CN103844346A - Burdock root ethanol extract and application thereof in tobacco - Google Patents
Burdock root ethanol extract and application thereof in tobacco Download PDFInfo
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- CN103844346A CN103844346A CN201410076110.6A CN201410076110A CN103844346A CN 103844346 A CN103844346 A CN 103844346A CN 201410076110 A CN201410076110 A CN 201410076110A CN 103844346 A CN103844346 A CN 103844346A
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- ethanol extract
- radix bardanae
- concentrated
- burdock root
- tobacco
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Abstract
The invention discloses burdock root ethanol extract and the application thereof in tobacco. The preparation process of the burdock root ethanol extract comprises the following steps that a, burdock root is subjected to impurity removal and is cleaned and sliced; b, the slices are dried under the temperature of 30-60 DEG C; c, the slices are smashed to realize the mesh of 10-100; d, ethanol is added to the smashed burdock root; e, the smashed burdock root is subjected to ultrasonic extraction for 45-75 minutes; f, the smashed burdock root is filtered, and filtrate is kept; g, the filtrate is concentrated, the volume after concentration is one seventh to one fifth of the volume before concentration, the burdock root ethanol extract is prepared and stored in the normal temperature. The application of the burdock root ethanol extract in tobacco comprises the following steps: a, the burdock root ethanol extract is sprayed to tobacco shreds, the weight of the concentrated solution is 0.1%-0.2% of the weight of the tobacco shreds; b, the tobacco shreds are processed into cigarette finished products. The burdock root ethanol extract and the application thereof in tobacco have the beneficial effects that the smoking quality of the cigarettes is improved under the condition that the original property of the cigarettes is not changed.
Description
Technical field
The present invention relates to a Plant Extracts and the application in tobacco thereof, relate in particular to a kind of radix bardanae ethanol extract and the application in tobacco thereof.
Background technology
Burdock is composite family biennial herb plant, it is good medicinal and edible plant, contain various bioactivators, comparatively extensive in pharmaceuticals industry application, under having stomach invigorating, beneficial gas, diuresis, rushing down, the effect such as nourishing and strengthening vital, clearing heat and detoxicating, inhibiting bacteria and diminishing inflammation, it is reported, the levulan extracting in radix bardanae, show that according to activity research it has stronger antitussive effect, suitable with conventional clinically non-narcotic class antitussive.Burdock research is at home mainly at aspects such as chemical constituents determination, medical, comprehensive processing and utilizations.
Along with smoking and healthy problem more and more receive publicity, the harmful components of sucking security, increase health care, reducing in cigarette smoke that improve cigarette are the inevitable development trend of cigarette.Therefore on market, occurred as kinds such as ginseng cigarette, peppermint cigarettes, in pipe tobacco, added ginseng, peppermint etc. to there is the material of unique health care or taste.The application of burdock in tobacco business mainly concentrates on the application of the aqueous extract of great burdock achene and radix bardanae, and the application of radix bardanae ethanol extract in cigarette yet there are no relevant report.
Summary of the invention
The problem existing for above-mentioned prior art, the invention provides a kind of radix bardanae ethanol extract and the application in tobacco thereof, prepares radix bardanae ethanol extract and is applied on cigarette shreds, realizes the effect of the sucking quality that improves cigarette.
A kind of radix bardanae ethanol extract, preparation process comprises the following steps:
A: section: get radix bardanae and remove impurity, clean section;
B: dry: will cut into slices and dry at 30-60 ℃;
C: pulverize: be crushed to 10 ~ 100 orders;
D: add ethanol: to pulverize after radix bardanae in add ethanol;
E: ultrasonic extraction: ultrasonic extraction 45-75 minute;
F: filter: filter and retain filtrate;
G: filtrate is concentrated: filtrate is concentrated, and concentrated rear volume is 1/5-1/7 of concentrated front volume, makes radix bardanae ethanol extract, and normal temperature is preserved;
Preferably, in d step, described ethanol is absolute ethyl alcohol.
Preferably, in d step, according to the ratio of mass ratio 1:5 to pulverize after radix bardanae in add ethanol.
Preferably, in g step, after filtrate is concentrated, volume is 1/6 of concentrated front volume.
Preferably, in g step, it is reduced pressure concentration at 50 ℃ that filtrate is carried out to concentrated mode.
The application of radix bardanae ethanol extract in tobacco, comprises the following steps:
A: radix bardanae ethanol extract is sprayed onto on pipe tobacco, and wherein the weight of concentrate is the 0.1%-0.2% of pipe tobacco weight;
B: pipe tobacco is processed into cigarette finished product.
