CN103859578A - Extracting method of burdock crude polysaccharide and application of burdock crude polysaccharide to tobacco - Google Patents
Extracting method of burdock crude polysaccharide and application of burdock crude polysaccharide to tobacco Download PDFInfo
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- CN103859578A CN103859578A CN201410074836.6A CN201410074836A CN103859578A CN 103859578 A CN103859578 A CN 103859578A CN 201410074836 A CN201410074836 A CN 201410074836A CN 103859578 A CN103859578 A CN 103859578A
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- cigarette
- burdock
- crude polysaccharide
- thick polysaccharide
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Abstract
The invention discloses an extracting method of burdock crude polysaccharide and application of the burdock crude polysaccharide to tobacco, and belongs to the field of cigarette health care. The method comprises the following steps that burdock roots are subjected to impurity removal, are washed cleanly, are cut into slices and are placed into a pulp refiner, water is added, the materials are crushed by the pulp refiner, the ultrasonic extraction is carried out for 1 to 2 hours, water is used for extraction for 1 to 2 hours under the condition of 80 to 120 DEG C, filtering is carried out, filter liquor is concentrated, ethanol is added in the concentration liquid so that the ethanol concentration can reach higher than 80 percent, after the uniform mixing, the materials are subjected to still standing for more than 8 hours at 4 DEG C, and the burdock root crude polysaccharide is obtained after centrifugation, filtering and precipitation; the burdock root crude polysaccharide is diluted and dissolved by clean water to obtain material liquor, and in addition, the material liquor is added onto cut tobacco of the cigarette. The burdock root crude polysaccharide is used as the material liquor for the cigarette to be added onto the cut tobacco of the cigarette, special chemical ingredients can be generated when the cigarette is ignited and smoked, the smoking quality of the cigarette is obviously improved, the smoking mouth feeling is improved, the stimulation and the harm of the cigarette to the human bodies are reduced, in addition, a good health care effect is realized on the human body, the cost is not high, and the practicability is high.
Description
Technical field
The present invention relates to extracting method and the application thereof of the thick polysaccharide of a kind of burdock, specifically the extracting method of the thick polysaccharide of a kind of burdock and the application in tobacco thereof, belong to cigarette healthcare field.
Background technology
Harmfulness of smoking healthy the old and the young all know, contains 4000 number of chemical materials in cigarette, wherein most to the toxic effect of human body.Smoking not only causes multiple injury to smoker's physical and mental health, but also contaminated environment, a large amount of innocent persons is done harm to because of passive smoking among unconscious, so people are more and more higher to the requirement of cigarette by cigarette.Along with smoking and healthy problem more and more receive publicity, improve sucking security, increase health care, reducing harmful components in cigarette smoke and become the inexorable trend of the development of cigarette of cigarette.
Summary of the invention
The object of the present invention is to provide the extracting method of the thick polysaccharide of a kind of burdock and the application in tobacco thereof, can improve the security of sucking of cigarette, increase fragrance concentration and the richness of cigarette, reduce the harmful components in cigarette smoke, what increase cigarette sucks mouthfeel and health care, reduces the stimulation of cigarette to human body.
To achieve these goals, the extracting method of the thick polysaccharide of a kind of burdock of technical scheme of the present invention, comprises following processing step:
1) select materials, remove matter: select radix bardanae, remove impurity;
2) clean, cut into slices: by the radix bardanae clear water wash clean except after matter, and cut into slices;
3) pulverize: the sheet cutting in step (2) is put into refiner, smash, the ratio of smashing rear gained material and water is 1:30;
4) ultrasonic extraction: with ultrasonic extraction 1h～2h, under 80 ℃～120 ℃ conditions, water extracts radix bardanae powder 1h～2h;
5) filter: the filtrate after radix bardanae powder extracting liquid filtering is concentrated, be concentrated to 1/5～1/7 of original volume;
6) add ethanol: concentrate is added to ethanol by a certain percentage, concentration of alcohol is reached more than 80%;
7) standing, centrifugal: after concentrate and ethanol mix, at 2 ℃～6 ℃, more than standing 8h, after centrifugal, filtration, precipitation, to make the thick polysaccharide of radix bardanae.
As preferably, in step (4), hyperacoustic power is 300W～450W.
As preferably, in step (6), the volume ratio of concentrate and ethanol is 1:4.
The application of the thick polysaccharide of burdock in tobacco, the consumption of the thick polysaccharide of described burdock is 0.08%～0.15% of pipe tobacco weight, makes cigarette feed liquid, and this cigarette is joined on cigarette shreds by feed liquid after clear water dilution is dissolved.
As preferably, cigarette adds on cigarette shreds by spray pattern by feed liquid.
