CN101999751B - Method for comprehensively utilizing burdock root in tobacco - Google Patents
Method for comprehensively utilizing burdock root in tobacco Download PDFInfo
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- CN101999751B CN101999751B CN 200910063800 CN200910063800A CN101999751B CN 101999751 B CN101999751 B CN 101999751B CN 200910063800 CN200910063800 CN 200910063800 CN 200910063800 A CN200910063800 A CN 200910063800A CN 101999751 B CN101999751 B CN 101999751B
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- tobacco
- radix bardanae
- extract
- water
- cigarette
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- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a method for comprehensively utilizing burdock roots in tobacco, which belongs to the technical field of cigarette. The technical scheme of the invention comprises the following steps: (1) preparing dry powder of burdock roots; (2) performing water extraction to obtain the extract-type water extract of burdock roots serving as tobacco spice with a wetting function; and (3)manufacturing a substrate of tobacco sheets by using filter residue. In the invention, a great amount of resources are available and the cost is low; the extract has functions of improving flavor andwetting at the same time; and the waste residue is used for manufacturing the substrate of the tobacco sheets, therefore, the lack of raw materials of the tobacco sheets by a papermaking method is relieved, and the sensory quality of the tobacco sheets by the papermaking method can be improved. The method of the invention ensures no waste during the processing and the comprehensive utilization ofthe burdock roots is realized.
Description
Technical field
The invention belongs to technical field of cigarettes, is a kind ofly from the root of plant burdock, to obtain water extract specifically, is used for cigarette additive, and the filter residue after will extracting simultaneously is used for the comprehensive utilization method of reconstituted tobacoo.
Background technology
In the prior art, the security of cigarette receives the high attention of People more and more, and the tar that reduces in the cigarette has become a kind of inexorable trend, is accompanied by the reduction of tar content, and smoke is thin out, and fragrance weakens, and mouthfeel and pleasant impression variation are difficult to accepted by the consumer.Flue gas concentration and fragrance in order to promote and improve cigarette improve cigarette mouthfeel and pleasant impression, and flavoring and casing becomes a valid approach.Simultaneously, in the production of cigarettes process, the polyhydroxy substance that common needs adding glycerine, propane diols, sorbierite etc. have the humectation effect is as humectant; Improve the physical property of tobacco; Strengthen the anti-processability of tobacco, it is broken that minimizing adds making of man-hour, simultaneously; The moisture content of keeping cigarette shreds remains on a suitable scope, and the great fluctuation process excessively of avoiding moisture in cut tobacco is to the influence of cigarette smoking quality.
In the prior art, the essence and flavoring agent that in perfuming cigarette is reinforced, uses, main flue gas concentration and the fragrance of promoting and improving cigarette that rises improves effects such as cigarette mouthfeel and pleasant impression, does not possess the humectation effect; And the humectant that in the production of cigarettes process, adds, do not have to promote and improve cigarette flue gas concentration and fragrance, improve effects such as cigarette mouthfeel and pleasant impression.Therefore, must add essence and flavoring agent and humectant simultaneously in the production of cigarettes process, cause the defective that production technology complicates, production cost increases thus.And chemical synthesis products such as the glycerine that uses as humectant in the prior art, propane diols, sorbierite, because the restriction of use cost, purity can not be very high, unavoidably can contain some impurity, possibly bring negative effect to the cigarette smoking quality.Still the cigarette additive that does not have flavouring and humectation effect in the prior art simultaneously.
Reconstituted tobacoo is to be raw material with the tobacco dead meal in the cigarette process such as offal, offal, tobacco leaf fragment and part discarded tobacco leaf etc., through reconfiguring the reconstituted tobacco that processes.For alleviating tobacco sheets by paper making method raw material problem in short supply day by day; 1mm～80 order cigarette ashes discarded in the cigarette process are just applied in each thin slice manufacturer; But still can not fundamentally alleviate raw material problem in short supply, therefore, be badly in need of widening the raw material field for tobacco sheets by paper making method.