The invention has the beneficial effects as follows: the radix bardanae ethanol extract obtaining is joined on cigarette shreds as cigarette feed liquid, in the time that burning and sucking, cigarette can produce distinctive chemical composition, obviously improve the sucking quality of cigarette, flue gas exquisiteness is soft, micro-pleasantly sweet, give clearly hereby note of cigarette, hamony is better, stimulate slightly and reduce, pleasant impression is cleaner; The present invention does not change original performance of cigarette, does not change or affect original sucking quality of cigarette, has the meaning and value of actual production.
The specific embodiment
Below in conjunction with embodiment, the invention will be further described.
Embodiment mono-:
A kind of radix bardanae ethanol extract, preparation process comprises the following steps:
A: section: get radix bardanae and remove impurity, clean section;
B: dry: will cut into slices and dry at 30 ℃;
C: pulverize: be crushed to 10 orders;
D: add ethanol: to pulverize after radix bardanae in add ethanol;
E: ultrasonic extraction: ultrasonic extraction 45 minutes;
F: filter: filter and retain filtrate;
G: filtrate is concentrated: filtrate is concentrated, and concentrated rear volume is 1/5 of concentrated front volume, makes radix bardanae ethanol extract, and normal temperature is preserved;
In order to obtain better effect, in d step, described ethanol is absolute ethyl alcohol; According to the ratio of mass ratio 1:5 to pulverize after radix bardanae in add absolute ethyl alcohol; In g step, it can be reduced pressure concentration at 50 ℃ that filtrate is carried out to concentrated mode.
The application of radix bardanae ethanol extract in tobacco, comprises the following steps:
A: radix bardanae ethanol extract is sprayed onto on pipe tobacco, and wherein the weight of concentrate is 0.2% of pipe tobacco weight;
B: pipe tobacco is processed into cigarette finished product.
Embodiment bis-:
A kind of radix bardanae ethanol extract, preparation process comprises the following steps:
A: section: get radix bardanae and remove impurity, clean section;
B: dry: will cut into slices and dry at 50 ℃;
C: pulverize: be crushed to 50 orders;
D: add ethanol: to pulverize after radix bardanae in add ethanol;
E: ultrasonic extraction: ultrasonic extraction 60 minutes;
F: filter: filter and retain filtrate;
G: filtrate is concentrated: filtrate is concentrated, and concentrated rear volume is 1/6 of concentrated front volume, makes radix bardanae ethanol extract, and normal temperature is preserved;
In order to obtain better effect, in d step, described ethanol is absolute ethyl alcohol; According to the ratio of mass ratio 1:5 to pulverize after radix bardanae in add absolute ethyl alcohol; In g step, it can be reduced pressure concentration at 50 ℃ that filtrate is carried out to concentrated mode.
The application of radix bardanae ethanol extract in tobacco, comprises the following steps:
A: radix bardanae ethanol extract is sprayed onto on pipe tobacco, and wherein the weight of concentrate is 0.15% of pipe tobacco weight;
B: pipe tobacco is processed into cigarette finished product.
Embodiment tri-:
A kind of radix bardanae ethanol extract, preparation process comprises the following steps:
A: section: get radix bardanae and remove impurity, clean section;
B: dry: will cut into slices and dry at 60 ℃;
C: pulverize: be crushed to 100 orders;
D: add ethanol: to pulverize after radix bardanae in add ethanol;
E: ultrasonic extraction: ultrasonic extraction 75 minutes;
F: filter: filter and retain filtrate;
G: filtrate is concentrated: filtrate is concentrated, and concentrated rear volume is 1/7 of concentrated front volume, makes radix bardanae ethanol extract, and normal temperature is preserved;
In order to obtain better effect, in d step, described ethanol is absolute ethyl alcohol; According to the ratio of mass ratio 1:5 to pulverize after radix bardanae in add absolute ethyl alcohol; In g step, it can be reduced pressure concentration at 50 ℃ that filtrate is carried out to concentrated mode.
The application of radix bardanae ethanol extract in tobacco, comprises the following steps:
A: radix bardanae ethanol extract is sprayed onto on pipe tobacco, and wherein the weight of concentrate is 0.1% of pipe tobacco weight;
B: pipe tobacco is processed into cigarette finished product.
