CN107981405A - A kind of preparation method and applications for heating the cigarette that do not burn - Google Patents
A kind of preparation method and applications for heating the cigarette that do not burn Download PDFInfo
- Publication number
- CN107981405A CN107981405A CN201711312963.5A CN201711312963A CN107981405A CN 107981405 A CN107981405 A CN 107981405A CN 201711312963 A CN201711312963 A CN 201711312963A CN 107981405 A CN107981405 A CN 107981405A
- Authority
- CN
- China
- Prior art keywords
- cigarette
- heating
- tobacco
- burn
- embossing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 168
- 238000010438 heat treatment Methods 0.000 title claims abstract description 80
- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- 241000208125 Nicotiana Species 0.000 claims abstract description 148
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 148
- 238000000034 method Methods 0.000 claims abstract description 73
- 239000000463 material Substances 0.000 claims abstract description 44
- 238000004049 embossing Methods 0.000 claims abstract description 39
- 238000004519 manufacturing process Methods 0.000 claims abstract description 30
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 24
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000011888 foil Substances 0.000 claims abstract description 24
- 239000005030 aluminium foil Substances 0.000 claims abstract description 22
- 238000005096 rolling process Methods 0.000 claims abstract description 7
- 239000000835 fiber Substances 0.000 claims description 42
- MDYZKJNTKZIUSK-UHFFFAOYSA-N tyloxapol Chemical compound O=C.C1CO1.CC(C)(C)CC(C)(C)C1=CC=C(O)C=C1 MDYZKJNTKZIUSK-UHFFFAOYSA-N 0.000 claims description 23
- 239000007787 solid Substances 0.000 claims description 22
- 238000002156 mixing Methods 0.000 claims description 19
- 230000001070 adhesive effect Effects 0.000 claims description 16
- 239000000853 adhesive Substances 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical group [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 12
- 239000000654 additive Substances 0.000 claims description 12
- 230000000996 additive effect Effects 0.000 claims description 12
- 159000000007 calcium salts Chemical class 0.000 claims description 10
- 239000000843 powder Substances 0.000 claims description 10
- 239000002994 raw material Substances 0.000 claims description 10
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 9
- 238000000227 grinding Methods 0.000 claims description 9
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 6
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 6
- 229910052799 carbon Inorganic materials 0.000 claims description 6
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 6
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 6
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 5
- 238000003825 pressing Methods 0.000 claims description 5
- 229960002901 sodium glycerophosphate Drugs 0.000 claims description 5
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical group CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 4
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 claims description 4
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 claims description 4
- GUPPESBEIQALOS-UHFFFAOYSA-L calcium tartrate Chemical compound [Ca+2].[O-]C(=O)C(O)C(O)C([O-])=O GUPPESBEIQALOS-UHFFFAOYSA-L 0.000 claims description 4
- 235000011035 calcium tartrate Nutrition 0.000 claims description 4
- 239000001427 calcium tartrate Substances 0.000 claims description 4
- 235000010408 potassium alginate Nutrition 0.000 claims description 4
- 239000000737 potassium alginate Substances 0.000 claims description 4
- MZYRDLHIWXQJCQ-YZOKENDUSA-L potassium alginate Chemical compound [K+].[K+].O1[C@@H](C([O-])=O)[C@@H](OC)[C@H](O)[C@H](O)[C@@H]1O[C@@H]1[C@@H](C([O-])=O)O[C@@H](O)[C@@H](O)[C@H]1O MZYRDLHIWXQJCQ-YZOKENDUSA-L 0.000 claims description 4
- 235000010413 sodium alginate Nutrition 0.000 claims description 4
- 239000000661 sodium alginate Substances 0.000 claims description 4
- 229940005550 sodium alginate Drugs 0.000 claims description 4
- REULQIKBNNDNDX-UHFFFAOYSA-M sodium;2,3-dihydroxypropyl hydrogen phosphate Chemical compound [Na+].OCC(O)COP(O)([O-])=O REULQIKBNNDNDX-UHFFFAOYSA-M 0.000 claims description 4
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 claims description 4
- 241000609240 Ambelania acida Species 0.000 claims description 3
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims description 3
- 235000017491 Bambusa tulda Nutrition 0.000 claims description 3
- 244000060011 Cocos nucifera Species 0.000 claims description 3
- 235000013162 Cocos nucifera Nutrition 0.000 claims description 3
- 229920001353 Dextrin Polymers 0.000 claims description 3
- 239000004375 Dextrin Substances 0.000 claims description 3
- 244000082204 Phyllostachys viridis Species 0.000 claims description 3
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims description 3
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 3
- 229920001131 Pulp (paper) Polymers 0.000 claims description 3
- 239000010905 bagasse Substances 0.000 claims description 3
- 239000011425 bamboo Substances 0.000 claims description 3
- MKJXYGKVIBWPFZ-UHFFFAOYSA-L calcium lactate Chemical compound [Ca+2].CC(O)C([O-])=O.CC(O)C([O-])=O MKJXYGKVIBWPFZ-UHFFFAOYSA-L 0.000 claims description 3
- 239000001527 calcium lactate Substances 0.000 claims description 3
- 235000011086 calcium lactate Nutrition 0.000 claims description 3
- 229960002401 calcium lactate Drugs 0.000 claims description 3
- 239000004832 casein glue Substances 0.000 claims description 3
- 235000019425 dextrin Nutrition 0.000 claims description 3
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 3
- FNAQSUUGMSOBHW-UHFFFAOYSA-H calcium citrate Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O.[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O FNAQSUUGMSOBHW-UHFFFAOYSA-H 0.000 claims description 2
- 239000001354 calcium citrate Substances 0.000 claims description 2
- 229960004256 calcium citrate Drugs 0.000 claims description 2
- 229920000447 polyanionic polymer Polymers 0.000 claims description 2
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 2
- 235000013337 tricalcium citrate Nutrition 0.000 claims description 2
- 239000001913 cellulose Substances 0.000 claims 1
- 229920002678 cellulose Polymers 0.000 claims 1
- 235000009508 confectionery Nutrition 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 15
- 230000007547 defect Effects 0.000 abstract description 6
- 238000005253 cladding Methods 0.000 abstract 1
- 239000000123 paper Substances 0.000 description 35
- 239000000523 sample Substances 0.000 description 14
- 238000012360 testing method Methods 0.000 description 9
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical group OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 8
- 230000001953 sensory effect Effects 0.000 description 7
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 6
- 239000003546 flue gas Substances 0.000 description 6
- 238000002290 gas chromatography-mass spectrometry Methods 0.000 description 6
- 239000002304 perfume Substances 0.000 description 6
- NIDGCIPAMWNKOA-WOJBJXKFSA-N Neophytadiene Natural products [C@H](CCC[C@@H](CCCC(C)C)C)(CCCC(C=C)=C)C NIDGCIPAMWNKOA-WOJBJXKFSA-N 0.000 description 5
- NIDGCIPAMWNKOA-UHFFFAOYSA-N neophytadiene Chemical compound CC(C)CCCC(C)CCCC(C)CCCC(=C)C=C NIDGCIPAMWNKOA-UHFFFAOYSA-N 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 238000004458 analytical method Methods 0.000 description 4
- 238000001514 detection method Methods 0.000 description 4
- 239000004205 dimethyl polysiloxane Substances 0.000 description 4
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 4
- 235000011187 glycerol Nutrition 0.000 description 4
