CN101692932B - Cigarette containing tea polysaccharide and preparation method thereof - Google Patents
Cigarette containing tea polysaccharide and preparation method thereof Download PDFInfo
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- CN101692932B CN101692932B CN2009101898478A CN200910189847A CN101692932B CN 101692932 B CN101692932 B CN 101692932B CN 2009101898478 A CN2009101898478 A CN 2009101898478A CN 200910189847 A CN200910189847 A CN 200910189847A CN 101692932 B CN101692932 B CN 101692932B
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- 150000004676 glycans Chemical class 0.000 title claims abstract description 70
- 229920001282 polysaccharide Polymers 0.000 title claims abstract description 70
- 239000005017 polysaccharide Substances 0.000 title claims abstract description 70
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 60
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 241001122767 Theaceae Species 0.000 title description 47
- 241000208125 Nicotiana Species 0.000 claims abstract description 47
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 47
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 244000269722 Thea sinensis Species 0.000 claims abstract 17
- 238000000034 method Methods 0.000 claims description 21
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 16
- 230000008569 process Effects 0.000 claims description 13
- 239000012141 concentrate Substances 0.000 claims description 8
- 239000000706 filtrate Substances 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 4
- -1 filter Substances 0.000 claims description 3
- 239000000779 smoke Substances 0.000 abstract description 9
- 210000004369 blood Anatomy 0.000 abstract description 8
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- 210000001124 body fluid Anatomy 0.000 abstract description 4
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- 230000032683 aging Effects 0.000 abstract 1
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- 239000004615 ingredient Substances 0.000 abstract 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 19
- 239000003546 flue gas Substances 0.000 description 14
- 230000000694 effects Effects 0.000 description 8
- 229910002091 carbon monoxide Inorganic materials 0.000 description 5
- XKLJHFLUAHKGGU-UHFFFAOYSA-N nitrous amide Chemical compound ON=N XKLJHFLUAHKGGU-UHFFFAOYSA-N 0.000 description 5
- 230000006837 decompression Effects 0.000 description 4
- 239000003205 fragrance Substances 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- 230000002218 hypoglycaemic effect Effects 0.000 description 4
- 238000011160 research Methods 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 3
- 206010012601 diabetes mellitus Diseases 0.000 description 3
- 238000000605 extraction Methods 0.000 description 3
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- 230000000259 anti-tumor effect Effects 0.000 description 2
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- 201000010099 disease Diseases 0.000 description 2
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- 239000002304 perfume Substances 0.000 description 2
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Landscapes
- Medicines Containing Plant Substances (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
The invention discloses a cigarette containing tea polysaccharide and a preparation method thereof, aiming at solving the technical problem of enhancing the feeling of promoting body fluid production,of smoke. The cigarette containing the tea polysaccharide has the tobacco shred containing the tea polysaccharide with the mass of 0.001-10% of the tobacco shred. The preparation method of the cigarette containing the tea polysaccharide comprises the following steps: dissolving the tea polysaccharide in the water to be solution with the mass concentration of 1-10%; spaying the tea polysaccharide solution onto the tobacco shred according to the proportion that the tea polysaccharide accounts for 0.001-10% of the tobacco shred; and finally, naturally drying and making into the cigarettes according to the conventional cigarette technology. Compared with the prior art, as the tobacco shred contains the ingredient of tea polysaccharide which can enters the human body along with the main stream smoke and is absorbed by the human body through blood circulation, thus playing the role of reducing the blood sugar, strengthening the organism immunity, reducing the blood pressure and the blood fat as well as resisting aging; furthermore, the smoke of the cigarettes is faint scent, full and mellow without impurity gas, so that the invention improves the quality of the cigarettes and reduces the hazard to the human health.
Description
Technical field
The present invention relates to a kind of cigarette and preparation method thereof, particularly a kind of low-harmful cigarette that increases cigarette flavor and preparation method thereof.
