CN104783323B - A kind of tobacco juice for electronic smoke containing Dry distillated flavor - Google Patents
A kind of tobacco juice for electronic smoke containing Dry distillated flavor Download PDFInfo
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- CN104783323B CN104783323B CN201510246335.6A CN201510246335A CN104783323B CN 104783323 B CN104783323 B CN 104783323B CN 201510246335 A CN201510246335 A CN 201510246335A CN 104783323 B CN104783323 B CN 104783323B
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- Prior art keywords
- tobacco
- dry distillated
- distillated flavor
- flavor
- glycerine
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a kind of tobacco juice for electronic smoke containing Dry distillated flavor, its be by 15～50% Dry distillated flavor, 30～60% glycerine and propane diols be mixed evenly to prepare.Wherein, Dry distillated flavor prepares by tobacco carries out under nitrogen atmosphere and preference temperature destructive distillation.The use of Dry distillated flavor in the present invention, hence it is evident that improve the organoleptic quality of electronic cigarette so that it is be closer to traditional cigarette in terms of fragrance, mouthfeel.
Description
Technical field
The present invention relates to a kind of tobacco juice for electronic smoke containing Dry distillated flavor, belong to electronic cigarette technical field.
Background technology
Electronic cigarette has another name called atomizer for electric, and the atomization of nicotine-containing liquid is formed aerosol and passes by the means typically heated by electronics
To respiratory system.As cigarette substitute, the outward appearance of its simulated cigarette and taste, but without burning, cigarette ash and stub will not be produced,
Avoid disaster hidden-trouble；Also second-hand-cigarette will not be produced, PE impact will not be produced；Also without tar, CO, hydrogen cyanide,
The harmful substances such as methacrylaldehyde, lead, arsenic.These advantages can break through the restriction of whole world Tobacco Control campaign, it is thus achieved that huge one-tenth
Long spacing, has attracted the eyeball of numerous consumer at short notice.
But, compared with real cigarette, mostly there is the shortcoming that organoleptic quality is the best in presently commercially available electronic cigarette, the electricity of serious restriction
The development of sub-cigarette.To this end, the work promoting electronic cigarette aesthetic quality is extensively launched.Wherein, one of effective means is at electronics
Cigarette tobacco juice is added the active ingredient in the tobacco extracted by suitable means and/or non-tobacco class plant.Patent CN
103054172A, CN103054171A and CN103070473A all use ultrasonic wave respectively to Luzhou-flavor, flat-flavor and
Delicate fragrance type tobacco leaf extracts, prepare fragrance, mouthfeel and traditional cigarette closer to electronic cigarette.Patent CN103989244A
Supercritical CO is used with CN103720030A2Non-tobacco natural plants and cigarette foam are extracted, the electronic cigarette sense organ matter obtained
Amount with traditional cigarette closer to.Patent CN103054173A uses 65 DEG C of gas bath shaking table succusions to be extracted discarded tobacco leaf
Taking, patent CN103919274A utilizes method that 80 DEG C of refluxing extraction and molecular clock combine to Zimbabwe's tobacco leaf, the U.S.
Burley tobacco leaf, Turkey's atomatic tobacco, Xinjiang tobacco leaf etc. are extracted, and patent CN103070472A is by Yunnan safflower
Big gold dollar tobacco leaf is soaked in ethanol, has obtained leaf tobacco extract by being centrifuged, be evaporated off solvent, and these work all improve electronics
The aesthetic quality of cigarette.But current, prior art there is not yet and promote the relevant of electronic cigarette organoleptic quality by addition Dry distillated flavor
Report.
Summary of the invention
The present invention is for avoiding the weak point existing for above-mentioned prior art, it is provided that a kind of tobacco juice for electronic smoke containing Dry distillated flavor,
To can further promote the aesthetic quality of electronic cigarette, making electronic cigarette closer to traditional cigarette, more consumer is accepted.