- CXQXSVUQTKDNFP-UHFFFAOYSA-N octamethyltrisiloxane Chemical compound C[Si](C)(C)O[Si](C)(C)O[Si](C)(C)C CXQXSVUQTKDNFP-UHFFFAOYSA-N 0.000 description 4
- 238000004806 packaging method and process Methods 0.000 description 4
- 238000004987 plasma desorption mass spectroscopy Methods 0.000 description 4
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 4
- 238000004088 simulation Methods 0.000 description 4
- 239000000779 smoke Substances 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 229920001661 Chitosan Polymers 0.000 description 3
- 206010013786 Dry skin Diseases 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- 230000032683 aging Effects 0.000 description 3
- 229930002875 chlorophyll Natural products 0.000 description 3
- 235000019804 chlorophyll Nutrition 0.000 description 3
- ATNHDLDRLWWWCB-AENOIHSZSA-M chlorophyll a Chemical compound C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC(C(CC)=C3C)=[N+]4C3=CC3=C(C=C)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 ATNHDLDRLWWWCB-AENOIHSZSA-M 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 238000002470 solid-phase micro-extraction Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 239000001707 (E,7R,11R)-3,7,11,15-tetramethylhexadec-2-en-1-ol Substances 0.000 description 2
- UFLHIIWVXFIJGU-ARJAWSKDSA-N (Z)-hex-3-en-1-ol Chemical compound CC\C=C/CCO UFLHIIWVXFIJGU-ARJAWSKDSA-N 0.000 description 2
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical group C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
- 235000005979 Citrus limon Nutrition 0.000 description 2
- 244000131522 Citrus pyriformis Species 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 244000246386 Mentha pulegium Species 0.000 description 2
- 235000016257 Mentha pulegium Nutrition 0.000 description 2
- 235000004357 Mentha x piperita Nutrition 0.000 description 2
- BLUHKGOSFDHHGX-UHFFFAOYSA-N Phytol Natural products CC(C)CCCC(C)CCCC(C)CCCC(C)C=CO BLUHKGOSFDHHGX-UHFFFAOYSA-N 0.000 description 2
- HNZBNQYXWOLKBA-UHFFFAOYSA-N Tetrahydrofarnesol Natural products CC(C)CCCC(C)CCCC(C)=CCO HNZBNQYXWOLKBA-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- 150000001299 aldehydes Chemical class 0.000 description 2
- 150000001335 aliphatic alkanes Chemical class 0.000 description 2
- BOTWFXYSPFMFNR-OALUTQOASA-N all-rac-phytol Natural products CC(C)CCC[C@H](C)CCC[C@H](C)CCCC(C)=CCO BOTWFXYSPFMFNR-OALUTQOASA-N 0.000 description 2
- 238000000889 atomisation Methods 0.000 description 2
- 229960005069 calcium Drugs 0.000 description 2
- 239000011575 calcium Substances 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 235000010216 calcium carbonate Nutrition 0.000 description 2
- 239000003610 charcoal Substances 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 238000001785 headspace extraction Methods 0.000 description 2
- 238000009775 high-speed stirring Methods 0.000 description 2
- 235000001050 hortel pimenta Nutrition 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
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- 229910052757 nitrogen Inorganic materials 0.000 description 2
- BOTWFXYSPFMFNR-PYDDKJGSSA-N phytol Chemical compound CC(C)CCC[C@@H](C)CCC[C@@H](C)CCC\C(C)=C\CO BOTWFXYSPFMFNR-PYDDKJGSSA-N 0.000 description 2
- 239000007790 solid phase Substances 0.000 description 2
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- DVWSXZIHSUZZKJ-UHFFFAOYSA-N 18:3n-3 Natural products CCC=CCC=CCC=CCCCCCCCC(=O)OC DVWSXZIHSUZZKJ-UHFFFAOYSA-N 0.000 description 1
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 1
- 206010016173 Fall Diseases 0.000 description 1
- FLIACVVOZYBSBS-UHFFFAOYSA-N Methyl hexadecanoate Natural products CCCCCCCCCCCCCCCC(=O)OC FLIACVVOZYBSBS-UHFFFAOYSA-N 0.000 description 1
- 229920002522 Wood fibre Polymers 0.000 description 1
- 239000000443 aerosol Substances 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 229920006321 anionic cellulose Polymers 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 229960003563 calcium carbonate Drugs 0.000 description 1
- QXDHJHQRJCJRAU-UHFFFAOYSA-N calcium;2-hydroxypropane-1,2,3-tricarboxylic acid Chemical compound [Ca].OC(=O)CC(O)(C(O)=O)CC(O)=O QXDHJHQRJCJRAU-UHFFFAOYSA-N 0.000 description 1
- SMHNUIFHMAGAFL-UHFFFAOYSA-N calcium;2-hydroxypropanoic acid Chemical compound [Ca].CC(O)C(O)=O SMHNUIFHMAGAFL-UHFFFAOYSA-N 0.000 description 1
- 239000012159 carrier gas Substances 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
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- 239000006185 dispersion Substances 0.000 description 1
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- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000011067 equilibration Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- HNZUNIKWNYHEJJ-FMIVXFBMSA-N geranyl acetone Chemical compound CC(C)=CCC\C(C)=C\CCC(C)=O HNZUNIKWNYHEJJ-FMIVXFBMSA-N 0.000 description 1
- HNZUNIKWNYHEJJ-UHFFFAOYSA-N geranyl acetone Natural products CC(C)=CCCC(C)=CCCC(C)=O HNZUNIKWNYHEJJ-UHFFFAOYSA-N 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- -1 heterocycle compound Chemical class 0.000 description 1
- 125000000623 heterocyclic group Chemical group 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000001819 mass spectrum Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- FLIACVVOZYBSBS-GZXVCZRGSA-N methyl hexadecanoate Chemical group CCCCCCCCCCCCCCC[14C](=O)OC FLIACVVOZYBSBS-GZXVCZRGSA-N 0.000 description 1
- DVWSXZIHSUZZKJ-YSTUJMKBSA-N methyl linolenate Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCC(=O)OC DVWSXZIHSUZZKJ-YSTUJMKBSA-N 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- 238000010606 normalization Methods 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- VHGBWHGICRTHIQ-UHFFFAOYSA-N phytadiene Natural products CCCCCCCCCCCCCCCC=C(/C)C=C VHGBWHGICRTHIQ-UHFFFAOYSA-N 0.000 description 1
- 235000019633 pungent taste Nutrition 0.000 description 1
- 238000013102 re-test Methods 0.000 description 1
- 239000003507 refrigerant Substances 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24C—MACHINES FOR MAKING CIGARS OR CIGARETTES
- A24C5/00—Making cigarettes; Making tipping materials for, or attaching filters or mouthpieces to, cigars or cigarettes
- A24C5/52—Incorporating filters or mouthpieces into a cigarette rod or a tobacco rod
-
- A24F47/008—
Landscapes
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
A kind of preparation method and applications for heating the cigarette that do not burn, using embossing roll-in new process, make to have certain thickness heating not burnt reconstituted tobacco surface irregularity, increase surface area, strengthen atomizing effect, increase skin-friction force, and use embossing clad aluminum foil cigarette paper, when making rolling up and connecting machine cigarette driving on the later stage, between the aluminium foil patterned surface of reconstituted tobacco and cigarette Material cladding aluminium foil cigarette paper, friction significantly strengthens, it is easy to process, the equipment parking frequency is reduced, production is carried out continuously, production efficiency is improved, reduces Material Cost and production cost；And low temperature cigarette pipe tobacco section is shorter, increase friction, which helps to reduce pipe tobacco, drops, and overcomes heating frictional force between the smooth embossing aluminium-foil paper non-with lapping in reconstituted tobacco surface of not burning smaller, skids seriously, cigarette paper band is motionless to cause equipment frequently to stop, and influences production efficiency；And low temperature cigarette pipe tobacco section is shorter, the defects of its small low temperature pipe tobacco of frictional force easily drops.
Description
Technical field
The present invention relates to heat novel tobacco field of not burning, and in particular to a kind of preparation method for heating the cigarette that do not burn
And its application.
