CN101999751A - Method for comprehensively utilizing burdock root in tobacco - Google Patents
Method for comprehensively utilizing burdock root in tobacco Download PDFInfo
- Publication number
- CN101999751A CN101999751A CN 200910063800 CN200910063800A CN101999751A CN 101999751 A CN101999751 A CN 101999751A CN 200910063800 CN200910063800 CN 200910063800 CN 200910063800 A CN200910063800 A CN 200910063800A CN 101999751 A CN101999751 A CN 101999751A
- Authority
- CN
- China
- Prior art keywords
- tobacco
- radix bardanae
- water
- extract
- cigarette
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 74
- 238000000034 method Methods 0.000 title claims abstract description 47
- 235000003130 Arctium lappa Nutrition 0.000 title abstract description 29
- 235000008078 Arctium minus Nutrition 0.000 title abstract description 13
- 240000005528 Arctium lappa Species 0.000 title description 26
- 244000061176 Nicotiana tabacum Species 0.000 title 1
- 241000208125 Nicotiana Species 0.000 claims abstract description 73
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 58
- 239000000284 extract Substances 0.000 claims abstract description 56
- 239000000758 substrate Substances 0.000 claims abstract description 14
- 239000000843 powder Substances 0.000 claims abstract description 11
- 235000013599 spices Nutrition 0.000 claims abstract description 9
- 239000000463 material Substances 0.000 claims description 18
- 238000000605 extraction Methods 0.000 claims description 12
- 238000010009 beating Methods 0.000 claims description 10
- 239000002002 slurry Substances 0.000 claims description 10
- 239000000706 filtrate Substances 0.000 claims description 7
- 239000002893 slag Substances 0.000 claims description 7
- 230000006837 decompression Effects 0.000 claims description 5
- 238000010790 dilution Methods 0.000 claims description 5
- 239000012895 dilution Substances 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 3
- 235000019504 cigarettes Nutrition 0.000 abstract description 44
- 238000004519 manufacturing process Methods 0.000 abstract description 17
- 239000002994 raw material Substances 0.000 abstract description 10
- 239000000796 flavoring agent Substances 0.000 abstract description 7
- 235000019634 flavors Nutrition 0.000 abstract description 5
- 238000012545 processing Methods 0.000 abstract description 3
- 239000002699 waste material Substances 0.000 abstract description 3
- 241000208843 Arctium Species 0.000 abstract 4
- 238000009736 wetting Methods 0.000 abstract 2
- 230000001953 sensory effect Effects 0.000 abstract 1
- 238000003809 water extraction Methods 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 34
- 230000008569 process Effects 0.000 description 16
- 239000003906 humectant Substances 0.000 description 15
- 239000003205 fragrance Substances 0.000 description 13
- 229920001202 Inulin Polymers 0.000 description 12
- JYJIGFIDKWBXDU-MNNPPOADSA-N inulin Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)OC[C@]1(OC[C@]2(OC[C@]3(OC[C@]4(OC[C@]5(OC[C@]6(OC[C@]7(OC[C@]8(OC[C@]9(OC[C@]%10(OC[C@]%11(OC[C@]%12(OC[C@]%13(OC[C@]%14(OC[C@]%15(OC[C@]%16(OC[C@]%17(OC[C@]%18(OC[C@]%19(OC[C@]%20(OC[C@]%21(OC[C@]%22(OC[C@]%23(OC[C@]%24(OC[C@]%25(OC[C@]%26(OC[C@]%27(OC[C@]%28(OC[C@]%29(OC[C@]%30(OC[C@]%31(OC[C@]%32(OC[C@]%33(OC[C@]%34(OC[C@]%35(OC[C@]%36(O[C@@H]%37[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O%37)O)[C@H]([C@H](O)[C@@H](CO)O%36)O)[C@H]([C@H](O)[C@@H](CO)O%35)O)[C@H]([C@H](O)[C@@H](CO)O%34)O)[C@H]([C@H](O)[C@@H](CO)O%33)O)[C@H]([C@H](O)[C@@H](CO)O%32)O)[C@H]([C@H](O)[C@@H](CO)O%31)O)[C@H]([C@H](O)[C@@H](CO)O%30)O)[C@H]([C@H](O)[C@@H](CO)O%29)O)[C@H]([C@H](O)[C@@H](CO)O%28)O)[C@H]([C@H](O)[C@@H](CO)O%27)O)[C@H]([C@H](O)[C@@H](CO)O%26)O)[C@H]([C@H](O)[C@@H](CO)O%25)O)[C@H]([C@H](O)[C@@H](CO)O%24)O)[C@H]([C@H](O)[C@@H](CO)O%23)O)[C@H]([C@H](O)[C@@H](CO)O%22)O)[C@H]([C@H](O)[C@@H](CO)O%21)O)[C@H]([C@H](O)[C@@H](CO)O%20)O)[C@H]([C@H](O)[C@@H](CO)O%19)O)[C@H]([C@H](O)[C@@H](CO)O%18)O)[C@H]([C@H](O)[C@@H](CO)O%17)O)[C@H]([C@H](O)[C@@H](CO)O%16)O)[C@H]([C@H](O)[C@@H](CO)O%15)O)[C@H]([C@H](O)[C@@H](CO)O%14)O)[C@H]([C@H](O)[C@@H](CO)O%13)O)[C@H]([C@H](O)[C@@H](CO)O%12)O)[C@H]([C@H](O)[C@@H](CO)O%11)O)[C@H]([C@H](O)[C@@H](CO)O%10)O)[C@H]([C@H](O)[C@@H](CO)O9)O)[C@H]([C@H](O)[C@@H](CO)O8)O)[C@H]([C@H](O)[C@@H](CO)O7)O)[C@H]([C@H](O)[C@@H](CO)O6)O)[C@H]([C@H](O)[C@@H](CO)O5)O)[C@H]([C@H](O)[C@@H](CO)O4)O)[C@H]([C@H](O)[C@@H](CO)O3)O)[C@H]([C@H](O)[C@@H](CO)O2)O)[C@@H](O)[C@H](O)[C@@H](CO)O1 JYJIGFIDKWBXDU-MNNPPOADSA-N 0.000 description 12
- 229940029339 inulin Drugs 0.000 description 12
- 239000002304 perfume Substances 0.000 description 12
- 238000012360 testing method Methods 0.000 description 11
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 10
- 239000003546 flue gas Substances 0.000 description 10
- 102000004169 proteins and genes Human genes 0.000 description 10
- 108090000623 proteins and genes Proteins 0.000 description 10
- 230000000391 smoking effect Effects 0.000 description 9
- 239000007789 gas Substances 0.000 description 8
- 239000000203 mixture Substances 0.000 description 8
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 description 8
- 239000000126 substance Substances 0.000 description 8
- 150000001413 amino acids Chemical class 0.000 description 7
- 238000004227 thermal cracking Methods 0.000 description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- 238000005516 engineering process Methods 0.000 description 6
- 150000008442 polyphenolic compounds Chemical class 0.000 description 6
- 235000013824 polyphenols Nutrition 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 239000003814 drug Substances 0.000 description 5
- 239000000523 sample Substances 0.000 description 5
- 239000000779 smoke Substances 0.000 description 5
- 238000010561 standard procedure Methods 0.000 description 5
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 4
- 239000000654 additive Substances 0.000 description 4
- 230000000996 additive effect Effects 0.000 description 4
- 239000012496 blank sample Substances 0.000 description 4
- 229920002678 cellulose Polymers 0.000 description 4
- 239000001913 cellulose Substances 0.000 description 4
- 230000000704 physical effect Effects 0.000 description 4
- 238000000197 pyrolysis Methods 0.000 description 4
