CN101692933A - Cigarette containing lentinan and preparation method thereof - Google Patents
Cigarette containing lentinan and preparation method thereof Download PDFInfo
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- CN101692933A CN101692933A CN200910189848A CN200910189848A CN101692933A CN 101692933 A CN101692933 A CN 101692933A CN 200910189848 A CN200910189848 A CN 200910189848A CN 200910189848 A CN200910189848 A CN 200910189848A CN 101692933 A CN101692933 A CN 101692933A
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Abstract
The invention discloses a cigarette containing lentinan and a preparation method thereof, aiming at solving the technical problem of reducing the harmful ingredients in cigarettes. The cigarette containing the lentinan has the tobacco shred containing the lentinan with the mass of 0.001-10% of the tobacco shred. The preparation method of the cigarette containing the lentinan comprises the following steps: dissolving the lentinan in the water to be solution with the mass concentration of 1-10%; evenly spaying the lentinan solution onto the tobacco shred according to the proportion that the lentinan accounts for 0.001-10% of the tobacco shred; and finally, naturally drying and making into the cigarettes according to the conventional cigarette technology. Compared with the prior art, as the tobacco shred contains the extract of the ingredient of the lentinan which has good dissolubility, can enters the human body along with the main stream smoke and is absorbed by the human body through blood circulation, thus playing the role of resisting tumour, oxidation and aging; furthermore, the smoke of the cigarettes is mellow without impurity gas, so that the invention improves the quality of the cigarettes and reduces the hazard to the human health.
Description
Technical field
The present invention relates to a kind of cigarette and preparation method thereof, particularly a kind of cigarette of reducing the harmful components in the cigarette and preparation method thereof.
Background technology
According to a research report of the World Health Organization, the whole world has 1,000,000 people every year at least because smoking and dead prematurely.China pays much attention to the harmful work of falling of cigarette, and since 2005, State Tobacco Monopoly Bureau has organized cigarette harmfulness index system and two great special research work of cigarette flavouring humectation, has obtained certain achievement.As Chinese patent application 200810058052.9 disclosed a kind of Chinese herbal medicine extract and preparation and usings method that are used for papermaking-method reconstituted tobaccos, extract with the seed of Oriental arborvitae, the tuber of dwarf lilyturf, radix glehniae, Momordica grosvenori, honeysuckle, dandelion, purple perilla seed and Radix Glycyrrhizae adds in the tobacco leaf, enrich the cigarette flavor musical tone, respiratory tract discomfort behind the reduction smoking cigarette.Chinese patent 200610128283.3 disclosed Sargassum fusiforme aqueous extracts and the application in tobacco thereof join Sargassum fusiforme aqueous extract on the cigarette shreds with feed liquid as cigarette, have the effect of promoting the production of body fluid significantly and certain relieving cough function.However, the needs that the cigarette of prior art can not be satisfied to be increased fragrance, reduce the harmful components in the cigarette also will further utilize the new industrial research new product.
Summary of the invention
The purpose of this invention is to provide a kind of cigarette that contains lentinan and preparation method thereof, the technical problem that solve is the harmful components that reduce in the cigarette.
The present invention is by the following technical solutions: a kind of cigarette that contains lentinan, have pipe tobacco, and contain the lentinan of tobacco quality 0.001～10% in the described pipe tobacco.
The lentinan that contains tobacco quality 1% in the pipe tobacco of the present invention.
Mushroom polysaccharide of the present invention obtains with following method: with 60 ℃ of oven dry of mushroom, and be crushed to the 10-100 order, add 100 ℃ of hot water of 10 times of quality, lixiviate 3 times each 5 hours, merges 3 times water extract, filter, filtrate decompression under 0.05Mpa, 60 ℃, 2 hours conditions, concentrate, the filtrate after concentrating is added 95% ethanol of 5 times of volumes again, 10 ℃ left standstill 12 hours, 3000 rev/mins, 30 minutes centrifugal treating are filtered, and obtain lentinan.
The lentinan that contains tobacco quality 0.1% in the pipe tobacco of the present invention.
