CN103844346B - A kind of radix bardanae ethanol extract and the application in tobacco thereof - Google Patents
A kind of radix bardanae ethanol extract and the application in tobacco thereof Download PDFInfo
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- CN103844346B CN103844346B CN201410076110.6A CN201410076110A CN103844346B CN 103844346 B CN103844346 B CN 103844346B CN 201410076110 A CN201410076110 A CN 201410076110A CN 103844346 B CN103844346 B CN 103844346B
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- radix bardanae
- ethanol extract
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Abstract
The invention discloses a kind of radix bardanae ethanol extract and the application in tobacco thereof; A kind of radix bardanae ethanol extract, preparation process comprises the following steps: a: get radix bardanae and remove impurity, clean section; B: oven dry at 30-60 DEG C of cutting into slices; C: be crushed to 10 ~ 100 orders; D: add ethanol in the radix bardanae after pulverizing; E: ultrasonic extraction 45-75 minute; F: filter and retain filtrate; G: filtrate is concentrated, after concentrated volume be condensate precursor long-pending 1/5-1/7, make radix bardanae ethanol extract, normal temperature is preserved; The application of radix bardanae ethanol extract in tobacco, comprises the following steps: a: be sprayed onto on pipe tobacco by radix bardanae ethanol extract, and wherein the weight of concentrate is the 0.1%-0.2% of pipe tobacco weight; B: pipe tobacco is processed into cigarette finished product.Beneficial effect is the sucking quality improving cigarette when not changing original performance of cigarette.
Description
Technical field
The present invention relates to a Plant Extracts and the application in tobacco thereof, particularly relate to a kind of radix bardanae ethanol extract and the application in tobacco thereof.
Background technology
Burdock is composite family biennial herb plant, it is good medicinal and edible plant, containing various bioactivators, comparatively extensive in pharmaceuticals industry application, under having stomach invigorating, beneficial gas, diuresis, rushing down, the effect such as nourishing and strengthening vital, clearing heat and detoxicating, inhibiting bacteria and diminishing inflammation, it is reported, the levulan extracted in radix bardanae, show it according to activity research and there is stronger antitussive effect, suitable with non-narcotic class antitussive conventional clinically.Burdock research is at home mainly in chemical constituents determination, medical, comprehensive processing and utilization etc.
Along with smoking and healthy problem more and more receive publicity, the harmful components of sucking in security, increase health care, reduction cigarette smoke improving cigarette are the inevitable development trend of cigarette.Therefore market has occurred as kinds such as ginseng cigarette, peppermint cigarettes, in pipe tobacco, namely added the material that ginseng, peppermint etc. have unique health care or taste.The application of burdock in tobacco business mainly concentrates on the application of the aqueous extract of great burdock achene and radix bardanae, and the application of radix bardanae ethanol extract in cigarette yet there are no relevant report.
Summary of the invention
For above-mentioned prior art Problems existing, the invention provides a kind of radix bardanae ethanol extract and the application in tobacco thereof, prepare radix bardanae ethanol extract and be applied on cigarette shreds, realize the effect of the sucking quality improving cigarette.
A kind of radix bardanae ethanol extract, preparation process comprises the following steps:
A: section: get radix bardanae and remove impurity, clean section;
B: dry: oven dry at 30-60 DEG C of cutting into slices;
C: pulverize: be crushed to 10 ~ 100 orders;
D: add ethanol: add ethanol in the radix bardanae after pulverizing;
E: ultrasonic extraction: ultrasonic extraction 45-75 minute;
F: filter: filter and retain filtrate;
G: filtrate concentrates: filtrate concentrated, after concentrated volume be condensate precursor long-pending 1/5-1/7, make radix bardanae ethanol extract, normal temperature is preserved;
Preferably, in Step d, described ethanol is absolute ethyl alcohol.
Preferably, in Step d, in the radix bardanae after pulverizing, add ethanol according to the ratio of mass ratio 1:5.
Preferably, in g step, filtrate concentrate rear volume be condensate precursor long-pending 1/6.
Preferably, in g step, be reduced pressure concentration at 50 DEG C by the mode that filtrate carrying out concentrates.
The application of radix bardanae ethanol extract in tobacco, comprises the following steps:
A: radix bardanae ethanol extract is sprayed onto on pipe tobacco, wherein the weight of concentrate is the 0.1%-0.2% of pipe tobacco weight;
B: pipe tobacco is processed into cigarette finished product.
The invention has the beneficial effects as follows: the radix bardanae ethanol extract obtained is joined on cigarette shreds as cigarette feed liquid, distinctive chemical composition can be produced when cigarette burns and sucks, obviously improve the sucking quality of cigarette, flue gas exquisiteness is soft, micro-pleasantly sweet, give cigarette clear hereby note, hamony is better, stimulate and slightly reduce, pleasant impression is cleaner; The present invention does not change original performance of cigarette, does not change or affects original sucking quality of cigarette, have the meaning and value of actual production.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described.
Embodiment one:
A kind of radix bardanae ethanol extract, preparation process comprises the following steps:
A: section: get radix bardanae and remove impurity, clean section;
B: dry: oven dry at 30 DEG C of cutting into slices;
C: pulverize: be crushed to 10 orders;
D: add ethanol: add ethanol in the radix bardanae after pulverizing;
E: ultrasonic extraction: ultrasonic extraction 45 minutes;
F: filter: filter and retain filtrate;
G: filtrate concentrates: filtrate concentrated, after concentrated volume be condensate precursor long-pending 1/5, make radix bardanae ethanol extract, normal temperature is preserved;
In order to obtain better effect, in Step d, described ethanol is absolute ethyl alcohol; In the radix bardanae after pulverizing, absolute ethyl alcohol is added according to the ratio of mass ratio 1:5; In g step, the mode concentrated by filtrate carrying out can be reduced pressure concentration at 50 DEG C.