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 3
- 230000009471 action Effects 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 239000000835 fiber Substances 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 150000004676 glycans Chemical class 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- 229920001282 polysaccharide Polymers 0.000 description 3
- 239000005017 polysaccharide Substances 0.000 description 3
- ZGXJTSGNIOSYLO-UHFFFAOYSA-N 88755TAZ87 Chemical compound NCC(=O)CCC(O)=O ZGXJTSGNIOSYLO-UHFFFAOYSA-N 0.000 description 2
- 230000032683 aging Effects 0.000 description 2
- 238000003556 assay Methods 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 239000000686 essence Substances 0.000 description 2
- 230000002349 favourable effect Effects 0.000 description 2
- 235000013355 food flavoring agent Nutrition 0.000 description 2
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 description 2
- -1 glycan compounds Chemical class 0.000 description 2
- 235000011187 glycerol Nutrition 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- HJOVHMDZYOCNQW-UHFFFAOYSA-N isophorone Chemical compound CC1=CC(=O)CC(C)(C)C1 HJOVHMDZYOCNQW-UHFFFAOYSA-N 0.000 description 2
- 229940118199 levulan Drugs 0.000 description 2
- 210000004072 lung Anatomy 0.000 description 2
- 230000000144 pharmacologic effect Effects 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 239000002243 precursor Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 230000001737 promoting effect Effects 0.000 description 2
- 238000010926 purge Methods 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- SGAWOGXMMPSZPB-UHFFFAOYSA-N safranal Chemical compound CC1=C(C=O)C(C)(C)CC=C1 SGAWOGXMMPSZPB-UHFFFAOYSA-N 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 230000000638 stimulation Effects 0.000 description 2
- 238000010998 test method Methods 0.000 description 2
- 238000010792 warming Methods 0.000 description 2
- 238000005303 weighing Methods 0.000 description 2
- HNSDLXPSAYFUHK-UHFFFAOYSA-N 1,4-bis(2-ethylhexyl) sulfosuccinate Chemical group CCCCC(CC)COC(=O)CC(S(O)(=O)=O)C(=O)OCC(CC)CCCC HNSDLXPSAYFUHK-UHFFFAOYSA-N 0.000 description 1
- BGTBFNDXYDYBEY-FNORWQNLSA-N 4-(2,6,6-Trimethylcyclohex-1-enyl)but-2-en-4-one Chemical compound C\C=C\C(=O)C1=C(C)CCCC1(C)C BGTBFNDXYDYBEY-FNORWQNLSA-N 0.000 description 1
- NOEGNKMFWQHSLB-UHFFFAOYSA-N 5-hydroxymethylfurfural Chemical compound OCC1=CC=C(C=O)O1 NOEGNKMFWQHSLB-UHFFFAOYSA-N 0.000 description 1
- 229940127291 Calcium channel antagonist Drugs 0.000 description 1
- WTEVQBCEXWBHNA-UHFFFAOYSA-N Citral Natural products CC(C)=CCCC(C)=CC=O WTEVQBCEXWBHNA-UHFFFAOYSA-N 0.000 description 1
- IMKHDCBNRDRUEB-UHFFFAOYSA-N Dihydroactinidiolide Natural products C1CCC(C)(C)C2=CC(=O)OC21C IMKHDCBNRDRUEB-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 235000002918 Fraxinus excelsior Nutrition 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N Furan Chemical class C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- 241001488334 Hyles Species 0.000 description 1
- 229930183419 Irisone Natural products 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 206010068319 Oropharyngeal pain Diseases 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 201000007100 Pharyngitis Diseases 0.000 description 1
- 208000004880 Polyuria Diseases 0.000 description 1
- PBCJIPOGFJYBJE-UHFFFAOYSA-N acetonitrile;hydrate Chemical compound O.CC#N PBCJIPOGFJYBJE-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- UZFLPKAIBPNNCA-BQYQJAHWSA-N alpha-ionone Chemical compound CC(=O)\C=C\C1C(C)=CCCC1(C)C UZFLPKAIBPNNCA-BQYQJAHWSA-N 0.000 description 1
- 230000000259 anti-tumor effect Effects 0.000 description 1
- 230000002155 anti-virotic effect Effects 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 239000002956 ash Substances 0.000 description 1
- 239000012298 atmosphere Substances 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- POIARNZEYGURDG-FNORWQNLSA-N beta-damascenone Chemical compound C\C=C\C(=O)C1=C(C)C=CCC1(C)C POIARNZEYGURDG-FNORWQNLSA-N 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
- 235000019658 bitter taste Nutrition 0.000 description 1
- 239000000480 calcium channel blocker Substances 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 235000014633 carbohydrates Nutrition 0.000 description 1
- 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 description 1
- 235000013351 cheese Nutrition 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 229940043350 citral Drugs 0.000 description 1
- 238000010835 comparative analysis Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- IMKHDCBNRDRUEB-LLVKDONJSA-N dihydroactinidiolide Chemical compound C1CCC(C)(C)C2=CC(=O)O[C@@]21C IMKHDCBNRDRUEB-LLVKDONJSA-N 0.000 description 1
- 230000035619 diuresis Effects 0.000 description 1
- 238000010828 elution Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- LTUMRKDLVGQMJU-UHFFFAOYSA-N famesylacetone Natural products CC(C)=CCCC(C)=CCCC(C)=CCCC(C)=O LTUMRKDLVGQMJU-UHFFFAOYSA-N 0.000 description 1
- LTUMRKDLVGQMJU-IUBLYSDUSA-N farnesyl acetone Chemical compound CC(C)=CCC\C(C)=C\CC\C(C)=C\CCC(C)=O LTUMRKDLVGQMJU-IUBLYSDUSA-N 0.000 description 1
- 210000003746 feather Anatomy 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 150000002240 furans Chemical class 0.000 description 1
- WTEVQBCEXWBHNA-JXMROGBWSA-N geranial Chemical compound CC(C)=CCC\C(C)=C\C=O WTEVQBCEXWBHNA-JXMROGBWSA-N 0.000 description 1
- HNZUNIKWNYHEJJ-FMIVXFBMSA-N geranyl acetone Chemical compound CC(C)=CCC\C(C)=C\CCC(C)=O HNZUNIKWNYHEJJ-FMIVXFBMSA-N 0.000 description 1
- HNZUNIKWNYHEJJ-UHFFFAOYSA-N geranyl acetone Natural products CC(C)=CCCC(C)=CCCC(C)=O HNZUNIKWNYHEJJ-UHFFFAOYSA-N 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 238000004128 high performance liquid chromatography Methods 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000000413 hydrolysate Substances 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- RJGBSYZFOCAGQY-UHFFFAOYSA-N hydroxymethylfurfural Natural products COC1=CC=C(C=O)O1 RJGBSYZFOCAGQY-UHFFFAOYSA-N 0.000 description 1
- 230000002218 hypoglycaemic effect Effects 0.000 description 1