The present invention joins on cigarette shreds by feed liquid thick radix bardanae polysaccharide as cigarette, in the time that burning and sucking, cigarette can produce distinctive chemical composition, obviously improve or improve the sucking quality of cigarette, can make cigarette flavor concentration increase, richness is better, flue gas tendency is very fast, with sweet perfume (or spice), improve and suck mouthfeel, hamony is better, reduce the stimulation of cigarette to human body, pleasant impression is more comfortable.The present invention does not change original performance of cigarette, improve the sucking quality of cigarette, reduce the harm of cigarette to human body, in addition, because burdock is composite family biennial herb plant, it is good medicinal and edible plant, contain various bioactivators, under thering is stomach invigorating, beneficial gas, diuresis, rushing down, the effect such as nourishing and strengthening vital, clearing heat and detoxicating, inhibiting bacteria and diminishing inflammation, human body is had to good health-care effect, and cost is not high, therefore there is very high practical value.
The specific embodiment
Below in conjunction with embodiment, the present invention is described further.
embodiment 1:
The cigarette preparation method that what the present embodiment provided contain the thick polysaccharide of burdock, processing step is as follows:
1) select materials, remove matter: select radix bardanae, remove impurity;
2) clean, cut into slices: by the radix bardanae clear water wash clean except after matter, and cut into slices;
3) pulverize: the sheet cutting in step (2) is put into refiner, smash, the ratio of smashing rear gained material and water is 1:30;
4) ultrasonic extraction: use ultrasonic extraction 1h, and under 120 ℃ of conditions, water extracts radix bardanae powder 2h;
5) filter: the filtrate after radix bardanae powder extracting liquid filtering is concentrated, be concentrated to 1/7 of original volume;
6) add ethanol: concentrate is added to ethanol by a certain percentage, concentration of alcohol is reached more than 80%;
7) standing, centrifugal: after concentrate and ethanol mix, at 2 ℃, to leave standstill 15h, after centrifugal, filtration, precipitation, make the thick polysaccharide of burdock.
As optimal way of the present invention, in described step (4), hyperacoustic power is 350W, and extraction efficiency is high, and impurity is few.
As optimal way of the present invention, in described step (6), the volume ratio of concentrate and ethanol is 1:4, and productive rate is higher.
embodiment 2:
The cigarette preparation method that what the present embodiment provided contain the thick polysaccharide of burdock, processing step is as follows:
1) select materials, remove matter: select radix bardanae, remove impurity;
2) clean, cut into slices: by the radix bardanae clear water wash clean except after matter, and cut into slices;
3) pulverize: the sheet cutting in step (2) is put into refiner, smash, the ratio of smashing rear gained material and water is 1:30;
4) ultrasonic extraction: then use ultrasonic extraction 1.5h, and under 90 ℃ of conditions, water extracts radix bardanae powder, 1.5h;
5) filter: the filtrate after radix bardanae powder extracting liquid filtering is concentrated, be concentrated to 1/6 of original volume;
6) add ethanol: concentrate is added to ethanol by a certain percentage, concentration of alcohol is reached more than 80%;
7) standing, centrifugal: after concentrate and ethanol mix, at 4 ℃, to leave standstill 12h, after centrifugal, filtration, precipitation, make the thick polysaccharide of burdock.
As optimal way of the present invention, in described step (4), hyperacoustic power is 400W, and extraction efficiency is high, and impurity is few.
As optimal way of the present invention, in described step (6), the volume ratio of concentrate and ethanol is 1:4, and productive rate is higher.
embodiment 3:
The cigarette preparation method that what the present embodiment provided contain the thick polysaccharide of burdock, processing step is as follows:
1) select materials, remove matter: select radix bardanae, remove impurity;
2) clean, cut into slices: by the radix bardanae clear water wash clean except after matter, and cut into slices;
3) pulverize: the sheet cutting in step (2) is put into refiner, smash; The ratio of smashing rear gained material and water is 1:30;
4) ultrasonic extraction: use ultrasonic extraction 2h, and under 80 ℃ of conditions, water extracts radix bardanae powder 1h;
5) filter: the filtrate after radix bardanae powder extracting liquid filtering is concentrated, be concentrated to 1/5 of original volume;
6) add ethanol: concentrate is added to ethanol by a certain percentage, concentration of alcohol is reached more than 80%;
7) standing, centrifugal: after concentrate and ethanol mix, at 6 ℃, to leave standstill 9h, after centrifugal, filtration, precipitation, make the thick polysaccharide of burdock.
As optimal way of the present invention, in described step (4), hyperacoustic power is 450W, and extraction efficiency is high, and impurity is few.
As optimal way of the present invention, in described step (6), the volume ratio of concentrate and ethanol is 1:4, and productive rate is higher.
embodiment 4:
The thick polysaccharide of prepared embodiment 1～3 burdock is applied in tobacco, the consumption of the thick polysaccharide of burdock is 0.08% of pipe tobacco weight, after dissolving, clear water dilution makes cigarette feed liquid, and this cigarette is joined on cigarette shreds by feed liquid, cigarette mouthfeel is best, health care is fully played, and can reduce preferably cigarette harm to human body in sucking process.