Lentinan of the present invention obtains with following method: with 50 ℃ of oven dry of mushroom, and be crushed to the 10-100 order, use flooding 2 hours, the feed liquid mass ratio is 1: 15, and ultrasonic power is 80W then, and the time is 30 minutes, filter, filtrate decompression under 0.05Mpa, 60 ℃, 2 hours conditions, concentrate, the filtrate after concentrating is added 75% ethanol of 10 times of volumes again, 10 ℃ left standstill 12 hours, 3000 rev/mins, 30 minutes centrifugal treating are filtered, and obtain lentinan.
The lentinan that contains tobacco quality 0.01% in the pipe tobacco of the present invention.
A kind of preparation method who contains the cigarette of lentinan, may further comprise the steps: after water-soluble separating, mass concentration is 1-10% with lentinan, and the ratio that accounts for tobacco quality 0.001-10% in lentinan evenly is sprayed onto on the pipe tobacco, naturally dry, cigarette process is made cigarette routinely again.
Method of the present invention evenly is sprayed onto on the pipe tobacco in the ratio that lentinan accounts for tobacco quality 1%.
The extraction of method lentinan of the present invention is according to the following steps: with 60 ℃ of oven dry of mushroom, and be crushed to the 10-100 order, add 100 ℃ of hot water of 10 times of quality, lixiviate 3 times each 5 hours, merges 3 times water extract, filter, filtrate decompression under 0.05Mpa, 60 ℃, 2 hours conditions, concentrate, the filtrate after concentrating is added 95% ethanol of 5 times of volumes again, 10 ℃ left standstill 12 hours, 3000 rev/mins, 30 minutes centrifugal treating are filtered, and obtain lentinan; Lentinan mass concentration after water-soluble separating is 10%, and lentinan is sprayed onto on the pipe tobacco by 0.1% of tobacco quality.
The extraction of method lentinan of the present invention is according to the following steps: with 50 ℃ of oven dry of mushroom, and be crushed to the 10-100 order, with flooding 2 hours, the feed liquid mass ratio is 1: 15, and ultrasonic power is 80W then, and the time is 30 minutes, filter, filtrate decompression under 0.05Mpa, 60 ℃, 2 hours conditions, concentrate, the filtrate after concentrating is added 75% ethanol of 10 times of volumes again, 10 ℃ left standstill 12 hours, 3000 rev/mins, 30 minutes centrifugal treating are filtered, and obtain lentinan; Lentinan mass concentration after water-soluble separating is 8%, and lentinan is sprayed onto on the pipe tobacco by 0.01% of tobacco quality.
The present invention compared with prior art, the extract that contains the lentinan composition in the pipe tobacco, the lentinan dissolubility is good, in smoking process, can enter human body with main flume, be absorbed by the body by blood circulation, thereby bring into play its antitumor, anti-oxidant, antidotal effect, the pure and mild nothing of the cigarette smoke gas of mixing, improve cigarette quality, reduce the harmfulness of flue gas human body.
The specific embodiment
Below in conjunction with embodiment the present invention is described in further detail.The cigarette that contains lentinan of the present invention adds the lentinan that tobacco quality 0.001～10% is arranged in pipe tobacco.After water-soluble separating, mass concentration is 1-10% with lentinan, and the ratio that accounts for tobacco quality 0.001-10% in lentinan evenly is sprayed onto on the pipe tobacco, dries naturally, and cigarette process is made cigarette routinely again.
The present invention is added to lentinan in the cigarette shreds with feed liquid as cigarette after water-soluble separating, and during smoking, the cigarette smoke free from extraneous odour has delicate fragrance and falls the evil effect.Have the flue gas that improves cigarette, reduce the harmful components in the cigarette mainstream flue gas, flavouring humectation, the effect that delicate fragrance, reduction stimulate.