- 230000036737 immune function Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 235000012054 meals Nutrition 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 230000035772 mutation Effects 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 238000010606 normalization Methods 0.000 description 1
- 238000011017 operating method Methods 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 235000017509 safranal Nutrition 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- PQDRXUSSKFWCFA-CFNZNRNTSA-N solanone Chemical compound CC(=O)CC[C@@H](C(C)C)\C=C\C(C)=C PQDRXUSSKFWCFA-CFNZNRNTSA-N 0.000 description 1
- PQDRXUSSKFWCFA-UHFFFAOYSA-N solanone Natural products CC(=O)CCC(C(C)C)C=CC(C)=C PQDRXUSSKFWCFA-UHFFFAOYSA-N 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 235000014347 soups Nutrition 0.000 description 1
- 230000003595 spectral effect Effects 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 235000013547 stew Nutrition 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 229940126680 traditional chinese medicines Drugs 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 229930007850 β-damascenone Natural products 0.000 description 1
Landscapes
- Manufacture Of Tobacco Products (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses a method for comprehensively utilizing burdock roots in tobacco, which belongs to the technical field of cigarette. The technical scheme of the invention comprises the following steps: (1) preparing dry powder of burdock roots; (2) performing water extraction to obtain the extract-type water extract of burdock roots serving as tobacco spice with a wetting function; and (3) manufacturing a substrate of tobacco sheets by using filter residue. In the invention, a great amount of resources are available and the cost is low; the extract has functions of improving flavor and wetting at the same time; and the waste residue is used for manufacturing the substrate of the tobacco sheets, therefore, the lack of raw materials of the tobacco sheets by a papermaking method is relieved, and the sensory quality of the tobacco sheets by the papermaking method can be improved. The method of the invention ensures no waste during the processing and the comprehensive utilization of the burdock roots is realized.
Description
Technical field
The invention belongs to technical field of cigarettes, is a kind ofly to obtain water extract from the root of plant burdock specifically, is used for cigarette additive, and the filter residue after will extracting simultaneously is used for the comprehensive utilization method of reconstituted tobacoo.
Background technology
In the prior art, the security of cigarette is subjected to the more and more higher attention of people, and the tar that reduces in the cigarette has become a kind of inexorable trend, is accompanied by the reduction of tar content, and smoke is thin out, and fragrance weakens, and mouthfeel and pleasant impression variation are difficult to be accepted by the consumer.Flue gas concentration and fragrance in order to promote and improve cigarette improve cigarette mouthfeel and pleasant impression, and flavoring and casing becomes a valid approach.Simultaneously, in the production of cigarettes process, usually need to add glycerine, propane diols, sorbierite etc. and have the polyhydroxy substance of humectation effect as humectant, improve the physical property of tobacco, strengthen the anti-processability of tobacco, it is broken that minimizing adds making of man-hour, simultaneously, the moisture content of keeping cigarette shreds remains on a suitable scope, and the great fluctuation process excessively of avoiding moisture in cut tobacco is to the influence of cigarette smoking quality.
In the prior art, the essence and flavoring agent that in perfuming cigarette is reinforced, uses, main flue gas concentration and the fragrance of promoting and improving cigarette that rises improves effects such as cigarette mouthfeel and pleasant impression, does not possess the humectation effect; And the humectant that in the production of cigarettes process, adds, do not have to promote and improve cigarette flue gas concentration and fragrance, improve effects such as cigarette mouthfeel and pleasant impression.Therefore, must add essence and flavoring agent and humectant simultaneously in the production of cigarettes process, cause the defective that production technology complicates, production cost increases thus.And chemical synthesis products such as the glycerine that uses as humectant in the prior art, propane diols, sorbierite, because the restriction of use cost, purity can not be very high, unavoidably can contain some impurity, may bring negative effect to the cigarette smoking quality.Still the cigarette additive that does not have flavouring and humectation effect in the prior art simultaneously.
Reconstituted tobacoo is to be raw material with the tobacco dead meal in the cigarette process such as offal, offal, tobacco leaf fragment and part discarded tobacco leaf etc., through reconfiguring the reconstituted tobacco that processes.For alleviating tobacco sheets by paper making method raw material problem in short supply day by day, 1mm～80 order cigarette ashes discarded in the cigarette process are just applied in each thin slice manufacturer, but still can not fundamentally alleviate raw material problem in short supply, therefore, be badly in need of widening the raw material field for tobacco sheets by paper making method.
Burdock is a composite family biennial herb plant, uses comparatively extensive in pharmaceuticals industry.What pharmaceuticals industry was used mainly is its fruit great burdock achene.Great burdock achene, " Pharmacopoeia of People's Republic of China (one one) " (version in 2005) includes.Cold in nature, flavor is hot, bitter.Attach to the lung and stomach meridians.Function cures mainly: dispelling wind and heat from the body, a surname's lung promoting eruption, detoxifcation relieve sore throat.Modern pharmacological research has found that great burdock achene has the function of following several respects: antibiotic, antivirus action; The effect of calcium antagonist sample; Strengthen immunologic function and hypoglycemic activity; Anti-ephrosis becomes; Antitumor, mutation effect; Diuresis and discharge function etc.
