CN110720663A - Sargassum fusiforme porous particle, preparation method and application in cigarette - Google Patents
Sargassum fusiforme porous particle, preparation method and application in cigarette Download PDFInfo
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- CN110720663A CN110720663A CN201910984669.1A CN201910984669A CN110720663A CN 110720663 A CN110720663 A CN 110720663A CN 201910984669 A CN201910984669 A CN 201910984669A CN 110720663 A CN110720663 A CN 110720663A
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- sargassum fusiforme
- porous
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- filter stick
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses a sargassum fusiforme porous particle, a preparation method and application thereof in cigarettes, wherein the preparation method comprises the following steps of taking a mixture of sargassum fusiforme powder and corn starch with the particle size of 100 ~ 150 meshes as a raw material, taking hydroxypropyl methylcellulose, sodium carboxymethylcellulose or xanthan gum as an adhesive, adding distilled water, mixing and stirring uniformly, then adopting an extrusion granulation process to prepare sargassum fusiforme porous wet particles with the particle size of 40 ~ 60 meshes, drying the sargassum fusiforme porous wet particles at 40 ~ 60 ℃ for 4 hours to prepare the sargassum fusiforme porous particles with the water content of 6 ~ 8%, and adding the prepared sargassum fusiforme porous particles into a cigarette filter stick of a composite cigarette filter stick containing the sargassum fusiforme porous particles according to the adding amount of 1 ~ 5mg/mm, so that the richness and the fineness of cigarette smoke can be obviously improved, and the irritation can be reduced.
Description
Technical Field
The invention relates to the technical field of cigarette auxiliary material materials, in particular to a sargassum fusiforme porous particle capable of improving smoking quality of cigarettes, a preparation method and application in cigarettes.
Technical Field
With the increasing concern about smoking and health, how to improve the smoking safety of cigarettes, reduce harmful ingredients in cigarette smoke and improve the comfort of smoking becomes a research and development hotspot of various cigarette manufacturing enterprises. At present, the existing spice particles are researched more, and the porous particle material with special fragrance is added into the cigarette filter stick, so that the method is a novel, effective and promising research direction, and can improve or promote the quality of cigarette products. In recent years, the development of marine biotechnology has accelerated the development of marine drugs, and thus, marine medicinal biological resources have become a new focus of attention.
The sargassum fusiforme is an algae plant, grows on low-tide rocks, grows luxuriantly on the coast in south China, contains 18 important amino acids and 14 trace elements required by a human body, and has high nutritional and health-care values. The sargassum fusiforme mainly has the effects of promoting digestion, removing blood stasis, clearing heat, reducing phlegm, promoting immunity and reducing blood fat and blood sugar. The use of sargassum fusiforme as a medicine has a long history in China, but reports that sargassum fusiforme is prepared into a porous particle material and applied to cigarettes are not seen.
Disclosure of Invention
The invention aims to provide a sargassum fusiforme porous particle capable of improving smoking quality of cigarettes, a preparation method and application in cigarettes.
To achieve the object of the present invention, the method for preparing the porous granules of sargassum fusiforme comprises the following steps:
a. drying fresh Cyrtymenia Sparsa at 40 ~ 60 deg.C to water content of 8 ~ 10%;
b. pulverizing dried Cyrtymenia Sparsa with a pulverizer, and sieving with 100 ~ 160 mesh sieve;
c. mixing 100 ~ 160 mesh sargassum fusiforme powder, corn starch and a binding agent uniformly, adding a certain amount of distilled water, stirring uniformly, and preparing 40 ~ 60 mesh sargassum fusiforme porous wet granules by adopting an extrusion granulation process, wherein the weight parts of the sargassum fusiforme powder, the corn starch and the binding agent are sargassum fusiforme powder, the corn starch, the binding agent and the distilled water are =450 ~ 650: 350 ~ 550: 20 ~ 50: 250 ~ 300;
d. drying the prepared sargassum fusiforme porous wet granules at 40 ~ 60 deg.C for 4h to obtain sargassum fusiforme porous granules with water content of 6 ~ 8%.
The binder may be any one of hydroxypropyl methylcellulose, sodium carboxymethylcellulose, or xanthan gum.