Burdock is a composite family biennial herb plant, uses comparatively extensive in pharmaceuticals industry.What pharmaceuticals industry was used mainly is its fruit great burdock achene.Great burdock achene, " Pharmacopoeia of People's Republic of China (one one) " (version in 2005) includes.Cold in nature, flavor is hot, bitter.Attach to the lung and stomach meridians.Function cures mainly: dispelling wind and heat from the body, a surname's lung promoting eruption, detoxifcation relieve sore throat.Modern pharmacological research has found that great burdock achene has the function of following several respects: antibiotic, antivirus action; The effect of calcium antagonist appearance; Raise immunity and hypoglycemic activity; Anti-ephrosis becomes; Antitumor, mutation effect; Diuresis and discharge function etc.
Burdock has been realized large-area artificial cultivation in China, and it is edible that its leaf and root can be used as vegetables.Radix bardanae and tender leaf can be mixed, fry, burn, stew, cook soup, cook congee, transfer filling, saucing and make auxiliary material edible.At present, the also uncomfortable edible burdock of China people, therefore, China's burdock mainly is as raw material, with form processings such as fresh-keeping, quick-frozen, dehydration and salt marsh outlet Japan and Southeast Asia.But the international market is very high to the specification requirement of outlet burdock, thereby causes outer radix bardanae such as a lot of grades to be taken as discarded object, and only some is used to animal feed, and whole value is not high.
A lot of technical staff have carried out the range of application of expansion radix bardanae and the research of aspect, field; As: Chinese patent document CN1267455C discloses edible burdock inulin and preparation method thereof; Radix bardanae is through very complicated extraction, separation, purge process; Remove materials such as small molecular weight impurity, pigment and protein, obtain the edible burdock inulin of higher degree; Chinese patent document CN100493375C discloses comprehensive burdock root processing method; Chinese patent document CN101218948 discloses a kind of burdok root beverage manufacturing method; Chinese patent document CN1620999 discloses a kind of radix bardanae Chinese health care thoothpick; Chinese patent document CN1806674 discloses burdock paste and preparation method; Chinese patent document CN101095553 discloses a kind of processing technology of burdock preserved fruit.More than the application of these radix bardanaes all concentrate on food or field of medicaments.And relevant report is not also seen in the application of radix bardanae in cigarette.
Summary of the invention
Above-mentioned deficiency to prior art; The technical problem that the present invention will solve provides a kind of radix bardanae comprehensive utilization method in tobacco; The radix bardanae water extract that water obtains after extracting is as cigarette additive, and this additive has the effect of flavouring and humectation simultaneously in cigarette; Filter residue after the extraction is used for the substrate of reconstituted tobacoo manufactures paper with pulp, and has both alleviated the nervous problem of tobacco sheets by paper making method raw material to a certain extent, the aesthetic quality that can improve tobacco sheets by paper making method again.
Technical scheme of the present invention is: radix bardanae comprehensive utilization method in tobacco is carried out according to following steps:
[1], the outer radix bardanae such as fresh that will be taken as discarded object cleans up with running water, dries naturally, cuts into sheet, under 40-60 ℃ of temperature, dries, and is crushed to 40 orders, obtains radix bardanae dry powder;
[2], with radix bardanae dry powder and water mixed according to mass ratio 1: 10-20; Under temperature 70-90 ℃ condition, extract 2-3 time; Each extraction time 0.5-2 hour, to filter and merging filtrate, the filtrate decompression of merging is condensed into medicinal extract shape material; Gained medicinal extract shape is the radix bardanae water extract, is a kind of tobacco spice that has the humectation function; Filter residue is left down step and uses;
[3], the filter residue that step [2] is kept is used for the substrate of reconstituted tobacoo and manufactures paper with pulp: the offal slag that above-mentioned filter residue and thin slice are extracted or/and the offal slag according to the mixed of mass ratio 1: 5-10; Send into the high-density paste mill making beating, making into beating degree is the slurry of 20 ° of SR～30 ° SR; Destroying the forebay with sending after above-mentioned slurry and outer fine the mixing, surfs the Net and processes the substrate of reconstituted tobacoo in the dilution back.
The resulting tobacco spice that has the humectation function of step [2] is diluted with water to 10%, and the 0.2-0.4% according to pipe tobacco weight adds in the pipe tobacco then.
Except as otherwise noted, percentage of the present invention and ratio all refer to percetage by weight and weight ratio.
Advantage of the present invention:
The present invention does raw material with the outer radix bardanae of grade of high quality and at a reasonable price, and the available resources amount is big, and is with low cost, realized the comprehensive utilization of waste resource.