Burdock has been realized large-area artificial cultivation in China, and it is edible that its leaf and root can be used as vegetables.Radix bardanae and tender leaf can be mixed, fry, burn, stew, cook soup, cook congee, transfer filling, saucing and make auxiliary material edible.At present, the also uncomfortable edible burdock of China people, therefore, China's burdock mainly is as raw material, with form processings such as fresh-keeping, quick-frozen, dehydration and salt marsh outlet Japan and Southeast Asia.But the international market is very high to the specification requirement of outlet burdock, thereby causes outer radix bardanae such as a lot of grades to be taken as discarded object, and only some is used to animal feed, and whole value is not high.
A lot of technical staff have carried out the range of application of expansion radix bardanae and the research of aspect, field, as: Chinese patent literature CN1267455C discloses edible burdock inulin and preparation method thereof, radix bardanae is through very complicated extraction, separation, purge process, remove materials such as small molecular weight impurity, pigment and protein, obtain the edible burdock inulin of higher degree; Chinese patent literature CN100493375C discloses comprehensive burdock root processing method; Chinese patent literature CN101218948 discloses a kind of burdok root beverage manufacturing method; Chinese patent literature CN1620999 discloses a kind of radix bardanae Chinese health care thoothpick; Chinese patent literature CN1806674 discloses burdock paste and preparation method; Chinese patent literature CN101095553 discloses a kind of processing technology of burdock preserved fruit.More than the application of these radix bardanaes all concentrate on food or field of medicaments.And the application of radix bardanae in cigarette yet there are no relevant report.
Summary of the invention
Above-mentioned deficiency at prior art, the technical problem to be solved in the present invention provides a kind of radix bardanae comprehensive utilization method in tobacco, the radix bardanae water extract that water obtains after extracting is as cigarette additive, and this additive has the effect of flavouring and humectation simultaneously in cigarette; Filter residue after the extraction is used for the substrate of reconstituted tobacoo manufactures paper with pulp, and has both alleviated the nervous problem of tobacco sheets by paper making method raw material to a certain extent, the aesthetic quality that can improve tobacco sheets by paper making method again.
Technical scheme of the present invention is: radix bardanae comprehensive utilization method in tobacco is carried out according to following steps:
[1], the outer radix bardanae such as fresh that will be taken as discarded object cleans up with running water, dries naturally, cuts into sheet, dries under 40-60 ℃ of temperature, is crushed to 40 orders, obtains radix bardanae dry powder;
[2], radix bardanae dry powder and water are mixed according to the ratio of mass ratio 1: 10-20, under temperature 70-90 ℃ condition, extract 2-3 time, each extraction time 0.5-2 hour, filter and merging filtrate, the filtrate decompression that merges is condensed into medicinal extract shape material, gained medicinal extract shape is the radix bardanae water extract, is a kind of tobacco spice that has the humectation function; Filter residue is left down step and uses;
[3], filter residue that step [2] the is kept substrate that is used for reconstituted tobacoo manufactures paper with pulp: the offal slag of above-mentioned filter residue and thin slice extraction or/and the offal slag mixes according to the ratio of mass ratio 1: 5-10, is sent into the high-density paste mill making beating, and making into beating degree is 20
OSR～30
OThe slurry of SR; Destroying the forebay with sending after above-mentioned slurry and outer fine the mixing, surfs the Net and makes the substrate of reconstituted tobacoo in the dilution back.
The resulting tobacco spice that has the humectation function of step [2] is diluted with water to 10%, and the 0.2-0.4% according to pipe tobacco weight adds in the pipe tobacco then.
Except as otherwise noted, percentage of the present invention and ratio all refer to percetage by weight and weight ratio.
Advantage of the present invention:
The present invention does raw material with the outer radix bardanae of grade of high quality and at a reasonable price, and the available resources amount is big, and is with low cost, realized the comprehensive utilization of waste resource.
The radix bardanae water extract that the present invention extracted is the tobacco spice that has the humectation function, is applied in the cigarette, both can effectively improve the sucking quality of cigarette, has certain humectation effect again, promptly has flavouring and humectation effect simultaneously.
The main component of the radix bardanae water extract that the present invention extracted is an edible burdock inulin, needs higher purity to compare with medicine with field of food, and this method need not complicated separation and purge process, and technology is simple, and is easy and simple to handle, saved cost greatly;
In the pyrolysis product of the radix bardanae water extract main component edible burdock inulin that employing the inventive method obtains the flavor component that often uses in a lot of tobacco blending is arranged, these compositions all have the effect that increases tobacco roasting perfume and ageing perfume (or spice) preferably.Simultaneously, the humectation effect of radix bardanae water extract is better than prior art humectant propane diols commonly used.Opened up the new purposes of edible burdock inulin as humectant.
The radix bardanae water extract that adopts the inventive method to obtain also contains compositions such as amino acids, Polyphenols, phytochrome class, and a spot of protein, these compositions are to need to remove in the application of medicine and field of food, but the aesthetic quality to cigarette has better effect in tobacco.The present invention is fully used the composition of radix bardanae.
Filter residue after the present invention extracts is except mainly containing cellulose, also contain the amino acids that is not extracted and remains, Polyphenols, phytochrome class, the material favourable such as protein-based to the cigarette aesthetic quality, therefore the substrate that is applied to reconstituted tobacoo is manufactured paper with pulp, both alleviated the nervous problem of tobacco sheets by paper making method raw material to a certain extent, the aesthetic quality that can improve tobacco sheets by paper making method again.
Do not have discarded object in the method process of the present invention, realized whole comprehensive utilizations of radix bardanae.
The specific embodiment
Below in conjunction with embodiments of the invention the relevant technologies problem is described in further detail.
Embodiment 1 cleans up outer radix bardanae such as fresh grade with running water, dry naturally, with manually or slicer be cut into the sheet of big or small thickness homogeneous, 40 ℃ of oven for drying, mechanical crushing obtain radix bardanae dry powder to 40 orders.With radix bardanae dry powder and water according to mass ratio 1: 10 ratio extract 3 times, 90 ℃ of temperature, each 0.5 hour extraction time, filter, filtrate decompression is condensed into the medicinal extract shape, gained medicinal extract shape material is the radix bardanae water extract.
