CN104432464A - Application of hypsizygus marmoreus polysaccharide and compound of hypsizygus marmoreus polysaccharide in cigarettes - Google Patents
Application of hypsizygus marmoreus polysaccharide and compound of hypsizygus marmoreus polysaccharide in cigarettes Download PDFInfo
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- CN104432464A CN104432464A CN201410610457.4A CN201410610457A CN104432464A CN 104432464 A CN104432464 A CN 104432464A CN 201410610457 A CN201410610457 A CN 201410610457A CN 104432464 A CN104432464 A CN 104432464A
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- mushroom polysaccharide
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
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Abstract
The invention discloses application of hypsizygus marmoreus polysaccharide and a compound of the hypsizygus marmoreus polysaccharide in cigarettes. The hypsizygus marmoreus polysaccharide or compounded hypsizygus marmoreus polysaccharide serves as a natural humectant to be applied to the cigarettes and added in a feeding mode in the process of processing cigarette shreds, and the adding ratio is 2g-100g/single box. Preferably, the compound of the hypsizygus marmoreus polysaccharide is formed by 10% of hypsizygus marmoreus polysaccharide, 1% of potassium glycyrrhefate, 0.1% of megastigmatrienone, 30% of propylene glycol, 25% of glycerinum, 15% of sorbitol, and the balance deionized water. The hypsizygus marmoreus polysaccharide is an edible natural product, ensures the safety, has special fragrance, and can increase the fragrance while keeping moisture of the cigarettes. The application of the hypsizygus marmoreus polysaccharide and the compound of the hypsizygus marmoreus polysaccharide in cigarettes can remarkably increase the cigarette moisture content maintaining capacity, increase the moisture keeping effect and effectively improve the cigarette suction comfort.
Description
Technical field
The invention belongs to cigarette additive technical field, specifically relate to true Ji mushroom polysaccharide or the application of compound in cigarette containing true Ji mushroom polysaccharide.
Background technology
In current Cigarette processing process, usually add the polyhydroxy chemical substances such as glycerine, propane diols, sorbierite as humectant, make broken to reduce in production process, reduce the dry sensation of flue gas in smoking property of cigarette process, strengthen the degree of promoting the production of body fluid of flue gas pleasant impression.These humectants mainly produce humectation effect by its hygroscopicity to tobacco, and suck comfort level for maintenance cigarette moisture content, improvement, and then effect is not ideal to promote suction fragrance.
True Ji mushroom (Hypsizygus marmoreus), formal name used at school Yu Qin, spot Yu Qin, Lyophyllum decastes etc., because it has unique crab delicate flavour therefore the crab flavour mushroom that is otherwise known as, seafood mushroom, be subordinate to Basidiomycotina, Hymenomycetes, Agaricales, Bai Mo section, belong to from gill fungus race, beautiful gill fungus.
About true Ji mushroom polysaccharide or its associated extraction thing, be applied in food and medicine more, many as fumet use in food, then research and develop as immunomodulator and anti-tumor activity medicine in medicine.
Be applied in cigarette by true Ji mushroom polysaccharide or its compound, by improving cigarette moisture content maintenance effect, to strengthen the method for cigarette physics humid keeping performance and suction comfort level and suction fragrance, there is not been reported.
Summary of the invention
The object of the invention is to improve unconspicuous present situation for existing humectant for smoke to cigarette moisture content maintenance poor effect, suction comfort level, polysaccharide is extracted from true Ji mushroom, by true Ji mushroom polysaccharide or true Ji mushroom polysaccharide is applied in cigarette as natural humectant after composite, ability is maintained to improve cigarette moisture content, strengthen humectation effect, and effectively improve cigarette smoking comfort level.
Object of the present invention is achieved by following scheme:
Except as otherwise noted, percentage of the present invention is percetage by weight.
I. the application of true Ji mushroom polysaccharide in production of cigarettes.
The described application of true Ji mushroom polysaccharide in production of cigarettes, is characterized in that: added in reinforced mode in cigarette shreds process by true Ji mushroom polysaccharide, adding proportion is the every single case of 2g ~ 100g/.This interpolation can at leaves storage, get damp again, mix and carry out with addition of process sections such as material.