The present invention solves that technical problem adopts the following technical scheme that
The present invention contains the tobacco juice for electronic smoke of Dry distillated flavor, and its feature is: each raw material of described tobacco juice for electronic smoke is by percent mass
The composition of ratio is:
Dry distillated flavor 15～50%；
Glycerine 30～60%；
Surplus is propane diols.
The present invention contains the tobacco juice for electronic smoke of Dry distillated flavor, and its feature lies also in: described Dry distillated flavor is condensation Dry distillated flavor and sweet
At least one in oil trap collection Dry distillated flavor.
Described condensation Dry distillated flavor is prepared as follows: in a nitrogen atmosphere, is done by tobacco at 200 DEG C-400 DEG C
Evaporating, distillate flows in receiving bottle through running water condensation and collects, and obtains condensation Dry distillated flavor.
Described glycerine trapping Dry distillated flavor is prepared as follows: in a nitrogen atmosphere, entered by tobacco at 200 DEG C-400 DEG C
Row destructive distillation, distillate is introduced directly in glycerine, obtains glycerine trapping Dry distillated flavor.Described tobacco with the mass ratio of described glycerine is
0.5-4:1.
Described tobacco is at least one in flue-cured tobacco, burley tobaccos and Turkish tobaccos, and the form of described tobacco is sheet, thread and powder
At least one in shape.
Compared with the prior art, advantages of the present invention is embodied in:
(1) tobacco juice for electronic smoke of the present invention is with the Dry distillated flavor of tobacco as main component, provide not only nicotine, additionally provides rich
Rich tobacco characteristic aroma substance, hence it is evident that improve the aesthetic quality of electronic cigarette so that it is with the fragrance of traditional cigarette, mouthfeel more
For close.
(2) tobacco juice for electronic smoke of the present invention is for the atomization of electronic cigarette, and harmful components are few, is greatly lowered consumer's harm, and
The harm of second-hand-cigarette will not be produced.
Detailed description of the invention
Below by way of detailed description of the invention, the invention will be further described, but embodiment is not the restriction to present invention.
Embodiment 1:
The formula of the present embodiment tobacco juice for electronic smoke is (mass percent): 10% condensation Dry distillated flavor A, 50% glycerine, 40% the third
Glycol.Mix after above-mentioned raw materials is proportionally weighed, and be stirred until homogeneous, i.e. obtain the electronic cigarette containing condensation Dry distillated flavor A
Tobacco juice, can directly be added in electronic cigarette device atomization and suck.
The present embodiment condensation Dry distillated flavor A preparation process is as follows: under nitrogen protection, by south, 900g Anhui flue-cured tobacco pipe tobacco and 100g
Greece's spices offal carries out destructive distillation at 220 DEG C, and distillate flows in receiving bottle through running water condensation, prepares and can improve electronic cigarette
The condensation Dry distillated flavor A of organoleptic quality.
Embodiment 2:
The formula of the present embodiment tobacco juice for electronic smoke is (mass percent): 50% glycerine trapping Dry distillated flavor B, 40% glycerine, 10%
Propane diols.Mix after above-mentioned raw materials is proportionally weighed, and be stirred until homogeneous, i.e. obtain containing glycerine trapping Dry distillated flavor B's
Tobacco juice for electronic smoke, can directly be added in electronic cigarette device atomization and suck.
The present embodiment glycerine trapping Dry distillated flavor B preparation process is as follows: under nitrogen protection, existed by 1000g Yunnan Flue-cured Tobacco pipe tobacco
Carrying out destructive distillation at 320 DEG C, distillate is the most condensed to be introduced directly in 800g glycerine, prepares and can improve the sweet of electronic cigarette organoleptic quality
Oil trap collection Dry distillated flavor B, its main chemical compositions is shown in Table 1 through GC-MS analysis result.
