CN1961762A - Sargassum fusiforme alcohol extract and application thereof in tobacco - Google Patents
Sargassum fusiforme alcohol extract and application thereof in tobacco Download PDFInfo
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- CN1961762A CN1961762A CN 200610128284 CN200610128284A CN1961762A CN 1961762 A CN1961762 A CN 1961762A CN 200610128284 CN200610128284 CN 200610128284 CN 200610128284 A CN200610128284 A CN 200610128284A CN 1961762 A CN1961762 A CN 1961762A
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- alcohol extract
- sargassum fusiforme
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Abstract
The invention relates to an application of goat vegetable extractive in the tobacco, wherein said extractive is prepared by a, pretreatment, and drying and breaking in 30-60Deg. C to be 10-100deals; b, under 80-120Deg. C, using water to extract the powder for 1-8h; c, concentrating the filtered solution into the extractive. Said extractive can be added into the tobacco, to generate special chemical component to improve the tobacco quality, while it has relieving cough function and reduces the harmful components.
Description
Technical field
The present invention relates to plant extract and application thereof, particularly Sargassum fusiforme alcohol extract and the application in tobacco thereof.This The Application of Technology does not change the existing processing technology of cigarette, can improve the quality of cigarette, reduces the harmfulness of cigarette.
Background technology
Along with the problem of smoking with health more and more receives publicity, the harmful components of sucking security, increase health care, reducing in the cigarette smoke that improve cigarette are the inevitable development trend of cigarette.Therefore occurred as kinds such as ginseng cigarette, peppermint cigarettes on the market, promptly in pipe tobacco, added the material that genseng, peppermint etc. have unique health care or taste.
Sheep dwells, and the style of cooking is eaten, the medicine dual purpose plant, according to record, it is to the enlargement of prevention thyroid gland, reduce cholesterol in the blood, treatment hypertension and colorectal cancer, cancer of the stomach all have certain effect, have the function of removing oxygen radical, to promoting children's bone growth, keep skin lubrication, recover brain fag, prevent that aging etc. from also having significant effect.Domestic relevant research mainly dwells sheep that dish is grown seedlings, food processing mode, chemical constituents determination, aspect such as medical.Do not find the application precedent in tobacco.
Goal of the invention
Purpose of the present invention just is being based on the situation of above-mentioned prior art and is specially studying and then developing Sargassum fusiforme alcohol extract and the application in tobacco thereof at the sheep dish of dwelling, Sargassum fusiforme alcohol extract is applied on the cigarette shreds, can improve the sucking quality of cigarette, reduce some harmful components in the cigarette mainstream flue gas.And this The Application of Technology does not change the existing processing technology of cigarette, can improve the quality of cigarette, reduces the harmfulness of cigarette.
The objective of the invention is to realize that by following scheme Sargassum fusiforme alcohol extract of the present invention is to be made by following method:
A, sheep are being crushed to 10～100 orders after the oven dry under 30～60 ℃ of temperature after dwelling and handling dish premenstruum (premenstrua);
B, under 20～100 ℃ of conditions, Sargassum fusiform powder material is extracted time 0.5～8h with ethanol;
Be the sheep of the present invention dish ethanol aqueous extract of dwelling after c, the filtering and concentrating.
In the present invention, described sheep dwells in earlier stage of dish handling and comprises washing, rejecting impurity, airing.The concentration that filtering and concentrating liquid contains dry is 0.5-10%.
The present invention is when extracting Sargassum fusiform powder material with ethanol, can adopt following multiple mode to extract: under at normal temperature condition, to adopt the alcohol immersion mode to extract, need to prove, adopt the required time of this kind method longer relatively, generally about 10 days; Under 70～100 ℃ of conditions, extract with ethanol; Under the ultrasonic wave heating condition, extract with ethanol; Adopt the carbon dioxide supercritical extraction mode to extract, used entrainer is an ethanol, and the ethanol consumption is the 5-25% of Sargassum fusiform powder material.
Sargassum fusiforme alcohol extract of the present invention is joined on the cigarette shreds with feed liquid as cigarette, when burning and sucking cigarette, the flue gas free from extraneous odour, have promote the production of body fluid, wet one's whistle, sharp phlegm and fall the evil effect.
Concrete addition manner is: be applied on the pipe tobacco by spray pattern, the Sargassum fusiforme alcohol extract consumption is the 0.01-50% of tobacco leaf weight.
Substantive features of the present invention are peculiar chemical compositions of utilizing Sargassum fusiforme alcohol extract to produce when cigarette burns and sucks, obviously improve or improve the quality quality of cigarette, have the effect of promoting the production of body fluid significantly and certain relieving cough function, can reduce the content of some harmful components in the cigarette mainstream flue gas.And do not change original performance of cigarette, do not change or influence the sucking quality of cigarette, therefore have more the meaning and the value of actual production.