Background technology
Heating do not burn reconstituted tobacco be one kind based on tobacco component, load heavy dose of Alevaire, when use passes through
High-temperature heating release Alevaire, forms the functional form reconstituted tobacco of haze effect.It is non-ignitable to the heating by external heat element
Reconstituted tobacco is burnt to be heated, make flavor component of Alevaire in reconstituted tobacco cigarette, tobacco and spices etc. by heating and
It is not that burning produces smog, reduces by harmful components caused by burning in traditional cigarette and thermal cracking.
Heating do not burn reconstituted tobacco process cigarette into Cigarette when, do not burn reconstituted tobacco surface there are the heating
The smooth frictional force between its lapping aluminium-foil paper aluminium foil surface is smaller, skids serious, cigarette paper band is motionless to cause equipment frequent
Parking, influences production efficiency；And low temperature cigarette pipe tobacco section is shorter, the defects of its small pipe tobacco of frictional force easily drops.
The content of the invention
According to it is above-mentioned deficiency and defect, the object of the present invention is to provide it is a kind of heat do not burn cigarette preparation method and its
Using, in last one of pressure roller process of roll-in method technique, one in two pressure rollers is used into knurling rolls, to roll-in method heating not
Burning reconstituted tobacco is embossed, and is made to have certain thickness heating not burnt reconstituted tobacco surface irregularity, is increased surface area,
Strengthen atomizing effect, increase skin-friction force, and using embossing clad aluminum foil cigarette paper cigarette, open later stage upper rolling up and connecting machine cigarette
Che Shi, rubbing between thin slice and aluminium foil cigarette paper aluminium foil surface significantly strengthens, easy to process, reduces the equipment parking frequency, enables production
Enough it is carried out continuously, improves production efficiency, reduces Material Cost and production cost；And low temperature cigarette pipe tobacco section is shorter, increase friction
Help to reduce pipe tobacco and drop, overcoming the heating not burn, reconstituted tobacco surface is smooth non-with lapping embosses between aluminium-foil paper
Frictional force is smaller, skids serious, cigarette paper band is motionless to cause equipment frequently to stop, and influences production efficiency；And low temperature cigarette pipe tobacco
The defects of section is shorter, its small low temperature pipe tobacco of frictional force easily drops.
The present invention is achieved through the following technical solutions：
A kind of preparation method for heating the cigarette that do not burn, includes the following steps：
(1) raw material prepares：Prepare raw material by percent mass proportioning：Tobacco material 50-70%, Alevaire 10~25%, consolidate
Body adhesive 3~10%, cigarette additive 1~10%, fiber 1~10%, warm water 15~35%；
(2) dry material co-grinding：Tobacco material, solid adhesive and solid cigarette additive calcium salt are put into proportion
In pulverizer, the mesh of 40 mesh~300 is crushed to, crushes and is uniformly mixed through low-temperature and high-speed at this time；
(3) wet stock mixing is uniformly dispersed：Fiber and warm water are poured into material barrel in proportion, while high-speed stirred, are adopted
Discongest fiber with ultrasonic cavitation effect auxiliary, it is scattered evenly, add above-mentioned steps 1) Alevaire of quality proportioning, after
Continuous ultrasonic wave added high-speed stirred makes fiber and Alevaire be uniformly dispersed, while wet stock and tobacco aromaticss are slowly added into above-mentioned step
In rapid 2) described uniformly mixed dry material powder, high-speed stirred is uniform together；
(4) it is embossed roll-in：Reconstituted tobacco is obtained through 3~9 roll pressings, during last one of pressure roller process, using embossing pressure roller
Roll-in is embossed to reconstituted tobacco, reheats drying, the method that is rolled heats the embossing reconstituted tobacco that do not burn；
(5) cigarette is packed：By cigarette process specification carry out the roll-in method heating do not burn embossing reconstituted tobacco cigarette bag
Fill, cigarette packaging is carried out using embossing clad aluminum foil cigarette paper, filter stick for cigarettes etc., be adding for raising production efficiency of the invention
The hot cigarette that do not burn.
Further, the tobacco material is tobacco leaf, one kind in offal or its mixing.
Further, the cigarette additive is tobacco aromaticss and calcium salt, and the calcium salt is calcium carbonate, calcium lactate, lemon
One or more of mixing in lemon acid calcium, calcium tartrate.
Further, the low-temperature grinding is 0~4 DEG C, 40-300 mesh.
Further, the solid adhesive be sodium alginate, potassium alginate, CMC (carboxymethyl cellulose), PAC it is (poly-
Anionic cellulose), polyvinyl alcohol, casein glue, rosin, dextrin, chitosan, sodium glycero-phosphate etc. it is therein one or more of
Mixing.
Further, the fiber for wood pulp, cigarette pole fiber, bagasse pulp, bamboo pulp, cocoanut fiber etc. it is therein a kind of or
Several mixing.
Further, the temperature of the warm water is 30~60 DEG C.
Further, the Alevaire is glycerine, propane diols, ethylene glycol one or more of mixing therein.
Further, the speed of the high-speed stirred is 300~1200r/min.
Further, the ultrasonic frequency is 20~130KHz.
Further, the do not burn thickness of reconstituted tobacco of the heating be 0.21~0.30mm, elongation at break is 1.0~
1.6%, tensile strength is 300~450N/m.
Further, the embossing clad aluminum foil cigarette paper, be twill or it is unordered embossing clad aluminum foil cigarette paper, wherein
It is 1~19 μm to emboss aluminum foil thickness, and the thickness of cigarette paper is 20~200 μm.
It is a kind of as the above method prepare heating do not burn cigarette electrical heating or carbon heating low temperature cigarette in apply.
The heating that the present invention improves production efficiency is not burnt cigarette, its reconstituted tobacco surface irregularity, enhancing atomization effect
Fruit, increases skin-friction force, and later stage upper rolling up and connecting machine cigarette is driven as cigarette material using embossing clad aluminum foil cigarette paper
When, the friction between the embossed aluminum foil face of thin slice and clad aluminum foil cigarette paper significantly strengthens, easy to process, reduces equipment parking frequency
It is secondary, production is carried out continuously, improve production efficiency, reduce Material Cost and production cost；And low temperature cigarette pipe tobacco section compared with
It is short, increase friction contribute to reduce cigarette end pipe tobacco drop, overcome the heating do not burn reconstituted tobacco surface it is smooth with parcel
Frictional force is smaller between the non-embossing aluminium-foil paper of material, skids serious, cigarette paper band is motionless to cause equipment frequently to stop, and influences to produce
Efficiency；And low temperature cigarette pipe tobacco section is shorter, the defects of its small end low temperature pipe tobacco of frictional force easily drops.
The beneficial effects of the invention are as follows：
(1) reconstituted tobacco that do not burn is heated using roll-in method, and be applied in the low temperature cigarettes such as electrical heating, charcoal heating, it is right
Than traditional cigarette, the tobacco material usage amount of every cigarette is reduced up to 20~50%, and tobacco material cost declines, and tobacco material
With the heated volatilization of tobacco aromaticss, without burning and thermal cracking, flue gas harm is reduced.
(2) it is using tobacco material, solid adhesive, solid calcium salt co-grinding to fine powder the characteristics of present invention process
(40-300 mesh) so that tobacco material, adhesive, solid calcium salt (including calcium carbonate, calcium lactate, calcium citrate, calcium tartrate etc.