The radix bardanae water extract that the present invention extracted is the tobacco spice that has the humectation function, is applied in the cigarette, both can effectively improve the sucking quality of cigarette, has certain humectation effect again, promptly has flavouring and humectation effect simultaneously.
The main component of the radix bardanae water extract that the present invention extracted is an edible burdock inulin, needs higher purity to compare with medicine with field of food, and this method need not complicated separation and purge process, and technology is simple, and is easy and simple to handle, practiced thrift cost greatly;
In the pyrolysis product of the radix bardanae water extract main component edible burdock inulin that employing the inventive method obtains the flavor component that often uses in a lot of tobacco blending is arranged, these compositions all have increases the effect that tobacco roasting is fragrant and ageing is fragrant preferably.Simultaneously, the humectation effect of radix bardanae water extract is better than prior art humectant propane diols commonly used.Opened up the new purposes of edible burdock inulin as humectant.
The radix bardanae water extract that adopts the inventive method to obtain also contains compositions such as amino acids, Polyphenols, phytochrome class; And a spot of protein; These compositions are in the application of medicine and field of food, to need to remove, but the aesthetic quality to cigarette has better effect in tobacco.The present invention is fully used the composition of radix bardanae.
Filter residue after the present invention extracts is except mainly containing the cellulose; Also contain the amino acids that is not extracted and remains, Polyphenols, phytochrome class, the material favourable such as protein-based to the cigarette aesthetic quality; Therefore the substrate that is applied to reconstituted tobacoo is manufactured paper with pulp; Both alleviated the nervous problem of tobacco sheets by paper making method raw material to a certain extent, the aesthetic quality that can improve tobacco sheets by paper making method again.
Do not have discarded object in the method process of the present invention, realized whole comprehensive utilizations of radix bardanae.
The specific embodiment
Below in conjunction with embodiments of the invention the relevant technologies problem is described in further detail.
Embodiment 1 cleans up outer radix bardanae such as fresh grade with running water, dry naturally, is cut into the sheet of big or small uniform in thickness with manual work or slicer, and 40 ℃ of oven for drying, mechanical disintegration obtain radix bardanae dry powder to 40 orders.With radix bardanae dry powder and water according to mass ratio 1: 10 ratio extract 3 times, 90 ℃ of temperature, each 0.5 hour extraction time, filter, filtrate decompression is condensed into the medicinal extract shape, gained medicinal extract shape material is the radix bardanae water extract.
Radix bardanae water extract of the present invention is diluted with water to 10%, adds in the high-grade cigarette pipe tobacco according to 0.2% of pipe tobacco weight then, smoke panel test according to national standard method behind the making cigarette.Smoking result is: tangible increase tobacco roasting perfume and the effect that promotes fragrance matter are arranged.
The offal slag that above-mentioned filter residue and prior art are produced is sent into the high-density paste mill making beating according to 1: 5 mixed of mass ratio, and making into beating degree is the slurry of 20 ° of SR～30 ° SR; Send after outer fibre that above-mentioned slurry and prior art are produced mixes and destroy the forebay, dilution is afterwards surfed the Net and is processed substrate.Then according to prior art production paper process thin slice.
Embodiment 2 cleans up outer radix bardanae such as fresh grade with running water, dry naturally, is cut into the sheet of big or small uniform in thickness with manual work or slicer, and 50 ℃ of oven for drying, mechanical disintegration obtain radix bardanae dry powder to 40 orders.With radix bardanae dry powder and water according to mass ratio 1: 15 ratio extract 3 times, 80 ℃ of temperature, each 1 hour extraction time, filter, filtrate decompression is condensed into the medicinal extract shape, gained medicinal extract shape material is the radix bardanae water extract.
Radix bardanae water extract of the present invention is diluted with water to 10%, adds in the middle-grade cigarette shreds according to 0.3% of pipe tobacco weight then, smoke panel test according to national standard method behind the making cigarette.Smoking result is: tangible increase tobacco roasting perfume and the effect that increases perfume quantity are arranged.
The offal slag that above-mentioned filter residue and prior art are produced is sent into the high-density paste mill making beating according to 1: 8 mixed of mass ratio, and making into beating degree is the slurry of 20 ° of SR～30 ° SR; Send after outer fibre that above-mentioned slurry and prior art are produced mixes and destroy the forebay, dilution is afterwards surfed the Net and is processed substrate.Then according to prior art production paper process thin slice.