The application of the sargassum fusiforme porous particles in cigarettes is to add the prepared sargassum fusiforme porous particles with the water content of 6 ~ 8% into a cigarette filter stick in the adding amount of 1 ~ 5 mg/mm.
The Sargassum fusiforme adopted by the invention is an algae plant, such as a sphaeroides, sargassaceae, alias antler tip, seaweed sprout, sea barley and the like. Cyrtymenia Sparsa grows on low-tide rock, grows luxuriantly in the south China coastal region, and is distributed in Shandong, Liaoning and other places. The sargassum fusiforme mainly has the effects of promoting digestion, removing blood stasis, clearing heat, reducing phlegm, promoting immunity and reducing blood fat and blood sugar.
The invention has the beneficial effects that:
the invention selects the dried sargassum fusiforme with the water content of 8 ~ 10 percent, crushes the sargassum fusiforme, screens out powder with the grain diameter of 100 ~ 160 meshes, prepares porous sargassum fusiforme particles with the grain diameter of 40 ~ 60 meshes by an extrusion granulation process, and then adds the porous sargassum fusiforme particles with the grain diameter of 40 ~ 60 meshes into a cigarette filter stick to be applied to the cigarette.
Detailed Description
The present invention is further illustrated by the following examples, but is not limited thereto in any way, and any alterations or modifications based on the teachings of the present invention are within the scope of the present invention.
The examples do not specify particular techniques or conditions, and are performed according to the techniques or conditions described in the literature in the art or according to the product specifications. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products available by purchase.
Example 1:
drying fresh sargassum fusiforme at 40 ~ 60 ℃ until the water content is 8 ~ 10%, selecting the dried sargassum fusiforme with the water content of 8 ~ 10%, crushing the sargassum fusiforme into powder with the average particle size of 100 meshes, weighing 450g, weighing 550g of corn starch and 50g of hydroxypropyl methyl cellulose, uniformly mixing the three kinds of powder, mixing the mixed powder with 300g of distilled water, stirring uniformly, adding the mixture into an extrusion granulator for extrusion granulation to obtain sargassum fusiforme porous wet granules with the particle size of 40 ~ 60 meshes, drying the sargassum fusiforme porous wet granules at 40 ~ 60 ℃ for 4 hours to obtain the sargassum fusiforme porous granules with the water content of 6 ~ 8%.
The prepared sargassum fusiforme porous particles are added into a cigarette filter stick with the diameter of 7.64mm according to the adding amount of 5mg/mm, and then the composite cigarette filter stick containing the sargassum fusiforme porous particles and having the effects of reducing irritation, improving cigarette smoking comfort and the like is prepared through a filter stick forming machine.
Example 2:
placing fresh sargassum fusiforme at 40 ~ 60 ℃ and drying until the water content is 8 ~ 10%, selecting sargassum fusiforme with the dried water content of 8 ~ 10%, crushing the sargassum fusiforme into powder with the average particle size of 160 meshes, weighing 650g, weighing 350g of corn starch and 25g of sodium carboxymethylcellulose, uniformly mixing the three kinds of powder, mixing the mixed powder with 250g of distilled water, stirring uniformly, adding the mixture into an extrusion granulator for extrusion granulation to obtain sargassum fusiforme porous wet granules with the particle size of 40 ~ 60 meshes, and drying the sargassum fusiforme porous wet granules at 40 ~ 60 ℃ for 4 hours to obtain the sargassum fusiforme porous granules with the water content of 6 ~ 8%.
Adding the prepared sargassum fusiforme porous particles into a cigarette filter stick with the diameter of 7.64mm according to the addition amount of 3mg/mm, and preparing the composite cigarette filter stick containing the sargassum fusiforme porous particles with the effects of reducing irritation, improving cigarette smoking comfort and the like by a filter stick forming machine.