Described true Ji mushroom polysaccharide preferably extracts with following method and obtains: get true Ji mushroom and put into extraction equipment, add the water of 8 ~ 30 times of volumes, after stirring under 65 ~ 80 DEG C of conditions lixiviate 2 ~ 4h, filtration discards filter residue, concentrated leaching liquor, add 75 ~ 95% ethanol of 7 ~ 20 times of volumes, alcohol filters after analysing 20 ~ 40h, gets filter residue after vacuum drying, obtains true Ji mushroom polysaccharide.Gains polysaccharide component content is high, purity good, and is satisfied with the requirement that the later stage adds separately or add as the formula components of compound.
II. the application of true Ji mushroom polysaccharide compound in production of cigarettes.
Containing true Ji mushroom polysaccharide 0.001% ~ 100% (weight ratio) in described true Ji mushroom polysaccharide compound.
In described true Ji mushroom polysaccharide compound, true Ji mushroom polyoses content is preferably 0.5% ~ 20% (weight ratio).
Described true Ji mushroom polysaccharide compound is preferably made up of following raw material: true Ji mushroom polysaccharide 10%, dipotassium glycyrrhizinate 1%, Megastigmatrienone 0.1%, and propane diols 30%, glycerine 25% and sorbierite 15%, surplus is deionized water.
The described application of true Ji mushroom polysaccharide compound in production of cigarettes, is characterized in that: added in reinforced mode in cigarette shreds process by the true Ji mushroom polysaccharide compound prepared, adding proportion is the every single case of 2g ~ 100g/.Described interpolation can at leaves storage, get damp again, mix and carry out with addition of process sections such as material.
Relative to prior art, the present invention has the following advantages:
1, secure as the security of edible natural prodcuts;
2, there is special aroma, can cigarette flavor be increased while humectation.
Accompanying drawing explanation
Fig. 1 is pipe tobacco moisturizing experiment water-cut variation figure;
Fig. 2 is pipe tobacco protection against the tide experiment water-cut variation figure.
Detailed description of the invention
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with drawings and Examples, the present invention is described in further detail.Described specific embodiment only in order to explain the present invention, the technical scheme be not intended to limit the present invention.
Embodiment 1
Get true Ji mushroom appropriate, put into extraction equipment, add 15 times of (w/w) water, after stirring under 75 DEG C of conditions lixiviate 2.5h, after filtration discards filter residue, concentrated leaching liquor, to appropriate, adds 95% ethanol of 8 times of volumes, alcohol filters after analysing 36h, get filter residue after vacuum drying both true Ji mushroom polysaccharide.
Added in tobacco leaf leaves storage process with feed way by true Ji mushroom polysaccharide, addition is 2g/B.C (every single case).
Embodiment 2
Get true Ji mushroom appropriate, put into extraction equipment, add 30 times of (w/w) water, after stirring under 65 DEG C of conditions lixiviate 2h, after filtration discards filter residue, concentrated leaching liquor, to appropriate, adds 85% ethanol of 15 times of volumes, alcohol filters after analysing 20h, get filter residue after toasting drying both true Ji mushroom polysaccharide.
Added in pipe tobacco resurgence process with feed way by true Ji mushroom polysaccharide, addition is 50g/B.C.
Embodiment 3
Get true Ji mushroom appropriate, put into extraction equipment, add 10 times of (w/w) water, after stirring under 70 DEG C of conditions lixiviate 3h, after filtration discards filter residue, concentrated leaching liquor, to appropriate, adds 75% ethanol of 20 times of volumes, alcohol filters after analysing 35h, get filter residue after vacuum drying both true Ji mushroom polysaccharide.True Ji mushroom polysaccharide compound is prepared by following formula table:
| Raw material | Percentage by weight |
| True Ji mushroom polysaccharide | 10 |
| Dipotassium glycyrrhizinate | 1 |
| Megastigmatrienone | 0.1 |
| Propane diols | 30 |
| Glycerine | 25 |
| Sorbierite | 15 |
| Deionized water | Mend to 100 |
The true Ji mushroom polysaccharide compound prepared is added in pipe tobacco with reinforced form, addition 20g/B.C.