Adopt YC/T184-2004 tobacco and tobacco product, the peculiar N-nitrosamine of tobacco is measured, press the mensuration of carbon monoxide in the YC/T30-1996 cigarette smoke gas phase, the cigarette that contains lentinan of the present invention is compared with the blank cigarette, reduce tobacco-specific nitrosamine 30%, carbon monoxide 20% in the flue gas, pure and fresh, pure and mild, the free from extraneous odour of flue gas, assorted gas when smokeing panel test.Animal toxicity test can reduce respiratory tract injury.
Embodiment 1, gets the Shitake Mushroom P.E of Xuancheng City, Anhui hundred careless plant industry and trade Co., Ltd, and mass concentration is 10% after water-soluble separating, and the ratio that accounts for tobacco quality 1% in lentinan evenly is sprayed onto on the pipe tobacco, dries naturally, and cigarette process is made cigarette routinely again.When national cigarette teacher of the smokeing panel test in Guangdong Province smoked panel test, cigarette smoke was pure and mild, full, delicate fragrance, free from extraneous odour, and flue gas detects tobacco-specific nitrosamine 30%, the carbon monoxide 20% that reduces in the flue gas, shows the evil effect of falling.
Embodiment 2, get the dry mushroom that produce in Shaoguan, Guangdong, remove impurity, 60 ℃ of oven dry, and be crushed to the 10-100 order, add 100 ℃ of hot water of 10 times of quality, lixiviate 3 times each 5 hours, merges 3 times water extract, filter, filtrate decompression under 0.05Mpa, 60 ℃, 2 hours conditions, concentrate, the filtrate after concentrating is added 95% ethanol of 5 times of volumes again, 10 ℃ left standstill 12 hours, and 3000 rev/mins, 30 minutes centrifugal treating, filter, obtain lentinan.With lentinan mass concentration after water-soluble separating is 10%, and the ratio that accounts for tobacco quality 0.1% in lentinan evenly is sprayed onto on the pipe tobacco, dries naturally, and cigarette process is made cigarette routinely again.When smokeing panel test, cigarette smoke is pure and mild, delicate fragrance, free from extraneous odour, and flue gas detects tobacco-specific nitrosamine 30%, the carbon monoxide 20% that reduces in the flue gas, shows the evil effect of falling.
Embodiment 3, get the dry mushroom that produce in Shaoguan, Guangdong, remove impurity, 50 ℃ of oven dry, and be crushed to the 10-100 order, use flooding 2 hours, the feed liquid mass ratio is 1: 15, and ultrasonic power is 80W then, and the time is 30 minutes, filter, filtrate decompression under 0.05Mpa, 60 ℃, 2 hours conditions, concentrate, the filtrate after concentrating is added 75% ethanol of 10 times of volumes again, 10 ℃ left standstill 12 hours, and 3000 rev/mins, 30 minutes centrifugal treating, filter, obtain lentinan.With lentinan mass concentration after water-soluble separating is 8%, and the ratio that accounts for tobacco quality 0.01% in lentinan evenly is sprayed onto on the pipe tobacco, dries naturally, and cigarette process is made cigarette routinely again.When smokeing panel test, the cigarette cigarette smoke is pure and mild, delicate fragrance, free from extraneous odour, assorted gas, and flue gas detects tobacco-specific nitrosamine 30%, the carbon monoxide 20% that reduces in the flue gas, shows the evil effect of falling.
About the consumption of lentinan, as long as in the 0.001-10% of pipe tobacco weight, all can reach certain effect.And lentinan can adopt the method for any known to prepare.