As optimal way of the present invention, the feed liquid in described step (7) is added on pipe tobacco by spray pattern, can make feed liquid be penetrated into more uniformly in pipe tobacco, reduces the loss of the thick polysaccharide of burdock.
embodiment 5:
The thick polysaccharide of prepared embodiment 1～3 burdock is applied in tobacco, the consumption of the thick polysaccharide of described burdock is 0.12% of pipe tobacco weight, after dissolving, clear water dilution makes cigarette feed liquid, and this cigarette is joined on cigarette shreds by feed liquid, cigarette mouthfeel is best, health care is fully played, and can reduce preferably cigarette harm to human body in sucking process.
As optimal way of the present invention, the feed liquid in described step (7) is added on pipe tobacco by spray pattern, can make feed liquid be penetrated into more uniformly in pipe tobacco, reduces the loss of the thick polysaccharide of burdock.
embodiment 6:
The thick polysaccharide of prepared embodiment 1～3 burdock is applied in tobacco, the consumption of the thick polysaccharide of described burdock is 0.15% of pipe tobacco weight, after dissolving, clear water dilution makes cigarette feed liquid, and this cigarette is joined on cigarette shreds by feed liquid, cigarette mouthfeel is best, health care is fully played, and can reduce preferably cigarette harm to human body in sucking process.
As optimal way of the present invention, the feed liquid in described step (7) is added on pipe tobacco by spray pattern, can make feed liquid be penetrated into more uniformly in pipe tobacco, reduces the loss of the thick polysaccharide of burdock.
Burdock polysaccharide is applied on cigarette shreds by feed liquid as cigarette after water-soluble solution, and while burning and sucking cigarette, flue gas free from extraneous odour, can make cigarette flavor concentration increase, richness is better, and flue gas tendency is very fast, and micro-have sweet perfume (or spice), hamony is better, stimulates micro-reduction that has, and pleasant impression is more comfortable.
The present invention can improve the sucking quality of cigarette; Do not change original performance and the Cigarette processing technique of cigarette; There is certain humectation effect; Cost is not high, has practicality; Expanded the scope of application of agricultural byproducts simultaneously.
Claims (5)
1. an extracting method for the thick polysaccharide of burdock, is characterized in that, comprises following processing step:
1) select materials, remove matter: select radix bardanae, remove impurity;
2) clean, cut into slices: by the radix bardanae clear water wash clean except after matter, and cut into slices;
3) pulverize: the sheet cutting in step (2) is put into refiner, smash, the ratio of smashing rear gained material and water is 1:30;
4) ultrasonic extraction: with ultrasonic extraction 1h～2h, and under 80 ℃～120 ℃ conditions, water extracts radix bardanae powder 1h～2h;
5) filter: the filtrate after radix bardanae powder extracting liquid filtering is concentrated, be concentrated to 1/5～1/7 of original volume;
6) add ethanol: concentrate is added to ethanol by a certain percentage, concentration of alcohol is reached more than 80%;
7) standing, centrifugal: after concentrate and ethanol mix, at 2 ℃～6 ℃, more than standing 8h, after centrifugal, filtration, precipitation, to make the thick polysaccharide of burdock.
2. the extracting method of the thick polysaccharide of a kind of burdock according to claim 1, is characterized in that, in described step (4), hyperacoustic power is 300W～450W.
3. the extracting method of the thick polysaccharide of a kind of burdock according to claim 1, is characterized in that, in described step (6), the volume ratio of concentrate and ethanol is 1:4.
4. the thick polysaccharide of burdock as claimed in claim 1 application in tobacco, it is characterized in that, the consumption of the thick polysaccharide of described burdock is 0.08%～0.15% of pipe tobacco weight, makes cigarette feed liquid, and this cigarette is joined on cigarette shreds by feed liquid after clear water dilution is dissolved.
5. the application of the thick polysaccharide of a kind of burdock according to claim 4 in tobacco, is characterized in that, described cigarette adds on cigarette shreds by spray pattern by feed liquid.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410074836.6A CN103859578B (en) | 2014-03-04 | 2014-03-04 | The extracting method of the thick polysaccharide of a kind of burdock and the application in tobacco thereof |
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| CN201410074836.6A CN103859578B (en) | 2014-03-04 | 2014-03-04 | The extracting method of the thick polysaccharide of a kind of burdock and the application in tobacco thereof |
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| CN103859578A true CN103859578A (en) | 2014-06-18 |
| CN103859578B CN103859578B (en) | 2016-05-18 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107129541A (en) * | 2017-06-13 | 2017-09-05 | 博德生物技术（德州）有限公司 | A kind of preparation method and applications of burdock polysaccharide pyrogen |
| CN115010820A (en) * | 2021-09-24 | 2022-09-06 | 江苏省农业科学院 | Extraction and optimization method of burdock polysaccharide |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107129541A (en) * | 2017-06-13 | 2017-09-05 | 博德生物技术（德州）有限公司 | A kind of preparation method and applications of burdock polysaccharide pyrogen |
| CN115010820A (en) * | 2021-09-24 | 2022-09-06 | 江苏省农业科学院 | Extraction and optimization method of burdock polysaccharide |
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| CN103859578B (en) | 2016-05-18 |
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