Embodiment 4
Get true Ji mushroom appropriate, put into extraction equipment, add 8 times of (w/w) water, after stirring under 75 DEG C of conditions lixiviate 2h, after filtration discards filter residue, concentrated leaching liquor, to appropriate, adds 95% ethanol of 10 times of volumes, alcohol filters after analysing 20h, get filter residue after vacuum drying both true Ji mushroom polysaccharide.True Ji mushroom polysaccharide compound is prepared by following formula table:
| Raw material | Percentage by weight |
| True Ji mushroom polysaccharide | 10 |
| Dorinone | 0.2 |
| Fructus Jujubae extract | 2 |
| Propane diols | 30 |
| Glycerine | 30 |
| Sorbierite | 15 |
| Deionized water | Mend to 100 |
The true Ji mushroom polysaccharide compound prepared is added in pipe tobacco with reinforced form, addition 25g/B.C.
Embodiment 5
Get true Ji mushroom appropriate, put into extraction equipment, add 10 times of (w/w) water, after stirring under 80 DEG C of conditions lixiviate 4h, after filtration discards filter residue, concentrated leaching liquor, to appropriate, adds 85% ethanol of 7 times of volumes, alcohol filters after analysing 40h, get filter residue after vacuum drying both true Ji mushroom polysaccharide.True Ji mushroom polysaccharide compound is prepared by following formula table:
| Raw material | Percentage by weight |
| True Ji mushroom polysaccharide | 10 |
| Eggplant Buddhist nun ketone | 0.1 |
| Tomato extract | 2 |
| Propane diols | 30 |
| Glycerine | 25 |
| Sorbierite | 15 |
| Deionized water | Mend to 100 |
The true Ji mushroom polysaccharide compound prepared is added in leaves storage process with reinforced form, addition 10g/B.C..
Embodiment 6
Get true Ji mushroom appropriate, put into extraction equipment, add 10 times of (w/w) water, after stirring under 80 DEG C of conditions lixiviate 4h, after filtration discards filter residue, concentrated leaching liquor, to appropriate, adds 85% ethanol of 7 times of volumes, alcohol filters after analysing 40h, get filter residue after vacuum drying both true Ji mushroom polysaccharide.True Ji mushroom polysaccharide compound is prepared by following formula table:
| Raw material | Percentage by weight |
| True Ji mushroom polysaccharide | 10 |
| Malic acid | 0.1 |
| Tobacco extract | 2 |
| Propane diols | 30 |
| Glycerine | 25 |
| Sorbierite | 15 |
| Deionized water | Mend to 100 |
The true Ji mushroom polysaccharide compound prepared is added in leaves storage process with reinforced form, addition 15g/B.C..
Application experiment: the humid keeping performance confirmatory experiment that true Ji mushroom polysaccharide adds in cigarette
The humid keeping performance of tobacco humectant refers to the environment at low humidity or high humidity, makes cigarette at the regulating power preventing moisture loss or suppression moisture absorption.The quality evaluating humectant humid keeping performance mainly judges with the variable quantity of certain hour inner wrap strip moisture content.
Experimental example 1: true Ji mushroom polysaccharide pipe tobacco performance of keeping humidity experiment
One. experimental technique
According to completing pipe tobacco moisture regain described in embodiment 2, the pipe tobacco adding equivalent PG not add true Ji mushroom polysaccharide in contrast, detects moisture in cut tobacco content at following time point moisture teller.
Two. experimental result
Experimental result is as following table 1, Fig. 1:
Table 1 pipe tobacco moisturizing experiment moisture content detects
From in upper table and Fig. 1, along with time lengthening, the humectation effect of two kinds of humectants declines all to some extent, the amplitude difference declined is little, but on every single time point, the pipe tobacco water content of adding true Ji mushroom polysaccharide is all higher than the pipe tobacco adding PG, and show that true Ji mushroom polysaccharide is reinforced in pipe tobacco as humectant, its effect is better than the traditional humectant PG commonly used.
Experimental example 2: true Ji mushroom polysaccharide pipe tobacco humidity resistance experiment
One. experimental technique
Feed in raw material according to completing tobacco leaf leaves storage described in embodiment 1, the tobacco leaf adding equivalent PG not add true Ji mushroom polysaccharide in contrast, detects moisture content in leaves content at following time point moisture teller.
Two. experimental result
Experimental result is as following table 2, Fig. 2:
Table 2 protection against the tide experiment moisture content detects
From upper table and Fig. 2, under humidity higher strip part (80%RH), when addition is 2g/B.C., the humidity resistance of true Ji mushroom polysaccharide humectant is better than contrasting PG, in whole testing time section, the pipe tobacco water content of adding true Ji mushroom polysaccharide, all a little less than the water content of adding PG, shows that the humidity resistance of true Ji mushroom polysaccharide is better than PG.