Mushroom is a medicine-food two-purpose fungi commonly used, and lentinan (Lentinan) is the polysaccharide that extracts the homogeneous component of separation and purification acquisition from Basidiomycetes Agaricaceae fungi mushroom [Lentinus Modes (Berk) Sing] fructification.Polysaccharide contains fucose, galactolipin, wood sugar, the arabinose of a spot of glucose, trace based on mannose; Peptide chain is made up of 18 seed amino acids such as aspartic acid, histidine, serine, lysine, glutamic acid.The chemical constitution of lentinan (Lentinan) be a kind of be main chain with p-D-(1-3) glucose residue, side chain is the glucan of (1-6) glucose residue.Mean molecule quantity is about 500,000 dalton.Lentinan is to improve one of immunity, antitumor, effective antiviral components in the mushroom, has pharmacologically active widely.The pharmacological action of lentinan has: 1, immunoregulation effect: lentinan has immunoregulatory effect.The similar a kind of host immune reinforcing agent of its effect can stimulate maturation, differentiation and the propagation of key cells, improves host's organism balance, reaches to recover or improve the reactivity effect of host cell to lymphokine, hormone and other bioactie agent.2, antitumor action: result of study shows that lentinan has antitumor action, especially cancer of the stomach, lung cancer, liver cancer, hematological system tumor, nasopharyngeal carcinoma, the carcinoma of the rectum and breast cancer etc. is had the effect that suppresses and prevent the postoperative micrometastasis.Lentinan does not have direct killing effect to tumour cell, mainly is to strengthen the macrophage and the killer T cell of inducing activation by the host, improves the NK cytoactive and strengthens antibody dependent macrophage toxic action and bring into play antitumor action.3, antivirus action: studies show that lentinan to virus infections, comprise that the infection of HIV all has therapeutic action.Lentinan all has inhibitory action to hepatitis viruse, herpes zoster virus, Abelson virus, A2 (H2N2) virus, adenovirus 12 types and influenza virus etc.
Claims (10)
1. a cigarette that contains lentinan has pipe tobacco, it is characterized in that: the lentinan that contains tobacco quality 0.001～10% in the described pipe tobacco.
2. the cigarette that contains lentinan according to claim 1 is characterized in that: the lentinan that contains tobacco quality 1% in the described pipe tobacco.
3. the cigarette that contains lentinan according to claim 1, it is characterized in that: described lentinan obtains with following method: with 60 ℃ of oven dry of mushroom, and be crushed to the 10-100 order, 100 ℃ of hot water that add 10 times of quality, lixiviate 3 times, each 5 hours, merge 3 times water extract, filter, filtrate decompression under 0.05Mpa, 60 ℃, 2 hours conditions, concentrate, 95% ethanol that filtrate after concentrating is added again 5 times of volumes, 10 ℃ left standstill 12 hours, and 3000 rev/mins, 30 minutes centrifugal treating, filter, obtain lentinan.
4. the cigarette that contains lentinan according to claim 3 is characterized in that: the lentinan that contains tobacco quality 0.1% in the described pipe tobacco.
5. the cigarette that contains lentinan according to claim 1, it is characterized in that: described lentinan obtains with following method: with 50 ℃ of oven dry of mushroom, and be crushed to the 10-100 order, with flooding 2 hours, the feed liquid mass ratio is 1: 15, ultrasonic power is 80W then, time is 30 minutes, filters, and filtrate decompression under 0.05Mpa, 60 ℃, 2 hours conditions, concentrates, 75% ethanol that filtrate after concentrating is added again 10 times of volumes, 10 ℃ left standstill 12 hours, and 3000 rev/mins, 30 minutes centrifugal treating, filter, obtain lentinan.
6. the cigarette that contains lentinan according to claim 5 is characterized in that: the lentinan that contains tobacco quality 0.01% in the described pipe tobacco.
7. preparation method who contains the cigarette of lentinan, may further comprise the steps: after water-soluble separating, mass concentration is 1-10% with lentinan, and the ratio that accounts for tobacco quality 0.001-10% in lentinan evenly is sprayed onto on the pipe tobacco, naturally dry, cigarette process is made cigarette routinely again.
8. the preparation method who contains the cigarette of lentinan according to claim 7 is characterized in that: the ratio that accounts for tobacco quality 1% in lentinan evenly is sprayed onto on the pipe tobacco.