Background technology
China pays much attention to the harmful work of falling of cigarette, and since 2005, State Tobacco Monopoly Bureau has organized cigarette harmfulness index system and two great special research work of cigarette flavouring humectation, has obtained certain achievement.The humectation of cigarette flavouring is to promote Chinese style cigarette quality, increase perfume quantity, carry raise note, to set off the nature cigarette fragrant, reduce the flue gas drying sense, strengthen the promote the production of body fluid key of sense, raising cigarette comfort level of flue gas.The humectation of research cigarette flavouring helps improving cigarette product design, processing complex art level comprehensively, helps outstanding Chinese style cigarette style characteristic, strengthens Chinese style cigarette competitiveness.The cigarette of prior art can not be satisfied increases fragrance, strengthen the needs that flue gas promotes the production of body fluid and feels, and also will further utilize the new industrial research new product.
Summary of the invention
The purpose of this invention is to provide a kind of cigarette that contains tea polysaccharide and preparation method thereof, the technical problem that solve is to increase cigarette flavor, strengthen the flue gas sense of promoting the production of body fluid.
The present invention adopts following technical scheme: a kind of cigarette that contains tea polysaccharide, have pipe tobacco, and contain the tea polysaccharide of tobacco quality 0.001～10% in the said pipe tobacco.
The tea polysaccharide that contains tobacco quality 1% in the pipe tobacco of the present invention.
Tea polysaccharide of the present invention obtains with following method: with 50 ℃ of oven dry of tealeaves, and be crushed to the 10-100 order, add the hot water of 10 times of quality, 100 ℃ of lixiviates 3 times; Each 5 hours, merge 3 times water extract, filter, filtrate at 0.05Mpa, reduced pressure under the condition in 60 ℃, 1 hour, concentrate; Filtrating after concentrating is added 95% ethanol of 5 times of volumes again, leave standstill more than 12 hours 3000 rev/mins below 4 ℃; 30 minutes centrifugal treating are filtered, and obtain tea polysaccharide.
The tea polysaccharide that contains tobacco quality 0.1% in the pipe tobacco of the present invention.
Tea polysaccharide of the present invention obtains with following method: with 50 ℃ of oven dry of tealeaves, with flooding 2 hours, the feed liquid mass ratio was 1: 15, and ultrasonic power is 80W; 30 minutes time, filter, filtrate at 0.05Mpa, reduced pressure under the condition in 60 ℃, 2 hours, concentrate; Filtrating after concentrating is added 75% ethanol of 10 times of volumes again, leave standstill more than 12 hours 3000 rev/mins below 10 ℃; 30 minutes centrifugal treating are filtered, and obtain tea polysaccharide.
The tea polysaccharide that contains tobacco quality 0.01% in the pipe tobacco of the present invention.
A kind of preparation method who contains the cigarette of tea polysaccharide; May further comprise the steps: the solution that the tea polysaccharide water is dissolved as mass concentration 1-10%; The ratio that accounts for tobacco quality 0.001-10% in tea polysaccharide is sprayed onto on the pipe tobacco, dries naturally, processes cigarette by conventional cigarette process again.
Method of the present invention is sprayed onto on the pipe tobacco in the ratio that tea polysaccharide accounts for tobacco quality 1%.
The extraction of method tea polysaccharide of the present invention is according to the following steps: with 50 ℃ of oven dry of tealeaves, and be crushed to the 10-100 order, add the hot water of 10 times of quality, 100 ℃ of lixiviates 3 times; Each 5 hours, merge 3 times water extract, filter; Filtrating decompression under 0.05Mpa, 60 ℃, 1 hour condition, concentrate, the filtrating after concentrating is added 95% ethanol of 5 times of volumes again, leave standstill more than 12 hours below 4 ℃; 3000 rev/mins, 30 minutes centrifugal treating are filtered; The tea polysaccharide that obtains is sprayed onto on the pipe tobacco in the ratio of tobacco quality 0.1%.