Radix bardanae water extract of the present invention is diluted with water to 10%, adds in the high-grade cigarette pipe tobacco according to 0.2% of pipe tobacco weight then, smoke panel test according to national standard method behind the making cigarette.Smoking result is: the effect of tangible increase tobacco roasting perfume and lifting fragrance matter is arranged.
The offal slag of above-mentioned filter residue and prior art production is mixed according to 1: 5 ratio of mass ratio, send into the high-density paste mill making beating, making into beating degree is 20
OSR～30
OThe slurry of SR; Send after outer fibre that above-mentioned slurry and prior art are produced mixes and destroy the forebay, dilution is afterwards surfed the Net and is made substrate.Then according to prior art production paper process thin slice.
Embodiment 2 cleans up outer radix bardanae such as fresh grade with running water, dry naturally, with manually or slicer be cut into the sheet of big or small thickness homogeneous, 50 ℃ of oven for drying, mechanical crushing obtain radix bardanae dry powder to 40 orders.With radix bardanae dry powder and water according to mass ratio 1: 15 ratio extract 3 times, 80 ℃ of temperature, each 1 hour extraction time, filter, filtrate decompression is condensed into the medicinal extract shape, gained medicinal extract shape material is the radix bardanae water extract.
Radix bardanae water extract of the present invention is diluted with water to 10%, adds in the middle-grade cigarette shreds according to 0.3% of pipe tobacco weight then, smoke panel test according to national standard method behind the making cigarette.Smoking result is: the effect of tangible increase tobacco roasting perfume and increase perfume quantity is arranged.
The offal slag of above-mentioned filter residue and prior art production is mixed according to 1: 8 ratio of mass ratio, send into the high-density paste mill making beating, making into beating degree is 20
OSR～30
OThe slurry of SR; Send after outer fibre that above-mentioned slurry and prior art are produced mixes and destroy the forebay, dilution is afterwards surfed the Net and is made substrate.Then according to prior art production paper process thin slice.
Embodiment 3 cleans up outer radix bardanae such as fresh grade with running water, dry naturally, with manually or slicer be cut into the sheet of big or small thickness homogeneous, 60 ℃ of oven for drying, mechanical crushing obtain radix bardanae dry powder to 40 orders.With radix bardanae dry powder and water according to mass ratio 1: 20 ratio extract 2 times, 70 ℃ of temperature, each 2 hours extraction times, filter, filtrate decompression is condensed into the medicinal extract shape, gained medicinal extract shape material is the radix bardanae water extract.
Radix bardanae water extract of the present invention is diluted with water to 10%, adds in the high-grade cigarette pipe tobacco according to 0.4% of pipe tobacco weight then, smoke panel test according to national standard method behind the making cigarette.Smoking result is: tangible increase tobacco roasting perfume (or spice) is arranged, increase flue gas concentration and cover the effect of assorted gas.
The offal slag of above-mentioned filter residue and prior art production is mixed according to 1: 10 ratio of mass ratio, send into the high-density paste mill making beating, making into beating degree is 20
OSR～30
OThe slurry of SR; Send after outer fibre that above-mentioned slurry and prior art are produced mixes and destroy the forebay, dilution is afterwards surfed the Net and is made substrate.Then according to prior art production paper process thin slice.
Radix bardanae contains polyphenol, amino acid, synanthrin, cellulose, phytochrome, protein and glycan compounds etc., and wherein synanthrin about about 25%.The applicant through further investigation, recognizes that carbohydrate, amino acids, phytochrome class, the polyphenols in the radix bardanae all has better action to the aesthetic quality of tobacco before making the present invention.Glucide: can produce acidic materials on the one hand, suppress the alkalescence of flue gas neutral and alkali material, make the acid-base balance appropriateness of flue gas, reduce excitant, produce gratifying jealous; On the other hand, prop up in the process of burning and sucking in heating and cigarette, sugar is the important as precursors that forms aroma substance, when temperature at 300 degree when above, pyrolysis forms multiple aroma substance separately, and wherein most important have a furan derivatives, carbonyls such as simple ketone and aldehydes.The amino acids material: the burning of an amount of amino acid produces nitrogen-containing compound, and flue gas is enriched, energetically; Simultaneously can also and reduced sugar between the Maillard reaction takes place, generate have sweet, roasting, puffed rice, nut, the compound of feature fragrance such as cheese.Polyphenols: effect with extraordinary soft flue gas.Phytochrome: the precursor that is a lot of important fragrance matters in the tobacco, in cigarette heating and burn and suck in the process, but pyrolysis generates the compound that solanone, geranyl acetone, farnesyl acetone, isophorone and derivative, cyclisation citral and safranal, dihydroactinidiolide, irisone, damascenone, damascone etc. embody these notes of tobacco.Protein: the hydrolysate of protein and the product that further transforms are the hyles of many tobacco aroma materials, contain an amount of protein, can give sufficient tobacco aroma and plentiful jealous intensity, but protein content is too high, can cause flue gas intensity excessive, fragrance and jealous variation, produce acid, bitter taste and excitant, and when burning and sucking, the protein content height can produce a kind of albumen stink as the burning feather, and discover through the applicant, the contained protein content of radix bardanae is about 2% (Jiang Shumin, burdock chemical composition and Pharmacological action study present situation, the time precious traditional Chinese medical science traditional Chinese medicines, calendar year 2001, the 12nd volume, the 10th phase, the 941-942 page or leaf), far below tobacco leaf 4%-13%, average 7.6% protein content (Shao Hui virtue 1, permitted to have of one's own 1, the relation of Liu Li flue-cured tobacco total nitrogen and protein content and main volatile aroma substance, Xibei Univ. of Agricultural ﹠ Forest Science ﹠ Technology's journal (natural science edition) 2008, the 36th volume, the 12nd phase, the 69-76 page or leaf), therefore, protein content is relatively low in the radix bardanae, can not play the effect that influences the aesthetic quality.