Example 3:
fresh sargassum fusiforme is placed at 40 ~ 60 ℃ and dried until the moisture content is 8 ~ 10%, dried sargassum fusiforme with the moisture content of 8 ~ 10% is selected, the dried sargassum fusiforme is crushed into powder with the average particle size of 120 meshes, 550g is weighed, 450g of corn starch and 30g of xanthan gum are weighed, the three kinds of powder are uniformly mixed, then the mixed powder is mixed with 280g of distilled water and uniformly stirred, the mixture is added into an extrusion granulator for extrusion granulation, the sargassum fusiforme porous wet granules with the particle size of 40 ~ 60 meshes are prepared, the sargassum fusiforme porous wet granules are dried for 4 hours at the temperature of 40 ~ 60 ℃ to obtain sargassum fusiforme porous granules with the moisture content of 6 ~ 8%, the prepared sargassum fusiforme porous granules are added into a cigarette filter stick with the diameter of 7.64mm according to the adding amount of 2mg/mm, and the composite cigarette filter stick containing the sargassum fusiforme porous granules with the effects of reducing irritation, improving the smoking comfort of the cigarettes.
Application example 1:
the porous sargassum fusiforme particles prepared in the embodiment 1 are added into a cigarette filter stick with the diameter of 7.64mm through filter stick forming equipment and particle feeding equipment according to the addition amount of 5mg/mm, and a composite cigarette filter stick containing the porous sargassum fusiforme particles is prepared. The control filter stick is a filter stick added with particles which are obtained by extruding and drying pure corn starch. The two filter sticks are used for lofting to produce cigarettes, and except for the filter sticks, the cigarette materials and the leaf group formulas of the test cigarettes are the same as those of the reference sample. The smoke analysis results of the cigarette samples produced by lofting are shown in table 1, and the smoking evaluation results of the cigarette samples produced by lofting are shown in table 2.
TABLE 1 composite filter stick cigarette containing porous Cyrtymenia Sparsa particles and smoke analysis results of control sample
TABLE 2 composite filter stick cigarette containing sargassum fusiforme porous particles and control sample cigarette evaluation results
Application example 2:
the porous sargassum fusiforme particles prepared in the embodiment 2 are added into a cigarette filter stick with the diameter of 7.64mm through filter stick forming equipment and particle feeding equipment according to the addition amount of 3mg/mm, and a composite cigarette filter stick containing the porous sargassum fusiforme particles is prepared. The control filter stick is a filter stick added with particles which are obtained by extruding and drying pure corn starch. The two filter sticks are used for lofting to produce cigarettes, and except for the filter sticks, the cigarette materials and the leaf group formulas of the test cigarettes are the same as those of the reference sample. The smoke analysis results of the cigarette samples produced by lofting are shown in Table 3, and the smoking evaluation results of the cigarette samples produced by lofting are shown in Table 4.
TABLE 3 composite filter stick cigarette containing porous Cyrtymenia Sparsa particles and smoke analysis results of control sample
TABLE 4 composite filter stick cigarette containing sargassum fusiforme porous particles and control sample cigarette evaluation results
Application example 3:
the porous sargassum fusiforme particles prepared in the embodiment 3 are added into a cigarette filter stick with the diameter of 7.64mm through filter stick forming equipment and particle feeding equipment according to the addition amount of 2mg/mm, and a composite cigarette filter stick containing the porous sargassum fusiforme particles is prepared. The control filter stick is a filter stick added with particles which are obtained by extruding and drying pure corn starch. The two filter sticks are used for lofting to produce cigarettes, and except for the filter sticks, the cigarette materials and the leaf group formulas of the test cigarettes are the same as those of the reference sample. The smoke analysis results of the cigarette samples produced by lofting are shown in Table 5, and the smoking evaluation results of the cigarette samples produced by lofting are shown in Table 6.
TABLE 5 composite filter stick cigarette containing porous Cyrtymenia Sparsa particles and smoke analysis results of control sample
TABLE 6 composite filter stick cigarette containing sargassum fusiforme porous particles and control sample cigarette evaluation results
By analyzing the experimental results of the application example 1, the application example 2 and the application example 3, it can be seen that the content of tar and CO in the smoke can be obviously reduced and the content of carcinogens benzo [ a ] pyrene and phenol in the smoke can be reduced compared with the control cigarette which uses a particle filter stick which is extruded and dried by corn starch only after the porous sargassum fusiforme particles are added into the cigarette filter stick. The sensory evaluation of the cigarettes shows that the addition of the sargassum fusiforme porous particles in the filter tip can increase the aroma amount of cigarette smoke, improve the aroma quality and harmony, reduce the miscellaneous gas and irritation, and integrally improve the internal quality of the cigarettes.