In one or more) dispersion mixing it is uniform while, increase specific surface area simultaneously produce new microcellular structure, it is right to effectively improve its
The absorbability of Alevaire, improves the gas porosity and increase thickness of reconstituted tobacco, increase suction comfort level；And fiber and water premix,
Discongest, then mixed with Alevaire, be to reach homogenizing effect using high-speed stirred, make fiber abundant in water-Alevaire system
It is swollen, effectively interweaves between fiber, then the wet stock of fiber-water-Alevaire is slowly poured into the thin of tobacco-adhesive-calcium salt
In powder carry out high-speed stirred it is uniform so that tobacco fine powder is completely dispersed with adhesive, fiber and mixes, and between fiber, fiber and
Peripheral adhesive good bonding, makes reconstituted tobacco possess certain intensity, reduces powder rate, strengthens resist processing, shorten mixing,
The time of agitating procedure, overcome common roll-in method technique prepare roll-in method heating do not burn reconstituted tobacco when, fiber is in water
After middle defibering, first mix with tobacco powder, then mixed with remaining material, fiber can not be uniformly dispersed, easily agglomerating, manufactured
Fiber and the extremely non-uniform defect of Alevaire, tobacco in reconstituted tobacco；
(3) solid adhesive is sodium alginate, potassium alginate, CMC (carboxymethyl cellulose), PAC (polyanion fibers
Element), polyvinyl alcohol, casein glue, rosin, dextrin, chitosan, sodium glycero-phosphate, fiber and tobacco material can be helped to be tightly combined,
The tensile strength for heating the reconstituted tobacco that do not burn is improved, and there is collaboration to increase for the mixing such as chitosan-sodium glycero-phosphate therein
Effect increase adhesive action；Natural fiber has the function that to increase reconstituted tobacco intensity, improves resist processing；
(4) present invention is through 3~9 roll-ins so that fiber and tobacco disperse evenly, to add the heating and do not burn reconstruction
The density of tobacco leaf, intensity, thickness, improve its tensile strength and elongation at break, and in last one of pressure roller process, adopt
Roll-in is embossed to reconstituted tobacco with embossing pressure roller, then is thermally dried, the method that is rolled heats embossing reconstruction of not burning
Tobacco leaf, its reconstituted tobacco surface irregularity, strengthens atomizing effect, increases skin-friction force；
(5) twill or unordered embossing clad aluminum foil cigarette paper, filter stick for cigarettes for using etc. carry out cigarette packaging, make on the later stage
When rolling up and connecting machine cigarette is driven, rubbing between thin slice and the decorative pattern aluminium foil surface for embossing clad aluminum foil cigarette paper significantly strengthens, easy to process,
The equipment parking frequency is reduced, production is carried out continuously, improves production efficiency, reduce Material Cost and production cost；It is and low
Warm rolling cigarette pipe tobacco section is shorter, and increase friction, which helps to reduce cigarette end pipe tobacco, drops, and overcomes the heating not burn reconstituted tobacco
Frictional force is smaller between the smooth non-embossing aluminium-foil paper with lapping in surface, skids serious, and cigarette paper band is motionless to cause equipment frequency
Numerous parking, influences production efficiency；And low temperature cigarette pipe tobacco section is shorter, its small low temperature cigarette end pipe tobacco of frictional force, which easily drops, etc. lacks
Fall into.
And the embossing clad aluminum foil cigarette paper of the present invention is relatively thin, wherein embossing aluminum foil thickness is 1~19 μm, cigarette paper
Thickness is 20~200 μm, with authorizing invention " a kind of Composite flame-retardant electrical heating cigarette paper and preparation method thereof " to compare, the contrast
Invention is that the thickness of metal foil is 20~60 μm, and the thickness of cigarette paper is 40~100 μm, Comparatively speaking, clad aluminum of the invention
In paper tinsel cigarette paper, aluminum foil thickness substantially reduces, and aluminium foil is thinner, and aluminium foil used in composite aluminium foil paper unit area is fewer, aluminium foil cigarette
Paper cost is lower, and compound aluminium foil cigarette paper is more soft, and smaller to the tool wear of cutting in production, cigarette is taken round at mouth
Sliding, blocked up aluminium foil is taking meeting at mouth because soldering iron is deformed, it is impossible to springs back, influences cigarette beauty.
Present invention process condition is simply gentle, can realize the production for heating the reconstituted tobacco cigarette that do not burn, and production efficiency
Height, in electrical heating, charcoal heating novel tobacco product, has larger prospects for commercial application.
Brief description of the drawings
Fig. 1 is the structure diagram that the present invention heats the cigarette that do not burn；
Fig. 2 is to heat the cigarette end that do not burn to drop the measure schematic diagram of pipe tobacco amount；
Fig. 3 be the heating of 65 μm of PDMS/DVB solid phase microextraction roll-in methods do not burn reconstituted tobacco volatile ingredient always from
Subflow chromatogram.
Embodiment
The present invention is described in detail below in conjunction with specific embodiment.
Embodiment 1
A kind of preparation method for heating the cigarette that do not burn, including following technical step：
(1) raw material prepares：Prepare raw material by percent mass proportioning：Tobacco material 50%, Alevaire glycerine 25%, solid gum
Stick (sodium alginate, potassium alginate, CMC, PAC) 5%, cigarette additive 5% (solid calcium salt 3%, tobacco aromaticss 2%), fibre
Dimension (wood fibre and cocoanut fiber, in mass ratio 4:1) 2%, 45 DEG C of warm water 18%；
(2) dry material co-grinding：By tobacco material, solid adhesive and solid cigarette additive (calcium carbonate, lactic acid
Calcium, by mass percentage 2% and 1%) to be put into proportion in Lowtemperaturepulverizer, 2 DEG C are crushed to 200 mesh, are uniformly mixed；
(3) wet stock mixing is uniformly dispersed：Fiber and 45 DEG C of warm water are poured into material barrel in proportion, 400r/min high-speed stirrings
While mixing, discongest fiber using 50KHz ultrasonic cavitations effect auxiliary, disperse evenly, to add above-mentioned steps 1) matter
The Alevaire of proportioning is measured, continuing 50KHz ultrasonic wave added 400r/min high-speed stirreds makes fiber and Alevaire be uniformly dispersed, and at the same time will
Wet stock and tobacco aromaticss are slowly added into above-mentioned steps 2) in the uniformly mixed dry material powder, 400r/min is at a high speed together
Stir evenly；
(4) it is embossed roll-in：Reconstituted tobacco is obtained through 5 tanning roll pressings, during No. the 6th pressure roller process, using embossing pressure roller pair
Reconstituted tobacco is embossed roll-in, then 70 DEG C of heat dryings, and the method that is rolled heats the embossing reconstituted tobacco that do not burn；
(5) cigarette is packed：By cigarette process specification carry out the roll-in method heating do not burn embossing reconstituted tobacco cigarette bag
Dress, uses twill embossing clad aluminum foil cigarette paper (wherein embossing aluminum foil thickness as 10 μm, the thickness of cigarette paper is 100 μm), cigarette
Cigarette is carried out with filter stick etc. to pack, and is that the heating of the raising production efficiency of the present invention is not burnt cigarette, as shown in Figure 1.
The heating is not burnt, and reconstituted tobacco intensity is good, and frictional force is strong between reconstituted tobacco and aluminium foil when cigarette is processed, process
Continuity is good, and production efficiency is high, and made low temperature cigarette cigarette heats in electrical heating utensil or as carbon heating low temperature
Cigarette, smog release is uniform, and amount of smoke is big, and satisfaction is strong, has this perfume of tobacco, and simulation suction sensory effects are preferable.