Embodiment 3 cleans up outer radix bardanae such as fresh grade with running water, dry naturally, is cut into the sheet of big or small uniform in thickness with manual work or slicer, and 60 ℃ of oven for drying, mechanical disintegration obtain radix bardanae dry powder to 40 orders.With radix bardanae dry powder and water according to mass ratio 1: 20 ratio extract 2 times, 70 ℃ of temperature, each 2 hours extraction times, filter, filtrate decompression is condensed into the medicinal extract shape, gained medicinal extract shape material is the radix bardanae water extract.
Radix bardanae water extract of the present invention is diluted with water to 10%, adds in the high-grade cigarette pipe tobacco according to 0.4% of pipe tobacco weight then, smoke panel test according to national standard method behind the making cigarette.Smoking result is: have tangible increase tobacco roasting fragrant, increase flue gas concentration and cover the effect of assorted gas.
The offal slag that above-mentioned filter residue and prior art are produced is sent into the high-density paste mill making beating according to 1: 10 mixed of mass ratio, and making into beating degree is the slurry of 20 ° of SR～30 ° SR; Send after outer fibre that above-mentioned slurry and prior art are produced mixes and destroy the forebay, dilution is afterwards surfed the Net and is processed substrate.Then according to prior art production paper process thin slice.
Radix bardanae contains polyphenol, amino acid, synanthrin, cellulose, phytochrome, protein and glycan compounds etc., and wherein synanthrin about about 25%.The applicant through further investigation, recognizes that carbohydrate, amino acids, phytochrome class, the polyphenols in the radix bardanae all has better action to the aesthetic quality of tobacco before making the present invention.Glucide: can produce acidic materials on the one hand, suppress the alkalescence of flue gas neutral and alkali material, make the acid-base balance appropriateness of flue gas, reduce excitant, produce gratifying jealous; On the other hand, prop up in the process of burning and sucking in heating and cigarette, sugar is the important as precursors that forms aroma substance; When temperature at 300 degree when above; Pyrolysis forms multiple aroma substance separately, and wherein most important have a furan derivatives, carbonyls such as simple ketone and aldehydes.The amino acids material: the burning of an amount of amino acid produces nitrogen-containing compound, and flue gas is enriched, energetically; Simultaneously can also and reduced sugar between the Maillard reaction takes place, generate have sweet, roasting, puffed rice, nut, the compound of characteristic fragrance such as cheese.Polyphenols: effect with extraordinary soft flue gas.Phytochrome: the precursor that is a lot of important fragrance matters in the tobacco; In cigarette heating and burn and suck in the process, but pyrolysis generates the compound that solanone, geranyl acetone, farnesyl acetone, isophorone and derivative, cyclisation citral and safranal, dihydroactinidiolide, irisone, damascenone, damascone etc. embody these notes of tobacco.Protein: the hydrolysate of protein is the hyle of many tobacco aroma materials with the product that further transforms, and contains an amount of protein, can give sufficient tobacco aroma and plentiful jealous intensity, but protein content is too high; Can cause flue gas intensity excessive, fragrance and jealous variation produce acid, bitter taste and excitant, and the protein content height can produce a kind of albumen stink as the burning feather when burning and sucking; And discover through the applicant, the contained protein content of radix bardanae be about 2% (Jiang Shumin, burdock chemical composition and Pharmacological action study present situation, the time treasure traditional Chinese medical science traditional Chinese medicines; Calendar year 2001, the 12nd volume, the 10th phase; The 941-942 page or leaf), far below tobacco leaf 4%-13%, average 7.6% protein content (Shao Hui virtue 1; Permitted to have of one's own 1, the relation of Liu Li flue-cured tobacco total nitrogen and protein content and main volatile aroma substance, Xibei Univ. of Agricultural & Forest Science & Technology's journal (natural science edition) 2008; The 36th volume, the 12nd phase, 69-76 page or leaf); Therefore, protein content is relatively low in the radix bardanae, can not play the effect that influences the aesthetic quality.