Table 1 Dry distillated flavor chemical composition
| Compound name | Condensation Dry distillated flavor C (μ g/mL) | Glycerine trapping Dry distillated flavor B (μ g/mL) |
| Pyridine | 286.35 | 69.57 |
| Pyrazine | 5.19 | 1.11 |
| Geranyl acetone | 519.78 | 172.47 |
| 3-methyl-2-cyclopentene-1-one | 63.87 | 15.65 |
| 4-cyclopentene-1,3-diketone | 73.12 | 20.31 |
| 3-furfural | 302.45 | 110.13 |
| 2-furfuryl alcohol | 594.60 | 224.67 |
| 5 hydroxymethyl furfural | 66.54 | 17.79 |
| 2,3-dimethyl indole | 24.34 | 6.79 |
| 2 methyl indole | 74.69 | 29.42 |
| 2-cyclopentene-1,4-diketone | 56.86 | 17.07 |
| Valeric acid | 83.24 | 20.95 |
| Oleic acid | 39.80 | 11.09 |
| Acetic acid | 1519.84 | 514.78 |
| Nicotine | 3134.71 | 1648.37 |
Embodiment 3:
The formula of the present embodiment tobacco juice for electronic smoke is (mass percent): 5% condensation Dry distillated flavor C, and 40% glycerine trapping destructive distillation is fragrant
Material B, 40% glycerine, 15% propane diols.Mix after above-mentioned raw materials is proportionally weighed, and be stirred until homogeneous, i.e. obtain containing cold
Solidifying Dry distillated flavor C and the tobacco juice for electronic smoke of glycerine trapping Dry distillated flavor B, can directly be added in electronic cigarette device atomization and suck.
The present embodiment condensation Dry distillated flavor C preparation process is as follows: under nitrogen protection, by south, 900g Anhui flue-cured tobacco pipe tobacco and 100g
Greece's spices offal carries out destructive distillation at 350 DEG C, and distillate flows in receiving bottle through running water condensation, prepares and can improve electronic cigarette
The condensation Dry distillated flavor C of organoleptic quality, its main chemical compositions is shown in Table 1 through GC-MS analysis result.
Embodiment 4:
The formula of the present embodiment tobacco juice for electronic smoke is (mass percent): 10% condensation Dry distillated flavor C, 20% glycerine trapping destructive distillation
Spices B, 40% glycerine, 20% propane diols.Mix after above-mentioned raw materials is proportionally weighed, and be stirred until homogeneous, i.e. contained
Condensation Dry distillated flavor C and the tobacco juice for electronic smoke of glycerine trapping Dry distillated flavor B, can directly be added in electronic cigarette device atomization and suck.
It is added in electronic cigarette carry out sensory evaluation by tobacco juice prepared by embodiment 1, embodiment 2, embodiment 3 and embodiment 4, comments
Valency the results are shown in Table 2, it is known that, in the present invention, electronic cigarette organoleptic quality is had by consumption and the different Dry distillated flavor ratio of Dry distillated flavor
When impact, specially Dry distillated flavor are less than 15% (embodiment 1), cigarette sense is more weak, (embodiment when consumption is between 15～50%
2,3 and 4), integrated sensory's mass is preferable.
Table 2 electronic cigarette sensory quality assessment result
| Sample number into spectrum | Aesthetic quality describes |
| Embodiment 1 | Cigarette sense is weak, pleasant impression is low |
| Embodiment 2 | Fragrance is preferable, cigarette sense is moderate, good after-taste |
| Embodiment 3 | Fragrance is good, mouthfeel is full, cigarette sense enhancing, good after-taste |
| Embodiment 4 | Fragrance preferably, cigarette sense by force, slightly Ipomoea batatas burnt odor, good after-taste |
Claims (3)
1. the tobacco juice for electronic smoke containing Dry distillated flavor, it is characterised in that: percent mass pressed by each raw material of described tobacco juice for electronic smoke
The composition of ratio is:
Dry distillated flavor 15～50%；
Glycerine 30～60%；
Surplus is propane diols；
Described Dry distillated flavor is at least one in condensation Dry distillated flavor and glycerine trapping Dry distillated flavor；
Described condensation Dry distillated flavor is prepared as follows: in a nitrogen atmosphere, is done by tobacco at 200 DEG C-400 DEG C
Evaporating, distillate flows in receiving bottle through running water condensation and collects, and obtains condensation Dry distillated flavor；
Described glycerine trapping Dry distillated flavor is prepared as follows: in a nitrogen atmosphere, entered by tobacco at 200 DEG C-400 DEG C
Row destructive distillation, distillate is introduced directly in glycerine, obtains glycerine trapping Dry distillated flavor.
