CN1962699A - Hijiki polysaccharide and its uses in tobacco - Google Patents
Hijiki polysaccharide and its uses in tobacco Download PDFInfo
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- CN1962699A CN1962699A CN 200610128282 CN200610128282A CN1962699A CN 1962699 A CN1962699 A CN 1962699A CN 200610128282 CN200610128282 CN 200610128282 CN 200610128282 A CN200610128282 A CN 200610128282A CN 1962699 A CN1962699 A CN 1962699A
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Abstract
The invention discloses a goat-inhabiting vegetable polysaccharide and application in the tobacco, which comprises the following steps: a. disposing the vegetable; drying at 30-60 Deg C; grinding to 10-100order; b. extracting vegetable powder through water at 80-120 Deg C for 1-8h; c. filtering; condensing the filtrate; d. adding alcohol in the condensed slurry to mix; stewing under 4 Deg C over 8h; centrifuging; filtering; obtaining the product. The invention can be applied on the cigarette pipe-tobacco, which improves the quality of cigarette.
Description
Technical field
The present invention relates to plant extract and application thereof, particularly Hijiki polysaccharide and the application in tobacco thereof.This The Application of Technology does not change the existing complete processing of cigarette, can improve the quality of cigarette, reduces the hazardness of cigarette.
Background technology
Along with the problem of smoking with health more and more receives publicity, the objectionable constituent of sucking security, increase nourishing function, reducing in the cigarette smoke that improve cigarette are the inevitable development trend of cigarette.Therefore occurred as kinds such as ginseng cigarette, peppermint cigarettes on the market, promptly in pipe tobacco, added the material that genseng, peppermint etc. have unique nourishing function or taste.
Sargassum fusiforme system food, medicine dual purpose plant, Hijiki polysaccharide can be extracted by Sargassum fusiforme and make.Hijiki polysaccharide comprises alginic acid, algal polysaccharide sulfate and laminaran etc., to the prevention thyromegaly, reduce cholesterol in the blood, treatment hypertension and large bowel cancer, cancer of the stomach all have certain effect, has the function of removing oxyradical, to keeping skin lubrication, recover brain fag, prevent that aging etc. from also having significant effect.Domestic relevant research is mainly at the chemical constituents determination of Hijiki polysaccharide, aspect such as medical.Do not find the application precedent in tobacco.
Goal of the invention
Purpose of the present invention just is being based on the situation of above-mentioned prior art and is studying and then developing Hijiki polysaccharide and the application in tobacco thereof at Sargassum fusiforme specially, the Hijiki polysaccharide extraction separation is come out, join on the cigarette shreds, can improve the sucking quality of cigarette, reduce some objectionable constituent in the cigarette mainstream flue gas.And this The Application of Technology does not change the existing complete processing of cigarette, can improve the quality of cigarette, reduces the hazardness of cigarette.
The objective of the invention is to realize that by following scheme Hijiki polysaccharide of the present invention is to be made by following method:
After a, Sargassum fusiforme processing premenstruum, be crushed to 10～100 orders after the oven dry under 30～60 ℃ of temperature;
B, under 80～120 ℃ of conditions, water extracts Sargassum fusiform powder material, time 1～8h;
C, filtering and concentrating;
D, in concentrated filtrate, add ethanol, leaving standstill under 4 ℃ more than 8 hours behind the mixing, through centrifugal, filter after, promptly obtain Hijiki polysaccharide of the present invention.
In the present invention, processing in the early stage of described Sargassum fusiforme comprises washing, rejects impurity, airing; In the c step, the concentration that filtering and concentrating liquid contains dry-matter is 1-10%.By concentrating feed liquid: ethanol is that 1: 3 volume ratio adds ethanol, and purity of alcohol is 90%～98%.
With Hijiki polysaccharide of the present invention through being applied on the cigarette shreds with feed liquid as cigarette after the water dissolution, when burning and sucking cigarette, the flue gas free from extraneous odour, have promote the production of body fluid, wet one's whistle, sharp phlegm and fall the evil effect.Concrete usage ratio is: the Hijiki polysaccharide consumption is the 0.001-0.5% of pipe tobacco weight, Hijiki polysaccharide is a brown solid, and water soluble is during use, the strength of solution of Hijiki polysaccharide after water dissolution is 1-10%, by spray pattern Hijiki polysaccharide solution added on the pipe tobacco.
Substantive features of the present invention are peculiar chemical ingredientss of utilizing Hijiki polysaccharide to produce when cigarette burns and sucks, obviously improve or improve the quality quality of cigarette, have the effect of promoting the production of body fluid significantly and certain relieving cough function, can reduce the content of some objectionable constituent in the cigarette mainstream flue gas, and do not change original performance of cigarette, do not change or influence the sucking quality of cigarette, therefore have more the meaning and the value of actual production.