Experimental example 3: the flavouring performance verification experiment that true Ji mushroom polysaccharide adds in cigarette
Experimental principle: with reference to the thinking about cigarette Style Evaluation in " Chinese-style cigarette style sensory evaluation method ", for fragrance surface, flue gas performance and mouthfeel aspect, sensory evaluation is carried out to the sample adding true Ji mushroom polysaccharide compound, participation is smoked panel test marking number 11 people, and design evaluatio marking form and fractional value are as following table 3:
Using embodiment 3 gained true Ji mushroom polysaccharide compound as laboratory sample.
Table 3 sense organ evaluating meter and marking numerical value
Experimental example 4: the flavouring experiment of true Ji mushroom polysaccharide
One. experimental technique
Feed in raw material according to completing purple cloud leaf group silk described in embodiment 3, with replace true Ji mushroom polysaccharide change and the purple cloud leaf group silk of the water gagings such as interpolation in contrast, carry out 11 people after by hand making cigarette and smoke panel test.
Two. experimental result
According to marking form designed in experimental principle, give a mark after cigarette after 11 people smoke panel test respectively, calculate average mark and obtain following result, in table 4:
Table 4 purple cloud leaf group control sample and sample contrast to smoke panel test and add up
From upper table statistics, add true Ji mushroom polysaccharide in the compound that purple cloud tobacco leaf formulation uses after, the suction sensory scores of cigarette obtains certain raising, promote larger in fragrance performance and flue gas performance, the compound showing with the addition of the true Ji mushroom polysaccharide compound not adding polysaccharide of comparing has certain flavouring effect, separately in moist feeling and comfortableness, also has certain effect.
Claims (8)
1. the application of true Ji mushroom polysaccharide in production of cigarettes.
2. the application of true Ji mushroom polysaccharide according to claim 1 in production of cigarettes, is characterized in that: added in reinforced mode in cigarette shreds process by true Ji mushroom polysaccharide, adding proportion is the every single case of 2g ~ 100g/.
3. the application of true Ji mushroom polysaccharide according to claim 1 in production of cigarettes, it is characterized in that, described true Ji mushroom polysaccharide preferably extracts with following method and obtains: get true Ji mushroom and put into extraction equipment, add the water of 8 ~ 30 times of volumes, after stirring under 65 ~ 80 DEG C of conditions lixiviate 2 ~ 4h, filter discard filter residue, concentrated leaching liquor, add 75 ~ 95% ethanol of 7 ~ 20 times of volumes, alcohol filters after analysing 20 ~ 40h, gets filter residue after vacuum drying, obtains true Ji mushroom polysaccharide.
4. the application of true Ji mushroom polysaccharide compound in production of cigarettes.
5. the application of true Ji mushroom polysaccharide compound according to claim 4 in production of cigarettes, it is characterized in that: added in reinforced mode in cigarette shreds process by the true Ji mushroom polysaccharide compound prepared, adding proportion is the every single case of 2g ~ 100g/.
6. the application of true Ji mushroom polysaccharide compound according to claim 5 in production of cigarettes, is characterized in that: in described true Ji mushroom polysaccharide compound, the content of true Ji mushroom polysaccharide is 0.001% ~ 100% percetage by weight.
7. the application of true Ji mushroom polysaccharide compound according to claim 6 in production of cigarettes, is characterized in that: in described true Ji mushroom polysaccharide compound, true Ji mushroom polyoses content is 0.5% ~ 20% percetage by weight.
8. the application of true Ji mushroom polysaccharide compound according to claim 5 in production of cigarettes, it is characterized in that, described true Ji mushroom polysaccharide compound is preferably made up of following raw material: true Ji mushroom polysaccharide 10%, dipotassium glycyrrhizinate 1%, Megastigmatrienone 0.1%, propane diols 30%, glycerine 25% and sorbierite 15%, surplus is deionized water.
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| CN201410610457.4A CN104432464B (en) | 2014-11-03 | 2014-11-03 | Application of hypsizygus marmoreus polysaccharide and compound of hypsizygus marmoreus polysaccharide in cigarettes |
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