The polysaccharide materials such as synanthrin that this method is primarily aimed in the radix bardanae extract, and are used for cigarette flavors, can increase cigarette flavor.The applicant thinks that the radix bardanae water extract has humectation effect preferably, may be because synanthrin is a compound sugar, has a plurality of hydroxyls in its molecular structure, can be preferably and water molecules, form chemical bond (hydrogen bond), and therefore have humectation effect preferably.And polysaccharide materials such as synanthrin have dissolubility preferably in water, and water of the present invention extracts as solvent, and the filter residue after the extraction is rich in cellulose substances, can satisfy the tobacco slice production requirement, and the substrate that is used for tobacco sheets by paper making method is manufactured paper with pulp.Water extracts in the process of polysaccharide materials such as synanthrin, and amino acids, Polyphenols, phytochrome class etc. have the material of better effect to the aesthetic quality of tobacco, and a small amount of water-soluble protein substance all can have part to be extracted simultaneously; These that are not extracted are out then stayed in the filter residue with cellulose the material that the aesthetic quality of tobacco has better effect, can to a certain degree improve the aesthetic quality of tobacco sheets by paper making method.Therefore, method of the present invention all is fully utilized the main component of radix bardanae.Opened up radix bardanae range of application.Simultaneously, this method does not have discarded object, is the real comprehensive utilization of radix bardanae.Water extracts also has inexpensive advantage, therefore helps the popularization of commercial Application.
The applicant also just relevant with the present invention technical problem has carried out deep discussion.AOAC OfficialMethod 997.08 has stipulated levulan Determination on content method, and synanthrin belongs to levulan.The content of edible burdock inulin is measured in the radix bardanae water extract that the inventor obtains the present invention with high performance liquid chromatography according to this method, and condition determination is as follows:
Instrument is Dionex 3000 highly effective liquid phase chromatographic systems.Chromatographic column: the PrevailCarbohydrate of Alltech company sugar post; EISD: 81.5 ℃ of drift tube temperatures, throughput 2.2L/min.30 ℃ of column temperatures, flow velocity 1.0ml/min; Sample size: 10 μ l.Condition of gradient elution is: acetonitrile-water, elution program (table 1).
Table 1 gradient elution program
| Time (min) | Acetonitrile (%) | Water (%) |
| 0-3 | 70 | 30 |
| 3-4 | 70-75 | 30-25 |
| 4-10 | 75 | 25 |
| 10-11 | 75-65 | 25-35 |
| 11-25 | 65 | 35 |
Synanthrin assay result such as following table 2 in the radix bardanae water extract that the present invention obtains.
Table 2 synanthrin assay result
| Synanthrin (%) | |
| Embodiment 1 | 65.64 |
| Embodiment 2 | 65.43 |
| Embodiment 3 | 66.17 |
The inventor is by prior art, prepared in laboratory the higher edible burdock inulin (Chinese patent literature CN1267455C) of purity, then the thermal cracking products of edible burdock inulin is studied, condition determination is as follows:
Instrument: Pyroprobe 2000 thermal cracking instrument (U.S. CDS company), DSQ II gas chromatograph-mass spectrometer (GC-MS) (U.S. Thermo Fisher company).Thermal cracking atmosphere: nitrogen.Thermal cracking probe (pyrolysis head) initial temperature: 30 ℃, rise to 300 ℃ of final temperatures, 600 ℃ and 900 ℃, duration 10s respectively with 20 ℃/ms speed.DB-5ms 30 * 0.25mm * 0.25 μ m; Temperature programming: 40 ℃ (keeping 1min), be warming up to 100 ℃ (keeping 1min) with 2 ℃/min, with 8 ℃/min, be warming up to 280 ℃ (keeping 5min); Injector temperature: 260 ℃; Interface temperature: 280 ℃; Input mode: shunting, flow velocity 1.0ml/min; Ionization energy: 70eV.Sweep limits: 35-400amu, standard mass spectral database: NIST98 and WILEY275 spectrum storehouse.Area normalization is quantitative.
Edible burdock inulin is thermal cracking result under the different temperatures such as following table 4 in nitrogen environment.
The thermal cracking primary product result (%) of table 3 edible burdock inulin
"-" expression does not detect.
As seen, the edible burdock inulin composition that content is bigger in the thermal cracking products under the different temperatures mainly contains: furfuran compounds such as furfural, 5 hydroxymethyl furfural from last table.These compositions all have the effect that increases tobacco roasting perfume and ageing perfume (or spice) preferably.Edible burdock inulin is the main component of radix bardanae water extract, and result of the test has proved the flavouring effect of radix bardanae water extract.
In the radix bardanae water extract that the inventor also obtains extraction and the prior art the humectant propane diols of frequent use put in the cigarette shreds according to identical ratio and program, estimate humectation effect separately under different temperature and humidity conditions.Having investigated in temperature is that 40 ± 1 ℃, relative humidity are the humectation effect of each humectant under 35 ± 3% conditions.
Undertaken by following operating procedure: it is that 22 ± 1 ℃, relative humidity are 60 ± 2% climatic chamber balance after 48 hours that certain cigarette composition pipe tobacco is put into temperature, takes by weighing the 100g that cuts filler respectively; Every kind of humectant takes by weighing 0.40g, is diluted with water to 10g respectively and is sprayed in the pipe tobacco, and blank sample is sprayed water to 10g; Pipe tobacco is divided in sample disc, put into temperature and be 40 ± 1 ℃, relative humidity and be 35 ± 3% climatic chamber balance; Test specimen weighed in per 2 hours and detect once, continue to detect 10 hours, detect altogether 6 times; Calculate the weight rate of each sample at different detection time of pipe tobacco.The result is as shown in table 4 below.
The weight rate (%) of different time pipe tobacco under the table 4 high temperature low humidity condition
| The humectant title | 0(h) | 2(h) | 4(h) | 6(h) | 8(h) | 10(h) |
| Propane diols | 0.00 | 5.43 | 5.88 | 6.49 | 6.75 | 6.88 |
| The radix bardanae water extract | 0.00 | 4.91 | 5.14 | 5.76 | 5.92 | 6.13 |
| Blank sample | 0.00 | 5.89 | 6.26 | 6.77 | 7.05 | 7.41 |
Also having investigated in temperature is that 10 ± 1 ℃, relative humidity are the humectation effect of each humectant under 60 ± 3% conditions.Test method is the same, and the result is as shown in table 5 below.
The weight rate (%) of different time pipe tobacco under the wet condition in table 5 low temperature
| The humectant title | 0(h) | 2(h) | 4(h) | 6(h) | 8(h) | 10(h) |
| Propane diols | 0.00 | 4.28 | 4.66 | 4.92 | 5.23 | 5.54 |
| The radix bardanae water extract | 0.00 | 3.85 | 4.04 | 4.22 | 4.39 | 4.55 |
| Blank sample | 0.00 | 5.89 | 6.26 | 6.77 | 7.05 | 7.41 |
Also having investigated in temperature is that 30 ± 1 ℃, relative humidity are the humectation effect of each humectant under 60 ± 3% conditions.Test method is the same, and the result is as shown in table 6 below.