The polysaccharide materials such as synanthrin that this method is primarily aimed in the radix bardanae extract, and are used for cigarette flavors, can increase cigarette flavor.The applicant thinks that the radix bardanae water extract has humectation effect preferably, possibly be because synanthrin is a compound sugar, has a plurality of hydroxyls in its molecular structure, can be preferably and water molecules, form chemical bond (hydrogen bond), and therefore have humectation effect preferably.And polysaccharide materials such as synanthrin have dissolubility preferably in water, and water of the present invention extracts as solvent, and the filter residue after the extraction is rich in cellulose substances, can satisfy the tobacco slice production requirement, and the substrate that is used for tobacco sheets by paper making method is manufactured paper with pulp.Water extracts in the process of polysaccharide materials such as synanthrin, and amino acids, Polyphenols, phytochrome class etc. have the material of better effect to the aesthetic quality of tobacco, and a small amount of water-soluble protein substance all can have part to be extracted simultaneously; These that are not extracted are out then stayed in the filter residue with cellulose the material that the aesthetic quality of tobacco has better effect, can to a certain degree improve the aesthetic quality of tobacco sheets by paper making method.Therefore, method of the present invention all is fully utilized the main component of radix bardanae.Opened up radix bardanae range of application.Simultaneously, this method does not have discarded object, is the real comprehensive utilization of radix bardanae.Water extracts also has inexpensive advantage, therefore helps the popularization of commercial Application.
The applicant also just relevant with the present invention technical problem has carried out deep discussion.AOAC OfficialMethod 997.08 has stipulated levulan Determination on content method, and synanthrin belongs to levulan.The content of edible burdock inulin is measured in the radix bardanae water extract that the inventor obtains the present invention with high performance liquid chromatography according to this method, and condition determination is following:
Instrument is Dionex 3000 highly effective liquid phase chromatographic systems.Chromatographic column: the PrevailCarbohydrate of Alltech company sugar post; EISD: 81.5 ℃ of drift tube temperatures, throughput 2.2L/min.30 ℃ of column temperatures, flow velocity 1.0ml/min; Sample size: 10 μ l.Condition of gradient elution is: acetonitrile-water, elution program (table 1).
Table 1 gradient elution program
| Time (min) | Acetonitrile (%) | Water (%) |
| 0-3 | 70 | 30 |
| 3-4 | 70-75 | 30-25 |
| 4-10 | 75 | 25 |
| 10-11 | 75-65 | 25-35 |
| 11-25 | 65 | 35 |
Synanthrin assay result such as following table 2 in the radix bardanae water extract that the present invention obtains.
Table 2 synanthrin assay result
| Synanthrin (%) | |
| Embodiment 1 | 65.64 |
| Embodiment 2 | 65.43 |
| Embodiment 3 | 66.17 |
The inventor is by prior art, prepared in laboratory the higher edible burdock inulin (Chinese patent document CN1267455C) of purity, then the thermal cracking products of edible burdock inulin is studied, condition determination is following:
Instrument: Pyroprobe 2000 thermal cracking appearance (U.S. CDS company), DSQ II gas chromatograph-mass spectrometer (GC-MS) (U.S. Thermo Fisher company).Thermal cracking atmosphere: nitrogen.Thermal cracking probe (pyrolysis head) initial temperature: 30 ℃, rise to 300 ℃ of final temperatures, 600 ℃ and 900 ℃, duration 10s respectively with 20 ℃/ms speed.DB-5ms 30 * 0.25mm * 0.25 μ m; Temperature programming: 40 ℃ (keeping 1min), be warming up to 100 ℃ (keeping 1min) with 2 ℃/min, with 8 ℃/min, be warming up to 280 ℃ (keeping 5min); Injector temperature: 260 ℃; Interface temperature: 280 ℃; Input mode: shunting, flow velocity 1.0ml/min; Ionization energy: 70eV.Sweep limits: 35-400amu, standard mass spectral database: NIST98 and WILEY275 spectrum storehouse.Area normalization is quantitative.
Edible burdock inulin is thermal cracking result under the different temperatures such as following table 4 in nitrogen environment.
