022-06-14 | 山东省食品发酵工业研究设计院 | Nano essence particles for cigarette filter stick and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111466613A (en) * | 2020-04-09 | 2020-07-31 | 上海华宝生物科技有限公司 | Flavoring particle for filter stick, preparation method thereof and filter stick |
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| CN114621818A (en) * | 2022-03-09 | 2022-06-14 | 山东省食品发酵工业研究设计院 | Nano essence particles for cigarette filter stick and preparation method thereof |
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Application publication date: 20190830 |