The weight rate (%) of different time pipe tobacco under the condition that wets in the temperature in the table 6
| The humectant title | 0(h) | 2(h) | 4(h) | 6(h) | 8(h) | 10(h) |
| Propane diols | 0.00 | 4.41 | 4.72 | 5.05 | 5.38 | 5.69 |
| The radix bardanae water extract | 0.00 | 4.02 | 4.15 | 4.39 | 4.56 | 4.72 |
| Blank sample | 0.00 | 5.92 | 6.44 | 6.89 | 7.15 | 7.48 |
From above experiment as seen, under different temperatures, the damp condition, the humectation effect of radix bardanae water extract all is better than the humectant propane diols that prior art is used.
According to protein content in the filter residue after standard GB/T 5009.5-1985 employing Kjeldahl is measured the radix bardanae water extract and extracted.Measurement result such as following table 7.Generally about 1%, visible radix bardanae water extract low percentages of protein adds the negative effect that can not bring the cigarette aesthetic quality in the pipe tobacco to protein content in the leaf tobacco extract that often uses during tobacco flavoring is reinforced; And in the tobacco sheets by paper making method in the most frequently used raw material offal protein content generally at 4%-13%, average 7.6%, low percentages of protein in the visible filter residue, being used for tobacco sheets by paper making method has favourable effect to the aesthetic quality.
Table 7 protein content determination result
| Radix bardanae water extract protein content (%) | Filter residue protein content (%) | |
| Embodiment 1 | 0.33 | 2.72 |
| Embodiment 2 | 0.35 | 2.67 |
| Embodiment 3 | 0.32 | 2.69 |
The radix bardanae water extract that the applicant obtains extraction adds in the cigarette smokes panel test, and smokes panel test and carries out according to national standard method, and 7 people form the group of smokeing panel test, 2 national judging panels, 5 provincial judging panels, smoking result such as following table 8.As seen from the table, after radix bardanae water extract of the present invention puts on pipe tobacco, the aesthetic quality that can improve cigarette.
Table 8 radix bardanae water extract puts on smoking result behind the pipe tobacco
| Embodiment 1 | The effect of tangible increase tobacco roasting perfume and lifting fragrance matter is arranged. |
| Embodiment 2 | The effect of tangible increase tobacco roasting perfume and increase perfume quantity is arranged. |
| Embodiment 3 | Tangible increase tobacco roasting perfume (or spice) is arranged, increase flue gas concentration and cover the effect of assorted gas. |
Manufacture paper with pulp thin slice that obtains and the thin slice that does not add filter residue of the substrate that filter residue after the inventor also extracts radix bardanae water of the present invention is applied to reconstituted tobacoo carried out the physical property detection, result such as following table 9:
The contrast of table 9 thin slice physical property testing result
As seen, thin slice of the present invention and prior art thin slice are more approaching on physical property, do not have notable difference.
The substrate that filter residue after the inventor also extracts radix bardanae water the is applied to reconstituted tobacoo thin slice that thin slice that obtains and the prior art of not adding filter residue produce of manufacturing paper with pulp has carried out the aesthetic quality comparative evaluation, smoke panel test and carry out according to national standard method, 7 people form the group of smokeing panel test, 2 national judging panels, 5 provincial judging panels, smoking result such as following table 10:
Table 10 thin slice contrast smoking result
| Prior art | Fragrance is still plentiful, and strength is medium, and assorted gas is big slightly, and stimulation is arranged, and pleasant impression is more comfortable |
| Embodiment 1 | Fragrance is still plentiful, and strength is medium, and slightly assorted gas has than pinprick, and pleasant impression is more comfortable. |
| Embodiment 2 | Fragrance is still plentiful, and strength is medium, and slightly assorted gas has than pinprick, and pleasant impression is comfortable. |
| Embodiment 3 | Fragrance is still plentiful, and strength is medium, and slightly assorted gas has than pinprick, and pleasant impression is comfortable |
As seen, the thin slice produced of the thin slice that obtains of the present invention and prior art is having improvement aspect assorted gas, stimulation and the pleasant impression.
Claims (2)
1. radix bardanae comprehensive utilization method in tobacco is characterized in that described comprehensive utilization method carries out according to following steps:
[1], outer radix bardanae such as fresh is cleaned up with running water, dry naturally, cut into sheet, under 40-60 ℃ of temperature, dry, be crushed to 40 orders, obtain radix bardanae dry powder;
[2], radix bardanae dry powder and water are mixed according to the ratio of mass ratio 1: 10-20, under temperature 70-90 ℃ condition, extract 2-3 time, each extraction time 0.5-2 hour, filter and merging filtrate, the merging filtrate decompression is condensed into medicinal extract shape material, and gained medicinal extract shape material is the radix bardanae water extract; Filter residue is left down step and uses;
[3], filter residue that step [2] the is kept substrate that is used for reconstituted tobacoo manufactures paper with pulp: the offal slag of above-mentioned filter residue and thin slice extraction or/and the offal slag mixes according to the ratio of mass ratio 1: 5-10, is sent into the high-density paste mill making beating, and making into beating degree is 20
OSR～30
OThe slurry of SR; Destroying the forebay with sending after above-mentioned slurry and outer fine the mixing, surfs the Net and makes the substrate of reconstituted tobacoo in the dilution back.