The present invention has the following advantages compared to existing technology:
1, can improve the sucking quality of cigarette;
2, can reduce the content of some harmful components in the cigarette mainstream flue gas;
3, do not change the original performance and the cigarette producing process of cigarette;
4, has effects such as promoting the production of body fluid, wet one's whistle, eliminate the phlegm, reduce stimulation;
5, cost is not high, has practicality;
6, without any side effects.
After tested: the cigarette by made of the present invention is compared with the contrast cigarette, and the content of some harmful components in the cigarette mainstream flue gas obviously reduces, and as tobacco-specific nitrosamine, smoke gaseous phase free radical etc., the reduction amplitude is between 5%～15%; When burning and sucking cigarette, the flue gas free from extraneous odour, have promote the production of body fluid, wet one's whistle, effect such as sharp phlegm.
The specific embodiment
The present invention is described further below in conjunction with embodiment, but is not restriction the present invention.
Embodiment 1
Get the sheep bright product of dish of dwelling, behind fresh water washes clean, rejecting impurity, dry or dry.After oven dry under 50 ℃ of temperature, be crushed to 10～100 orders.Under 80 ℃ of conditions, with the alcohol extract sheep dish 5h of dwelling, filtrate filtered is concentrated to after dry matter content is 0.5-10% by Soxhlet extractor, and normal temperature is preserved.
With above-mentioned concentrated filtrate, the ratio in adding 15 gram concentrated filtrates in every kilogram of pipe tobacco is uniformly applied to behind the dilute with water on the cigarette shreds, gets final product.
Through smokeing panel test, the flue gas free from extraneous odour has the effect of promoting the production of body fluid significantly and certain relieving cough function.
Embodiment 2
Get the sheep dried vegetable product of dwelling, send out at light bubbly water.With the fresh water washes clean, reject impurity after, dry or dry.After oven dry under 40 ℃ of temperature, be crushed to 10～100 orders.Under the ultrasonic wave heating condition, with the alcohol extract sheep dish 45min of dwelling, filtrate filtered is concentrated to after dry matter content is 0.5-10% by Soxhlet extractor, and normal temperature is preserved.
With above-mentioned concentrated filtrate, the ratio in adding 10 gram concentrated filtrates in every kilogram of pipe tobacco is uniformly applied to behind the dilute with water on the cigarette shreds, gets final product.
The ultrasonic wave of this embodiment extracts the extraction of comparing embodiment 1 can make extraction time shorten greatly, and capable of reducing energy consumption.
Through smokeing panel test, the flue gas free from extraneous odour has the effect of promoting the production of body fluid significantly and certain relieving cough function.
Embodiment 3
Get sheep dwell bright product of dish or dry product, send out at light bubbly water.With the fresh water washes clean, reject impurity after, dry or dry.After oven dry under 50 ℃ of temperature, be crushed to 10～100 orders.Carry out carbon dioxide supercritical extraction: extracting pressure 25Mpa under the following conditions, 45 ℃ of extraction temperature; Separating pressure 6Mpa, 60 ℃ of separation temperatures.Ethanol with 95% is as entrainer, and the ethanol consumption is 17% of a Sargassum fusiform powder material.
Adopt the carbon dioxide supercritical extraction mode to extract Sargassum fusiform powder material 2h, after 3 separation, gained
Extract and separate thing tincture concentration is 5-10%, and normal temperature is preserved.
With above-mentioned tincture,,, get final product with being uniformly applied on the cigarette shreds after 75% the ethanolic solution dilution in the ratio that adds 2 gram tinctures in every kilogram of pipe tobacco.
Adopt the major advantage of carbon dioxide supercritical extraction mode to be: extraction temperature is lower, does not destroy the dwell chemical composition of dish of sheep; Can shorten extraction time, reduce consumption of ethanol, cut down the consumption of energy.
On the concrete consumption, in the scope of the 0.01-1.50% of cigarette shreds weight, all can reach certain effect.
Claims (8)
1, a kind of Sargassum fusiforme alcohol extract is characterized in that: it is to be made by following method:
A, sheep are being crushed to 10～100 orders after the oven dry under 30～60 ℃ of temperature after dwelling and handling dish premenstruum (premenstrua);
B, under 20～100 ℃ of conditions, Sargassum fusiform powder material is extracted time 0.5～8h with ethanol;
Be Sargassum fusiforme alcohol extract of the present invention after c, the filtering and concentrating.
2, Sargassum fusiforme alcohol extract according to claim 1 is characterized in that: sheep dwells in earlier stage of dish handling and comprises washing, rejecting impurity, airing.
3, Sargassum fusiforme alcohol extract according to claim 1 is characterized in that: the concentration that filtering and concentrating liquid contains dry is 0.5-10%.
4, Sargassum fusiforme alcohol extract according to claim 1 is characterized in that: when with ethanol Sargassum fusiform powder material being extracted, adopt the alcohol immersion mode to extract.