The application of radix bardanae ethanol extract in tobacco, comprises the following steps:
A: radix bardanae ethanol extract is sprayed onto on pipe tobacco, wherein the weight of concentrate is 0.2% of pipe tobacco weight;
B: pipe tobacco is processed into cigarette finished product.
Embodiment two:
A kind of radix bardanae ethanol extract, preparation process comprises the following steps:
A: section: get radix bardanae and remove impurity, clean section;
B: dry: oven dry at 50 DEG C of cutting into slices;
C: pulverize: be crushed to 50 orders;
D: add ethanol: add ethanol in the radix bardanae after pulverizing;
E: ultrasonic extraction: ultrasonic extraction 60 minutes;
F: filter: filter and retain filtrate;
G: filtrate concentrates: filtrate concentrated, after concentrated volume be condensate precursor long-pending 1/6, make radix bardanae ethanol extract, normal temperature is preserved;
In order to obtain better effect, in Step d, described ethanol is absolute ethyl alcohol; In the radix bardanae after pulverizing, absolute ethyl alcohol is added according to the ratio of mass ratio 1:5; In g step, the mode concentrated by filtrate carrying out can be reduced pressure concentration at 50 DEG C.
The application of radix bardanae ethanol extract in tobacco, comprises the following steps:
A: radix bardanae ethanol extract is sprayed onto on pipe tobacco, wherein the weight of concentrate is 0.15% of pipe tobacco weight;
B: pipe tobacco is processed into cigarette finished product.
Embodiment three:
A kind of radix bardanae ethanol extract, preparation process comprises the following steps:
A: section: get radix bardanae and remove impurity, clean section;
B: dry: oven dry at 60 DEG C of cutting into slices;
C: pulverize: be crushed to 100 orders;
D: add ethanol: add ethanol in the radix bardanae after pulverizing;
E: ultrasonic extraction: ultrasonic extraction 75 minutes;
F: filter: filter and retain filtrate;
G: filtrate concentrates: filtrate concentrated, after concentrated volume be condensate precursor long-pending 1/7, make radix bardanae ethanol extract, normal temperature is preserved;
In order to obtain better effect, in Step d, described ethanol is absolute ethyl alcohol; In the radix bardanae after pulverizing, absolute ethyl alcohol is added according to the ratio of mass ratio 1:5; In g step, the mode concentrated by filtrate carrying out can be reduced pressure concentration at 50 DEG C.
The application of radix bardanae ethanol extract in tobacco, comprises the following steps:
A: radix bardanae ethanol extract is sprayed onto on pipe tobacco, wherein the weight of concentrate is 0.1% of pipe tobacco weight;
B: pipe tobacco is processed into cigarette finished product.
Claims (4)
1. a radix bardanae ethanol extract, is characterized in that, preparation process comprises the following steps:
A: section: get radix bardanae and remove impurity, clean section;
B: dry: oven dry at 30 ~ 60 DEG C of cutting into slices;
C: pulverize: be crushed to 10 ~ 100 orders;
D: add ethanol: add ethanol in the radix bardanae after pulverizing, adds ethanol according to the ratio of mass ratio 1:5 in the radix bardanae after pulverizing;
E: ultrasonic extraction: ultrasonic extraction 45-75 minute;
F: filter: filter and retain filtrate;
G: filtrate concentrates: filtrate concentrated, after concentrated volume be condensate precursor long-pending 1/5-1/7, make radix bardanae ethanol extract, normal temperature is preserved.
2. a kind of radix bardanae ethanol extract according to claim 1, is characterized in that, in Step d, described ethanol is absolute ethyl alcohol.
3. a kind of radix bardanae ethanol extract according to claim 1, is characterized in that, in g step, filtrate concentrate rear volume be condensate precursor long-pending 1/6.
4. a kind of radix bardanae ethanol extract according to claim 1, is characterized in that, in g step, is reduced pressure concentration at 50 DEG C by the mode that filtrate carrying out concentrates.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410076110.6A CN103844346B (en) | 2014-03-04 | 2014-03-04 | A kind of radix bardanae ethanol extract and the application in tobacco thereof |
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| CN201410076110.6A CN103844346B (en) | 2014-03-04 | 2014-03-04 | A kind of radix bardanae ethanol extract and the application in tobacco thereof |
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| CN103844346A CN103844346A (en) | 2014-06-11 |
| CN103844346B true CN103844346B (en) | 2016-04-06 |
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Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100508801C (en) * | 2006-11-25 | 2009-07-08 | 中国烟草总公司郑州烟草研究院 | Preparing method of sargassum fusiforme alcohol extract and application of sargassum fusiforme in tobacco |
| CN102002437B (en) * | 2009-09-02 | 2012-12-26 | 湖北中烟工业有限责任公司 | Method for extracting cigarette additives from pre-degreased burdock by ethanol and application thereof |
| CN102002426B (en) * | 2009-09-02 | 2013-02-27 | 湖北中烟工业有限责任公司 | Method for extracting volatile oil by supercritically extracting pre-degreased great burdock achene and application |
| CN101999751B (en) * | 2009-09-02 | 2012-12-05 | 湖北中烟工业有限责任公司 | Method for comprehensively utilizing burdock root in tobacco |
| GB201213870D0 (en) * | 2012-08-03 | 2012-09-19 | British American Tobacco Co | Tobacco extract, preparation thereof |
| CN103396889A (en) * | 2013-07-10 | 2013-11-20 | 红云红河烟草(集团)有限责任公司 | Preparation method of vetiver oil and application of vetiver oil in cigarettes |
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