The extraction of method tea polysaccharide of the present invention is according to the following steps: with 50 ℃ of oven dry of tealeaves, with flooding 2 hours, the feed liquid mass ratio was 1: 15; Ultrasonic power is 80W, and the processing time is 30 minutes, filters; Filtrating decompression under 0.05Mpa, 60 ℃, 2 hours conditions, concentrate, the filtrating after concentrating is added 75% ethanol of 10 times of volumes again, leave standstill more than 12 hours below 10 ℃; 3000 rev/mins, 30 minutes centrifugal treating are filtered; The tea polysaccharide that obtains is sprayed onto on the pipe tobacco in the ratio of tobacco quality 0.01%.
The present invention compared with prior art contains the tea polysaccharide composition in the pipe tobacco, tea polysaccharide is soluble in water; Dissolubility is good, in smoking process, can get into human body with main flume, is absorbed by the body through blood circulation; Thereby bring into play that it is hypoglycemic, enhancing body rabbit epidemic disease power, hypotensive, reducing blood lipid, antidotal effect; Cigarette smoke delicate fragrance, full, pure and mild, the assorted gas of nothing can improve the cigarette quality, reduce the harmfulness of flue gas to human body.
The specific embodiment
Below in conjunction with embodiment the present invention is done further explain.The cigarette that contains tea polysaccharide of the present invention, in the pipe tobacco of cigarette, adding has tobacco quality 0.001～10% tea polysaccharide.After the dissolving of tea polysaccharide water, mass concentration is 1-10%, and the ratio that accounts for tobacco quality 0.001-10% in tea polysaccharide evenly is sprayed onto on the pipe tobacco, dries naturally, processes cigarette by conventional cigarette process again.
Tea polysaccharide of the present invention joins in the cigarette shreds, during smoking, and the cigarette smoke free from extraneous odour; Hui Tian is arranged, fall the evil effect, can improve the strength of cigarette, reduce the harmful components in the cigarette mainstream flue gas; The flavouring humectation can obviously keep moisture in cut tobacco, has the delicate fragrance of tea; Enrich cigarette perfume (or spice), improve the cigarette comfort level, have Hui Tian, reduce effect the stimulation of throat
Adopt YC/T184-2004 tobacco and tobacco product; The peculiar N-nitrosamine of tobacco is measured; Press the mensuration of carbon monoxide in the YC/T30-1996 cigarette smoke gas phase, the cigarette that contains tea polysaccharide of the present invention is compared with the blank cigarette, reduces tobacco-specific nitrosamine, carbon monoxide in the flue gas; Reduction scope 15-20%, flue gas delicate fragrance when smokeing panel test, full, pure and mild, free from extraneous odour, assorted gas.The animal toxicity test demonstration has no side effect, and can reduce respiratory tract injury.
Embodiment 1, gets the tea extract of Xuancheng City, Anhui hundred careless plant industry and trade Co., Ltd, and mass concentration is 10% after water-soluble separating, and the ratio that accounts for tobacco quality 1% in tea polysaccharide evenly is sprayed onto on the pipe tobacco, dries naturally, processes cigarette by conventional cigarette process again.When Guangdong provincial cigarette teacher of the smokeing panel test, cigarette smoke was pure and mild, full, free from extraneous odour, and flue gas detects tobacco-specific nitrosamine, the carbon monoxide that reduces in the flue gas, reduced scope 15-20%, and the evil effect of falling is arranged.
Embodiment 2, get Guangdong Province Germany and Britain and produce dry tealeaves, remove impurity, 50 ℃ of oven dry, and be crushed to the 10-100 order; The hot water that adds 10 times of quality, 100 ℃ of lixiviates, each 5 hours, lixiviate was 3 times altogether, merges 3 times water extract; Filter, filtrating decompression under 0.05Mpa, 60 ℃, 1 hour condition, concentrate, the filtrating after concentrating is added 95% ethanol of 5 times of volumes again, left standstill below 4 ℃ 12 hours; 3000 rev/mins, 30 minutes centrifugal treating are filtered, and obtain tea polysaccharide.With tea polysaccharide mass concentration after water-soluble separating is 10%, and the ratio that accounts for tobacco quality 0.1% in tea polysaccharide evenly is sprayed onto on the pipe tobacco, dries naturally, processes cigarette by conventional cigarette process again.When smokeing panel test, pure and mild, the free from extraneous odour of cigarette smoke, flue gas detects tobacco-specific nitrosamine, the carbon monoxide that reduces in the flue gas, reduces scope 15-20%, and the evil effect of falling is arranged.