The thermal cracking primary product result (%) of table 3 edible burdock inulin
| Sequence number | The product title | 300℃ | 600℃ | 900℃ |
| 1 | 2, the 5-dimethyl furan | - | - | 0.49 |
| 2 | Phenol | - | 0.37 | - |
| 3 | 2-methyl-furans | 0.26 | 0.32 | 0.41 |
| 4 | Toluene | - | - | 0.08 |
| 5 | Furfural | 80.93 | 55.67 | 39.63 |
| 6 | Benzocyclobutane | - | - | 0.25 |
| 7 | 1-(2-Furan Aldehydes)-ethyl ketone | 0.16 | 0.21 | 0.13 |
| 8 | Benzaldehyde | - | 0.04 | 0.08 |
| 9 | 5-methyl-2-furfural | 0.57 | 1.74 | 1.92 |
| 10 | Benzofuran | - | 0.28 | 0.16 |
| 11 | 2, the 2-bifuran | 0.37 | 0.08 | 0.08 |
| 12 | Indenes | - | - | 0.29 |
| 13 | 3-hydroxyl-benzaldehyde | - | 0.06 | 0.1 |
| 14 | 2-methyl-phenol | - | 0.11 | 0.22 |
| 15 | Acetophenone | - | - | 0.11 |
| 16 | The 5-methyl isophthalic acid, the 3-benzenediol | - | 1.14 | 2.41 |
| 17 | Methylfuroate | - | 1.63 | 1.48 |
| 18 | Aldehyde C-9 | 0.87 | 0.15 | - |
| 19 | 2-methyl-benzofuran | 0.87 | 0.15 | 1.51 |
| 20 | 1-methyl isophthalic acid H-indenes | - | - | 0.54 |
| 21 | 1-propinyl-benzene | - | - | - |
| 22 | Naphthalene | - | 0.06 | 4.27 |
| 23 | 2-(2-furyl methyl)-5-methyl-furans | - | 0.31 | ?- |
| 24 | 2-ethyl-1H-benzimidazole | - | 0.19 | 0.18 |
| 25 | Benzothiazole | 0.48 | 0.29 | 0.24 |
| 26 | 5-methylol-furfural | - | 27.72 | 27.59 |
| 27 | 1-(2-furyl)-1-acetone | - | - | 0.26 |
| 28 | 2-methyl-naphthalene | - | 0.27 | 1.84 |
| 29 | 4-methyl isophthalic acid-naphthalene alcohol | - | 0.1 | 0.17 |
| 30 | Phenylbenzene | - | - | 0.68 |
| 31 | 2,7-dimethyl-naphthalene | - | 0.18 | 0.15 |
| 32 | 2,6-dimethyl-naphthalene | - | 0.05 | 0.13 |
| 33 | 2,3-dihydro-3,5-dihydroxy-6-methyl-4H-pyrans-4-ketone | - | 0.14 | 0.51 |
| 34 | Luxuriant and rich with fragrance | - | 0.1 | 1.13 |
| 35 | Diisobutyl phthalate | 1.28 | 3.68 | 0.53 |
"-" expression does not detect.
Visible from last table, the edible burdock inulin composition that content is bigger in the thermal cracking products under the different temperatures mainly contains: furfuran compounds such as furfural, 5 hydroxymethyl furfural.These compositions all have increases the effect that tobacco roasting is fragrant and ageing is fragrant preferably.Edible burdock inulin is the main component of radix bardanae water extract, and result of the test has proved the flavouring effect of radix bardanae water extract.
The humectant propane diols that the most often uses in the radix bardanae water extract that the inventor also obtains extraction and the prior art puts in the cigarette shreds according to identical ratio and program, evaluation separately humectation effect under different temperature and humidity conditions.Having investigated in temperature is that 40 ± 1 ℃, relative humidity are the humectation effect of each humectant under 35 ± 3% conditions.
Undertaken by following operating procedure: it is that 22 ± 1 ℃, relative humidity are 60 ± 2% climatic chamber balance after 48 hours that certain cigarette composition pipe tobacco is put into temperature, takes by weighing the 100g that cuts filler respectively; Every kind of humectant takes by weighing 0.40g, is diluted with water to 10g respectively and is sprayed in the pipe tobacco, and blank sample is sprayed water to 10g; Pipe tobacco is divided in sample disc, put into temperature and be 40 ± 1 ℃, relative humidity and be 35 ± 3% climatic chamber balance; Test specimen weighed in per 2 hours and detect once, continue to detect 10 hours, detect altogether 6 times; Calculate the weight rate of each sample at different detection time pipe tobacco.The result is as shown in table 4 below.