5, Sargassum fusiforme alcohol extract according to claim 1 is characterized in that: when with ethanol Sargassum fusiform powder material being extracted, adopt under the ultrasonic wave heating environment and extract with ethanolic solution.
6, Sargassum fusiforme alcohol extract according to claim 1, it is characterized in that: when Sargassum fusiform powder material being extracted with ethanol, adopt the carbon dioxide supercritical extraction mode to extract, used entrainer is an ethanol, and the ethanol consumption is the 5-25% of Sargassum fusiform powder material.
7, the application of Sargassum fusiforme alcohol extract according to claim 1 in tobacco, it is characterized in that: Sargassum fusiforme alcohol extract of the present invention is joined on the cigarette shreds with feed liquid as cigarette, when burning and sucking cigarette, the flue gas free from extraneous odour, have promote the production of body fluid, wet one's whistle, sharp phlegm and fall the evil effect.
8, the application of Sargassum fusiforme alcohol extract according to claim 7 in tobacco is characterized in that: the Sargassum fusiforme alcohol extract consumption is the 0.01-1.5% of pipe tobacco weight, is applied on the cigarette shreds by spray pattern.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006101282848A CN100508801C (en) | 2006-11-25 | 2006-11-25 | Preparing method of sargassum fusiforme alcohol extract and application of sargassum fusiforme in tobacco |
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| CNB2006101282848A CN100508801C (en) | 2006-11-25 | 2006-11-25 | Preparing method of sargassum fusiforme alcohol extract and application of sargassum fusiforme in tobacco |
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| CN1961762A true CN1961762A (en) | 2007-05-16 |
| CN100508801C CN100508801C (en) | 2009-07-08 |
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Cited By (8)
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|---|---|---|---|---|
| CN101250232B (en) * | 2008-03-27 | 2010-06-23 | 钱国英 | Extraction technique of sargassum fusiform active polysaccharides |
| CN101862031A (en) * | 2010-06-22 | 2010-10-20 | 中国烟草总公司郑州烟草研究院 | Preparation of undaria pinnitafida ethanol extracting solution and application thereof to cigarette |
| CN101862030A (en) * | 2010-06-22 | 2010-10-20 | 中国烟草总公司郑州烟草研究院 | Preparation of asparagus ethanol extract and application thereof in cigarette |
| CN103844346A (en) * | 2014-03-04 | 2014-06-11 | 江苏中烟工业有限责任公司 | Burdock root ethanol extract and application thereof in tobacco |
| CN108668732A (en) * | 2018-04-01 | 2018-10-19 | 广西陆川和合生物科技有限公司 | A kind of method for culturing seedlings of selenium-rich camellia tree |
| CN109566807A (en) * | 2018-11-30 | 2019-04-05 | 龚士华 | Selenium-enriched vine tea and its processing method |
| CN109566806A (en) * | 2018-11-30 | 2019-04-05 | 龚士华 | It is a kind of for promoting the sargassum fusifome extracting solution of selenium-enriched vine tea health-care effect |
| CN110720663A (en) * | 2019-10-16 | 2020-01-24 | 山西昆明烟草有限责任公司 | Sargassum fusiforme porous particle, preparation method and application in cigarette |
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| CN103087824B (en) * | 2013-01-31 | 2014-08-20 | 中国烟草总公司郑州烟草研究院 | Preparation method of cigarette flavor and application thereof |
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- 2006-11-25 CN CNB2006101282848A patent/CN100508801C/en active Active
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101250232B (en) * | 2008-03-27 | 2010-06-23 | 钱国英 | Extraction technique of sargassum fusiform active polysaccharides |
| CN101862031A (en) * | 2010-06-22 | 2010-10-20 | 中国烟草总公司郑州烟草研究院 | Preparation of undaria pinnitafida ethanol extracting solution and application thereof to cigarette |
| CN101862030A (en) * | 2010-06-22 | 2010-10-20 | 中国烟草总公司郑州烟草研究院 | Preparation of asparagus ethanol extract and application thereof in cigarette |
| CN103844346A (en) * | 2014-03-04 | 2014-06-11 | 江苏中烟工业有限责任公司 | Burdock root ethanol extract and application thereof in tobacco |
| CN108668732A (en) * | 2018-04-01 | 2018-10-19 | 广西陆川和合生物科技有限公司 | A kind of method for culturing seedlings of selenium-rich camellia tree |
| CN109566807A (en) * | 2018-11-30 | 2019-04-05 | 龚士华 | Selenium-enriched vine tea and its processing method |
| CN109566806A (en) * | 2018-11-30 | 2019-04-05 | 龚士华 | It is a kind of for promoting the sargassum fusifome extracting solution of selenium-enriched vine tea health-care effect |
| CN110720663A (en) * | 2019-10-16 | 2020-01-24 | 山西昆明烟草有限责任公司 | Sargassum fusiforme porous particle, preparation method and application in cigarette |
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| CN100508801C (en) | 2009-07-08 |
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