Embodiment 3, get Guangdong Province Germany and Britain and produce dry tealeaves, remove impurity, 50 ℃ of oven dry; With flooding 2 hours, the feed liquid mass ratio was 1: 15, and ultrasonic power is 80W, and the time is 30 minutes; Filter, decompression under filtrating 0.05Mpa, 60 ℃, the 2 hours conditions, concentrate, the filtrating after concentrating is added 75% ethanol of 10 times of volumes again, left standstill below 10 ℃ 12 hours; 3000 rev/mins, 30 minutes centrifugal treating are filtered, and obtain tea polysaccharide.With tea polysaccharide mass concentration after water-soluble separating is 8%, and the ratio that accounts for tobacco quality 0.01% in tea polysaccharide evenly is sprayed onto on the pipe tobacco, dries naturally, processes cigarette by conventional cigarette process again.When smokeing panel test, the cigarette cigarette smoke is pure and mild, free from extraneous odour, assorted gas, and flue gas detects tobacco-specific nitrosamine, the carbon monoxide that reduces in the flue gas, reduces scope 15-20%, and the evil effect of falling is arranged.
About the consumption of tea polysaccharide, as long as in the 0.001-10% of pipe tobacco weight, all can reach effect preferably.And tea polysaccharide can also adopt the method for any known to prepare.
Tea polysaccharide (Tea Polysaccharide) is one of main active ingredient of tea, more and more receives people's attention because of having multiple physiologically active.Also more and more deep to the pharmacological research of tea polysaccharide both at home and abroad, and demonstrate good prospects for application.Modern age, pharmacological evaluation showed, tea polysaccharide have immunological regulation, anti-ageing, reducing blood lipid, hypoglycemic, protect functions such as liver, radiation proof, antifatigue, protection reproductive system, antitumor, anti-anoxic.The pharmacological action of tea polysaccharide has:
Tea is plant commonly used; Used several thousand in China, tea polysaccharide also is tealeaves polysaccharide (TeaPolysaccharide; Be called for short TPS) be the complex polysaccharide that leaf, branch, the extraction of root position from the natural plants tea tree are separated, it is one of main active ingredient in the tealeaves; The tea polysaccharide average molecular mass is all 10
4～10
5The order of magnitude does not wait; Have the various biological function: 1, hypoglycemic: tea polysaccharide can hypoglycemicly be generally acknowledged; China's bubble that always spreading among the people is drunk the saying that coarse tea can be treated diabetes; Tea polysaccharide has significant prevention and therapeutic action to diabetes, through improving the body anti-oxidation function and strengthening liver glucose kinase activity performance hypoglycemic activity.2, reducing blood lipid: tea polysaccharide can reduce LDL-C in the serum, strengthens the drainage of cholesterol through liver.Tea polysaccharide can also combine, promote the arterial wall lipoproteinesterase to go into blood and play antiatherogenic effect with lipoproteinesterase.3, antithrombotic is done: tea polysaccharide can obviously suppress hematoblastic adhesive attraction, and reduces blood viscosity.Improve Fibrinolytic vigor.4, improve immunologic function: improve immunity; Can reduce simultaneously blood sugar, serum cholesterol and triglycerides trend, this is for senile retrograde disease, like diabetes; The control of angiocardiopathy has great significance, and the elderly's Abwehrkraft des Koepers descends, plays important immunity raising effect simultaneously.In addition, tea polysaccharide is to the scavenging action of hydroxyl radical free radical, and the clearance rate of right-OH is 5.5%～74.7%.Tea polysaccharide also has radiation proof, antitumor, antiviral, hypotensive, anti-anoxic and increases the various biological function of coronary blood flow.