The weight rate (%) of different time pipe tobacco under the table 4 high temperature low humidity condition
| The humectant title | 0(h) | 2(h) | 4(h) | 6(h) | 8(h) | 10(h) |
| Propane diols | 0.00 | 5.43 | 5.88 | 6.49 | 6.75 | 6.88 |
| The radix bardanae water extract | 0.00 | 4.91 | 5.14 | 5.76 | 5.92 | 6.13 |
| Blank sample | 0.00 | 5.89 | 6.26 | 6.77 | 7.05 | 7.41 |
Also having investigated in temperature is that 10 ± 1 ℃, relative humidity are the humectation effect of each humectant under 60 ± 3% conditions.Test method is the same, and the result is as shown in table 5 below.
The weight rate (%) of different time pipe tobacco under the wet condition in table 5 low temperature
| The humectant title | 0(h) | 2(h) | 4(h) | 6(h) | 8(h) | 10(h) |
| Propane diols | 0.00 | 4.28 | 4.66 | 4.92 | 5.23 | 5.54 |
| The radix bardanae water extract | 0.00 | 3.85 | 4.04 | 4.22 | 4.39 | 4.55 |
| Blank sample | 0.00 | 5.89 | 6.26 | 6.77 | 7.05 | 7.41 |
Also having investigated in temperature is that 30 ± 1 ℃, relative humidity are the humectation effect of each humectant under 60 ± 3% conditions.Test method is the same, and the result is as shown in table 6 below.
The weight rate (%) of different time pipe tobacco under the condition that wets in the temperature in the table 6
| The humectant title | 0(h) | 2(h) | 4(h) | 6(h) | 8(h) | 10(h) |
| Propane diols | 0.00 | 4.41 | 4.72 | 5.05 | 5.38 | 5.69 |
| The radix bardanae water extract | 0.00 | 4.02 | 4.15 | 4.39 | 4.56 | 4.72 |
| Blank sample | 0.00 | 5.92 | 6.44 | 6.89 | 7.15 | 7.48 |
Visible from above experiment, under different temperatures, the damp condition, the humectation effect of radix bardanae water extract all is better than the humectant propane diols that prior art is used.
Adopt protein content in the filter residue after Kjeldahl is measured radix bardanae water extract and extraction according to standard GB/T 5009.5-1985.Measure result such as following table 7.Generally about 1%, visible radix bardanae water extract low percentages of protein adds the negative effect that can not bring the cigarette aesthetic quality in the pipe tobacco to protein content in the leaf tobacco extract that often uses during tobacco flavoring is reinforced; And in the tobacco sheets by paper making method in the most frequently used raw material offal protein content generally at 4%-13%, average 7.6%, low percentages of protein in the visible filter residue, being used for tobacco sheets by paper making method has favourable effect to the aesthetic quality.
Table 7 protein content determination result
| Radix bardanae water extract protein content (%) | Filter residue protein content (%) | |
| Embodiment 1 | 0.33 | 2.72 |
| Embodiment 2 | 0.35 | 2.67 |
| Embodiment 3 | 0.32 | 2.69 |
The radix bardanae water extract that the applicant obtains extraction adds in the cigarette smokes panel test, and smokes panel test and carries out according to national standard method, and 7 people form the group of smokeing panel test, 2 national judging panels, 5 provincial judging panels, smoking result such as following table 8.Visible from table, after radix bardanae water extract of the present invention puts on pipe tobacco, the aesthetic quality that can improve cigarette.
Table 8 radix bardanae water extract puts on smoking result behind the pipe tobacco
| Embodiment 1 | Tangible increase tobacco roasting perfume and the effect that promotes fragrance matter are arranged. |
| Embodiment 2 | Tangible increase tobacco roasting perfume and the effect that increases perfume quantity are arranged. |
| Embodiment 3 | Have tangible increase tobacco roasting fragrant, increase flue gas concentration and cover the effect of assorted gas. |
Manufacture paper with pulp thin slice that obtains and the thin slice that does not add filter residue of the substrate that filter residue after the inventor also extracts radix bardanae water of the present invention is applied to reconstituted tobacoo carried out the physical property detection, result such as following table 9:
The contrast of table 9 thin slice physical property testing result
| Project | The prior art thin slice | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Quantitative (g/m 2) | 110 | 106 | 109 | 112 |
| Thickness average value (mm) | 0.208 | 0.212 | 0.210 | 0.207 |
| Filling value (cm 3/g) | 7.62 | 7.48 | 7.59 | 7.66 |
| Substrate tensile strength (CN/mm 2) | 369.4 vertical 268.4 is horizontal | 365.1 vertical 265.2 is horizontal | 367.3 vertical 271.4 is horizontal | 370.0 vertical 272.4 is horizontal |
It is thus clear that thin slice of the present invention and prior art thin slice are more approaching on physical property, do not have notable difference.