Tobacco juice for electronic smoke containing Dry distillated flavor the most according to claim 1, it is characterised in that: described tobacco is sweet with described
The mass ratio of oil is 0.5-4:1.
Tobacco juice for electronic smoke containing Dry distillated flavor the most according to claim 1, it is characterised in that: described tobacco be flue-cured tobacco,
At least one in burley tobaccos and Turkish tobaccos, the form of described tobacco is at least one in sheet, thread and powder.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510246335.6A CN104783323B (en) | 2015-05-14 | 2015-05-14 | A kind of tobacco juice for electronic smoke containing Dry distillated flavor |
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| CN201510246335.6A CN104783323B (en) | 2015-05-14 | 2015-05-14 | A kind of tobacco juice for electronic smoke containing Dry distillated flavor |
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| CN104783323A CN104783323A (en) | 2015-07-22 |
| CN104783323B true CN104783323B (en) | 2016-08-17 |
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105167170A (en) * | 2015-09-14 | 2015-12-23 | 浙江中烟工业有限责任公司 | Method for preparing electronic cigarette nicotine liquid by means of tobacco subjected to dry distillation pyrolysis |
| CN105249518B (en) * | 2015-09-25 | 2017-10-03 | 安徽中烟工业有限责任公司 | A kind of preparation method for heating the porous tobacco-containing material of non-combustion-type cigarette |
| CN105595411B (en) * | 2016-02-01 | 2017-05-17 | 湖北中烟工业有限责任公司 | Method for preparing tobacco-characteristic-taste tobacco flavor material and electronic cigarette fluid containing tobacco flavor material |
| CN105725265A (en) * | 2016-04-28 | 2016-07-06 | 湖南中烟工业有限责任公司 | Device and method for preparing tobacco source basic cigarette flavor material for novel tobacco products |
| CN113142643A (en) * | 2021-02-08 | 2021-07-23 | 广东中烟工业有限责任公司 | Cigarette essence for heating non-combustible cigarettes and preparation method and application thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5235992A (en) * | 1991-06-28 | 1993-08-17 | R. J. Reynolds Tobacco Company | Processes for producing flavor substances from tobacco and smoking articles made therewith |
| CN1742636A (en) * | 2004-09-02 | 2006-03-08 | 邹宝安 | Technology for producing pollution-free liquid cigarette |
| CN104041936A (en) * | 2014-06-06 | 2014-09-17 | 山东中烟工业有限责任公司 | Method for extracting Chinese style mixed-fragrance cigarette juice for electronic cigarette |
| CN104041935A (en) * | 2014-06-06 | 2014-09-17 | 山东中烟工业有限责任公司 | Method for extracting Chinese-style flue-cured tobacco fragrance cigarette juice for electronic cigarette |
-
2015
- 2015-05-14 CN CN201510246335.6A patent/CN104783323B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5235992A (en) * | 1991-06-28 | 1993-08-17 | R. J. Reynolds Tobacco Company | Processes for producing flavor substances from tobacco and smoking articles made therewith |
| CN1742636A (en) * | 2004-09-02 | 2006-03-08 | 邹宝安 | Technology for producing pollution-free liquid cigarette |
| CN104041936A (en) * | 2014-06-06 | 2014-09-17 | 山东中烟工业有限责任公司 | Method for extracting Chinese style mixed-fragrance cigarette juice for electronic cigarette |
| CN104041935A (en) * | 2014-06-06 | 2014-09-17 | 山东中烟工业有限责任公司 | Method for extracting Chinese-style flue-cured tobacco fragrance cigarette juice for electronic cigarette |
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