Claims (6)
1. a radix bardanae ethanol extract, is characterized in that preparation process comprises the following steps:
A: section: get radix bardanae and remove impurity, clean section;
B: dry: will cut into slices and dry at 30-60 ℃;
C: pulverize: be crushed to 10 ~ 100 orders;
D: add ethanol: to pulverize after radix bardanae in add ethanol;
E: ultrasonic extraction: ultrasonic extraction 45-75 minute;
F: filter: filter and retain filtrate;
G: filtrate is concentrated: filtrate is concentrated, and concentrated rear volume is 1/5-1/7 of concentrated front volume, makes radix bardanae ethanol extract, and normal temperature is preserved.
2. a kind of radix bardanae ethanol extract according to claim 1, is characterized in that, in d step, described ethanol is absolute ethyl alcohol.
3. a kind of radix bardanae ethanol extract according to claim 1, is characterized in that, in d step, according to the ratio of mass ratio 1:5 to pulverize after radix bardanae in add ethanol.
4. a kind of radix bardanae ethanol extract according to claim 1, is characterized in that, in g step, after filtrate is concentrated, volume is 1/6 of concentrated front volume.
5. a kind of radix bardanae ethanol extract according to claim 1, is characterized in that, in g step, it is reduced pressure concentration at 50 ℃ that filtrate is carried out to concentrated mode.
6. the application of radix bardanae ethanol extract in tobacco, is characterized in that comprising the following steps:
A: radix bardanae ethanol extract is sprayed onto on pipe tobacco, and wherein the weight of concentrate is the 0.1%-0.2% of pipe tobacco weight;
B: pipe tobacco is processed into cigarette finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410076110.6A CN103844346B (en) | 2014-03-04 | 2014-03-04 | A kind of radix bardanae ethanol extract and the application in tobacco thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410076110.6A CN103844346B (en) | 2014-03-04 | 2014-03-04 | A kind of radix bardanae ethanol extract and the application in tobacco thereof |
Publications (2)
| Publication Number | Publication Date |
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| CN103844346A true CN103844346A (en) | 2014-06-11 |
| CN103844346B CN103844346B (en) | 2016-04-06 |
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| CN201410076110.6A Active CN103844346B (en) | 2014-03-04 | 2014-03-04 | A kind of radix bardanae ethanol extract and the application in tobacco thereof |
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Citations (6)
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|---|---|---|---|---|
| CN1961762A (en) * | 2006-11-25 | 2007-05-16 | 中国烟草总公司郑州烟草研究院 | Sargassum fusiforme alcohol extract and application thereof in tobacco |
| CN101999751A (en) * | 2009-09-02 | 2011-04-06 | 湖北中烟工业有限责任公司 | Method for comprehensively utilizing burdock root in tobacco |
| CN102002426A (en) * | 2009-09-02 | 2011-04-06 | 湖北中烟工业有限责任公司 | Method for extracting volatile oil by supercritically extracting pre-degreased great burdock achene and application |
| CN102002437A (en) * | 2009-09-02 | 2011-04-06 | 湖北中烟工业有限责任公司 | Method for extracting cigarette additives from pre-degreased burdock by ethanol and application thereof |
| CN103396889A (en) * | 2013-07-10 | 2013-11-20 | 红云红河烟草(集团)有限责任公司 | Preparation method of vetiveria zizanioides L. oil and application of vetiver vetiveria zizanioides L. oil in cigarettes |
| WO2014020337A1 (en) * | 2012-08-03 | 2014-02-06 | British American Tobacco (Investments) Limited | Tobacco extract, preparation thereof |
-
2014
- 2014-03-04 CN CN201410076110.6A patent/CN103844346B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1961762A (en) * | 2006-11-25 | 2007-05-16 | 中国烟草总公司郑州烟草研究院 | Sargassum fusiforme alcohol extract and application thereof in tobacco |
| CN101999751A (en) * | 2009-09-02 | 2011-04-06 | 湖北中烟工业有限责任公司 | Method for comprehensively utilizing burdock root in tobacco |
| CN102002426A (en) * | 2009-09-02 | 2011-04-06 | 湖北中烟工业有限责任公司 | Method for extracting volatile oil by supercritically extracting pre-degreased great burdock achene and application |
| CN102002437A (en) * | 2009-09-02 | 2011-04-06 | 湖北中烟工业有限责任公司 | Method for extracting cigarette additives from pre-degreased burdock by ethanol and application thereof |
| WO2014020337A1 (en) * | 2012-08-03 | 2014-02-06 | British American Tobacco (Investments) Limited | Tobacco extract, preparation thereof |
| CN103396889A (en) * | 2013-07-10 | 2013-11-20 | 红云红河烟草(集团)有限责任公司 | Preparation method of vetiveria zizanioides L. oil and application of vetiver vetiveria zizanioides L. oil in cigarettes |
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| CN103844346B (en) | 2016-04-06 |
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