The substrate that filter residue after the inventor also extracts radix bardanae water the is applied to reconstituted tobacoo thin slice that thin slice that obtains and the prior art of not adding filter residue produce of manufacturing paper with pulp has carried out the aesthetic quality comparative evaluation; Smoke panel test and carry out according to national standard method; 7 people form the group of smokeing panel test; 2 national judging panels, 5 provincial judging panels, smoking result such as following table 10:
Table 10 thin slice contrast smoking result
| Prior art | Fragrance is still plentiful, and strength is medium, and assorted gas is big slightly, and stimulation is arranged, and pleasant impression is more comfortable |
| Embodiment 1 | Fragrance is still plentiful, and strength is medium, and slightly assorted gas has than pinprick, and pleasant impression is more comfortable. |
| Embodiment 2 | Fragrance is still plentiful, and strength is medium, and slightly assorted gas has than pinprick, and pleasant impression is comfortable. |
| Embodiment 3 | Fragrance is still plentiful, and strength is medium, and slightly assorted gas has than pinprick, and pleasant impression is comfortable |
It is thus clear that the thin slice that thin slice that the present invention obtains and prior art are produced is having improvement aspect assorted gas, stimulation and the pleasant impression.
Claims (1)
1. radix bardanae comprehensive utilization method in tobacco is characterized in that described comprehensive utilization method carries out according to following steps:
[1], the fresh radix bardanae that will be taken as discarded object cleans up with running water, dries naturally, cuts into sheet, under 40-60 ℃ of temperature, dries, and is crushed to 40 orders, obtains radix bardanae dry powder;
[2], with radix bardanae dry powder and water mixed according to mass ratio 1: 10-20; Under temperature 70-90 ℃ condition, extract 2-3 time, each extraction time 0.5-2 hour, filter and merging filtrate; The merging filtrate decompression is condensed into medicinal extract shape material, and gained medicinal extract shape material is the radix bardanae water extract; Described radix bardanae water extract is diluted with water to 10%, and the 0.2-0.4% according to pipe tobacco weight adds in the pipe tobacco then; Filter residue is left down step and uses;
[3], the filter residue that step [2] is kept is used for the substrate of reconstituted tobacoo and manufactures paper with pulp: the offal slag that above-mentioned filter residue and thin slice are extracted or/and the offal slag according to the mixed of mass ratio 1: 5-10; Send into the high-density paste mill making beating, making into beating degree is the slurry of 20 ° of SR～30 ° SR; Destroying the forebay with sending after above-mentioned slurry and outer fine the mixing, surfs the Net and processes the substrate of reconstituted tobacoo in the dilution back.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102754914A (en) * | 2012-07-27 | 2012-10-31 | 红云红河烟草(集团)有限责任公司 | Fructo-oligosaccharide cigarette humectant and use method thereof |
| CN103645272B (en) * | 2013-12-23 | 2015-02-04 | 深圳出入境检验检疫局工业品检测技术中心 | Method for detecting high-boiling-point substances in industrial products |
| CN103859578B (en) * | 2014-03-04 | 2016-05-18 | 江苏中烟工业有限责任公司 | The extracting method of the thick polysaccharide of a kind of burdock and the application in tobacco thereof |
| CN103844346B (en) * | 2014-03-04 | 2016-04-06 | 江苏中烟工业有限责任公司 | A kind of radix bardanae ethanol extract and the application in tobacco thereof |
| CN112030608B (en) * | 2020-08-27 | 2023-06-09 | 重庆中烟工业有限责任公司 | Cigarette paper with improved taste and preparation method thereof |
| WO2022230891A1 (en) * | 2021-04-26 | 2022-11-03 | 日本たばこ産業株式会社 | Tobacco sheet for non-combustion-heating-type flavor inhaler, non-combustion-heating-type flavor inhaler, and non-combustion-heating-type flavor inhalation system |
| JPWO2022230885A1 (en) * | 2021-04-26 | 2022-11-03 |
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