The foregoing shows and describes the general principles, essential features, and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the invention as claimed. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (4)
1. A preparation method of sargassum fusiforme porous particles is characterized by comprising the following steps: the method comprises the following steps:
a. drying fresh Cyrtymenia Sparsa at 40 ~ 60 deg.C to water content of 8 ~ 10%;
b. pulverizing dried Cyrtymenia Sparsa with a pulverizer, and sieving with 100 ~ 160 mesh sieve;
c. uniformly mixing sargassum fusiforme powder with the grain size of 100 ~ 160 meshes with corn starch and a binder, adding a certain amount of distilled water, uniformly stirring, and preparing the sargassum fusiforme porous wet granules with the grain size of 40 ~ 60 meshes by adopting an extrusion granulation process, wherein the weight fraction ratio of the sargassum fusiforme powder to the corn starch to the binder to the distilled water is =450 ~ 650: 350 ~ 550: 20 ~ 50: 250 ~ 300;
d. drying the prepared sargassum fusiforme porous wet granules at 40 ~ 60 deg.C for 4h to obtain sargassum fusiforme porous granules with water content of 6 ~ 8%.
2. The method for preparing porous granules of sargassum fusiforme according to claim 1, wherein: the binder may be any one of hydroxypropyl methylcellulose, sodium carboxymethylcellulose, or xanthan gum.
3. A porous Cyrtymenia Sparsa granule with water content of 6 ~ 8% prepared by the method of claim 1.
4. The use of the porous Cyrtymenia Sparsa particles as claimed in claim 3, wherein the porous Cyrtymenia Sparsa particles with water content of 6 ~ 8% are added into cigarette filter stick at an addition amount of 1 ~ 5 mg/mm.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910984669.1A CN110720663A (en) | 2019-10-16 | 2019-10-16 | Sargassum fusiforme porous particle, preparation method and application in cigarette |
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| CN201910984669.1A CN110720663A (en) | 2019-10-16 | 2019-10-16 | Sargassum fusiforme porous particle, preparation method and application in cigarette |
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| CN110720663A true CN110720663A (en) | 2020-01-24 |
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| CN1961762A (en) * | 2006-11-25 | 2007-05-16 | 中国烟草总公司郑州烟草研究院 | Sargassum fusiforme alcohol extract and application thereof in tobacco |
| CN101238912A (en) * | 2008-02-29 | 2008-08-13 | 徐长保 | Cigarette filter tip |
| CN103087824A (en) * | 2013-01-31 | 2013-05-08 | 中国烟草总公司郑州烟草研究院 | Preparation method of cigarette flavor and application thereof |
| CN103750564A (en) * | 2014-01-23 | 2014-04-30 | 广西中烟工业有限责任公司 | Caper and porous starch composite particle, preparation of caper and porous starch composite particle and application of caper and porous starch composite particle in cigarette filter |
| CN108391850A (en) * | 2018-03-15 | 2018-08-14 | 河北中烟工业有限责任公司 | A kind of gloiopeltis porous particle preparation method and its application in cigarette |
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2019
- 2019-10-16 CN CN201910984669.1A patent/CN110720663A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1962699A (en) * | 2006-11-25 | 2007-05-16 | 中国烟草总公司郑州烟草研究院 | Hijiki polysaccharide and its uses in tobacco |
| CN1961762A (en) * | 2006-11-25 | 2007-05-16 | 中国烟草总公司郑州烟草研究院 | Sargassum fusiforme alcohol extract and application thereof in tobacco |
| CN101238912A (en) * | 2008-02-29 | 2008-08-13 | 徐长保 | Cigarette filter tip |
| CN103087824A (en) * | 2013-01-31 | 2013-05-08 | 中国烟草总公司郑州烟草研究院 | Preparation method of cigarette flavor and application thereof |
| CN103750564A (en) * | 2014-01-23 | 2014-04-30 | 广西中烟工业有限责任公司 | Caper and porous starch composite particle, preparation of caper and porous starch composite particle and application of caper and porous starch composite particle in cigarette filter |
| CN108391850A (en) * | 2018-03-15 | 2018-08-14 | 河北中烟工业有限责任公司 | A kind of gloiopeltis porous particle preparation method and its application in cigarette |
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Application publication date: 20200124 |