9. the preparation method who contains the cigarette of lentinan according to claim 7, it is characterized in that: the extraction of described lentinan according to the following steps: with 60 ℃ of oven dry of mushroom, and be crushed to the 10-100 order, 100 ℃ of hot water that add 10 times of quality, lixiviate 3 times, each 5 hours, merge 3 times water extract, filter, filtrate decompression under 0.05Mpa, 60 ℃, 2 hours conditions, concentrate, 95% ethanol that filtrate after concentrating is added again 5 times of volumes, 10 ℃ left standstill 12 hours, and 3000 rev/mins, 30 minutes centrifugal treating, filter, obtain lentinan; Lentinan mass concentration after water-soluble separating is 10%, and lentinan is sprayed onto on the pipe tobacco by 0.1% of tobacco quality.
10. the preparation method who contains the cigarette of lentinan according to claim 7, it is characterized in that: the extraction of described lentinan according to the following steps: with 50 ℃ of oven dry of mushroom, and be crushed to the 10-100 order, with flooding 2 hours, the feed liquid mass ratio is 1: 15, ultrasonic power is 80W then, time is 30 minutes, filters, and filtrate decompression under 0.05Mpa, 60 ℃, 2 hours conditions, concentrates, 75% ethanol that filtrate after concentrating is added again 10 times of volumes, 10 ℃ left standstill 12 hours, and 3000 rev/mins, 30 minutes centrifugal treating, filter, obtain lentinan; Lentinan mass concentration after water-soluble separating is 8%, and lentinan is sprayed onto on the pipe tobacco by 0.01% of tobacco quality.
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| Application Number | Priority Date | Filing Date | Title |
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| CN200910189848A CN101692933A (en) | 2009-09-01 | 2009-09-01 | Cigarette containing lentinan and preparation method thereof |
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| CN200910189848A CN101692933A (en) | 2009-09-01 | 2009-09-01 | Cigarette containing lentinan and preparation method thereof |
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| CN101692933A true CN101692933A (en) | 2010-04-14 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102793263A (en) * | 2012-08-27 | 2012-11-28 | 福建中烟工业有限责任公司 | Extraction method of tremella water extract concentrate and application of concentrate in tobaccos |
| CN102952833A (en) * | 2012-10-29 | 2013-03-06 | 云南省微生物发酵工程研究中心有限公司 | Agrocybe cylindracea polysaccharide and application thereof |
| CN103980379A (en) * | 2014-05-20 | 2014-08-13 | 河南中烟工业有限责任公司 | Lentinan, extraction and purification method thereof and application of lentinan as tobacco humectant |
| CN104432464A (en) * | 2014-11-03 | 2015-03-25 | 云南中烟工业有限责任公司 | Application of hypsizygus marmoreus polysaccharide and compound of hypsizygus marmoreus polysaccharide in cigarettes |
-
2009
- 2009-09-01 CN CN200910189848A patent/CN101692933A/en active Pending
Non-Patent Citations (3)
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| LONSENY T.等: "香菇多糖提取条件的优化研究", 《科技通报》 * |
| 徐若飞等: "天然菌类香菇烟用香原料的开发及应用", 《精细化工》 * |
| 边洪荣等: "用正交试验法研究超声提取香菇多糖的最佳工艺", 《中药材》 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102793263A (en) * | 2012-08-27 | 2012-11-28 | 福建中烟工业有限责任公司 | Extraction method of tremella water extract concentrate and application of concentrate in tobaccos |
| CN102952833A (en) * | 2012-10-29 | 2013-03-06 | 云南省微生物发酵工程研究中心有限公司 | Agrocybe cylindracea polysaccharide and application thereof |
| CN103980379A (en) * | 2014-05-20 | 2014-08-13 | 河南中烟工业有限责任公司 | Lentinan, extraction and purification method thereof and application of lentinan as tobacco humectant |
| CN104432464A (en) * | 2014-11-03 | 2015-03-25 | 云南中烟工业有限责任公司 | Application of hypsizygus marmoreus polysaccharide and compound of hypsizygus marmoreus polysaccharide in cigarettes |
| CN104432464B (en) * | 2014-11-03 | 2017-02-15 | 云南中烟工业有限责任公司 | Application of hypsizygus marmoreus polysaccharide and compound of hypsizygus marmoreus polysaccharide in cigarettes |
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Application publication date: 20100414 |