The present invention has the following advantages compared to existing technology:
1, can improve the sucking quality of cigarette;
2, can reduce some objectionable constituent in the cigarette mainstream flue gas;
3, do not change the original performance and the cigarette complete processing of cigarette;
4, has certain humectation effect;
5, has effects such as promoting the production of body fluid, wet one's whistle, eliminate the phlegm, reduce stimulation;
6, cost is not high, has practicality;
7, without any side effects.
After tested: the cigarette by made of the present invention is compared with the contrast cigarette, and the content of some objectionable constituent obviously reduces in the cigarette mainstream flue gas, and as tobacco-specific nitrosamine, smoke gaseous phase free radical etc., the reduction amplitude is between 5%-20%; When burning and sucking cigarette, the flue gas free from extraneous odour, have promote the production of body fluid, wet one's whistle, effect such as sharp phlegm; Be added with the cigarette of Hijiki polysaccharide solution, the lethal time of animal acute exposure cigarette smoke has increased by 40%, respiratory tract reaction and pathology damage all obviously alleviate due to the chronic exposure cigarette smoke, the performance cough latent period prolongs, the cough number of times reduces, tracheae is secreted the phlegm ability to be increased, and the maximum no-effect dose of the sensitive indicator of peripheral blood, organ weights coefficient and blood biochemical has all increased about 50%.
Embodiment
The present invention is described further below in conjunction with embodiment, but is not restriction the present invention.
Embodiment 1
Get the bright product of Sargassum fusiforme, behind fresh water washes clean, rejecting impurity, dry or dry.After oven dry under 50 ℃ of temperature, be crushed to 10～100 orders.Under 90 ℃ of conditions, with water extraction Sargassum fusiforme 7h, after the content that filtrate filtered is concentrated to dry-matter is 5%, with the filtrate after concentrating, by filtrate: ethanol is that 1: 3 volume ratio adds ethanol (concentration 95%), under 4 ℃, leave standstill more than the 8h behind the mixing, through centrifugal, filter after, promptly get Hijiki polysaccharide of the present invention.
Hijiki polysaccharide joins on the cigarette shreds with feed liquid through making cigarette after the water dissolution, and the ratio that specifically applies is: the consumption of Hijiki polysaccharide is 0.05% of a pipe tobacco weight, adds on the pipe tobacco by spray pattern behind the dilute with water.The concentration of Hijiki polysaccharide solution is 5%, stored refrigerated.
Through test and appraisal, the content of some objectionable constituent reduces in the cigarette mainstream flue gas, the flue gas free from extraneous odour, and have significantly promote the production of body fluid, sharp phlegm and antitussive action.
Embodiment 2
Get the Sargassum fusiforme dry product, send out at light bubbly water.With the fresh water washes clean, reject impurity after, dry or dry.After oven dry under 40 ℃ of temperature, be crushed to 10～100 orders.Under the ultrasonic wave condition, with water extraction Sargassum fusiforme 1h, filtrate filtered is concentrated to after the concentration that contains dry-matter is 8%, with the filtrate after concentrating, by filtrate: ethanol is that 1: 3 volume ratio adds ethanol (concentration 95%), under 4 ℃, leave standstill more than the 8h behind the mixing, through centrifugal, filter after, promptly get Hijiki polysaccharide of the present invention.
Hijiki polysaccharide is added on the cigarette shreds with the feed liquid spray through can be used as cigarette after the water dissolution, and the ratio that specifically applies is: the consumption of Hijiki polysaccharide is 0.01% of a pipe tobacco weight, is applied on the pipe tobacco by spray pattern behind the dilute with water.The concentration of Hijiki polysaccharide solution is 7.5%, stored refrigerated.
Through test and appraisal, the flue gas free from extraneous odour has the effect of promoting the production of body fluid significantly and certain relieving cough function.
About the usage quantity of Hijiki polysaccharide, as long as in the 0.001-0.5% of pipe tobacco weight scope, all can reach certain effect.
Claims (8)
1, a kind of Hijiki polysaccharide is characterized in that: it is to be made by following method:
After a, Sargassum fusiforme processing premenstruum, be crushed to 10～100 orders after the oven dry under 30～60 ℃ of temperature;
B, under 80～120 ℃ of conditions, water extracts Sargassum fusiform powder material, time 1～8h;
C, filtering and concentrating;
D, in concentrating feed liquid, add ethanol, leaving standstill under 4 ℃ more than 8 hours behind the mixing, through centrifugal, filter after, promptly obtain Hijiki polysaccharide of the present invention.