Embodiment 2
A kind of preparation method for heating the cigarette that do not burn, including following technical step：
(1) raw material prepares：Prepare raw material by percent mass proportioning：Tobacco material 65%, Alevaire 11% (glycerine, the third two
Alcohol, ethylene glycol by mass percentage be respectively 6%, 3%, 2%), solid adhesive 4%, 3.5% (solid calcium of cigarette additive
Salt 3%, tobacco aromaticss peppermint 0.5%), fiber 1.5% (cigarette pole fiber, bagasse pulp by mass percentage be respectively 1% and
0.5%), 55 DEG C of warm water 15%；
(2) dry material co-grinding：By tobacco material, solid adhesive and solid cigarette additive (calcium carbonate, citric acid
Calcium, calcium tartrate are respectively 1%) to be put into proportion in liquid nitrogen cryogenics pulverizer by mass percentage, and 3 DEG C are crushed to 240 mesh, this
When through low-temperature and high-speed crush and be uniformly mixed；
(3) wet stock mixing is uniformly dispersed：Fiber is poured into material barrel in proportion with warm water, 500r/min high-speed stirreds
Meanwhile discongest fiber using 80KHz ultrasonic cavitations effect auxiliary, it is scattered evenly, add above-mentioned steps 1) quality matches somebody with somebody
The Alevaire of ratio, continuing 80KHz ultrasonic wave added 500r/min high-speed stirreds makes fiber and Alevaire be uniformly dispersed, while by wet thing
Material and tobacco aromaticss are slowly added into above-mentioned steps 2) in the uniformly mixed dry material powder, 500r/min high-speed stirreds together
Uniformly；
(4) it is embossed roll-in：Reconstituted tobacco is obtained through 6 tanning roll pressings, during No. the 7th pressure roller process, using embossing pressure roller pair
Reconstituted tobacco is embossed roll-in, then 60 DEG C of heat dryings, and the method that is rolled heats the embossing reconstituted tobacco that do not burn；
(5) cigarette is packed：By cigarette process specification carry out the roll-in method heating do not burn embossing reconstituted tobacco cigarette bag
Dress, uses unordered embossing clad aluminum foil cigarette paper (wherein embossing aluminum foil thickness as 8 μm, the thickness of cigarette paper is 120 μm), cigarette to use
Filter stick etc. carries out cigarette packaging, is that the heating of the raising production efficiency of the present invention is not burnt cigarette.
The heating is not burnt, and reconstituted tobacco intensity is good, and frictional force is strong between reconstituted tobacco and aluminium foil when cigarette is processed, process
Continuity is good, and production efficiency is high, and made low temperature cigarette cigarette heats in electrical heating utensil or as carbon heating low temperature
Cigarette, smog release is uniform, and amount of smoke is big, and satisfaction is strong, has this perfume of tobacco and peppermint refrigerant sense, throat is comfortable, mould
It is preferable to intend suction sensory effects.
Embodiment 3
A kind of preparation method for heating the cigarette that do not burn, including following technical step：
(1) raw material prepares：Prepare raw material by percent mass proportioning：Tobacco material 70%, Alevaire 10% (glycerine, the third two
Alcohol account for mass percent be respectively 8% and 2%), solid adhesive 3% (rosin, chitosan, sodium glycero-phosphate for etc. quality
Than), cigarette additive 1% (calcium carbonate 0.5%, tobacco extract 0.5%), fiber 1% (mass ratio such as wood pulp, bamboo pulp), 60
DEG C warm water 15%；
(2) dry material co-grinding：Tobacco material, solid adhesive and solid cigarette additive calcium salt are put into proportion
In liquid nitrogen cryogenics pulverizer, 4 DEG C are crushed to 300 mesh, crush and are uniformly mixed through low-temperature and high-speed at this time；
(3) wet stock mixing is uniformly dispersed：Fiber is poured into material barrel in proportion with warm water, 600r/min high-speed stirreds
Meanwhile discongest fiber using 120KHz ultrasonic cavitations effect auxiliary, it is scattered evenly, add above-mentioned steps 1) quality matches somebody with somebody
The Alevaire of ratio, continuing 120KHz ultrasonic wave added 600r/min high-speed stirreds makes fiber and Alevaire be uniformly dispersed, while will be wet
Material and tobacco aromaticss are slowly added into above-mentioned steps 2) in the uniformly mixed dry material powder, 600r/min high-speed stirrings together
Mix uniformly；
(4) it is embossed roll-in：Reconstituted tobacco is obtained through 8 tanning roll pressings, during the 9th pressure roller process, using embossing pressure roller pair
Reconstituted tobacco is embossed roll-in, then 65 DEG C of heat dryings, and the method that is rolled heats the embossing reconstituted tobacco that do not burn；
(5) cigarette is packed：By cigarette process specification carry out the roll-in method heating do not burn embossing reconstituted tobacco cigarette bag
Dress, uses the embossing clad aluminum foil cigarette paper of staggeredly decorative pattern (wherein to emboss aluminum foil thickness as 6 μm, the thickness of cigarette paper is 80 μ
M), filter stick for cigarettes etc. carries out unordered pipe tobacco cigarette packaging, is that the heating of the raising production efficiency of the present invention is not burnt cigarette.
The heating is not burnt, and reconstituted tobacco intensity is good, and frictional force is strong between reconstituted tobacco and aluminium foil when cigarette is processed, process
Continuity is good, and production efficiency is high, and made low temperature cigarette cigarette heats in electrical heating utensil or as carbon heating low temperature
Cigarette, smog release is uniform, and amount of smoke is big, and satisfaction is strong, and flue gas concentration is higher, has this perfume of tobacco, throat is comfortable, mould
It is preferable to intend suction sensory effects.
Test example 1：Application effect contrasts
By roll-in method prepared by embodiment 1-3 heating do not burn reconstituted tobacco and the manufacture of routinely rolling process heating not
Burning reconstituted tobacco is contrasted, the results showed that：Roll-in method provided by the invention heats the reconstituted tobacco that do not burn, and is atomized agent content
While higher, it is evenly distributed, surface adhesion, and its fiber content improves, and uniform, reconstituted tobacco is crushed in reconstituted tobacco
Intensity improves, and resist processing is good, and intensity improving rate is up to 35.71%, and production efficiency improves more than 25% compared to control；And take out
Suction is more smooth, and satisfaction is strong, has this perfume of tobacco, and simulation suction sensory effects are preferable；Cigarette end tobacco-falling quantity reduces 20~
40%.
(1) present invention heats the intensity detection of the reconstituted tobacco for the cigarette that do not burn
The roll-forming of high atomization amount reconstituted tobacco, intensity are important indicators.
Detection method, with reference to GB/T 12914-2008 paper and the measure of cardboard tensile strength.
Testing principle：Under conditions of constant rate of extension, the sample of given size is stretched to fracture, measures its tension stress.
If desired, the elongation of sample can be measured, its maximum tension stress is recorded.
Instrument：TTM-30 computer tensile testing machines.
Collet：Two, in order to clamp the sample of Rack, each collet should be firm by the overall with of sample along straight line
Clamp, should not damage or slide sample.Collet should be furnished with the component for adjusting grip force.
Testing procedure：
1st, thin slice is cut into 15mm wide, 200mm long.
2nd, measured according to GB/T 12914.
3rd, rejected in measurement result do not cement, come off, non-integral fracture test sample.
Test result such as following table：
1 roll-in method of table heats reconstituted tobacco intensity of not burning
| Sample | Grammes per square metre g/m2 | Tensile strength N/m | Elongation at break % |
| Embodiment 1 | 184 | 312 | 1.1 |
| Embodiment 2 | 201 | 328 | 1.2 |
| Embodiment 3 | 220 | 380 | 1.3 |
| Control | 160 | 280 | 0.8 |
(2) present invention heats the sensory evaluation for the cigarette that do not burn
The do not burn aesthetic quality of cigarette of heating to the present invention compares progress comparative evaluation with it, and control sample cigarette is
Common roll-in method technique heats the reconstituted tobacco that do not burn and is prepared with smooth surface clad aluminum foil cigarette paper, the results are shown in Table 2.
The present invention of table 2 heats the sensory evaluation for the cigarette that do not burn
The cigarette the result shows that heating of the invention is not burnt, amount of smoke is big, and release is uniform, and satisfaction is strong, has tobacco sheet
Perfume (or spice), simulation suction sensory effects are preferable.
(3) present invention heating cigarette end pipe tobacco that do not burn drops test comparison
Dropped the current methods ISO3550-1 of pipe tobacco using test cigarette end《Cigarette end drops the measure the 1st of pipe tobacco
Part：Rotate cage method》The cigarette end pipe tobacco that drops that do not burn to heating is measured.