Claims (1)
1. a cigarette that contains tea polysaccharide has pipe tobacco, it is characterized in that: the tea polysaccharide that contains tobacco quality 1% in the said pipe tobacco;
Said tea polysaccharide obtains with following method: with 50 ℃ of oven dry of tealeaves, and be crushed to the 10-100 order, add the hot water of 10 times of quality, 100 ℃ of lixiviates 3 times; Each 5 hours, merge 3 times water extract, filter, filtrate at 0.05Mpa, reduced pressure under the condition in 60 ℃, 1 hour, concentrate; Filtrating after concentrating is added 95% ethanol of 5 times of volumes again, leave standstill more than 12 hours 3000 rev/mins below 4 ℃; 30 minutes centrifugal treating are filtered, and obtain tea polysaccharide;
Or said tea polysaccharide obtains with following method: with 50 ℃ of oven dry of tealeaves, with flooding 2 hours, the feed liquid mass ratio was 1: 15, and ultrasonic power is 80W; 30 minutes time, filter, filtrate at 0.05Mpa, reduced pressure under the condition in 60 ℃, 2 hours, concentrate; Filtrating after concentrating is added 75% ethanol of 10 times of volumes again, leave standstill more than 12 hours 3000 rev/mins below 10 ℃; 30 minutes centrifugal treating are filtered, and obtain tea polysaccharide;
The said cigarette that contains tea polysaccharide prepares with following preparation method; May further comprise the steps: the solution that the tea polysaccharide water is dissolved as mass concentration 1-10%; The ratio that accounts for tobacco quality 1% in tea polysaccharide is sprayed onto on the pipe tobacco, dries naturally, processes cigarette by conventional cigarette process again.
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| Application Number | Priority Date | Filing Date | Title |
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| CN2009101898478A CN101692932B (en) | 2009-09-01 | 2009-09-01 | Cigarette containing tea polysaccharide and preparation method thereof |
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| CN2009101898478A CN101692932B (en) | 2009-09-01 | 2009-09-01 | Cigarette containing tea polysaccharide and preparation method thereof |
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| CN101692932A CN101692932A (en) | 2010-04-14 |
| CN101692932B true CN101692932B (en) | 2012-06-27 |
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Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101864694B (en) * | 2010-06-13 | 2011-06-22 | 玉溪市星源油墨厂 | Tea flavonoids containing water-based coating for cigarette plug wrap paper |
| CN101864695B (en) * | 2010-06-13 | 2011-06-22 | 玉溪市星源油墨厂 | Tea polysaccharide containing water-based coating for cigarette plug wrap paper |
| CN102276749B (en) * | 2011-08-01 | 2013-04-17 | 澳华达香料科技(广州)有限公司 | Preparation method for iron Buddha tea polysaccharide extract and application thereof in tobacco sheets |
| CN104336775A (en) * | 2013-07-26 | 2015-02-11 | 江西中烟工业有限责任公司 | Hawk tea extract, preparation method thereof and application of extract in cigarette |
| CN105595407A (en) * | 2016-01-28 | 2016-05-25 | 寻甸牧工商茶叶进出口有限公司 | Puer tea-containing cigarettes capable of degrading tobacco toxin |
| CN111000288A (en) * | 2019-12-30 | 2020-04-14 | 福建中烟工业有限责任公司 | Gel for cigarettes and tobacco products |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1686014A (en) * | 2005-06-02 | 2005-10-26 | 戴亚 | Cigarette filter tip additive and additive carrier |
| CN101342011A (en) * | 2008-07-29 | 2009-01-14 | 红云烟草(集团)有限责任公司 | Black tea mellow wine extract, preparation and application thereof |
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- 2009-09-01 CN CN2009101898478A patent/CN101692932B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1686014A (en) * | 2005-06-02 | 2005-10-26 | 戴亚 | Cigarette filter tip additive and additive carrier |
| CN101342011A (en) * | 2008-07-29 | 2009-01-14 | 红云烟草(集团)有限责任公司 | Black tea mellow wine extract, preparation and application thereof |
Non-Patent Citations (1)
| Title |
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| 陈睿.茶叶功能性成分的化学组成及应用.《安徽农业科学》.2004,(第5期),第1031-1033，1036页. * |
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