2, Hijiki polysaccharide according to claim 1 is characterized in that: the processing in early stage of Sargassum fusiforme comprises washing, rejects impurity, airing.
3, Hijiki polysaccharide according to claim 1 is characterized in that: in the c step, the concentration that contains dry-matter in the filtering and concentrating liquid is 1-10%.
4, Hijiki polysaccharide according to claim 1 is characterized in that: Hijiki polysaccharide is a brown solid, water soluble.
5, Hijiki polysaccharide according to claim 1 is characterized in that: by concentrating feed liquid: ethanol is that 1: 3 volume ratio adds ethanol, and purity of alcohol is 90%～98%.
6, the application of Hijiki polysaccharide according to claim 1 in tobacco, it is characterized in that: with Hijiki polysaccharide of the present invention through joining on the cigarette shreds with feed liquid as cigarette after the water dissolution, when burning and sucking cigarette, the flue gas free from extraneous odour, have promote the production of body fluid, wet one's whistle, sharp phlegm and fall the evil effect.
7, the application of Hijiki polysaccharide according to claim 6 in tobacco is characterized in that: the Hijiki polysaccharide consumption is the 0.001-0.5% of pipe tobacco weight, by spray pattern Hijiki polysaccharide solution is added on the pipe tobacco.
8, Hijiki polysaccharide according to claim 6 is characterized in that: the strength of solution of Hijiki polysaccharide after water dissolution is 1-10%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2006101282829A CN1962699B (en) | 2006-11-25 | 2006-11-25 | Hijiki polysaccharide and its uses in tobacco |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2006101282829A CN1962699B (en) | 2006-11-25 | 2006-11-25 | Hijiki polysaccharide and its uses in tobacco |
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| Publication Number | Publication Date |
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| CN1962699A true CN1962699A (en) | 2007-05-16 |
| CN1962699B CN1962699B (en) | 2012-02-01 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN2006101282829A Active CN1962699B (en) | 2006-11-25 | 2006-11-25 | Hijiki polysaccharide and its uses in tobacco |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101250232B (en) * | 2008-03-27 | 2010-06-23 | 钱国英 | Extraction technique of sargassum fusiform active polysaccharides |
| CN102367281A (en) * | 2011-10-20 | 2012-03-07 | 广东中烟工业有限责任公司 | Preparation method and application of ethanol extract of laminarin |
| CN102793263A (en) * | 2012-08-27 | 2012-11-28 | 福建中烟工业有限责任公司 | Extraction method of tremella water extract concentrate and application of concentrate in tobaccos |
| CN105754000A (en) * | 2016-04-18 | 2016-07-13 | 安徽坤大生物工程技术有限公司 | Hizikia fusiforme polysaccharide extracting technology |
| CN110720663A (en) * | 2019-10-16 | 2020-01-24 | 山西昆明烟草有限责任公司 | Sargassum fusiforme porous particle, preparation method and application in cigarette |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1036067C (en) * | 1994-08-24 | 1997-10-08 | 沈阳医药工业研究所 | Method for extracting protein and polysaccharide from spirulina |
| CN1044607C (en) * | 1995-12-16 | 1999-08-11 | 中国科学院海洋研究所 | Medicine of alginic polysaccharide sulfate for treatment of nephrasthenia and angiopathy and preparation method thereof |
| CN1324051C (en) * | 2004-12-29 | 2007-07-04 | 中山大学 | Hijiki polysaccharide SFP-I, its separation purification method and application |
-
2006
- 2006-11-25 CN CN2006101282829A patent/CN1962699B/en active Active
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101250232B (en) * | 2008-03-27 | 2010-06-23 | 钱国英 | Extraction technique of sargassum fusiform active polysaccharides |
| CN102367281A (en) * | 2011-10-20 | 2012-03-07 | 广东中烟工业有限责任公司 | Preparation method and application of ethanol extract of laminarin |
| CN102793263A (en) * | 2012-08-27 | 2012-11-28 | 福建中烟工业有限责任公司 | Extraction method of tremella water extract concentrate and application of concentrate in tobaccos |
| CN105754000A (en) * | 2016-04-18 | 2016-07-13 | 安徽坤大生物工程技术有限公司 | Hizikia fusiforme polysaccharide extracting technology |
| CN105754000B (en) * | 2016-04-18 | 2018-03-27 | 安徽坤大生物工程技术有限公司 | Hijiki polysaccharide extraction process |
| CN110720663A (en) * | 2019-10-16 | 2020-01-24 | 山西昆明烟草有限责任公司 | Sargassum fusiforme porous particle, preparation method and application in cigarette |
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| Publication number | Publication date |
|---|---|
| CN1962699B (en) | 2012-02-01 |
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