Instrument：YDZ-II type cigarette end tobacco-falling measuring instruments (vibratory drilling method), (rotation of E44 type cigarette end tobacco-fallings measuring instrument
Cage method).
Method：By the requirement of ISO3402, sample balanced in (22+1) DEG C, RH (60+3) % environment more than 48h, 10d with
It is interior.
Parameter setting：ISO3550-2 measuring instruments velocity of rotation is 60rpm, rotates 2min.
Cigarette end drops the measure of pipe tobacco：Using ISO3550-2 to every kind of cigarette sample difference retest 40 times, survey
Test result is shown in Table 3 and Fig. 2.
Table 3 heats the cigarette end that do not burn and drops the measure of pipe tobacco amount
| Sample | Cigarette end tobacco-falling quantity (mg/cig) |
| Embodiment 1 | 8 |
| Embodiment 2 | 7 |
| Embodiment 3 | 6 |
| Control | 10 |
As a result as shown in Table 3 and Figure 2, the do not burn end tobacco-falling quantity of cigarette of heating of the invention is compared with control, is reduced
20~40%.
Test example 2：The heating that the present invention improves roll-in method technique is not burnt reconstituted tobacco volatile chemical component HS-
SPME-GC/MS is analyzed
Roll-in method technique is improved using 65 μm of PDMS/DVB (polydivinylbenezene) of solid phase micro-extracting head to the present invention to prepare
Heating do not burn reconstituted tobacco, test and analyze its aroma volatile using gaseous mass spectrum.
1 materials and methods
1.1 medicines and instrument
The present invention improves heating prepared by roll-in method technique and does not burn reconstituted tobacco；
Digital display thermostat water bath AHYQ HH-6：Changzhou Ao Hua Instrument Ltd.；Balance CP2202S-OCE：
Sartorius AG Germany；Manual SPME sample introductions handle, manual extracting fiber head (65 μm of poly- divinyl of PDMS/DVB
The special headspace extraction sample bottle of benzene, 15mL：Supelco companies of the U.S.；II type gas chromatography/mass spectrometries of TRACE GC Ultra-DSQ
(GC/MS) combined instrument：Thermoelectricity Science and Technology Ltd. of the U.S..
1.2 method
1.2.1 SPME conditions
Weigh the present invention and improve heating prepared by roll-in method technique and do not burn reconstituted tobacco sample 1g, shred straight to 0.2cm
Footpath fragment, is placed in the special headspace extraction sample bottles of 15mL, is inserted into the extracting head of aging, at a certain temperature pre-equilibration
10min, extraction certain time are stand-by.Extracting head aging：250 DEG C of aging 30min of injection port.
1.2.2 GC/MS analysis conditions
1.2.1.1 chromatographic condition
50 DEG C of column initial temperature, keeps 2min, is warming up to 180 DEG C with the speed of 8 DEG C/min, keeps 1min, then with 18 DEG C/min
Speed be warming up to 280 DEG C, keep 30min；Carrier gas is helium (He, purity 99.99%), constant current mode, flow velocity 1.0mL/
min；Split sampling mode, split ratio 1：10, solvent-free delay；250 DEG C of injector temperature.
1.2.1.2 Mass Spectrometry Conditions
Ionization mode：EI sources；Electron energy:70eV；Multiplier voltage：1.2kV；Ion source temperature：230℃；Level Four bar
Temperature:150℃；Interface temperature：280 DEG C, 280 DEG C of transmission line；Scanning range：33m/z~350m/z.Use NIST standard spectrums storehouse
Retrieval analysis is carried out, compound percentage contents are calculated by areas of peak normalization method.
2 results and analysis
The heating that the preparation of roll-in method technique is improved using the present invention does not burn reconstituted tobacco as research object, using extracting head 65
μm PDMS/DVB carries out HS-SPME-GC-MS detection and analysis, and total ion chromatogram is shown in Fig. 3, and volatile chemical component mainly collects
In in 14~25min, refer to table 4.The present invention of table 4 improve heating prepared by roll-in method technique do not burn reconstituted tobacco volatility into
The HS-SPME-GC/MS divided
Analysis
As shown in upper table 4, it is micro- through head space-solid phase that the present invention improves heating prepared by the roll-in method technique reconstituted tobacco that do not burn
Extraction-gaschromatographic mass spectrometry detection, identifies 84 kinds of volatile ingredients, total percentage contents are 97.91%, including alkene
Class 10 kinds (64.15%), esters 19 kinds (9.41%), ketone 19 kinds (7.45%), alcohols 11 kinds (1.84%), 3 kinds of acid
(0.45%), aldehyde 3 kinds (0.34%), alkane 2 kinds (0.21%), 19 kinds of other heterocycle compounds.From the point of view of single component, relatively
Highest percentage composition is neophytadiene (63.74%), and neophytadiene is a kind of C20 polyisoprenoids, is waved in tobacco neutrality
Content highest in stimulating food, is flavor matter important in tobacco leaf, which is the chlorophyll contained in tobacco leaf in ripe and modulation
During degraded form leaf-alcohol, then be further dehydrated by leaf-alcohol and formed.Neophytadiene itself has faint scent and irritation
It is smaller, and chlorophyll and phytol then have blue foreign smell, as chlorophyll and phytol largely change into newly in modulated process
Phytadiene, the blue foreign smell of tobacco leaf eliminates, and then produces faint scent.Neophytadiene can be directly entered flue gas in result of combustion of tobacco, tool
It is reduced the effect of irritation, alcohol and flue gas.Carrier of the neophytadiene as aroma substance in trapping flue gas aerosol, has and takes
Enter the ability of flue gas with Volatile infochemicals in tobacco leaf and aroma component, therefore be the important fumet of tobacco leaf again；Next is
á-nicotine (11.73%), is the important activity component in tobacco, has penetrating odor and pungent taste, and band gives people full
Foot sense；It is methyl hexadecanoate (3.61%) again；4th is geranyl acetone (1.94%), and the 5th is methyl linolenate
(1.92%).The aroma components such as all these aldehydes, alcohols, ketone, esters, alkanes, heterocycle compound, aromatic hydrocarbon
Bring roll-in method and heat the reconstituted tobacco that do not burn and enrich and coordinate cigarette perfume, good satisfaction, simulation cigarette suction effect is good.
The above description is merely a specific embodiment, but protection scope of the present invention is not limited thereto, any
Belong to those skilled in the art the invention discloses technical scope in, the change or replacement that can readily occur in, all should
It is included within the scope of the present invention.
Claims (10)
1. a kind of preparation method for heating the cigarette that do not burn, it is characterised in that include the following steps：
(1) raw material prepares：Prepare raw material by percent mass proportioning：Tobacco material 50-70%, Alevaire 10~25%, solid gum
Stick 3~10%, cigarette additive 1~10%, fiber 1~10%, warm water 15~35%；
(2) dry material co-grinding：Tobacco material, solid adhesive and solid cigarette additive calcium salt are put into low temperature in proportion
In pulverizer, the mesh of low-temperature grinding to 40 mesh~300, crushes and is uniformly mixed through low-temperature and high-speed at this time；
(3) wet stock mixing is uniformly dispersed：Fiber and warm water are poured into material barrel in proportion, while high-speed stirred, using super
Sound wave cavitation auxiliary discongests fiber, disperses evenly, to add the Alevaire of above-mentioned steps (1) quality proportioning, continues
Ultrasonic wave added high-speed stirred makes fiber and Alevaire be uniformly dispersed, while wet stock and tobacco aromaticss are slowly added into above-mentioned steps
(2) in the uniformly mixed dry material powder, high-speed stirred is uniform together；
(4) it is embossed roll-in：Reconstituted tobacco is obtained through 3~9 roll pressings, during last one of pressure roller process, using embossing pressure roller to again
Make tobacco leaf and be embossed roll-in, reheat drying, the method that is rolled heats the embossing reconstituted tobacco that do not burn；
(5) cigarette is packed：By cigarette process specification carry out the roll-in method heating do not burn embossing reconstituted tobacco cigarette pack, adopt
Carried out cigarette with embossing clad aluminum foil cigarette paper, filter stick for cigarettes and packed, the heating of the as raising production efficiency of the present invention is non-ignitable
Burn cigarette.