2. radix bardanae according to claim 1 comprehensive utilization method in tobacco is characterized in that: the resulting tobacco spice that has the humectation function of step [2] is diluted with water to 10%, and the 0.2-0.4% according to pipe tobacco weight adds in the pipe tobacco then.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200910063800 CN101999751B (en) | 2009-09-02 | 2009-09-02 | Method for comprehensively utilizing burdock root in tobacco |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200910063800 CN101999751B (en) | 2009-09-02 | 2009-09-02 | Method for comprehensively utilizing burdock root in tobacco |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101999751A true CN101999751A (en) | 2011-04-06 |
| CN101999751B CN101999751B (en) | 2012-12-05 |
Family
ID=43807640
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200910063800 Expired - Fee Related CN101999751B (en) | 2009-09-02 | 2009-09-02 | Method for comprehensively utilizing burdock root in tobacco |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101999751B (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102754914A (en) * | 2012-07-27 | 2012-10-31 | 红云红河烟草(集团)有限责任公司 | Fructo-oligosaccharide cigarette humectant and use method thereof |
| CN103645272A (en) * | 2013-12-23 | 2014-03-19 | 深圳出入境检验检疫局工业品检测技术中心 | Method for detecting high-boiling-point substances in industrial products |
| CN103844346A (en) * | 2014-03-04 | 2014-06-11 | 江苏中烟工业有限责任公司 | Burdock root ethanol extract and application thereof in tobacco |
| CN103859578A (en) * | 2014-03-04 | 2014-06-18 | 江苏中烟工业有限责任公司 | Extracting method of burdock crude polysaccharide and application of burdock crude polysaccharide to tobacco |
| CN112030608A (en) * | 2020-08-27 | 2020-12-04 | 重庆中烟工业有限责任公司 | Cigarette paper with improved taste and preparation method thereof |
| WO2022230891A1 (en) * | 2021-04-26 | 2022-11-03 | 日本たばこ産業株式会社 | Tobacco sheet for non-combustion-heating-type flavor inhaler, non-combustion-heating-type flavor inhaler, and non-combustion-heating-type flavor inhalation system |
| WO2022230885A1 (en) * | 2021-04-26 | 2022-11-03 | 日本たばこ産業株式会社 | Tobacco sheet for non-combustion heating-type flavor inhaler, non-combustion heating-type flavor inhaler, and non-combustion heating-type flavor inhalation system |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1106805C (en) * | 2000-06-26 | 2003-04-30 | 华南理工大学 | Tabacco sheet producing process by using the leftover of cigarette factory |
| CN1194642C (en) * | 2002-04-12 | 2005-03-30 | 中国农业大学 | Biologic enzyme treatment method for promoting natural alcoholization of re-flue-cured tobacco |
| CN1219470C (en) * | 2003-12-29 | 2005-09-21 | 江苏智思机械制造有限公司 | New Process for producing tobacco shred |
| CN1248604C (en) * | 2004-06-25 | 2006-04-05 | 云南瑞升科技有限公司 | Immobilized biological additive and its preparation method and uses |
| CN100563475C (en) * | 2007-01-19 | 2009-12-02 | 武汉烟草(集团)有限公司 | A kind of ramie external fiber that is used for reconstituted tobacoo and preparation method thereof |
-
2009
- 2009-09-02 CN CN 200910063800 patent/CN101999751B/en not_active Expired - Fee Related
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102754914A (en) * | 2012-07-27 | 2012-10-31 | 红云红河烟草(集团)有限责任公司 | Fructo-oligosaccharide cigarette humectant and use method thereof |
| CN103645272A (en) * | 2013-12-23 | 2014-03-19 | 深圳出入境检验检疫局工业品检测技术中心 | Method for detecting high-boiling-point substances in industrial products |
| CN103844346A (en) * | 2014-03-04 | 2014-06-11 | 江苏中烟工业有限责任公司 | Burdock root ethanol extract and application thereof in tobacco |
| CN103859578A (en) * | 2014-03-04 | 2014-06-18 | 江苏中烟工业有限责任公司 | Extracting method of burdock crude polysaccharide and application of burdock crude polysaccharide to tobacco |
| CN103859578B (en) * | 2014-03-04 | 2016-05-18 | 江苏中烟工业有限责任公司 | The extracting method of the thick polysaccharide of a kind of burdock and the application in tobacco thereof |
| CN112030608A (en) * | 2020-08-27 | 2020-12-04 | 重庆中烟工业有限责任公司 | Cigarette paper with improved taste and preparation method thereof |
| WO2022230891A1 (en) * | 2021-04-26 | 2022-11-03 | 日本たばこ産業株式会社 | Tobacco sheet for non-combustion-heating-type flavor inhaler, non-combustion-heating-type flavor inhaler, and non-combustion-heating-type flavor inhalation system |
| WO2022230885A1 (en) * | 2021-04-26 | 2022-11-03 | 日本たばこ産業株式会社 | Tobacco sheet for non-combustion heating-type flavor inhaler, non-combustion heating-type flavor inhaler, and non-combustion heating-type flavor inhalation system |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101999751B (en) | 2012-12-05 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101999751B (en) | Method for comprehensively utilizing burdock root in tobacco | |
| CN101548797B (en) | Cigarette and preparation method thereof | |
| CN101496636B (en) | Method for preparing and using functional plant stuffing for thin sheet raw material of paper-making process | |
| CN101518358B (en) | Cigarette perfume solvent and preparation method thereof | |
| KR101992344B1 (en) | Manufacturing method of high quality red platycodon and red platycodon thereof | |
| CN101322579A (en) | Low-harm type cigarette capable of reducing cigarette harm and manufacture method thereof | |
| CN106281690A (en) | A kind of flavoring essence improving bamboo pulp Chip Quality and application thereof | |
| CN109953366A (en) | A kind of cordyceps extracting liquid and preparation method thereof, composition and application | |
| KR100707345B1 (en) | Steamed bellflower | |
| CN102793265B (en) | Preparation method of natural tobacco moisture retaining fumet and applications of natural tobacco moisture retaining fumet in cigarette | |
| CN109258877A (en) | A kind of alternative tea process of granulation polygonatum kingianurn | |
| KR101862834B1 (en) | A preparing mehod of puffed ginseng with excellent taste and functionality using ginseng berry | |
| KR20100068668A (en) | Cooking sauce and method for making the sauce able to be added to cooking of meat or fish | |
| CN102002437B (en) | Method for extracting cigarette additives from pre-degreased burdock by ethanol and application thereof | |
| KR102490852B1 (en) | Manufacturing method for rehmannia radix | |
| CN105533098A (en) | Functional tablet candy and preparation method thereof | |
| CN102002438B (en) | Method for extracting additive from geotrichum candidum fermented burdock by using alcohol and application of additive | |
| CN106590914B (en) | Natural spicy essence and preparation method and application thereof | |
| JP5565924B2 (en) | Total amount of potato shochu and its production method | |
| CN114525173A (en) | Licorice composite spice and preparation method and application thereof | |
| CN113693276A (en) | Fermented glutinous rice aroma-enhancing granule and preparation method thereof | |
| KR102141702B1 (en) | Manufacturing method of fermented rice cake using cudrania tricuspidata fermented liquor | |
| KR20130034905A (en) | Method for preparation of a functional drink having artemisia capillaris | |
| KR101144336B1 (en) | Method for preparing of meat stock for rice noodles | |
| CN101461563B (en) | Top dressing flavor of fire-cured tobacco as well as preparation method and use method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20121205 Termination date: 20140902 |
|
| EXPY | Termination of patent right or utility model |