The preparation method of cigarette 2. heating as claimed in claim 1 is not burnt, it is characterised in that：The tobacco material is cigarette
One kind or its mixing in leaf, offal.
The preparation method of cigarette 3. heating as claimed in claim 1 is not burnt, it is characterised in that：The cigarette additive is
Tobacco aromaticss and calcium salt, the calcium salt is calcium carbonate, one or more of mixing in calcium lactate, calcium citrate, calcium tartrate.
The preparation method of cigarette 4. heating as claimed in claim 1 is not burnt, it is characterised in that：The low-temperature grinding is 0
~4 DEG C, 40-300 mesh.
The preparation method of cigarette 5. heating as claimed in claim 1 is not burnt, it is characterised in that：The solid adhesive is
Sodium alginate, potassium alginate, carboxymethyl cellulose, polyanion cellulose, polyvinyl alcohol, casein glue, rosin, dextrin, shell gather
One or more of mixing therein such as sugar, sodium glycero-phosphate.
The preparation method of cigarette 6. heating as claimed in claim 1 is not burnt, it is characterised in that：The fiber for wood pulp,
One or more of mixing in cigarette pole fiber, bagasse pulp, bamboo pulp, cocoanut fiber.
The preparation method of cigarette 7. heating as claimed in claim 1 is not burnt, it is characterised in that：The temperature of the warm water is 30
~60 DEG C.
The preparation method of cigarette 8. heating as claimed in claim 1 is not burnt, it is characterised in that：The Alevaire is sweet
The one or more of mixing therein of oil, propane diols, ethylene glycol.
The preparation method of cigarette 9. heating as claimed in claim 1 is not burnt, it is characterised in that：The embossing aluminium foil cigarette
Paper, is twill or unordered pre-embossed aluminium-foil paper, wherein embossing aluminum foil thickness is 1~19 μm, the thickness of cigarette paper is 20~200 μ
m。
10. heating prepared by a kind of method any one of claim 1-9 is not burnt, cigarette is low in electrical heating or carbon heating
Applied in warm rolling cigarette.
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|---|---|---|---|
| CN201711312963.5A CN107981405B (en) | 2017-12-12 | 2017-12-12 | Preparation method and application of cigarette without burning by heating |
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|---|---|---|---|
| CN201711312963.5A CN107981405B (en) | 2017-12-12 | 2017-12-12 | Preparation method and application of cigarette without burning by heating |
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| CN107981405B CN107981405B (en) | 2020-03-10 |
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Cited By (28)
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| CN108783562A (en) * | 2018-07-02 | 2018-11-13 | 云南拓宝科技有限公司 | A kind of pipe tobacco preparation method suitable for new cigarette |
| CN108783584A (en) * | 2018-07-20 | 2018-11-13 | 东莞市香草生物工程有限公司 | A kind of sugarcane crude fibre health-care cigarette and preparation method and sugarcane crude fibre health tobacco composition and application |
| CN108936781A (en) * | 2018-09-17 | 2018-12-07 | 中烟施伟策（云南）再造烟叶有限公司 | The method for heating cigarette sucked material of not burning using wet granulation preparation |
| CN108936780A (en) * | 2018-09-17 | 2018-12-07 | 中烟施伟策（云南）再造烟叶有限公司 | The method for heating cigarette sucked material of not burning using centrifugal process granulation preparation |
| CN108949347A (en) * | 2018-06-08 | 2018-12-07 | 湖北中烟工业有限责任公司 | Increase the essence and its preparation method and application for heating the new cigarette flue gas moist feeling that do not burn |
| CN109288137A (en) * | 2018-11-21 | 2019-02-01 | 湖北中烟工业有限责任公司 | A kind of pipe tobacco preparation method and applications for adding Alevaire |
| CN109393577A (en) * | 2018-12-11 | 2019-03-01 | 何书杰 | A kind of plant is slices reconstituted, preparation method and electrical heating method |
| CN109602063A (en) * | 2019-02-01 | 2019-04-12 | 江苏中烟工业有限责任公司 | A kind of acid modification agent and its application method in low temperature cigarette reconstituted tobacoo |
| CN110055787A (en) * | 2019-04-11 | 2019-07-26 | 湖北中烟工业有限责任公司 | The method for preparing cigarette case or box packaging paper as raw material using tobacco rod |
| WO2019224015A1 (en) * | 2018-05-22 | 2019-11-28 | Hauni Maschinenbau Gmbh | Method for producing tobacco material for use in an hnb tobacco article and hnb tobacco article |
| CN110643303A (en) * | 2019-08-23 | 2020-01-03 | 广东中烟工业有限责任公司 | Adhesive for heating non-combustible tobacco products and application thereof |
| CN110679984A (en) * | 2019-11-15 | 2020-01-14 | 湖北中烟工业有限责任公司 | Preparation method of special slice for heating cigarettes |
| CN110742298A (en) * | 2019-11-15 | 2020-02-04 | 湖北中烟工业有限责任公司 | Method for preventing tobacco sheets from being adhered during storage |
| CN110934323A (en) * | 2020-01-07 | 2020-03-31 | 湖北中烟工业有限责任公司 | Method for preparing tobacco sheets by compounding gypsum whiskers |
| CN110934321A (en) * | 2020-01-07 | 2020-03-31 | 湖北中烟工业有限责任公司 | Method for preparing thermosensitive non-combustion tobacco sheet based on kraft lignin |
| CN110946320A (en) * | 2019-12-12 | 2020-04-03 | 河南卷烟工业烟草薄片有限公司 | Damp-proof heating non-combustion reconstituted tobacco, preparation method and application |
| WO2020098320A1 (en) * | 2018-11-14 | 2020-05-22 | 云南中烟工业有限责任公司 | Cigarette rod for circumferentially heating non-burning cigarette |
| CN111213909A (en) * | 2020-01-22 | 2020-06-02 | 云南中烟工业有限责任公司 | A cigarette containing flos Chrysanthemi extract and capable of reducing oral risk |
| CN111374343A (en) * | 2018-12-28 | 2020-07-07 | 湖南中烟工业有限责任公司 | Reconstituted tobacco for low-combustion-temperature cigarettes and preparation method thereof |
| CN111789279A (en) * | 2020-07-24 | 2020-10-20 | 吉林烟草工业有限责任公司 | Preparation method of tobacco leaf-imitated reconstituted tobacco |
| CN112334022A (en) * | 2018-06-29 | 2021-02-05 | 菲利普莫里斯生产公司 | Method for producing logs comprising material containing alkaloids |
| CN112334019A (en) * | 2018-06-29 | 2021-02-05 | 菲利普莫里斯生产公司 | Casting apparatus and method for producing a cast web of alkaloid containing material |
| CN112367867A (en) * | 2018-06-29 | 2021-02-12 | 尼科创业贸易有限公司 | Aerosol generating component for tobacco heating device and cigarette holder thereof |
| CN112914151A (en) * | 2021-02-01 | 2021-06-08 | 南通金源新材料有限公司 | Heating cigarette |
| CN112956725A (en) * | 2021-03-17 | 2021-06-15 | 云南中烟工业有限责任公司 | Double-layer composite paper filter stick for reconstituted tobacco and preparation method thereof |
| WO2021190036A1 (en) * | 2020-03-24 | 2021-09-30 | 青岛海大新星科技有限公司 | Heat-not-burn cartridge and auxiliary apparatus |
| CN113876018A (en) * | 2021-10-21 | 2022-01-04 | 湖北中烟工业有限责任公司 | Preparation method of special slice for homogenizing and heating cigarettes |
| RU2795492C2 (en) * | 2018-11-14 | 2023-05-04 | Чайна Табакко Юньнань Индастриал Ко., Лтд | Smoking part intended for use in a circular heated non-combustible cigarette |
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| WO2019224015A1 (en) * | 2018-05-22 | 2019-11-28 | Hauni Maschinenbau Gmbh | Method for producing tobacco material for use in an hnb tobacco article and hnb tobacco article |
| CN108949347A (en) * | 2018-06-08 | 2018-12-07 | 湖北中烟工业有限责任公司 | Increase the essence and its preparation method and application for heating the new cigarette flue gas moist feeling that do not burn |
| CN108949347B (en) * | 2018-06-08 | 2021-07-20 | 湖北中烟工业有限责任公司 | Essence for increasing smoke moisture of heated non-combustible cigarette and preparation method and application thereof |
| CN112334022A (en) * | 2018-06-29 | 2021-02-05 | 菲利普莫里斯生产公司 | Method for producing logs comprising material containing alkaloids |
| CN112334022B (en) * | 2018-06-29 | 2022-09-13 | 菲利普莫里斯生产公司 | Method for producing logs comprising material containing alkaloids |
| CN112334019B (en) * | 2018-06-29 | 2022-12-09 | 菲利普莫里斯生产公司 | Casting apparatus and method for producing a cast web of alkaloid containing material |
| CN112367867B (en) * | 2018-06-29 | 2024-06-11 | 尼科创业贸易有限公司 | Aerosol generating component for a tobacco heating device and mouthpiece therefor |
| CN112367867A (en) * | 2018-06-29 | 2021-02-12 | 尼科创业贸易有限公司 | Aerosol generating component for tobacco heating device and cigarette holder thereof |
| CN112334019A (en) * | 2018-06-29 | 2021-02-05 | 菲利普莫里斯生产公司 | Casting apparatus and method for producing a cast web of alkaloid containing material |
| CN108783562B (en) * | 2018-07-02 | 2021-08-31 | 云南拓宝科技有限公司 | Preparation method of tobacco shreds suitable for novel cigarettes |
| CN108783562A (en) * | 2018-07-02 | 2018-11-13 | 云南拓宝科技有限公司 | A kind of pipe tobacco preparation method suitable for new cigarette |
| CN108783584A (en) * | 2018-07-20 | 2018-11-13 | 东莞市香草生物工程有限公司 | A kind of sugarcane crude fibre health-care cigarette and preparation method and sugarcane crude fibre health tobacco composition and application |
| CN108936780A (en) * | 2018-09-17 | 2018-12-07 | 中烟施伟策（云南）再造烟叶有限公司 | The method for heating cigarette sucked material of not burning using centrifugal process granulation preparation |
| CN108936781A (en) * | 2018-09-17 | 2018-12-07 | 中烟施伟策（云南）再造烟叶有限公司 | The method for heating cigarette sucked material of not burning using wet granulation preparation |
| CN108936780B (en) * | 2018-09-17 | 2021-07-23 | 中烟施伟策（云南）再造烟叶有限公司 | Method for preparing smoking material for heating non-combustible cigarettes by utilizing centrifugal granulation |
| CN108936781B (en) * | 2018-09-17 | 2021-07-23 | 中烟施伟策（云南）再造烟叶有限公司 | Method for preparing smoking material for heating non-combustible cigarettes by wet granulation |
| RU2795492C2 (en) * | 2018-11-14 | 2023-05-04 | Чайна Табакко Юньнань Индастриал Ко., Лтд | Smoking part intended for use in a circular heated non-combustible cigarette |
| WO2020098320A1 (en) * | 2018-11-14 | 2020-05-22 | 云南中烟工业有限责任公司 | Cigarette rod for circumferentially heating non-burning cigarette |
| CN109288137A (en) * | 2018-11-21 | 2019-02-01 | 湖北中烟工业有限责任公司 | A kind of pipe tobacco preparation method and applications for adding Alevaire |
| CN109288137B (en) * | 2018-11-21 | 2020-11-03 | 湖北中烟工业有限责任公司 | Preparation method and application of tobacco shreds added with atomizing agent |
| CN109393577A (en) * | 2018-12-11 | 2019-03-01 | 何书杰 | A kind of plant is slices reconstituted, preparation method and electrical heating method |
| CN111374343A (en) * | 2018-12-28 | 2020-07-07 | 湖南中烟工业有限责任公司 | Reconstituted tobacco for low-combustion-temperature cigarettes and preparation method thereof |
| CN109602063A (en) * | 2019-02-01 | 2019-04-12 | 江苏中烟工业有限责任公司 | A kind of acid modification agent and its application method in low temperature cigarette reconstituted tobacoo |
| CN110055787B (en) * | 2019-04-11 | 2020-07-24 | 湖北中烟工业有限责任公司 | Method for preparing cigarette case or carton packing paper by taking cigarette rods as raw materials |
| CN110055787A (en) * | 2019-04-11 | 2019-07-26 | 湖北中烟工业有限责任公司 | The method for preparing cigarette case or box packaging paper as raw material using tobacco rod |
| CN110643303A (en) * | 2019-08-23 | 2020-01-03 | 广东中烟工业有限责任公司 | Adhesive for heating non-combustible tobacco products and application thereof |
| CN110679984A (en) * | 2019-11-15 | 2020-01-14 | 湖北中烟工业有限责任公司 | Preparation method of special slice for heating cigarettes |
| CN110742298A (en) * | 2019-11-15 | 2020-02-04 | 湖北中烟工业有限责任公司 | Method for preventing tobacco sheets from being adhered during storage |
| CN110742298B (en) * | 2019-11-15 | 2022-04-08 | 湖北中烟工业有限责任公司 | Method for preventing tobacco sheets from being adhered during storage |
| CN110946320A (en) * | 2019-12-12 | 2020-04-03 | 河南卷烟工业烟草薄片有限公司 | Damp-proof heating non-combustion reconstituted tobacco, preparation method and application |
| CN110934321A (en) * | 2020-01-07 | 2020-03-31 | 湖北中烟工业有限责任公司 | Method for preparing thermosensitive non-combustion tobacco sheet based on kraft lignin |
| CN110934321B (en) * | 2020-01-07 | 2021-12-10 | 湖北中烟工业有限责任公司 | Method for preparing thermosensitive non-combustion tobacco sheet based on kraft lignin |
| CN110934323A (en) * | 2020-01-07 | 2020-03-31 | 湖北中烟工业有限责任公司 | Method for preparing tobacco sheets by compounding gypsum whiskers |
| CN111213909A (en) * | 2020-01-22 | 2020-06-02 | 云南中烟工业有限责任公司 | A cigarette containing flos Chrysanthemi extract and capable of reducing oral risk |
| WO2021190036A1 (en) * | 2020-03-24 | 2021-09-30 | 青岛海大新星科技有限公司 | Heat-not-burn cartridge and auxiliary apparatus |
| CN111789279A (en) * | 2020-07-24 | 2020-10-20 | 吉林烟草工业有限责任公司 | Preparation method of tobacco leaf-imitated reconstituted tobacco |
| CN112914151A (en) * | 2021-02-01 | 2021-06-08 | 南通金源新材料有限公司 | Heating cigarette |
| CN112956725A (en) * | 2021-03-17 | 2021-06-15 | 云南中烟工业有限责任公司 | Double-layer composite paper filter stick for reconstituted tobacco and preparation method thereof |
| CN113876018A (en) * | 2021-10-21 | 2022-01-04 | 湖北中烟工业有限责任公司 | Preparation method of special slice for homogenizing and heating cigarettes |
| CN113876018B (en) * | 2021-10-21 | 2023-01-31 | 湖北中烟工业有限责任公司 | Preparation method of special slice for homogenizing and heating cigarettes |
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