CN105105316B - A kind of agilawood essential oil atomized liquid and preparation method thereof - Google Patents
A kind of agilawood essential oil atomized liquid and preparation method thereof Download PDFInfo
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- CN105105316B CN105105316B CN201510414917.0A CN201510414917A CN105105316B CN 105105316 B CN105105316 B CN 105105316B CN 201510414917 A CN201510414917 A CN 201510414917A CN 105105316 B CN105105316 B CN 105105316B
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Abstract
The invention provides a kind of agilawood essential oil atomized liquid, mainly it is made up of following raw material: in terms of mass fraction, agilawood essential oil 1 20 parts, natural botanical extraction liquid 60 90 parts, the component of wherein said agilawood essential oil includes that aromatic series compounds and sesquiterpenoids, the component of described natural botanical extraction liquid include N-acetyl-glucosamine, Aloe gel and Aloe polysaccharide.Preparation method comprises the steps: described agilawood essential oil and described natural botanical extraction liquid are sequentially added into mixing and stirring, to obtain final product.The agilawood essential oil atomized liquid of the embodiment of the present invention does not contains glycerol and propylene glycol, has health, health care, environmental protection and delicate mouthfeel uniqueness soft, mellow, elegant fragrance, noble effect.
Description
Technical field
The present invention relates to essential oil and make field, in particular to a kind of agilawood essential oil atomized liquid and preparation method thereof.
Background technology
Electronic cigarette liquid has another name called electronics ree-oil, is to cooperate with the electronic atomized liquid that electronic cigarette uses, is heated by electronic smoke atomizer, it is possible to produce the fog as medicated cigarette.Electronics ree-oil main component of the prior art is food grade or the other glycerol of pharmaceutical grade, propylene glycol, and Nicotiana tabacum L. essence special.Some electronics ree-oil also contains nicotine composition, primarily to its mouthfeel more presses close to medicated cigarette.Mainly using glycerol and propylene glycol as solvent, though bigger than the ree-oil using propylene glycol as solvent as the ree-oil amount of smoke of solvent with glycerol, taste is the sweetest, and mouthfeel is poor.
Additionally in addition to taste, the proportion (about 1.26) of glycerol is bigger than propylene glycol (about 1.04), and therefore the ree-oil of the pure glycerin of same capacity weighs about about 20% compared with the ree-oil of pure propylene glycol.In actual allocation process, glycerol and propylene glycol are to mix the solvent as ree-oil according to a certain percentage, the advantage that so can take into account two kinds of solvents, reach amount of smoke and effect that mouthfeel is taken into account, but both solvents likely can produce harmful object after atomizer for electric back warp crosses Pintsch process, harm human health, suck for a long time and can increase the weight of body burden, and taste is the sweetest greasy, cannot accomplish that the fragrance close to conventional cigarette is experienced, can not meet the demand of different crowd, affect user and sucking the sense of reality of electronic cigarette liquid.
In view of this, the special proposition present invention.
Summary of the invention
The first object of the present invention is to provide a kind of agilawood essential oil atomized liquid, described agilawood essential oil atomized liquid overcomes above-mentioned technical problem, it does not contains glycerol and propylene glycol, has the advantages such as health, health care, environmental protection and delicate mouthfeel uniqueness soft, mellow, elegant fragrance, noble quality.
The second object of the present invention is to provide the preparation method of a kind of described agilawood essential oil atomized liquid, and the method has making and is simple and convenient to operate and cost of manufacture is low, the advantage such as the active ingredient of each component in can completely retention of oil.
In order to realize the above-mentioned purpose of the present invention, spy by the following technical solutions:
Embodiments provide a kind of agilawood essential oil atomized liquid formula being formed by raw material and being defined, mainly prepared by following raw material: agilawood essential oil 1-20 part, natural botanical extraction liquid 60-90 part, the component of wherein said agilawood essential oil includes that aromatic series compounds and sesquiterpenoids, the component of described natural botanical extraction liquid include N-acetyl-glucosamine, Aloe gel and Aloe polysaccharide.
Electronic cigarette liquid of the prior art is during being prepared, will addition glycerol in various degree or propylene glycol as solvent to be used for carrying major part ree-oil local flavor, fog is produced when sucking, and have and make throat more happy to bring the effect of the pleasant sensation sucked, but the respiratory tract of human body can be formed after atomizer for electric high-temperature heating and stimulate by propylene glycol itself, there is the sensation of dizziness and nausea, also can produce harmful gas and affect health, but the zest of glycerol its taste less is the sweetest comparatively speaking, cannot accomplish that the fragrance close to conventional cigarette is experienced, can not meet the demand of different crowd, affect user and suck the sense of reality of electronic cigarette liquid.
In order to solve the technical problem appeared above, the invention provides one and make solvent without propylene glycol and glycerol, also the agilawood essential oil atomized liquid without nicotine composition is used for doing electronic cigarette liquid, its flue gas being possible not only to simulate conventional cigarette, there is no sweet soapy feeling, and equally make throat more happy to bring the pleasant sensation sucked, on the premise of its Experience Degree can compare favourably with conditional electronic tobacco juice, more healthy to human body, taste the most more delicate fragrance is soft.
It is on raw material composition and ratio, the consumption of agilawood essential oil is 1-20 part, the consumption of natural botanical extraction liquid is 60-90 part, owing to the price of agilawood essential oil itself is more expensive than gold, unsuitable excessive from its consumption of cost consideration, if the excessive mouthfeel of addition is the strongest, the very few mouthfeel of addition is the lightest, therefore suitably addition is necessary, the colorless and odorless of natural botanical extraction liquid own, do not interfere with the original taste of Lignum Aquilariae Resinatum edible vegetable oil, and well merge after atomizer for electric is atomized with agilawood essential oil, a large amount of smog can be produced, sweetless oiliness, absolutely not affect ree-oil mouthfeel, its consumption is also to find both can well merge with agilawood essential oil under this addition by great many of experiments, the highest Experience Degree can be brought again to smoker.
From the point of view of from source, agilawood essential oil and natural botanical extraction liquid both raw materials all can be by commercially available acquisitions, it is possible to be prepared voluntarily.In the component of the agilawood essential oil used by the present invention, great majority are aromatic series compounds and sesquiterpenoids, aromatic series compounds mainly has: in terms of mass fraction, 1-benzyloxy-8-naphthols 25-30 part, ditridecyl phthalate 13-18 part, 1,3-benzhydryl-5-fluorouracil 3-5 part, sesquiterpenoids mainly has: in terms of mass fraction, palustrol 1-2 part, furanoeremophilone 7-10 part, floss Virgin's milk mushroom aldehyde 1-3 part.The component of natural botanical extraction liquid then includes: in terms of mass fraction, N-acetyl-glucosamine 20-30 part, aloe gel 20:1-30 parts and Aloe polysaccharide 20-30 part, may also include that β-1,3 dextran 5-10 parts.
Because only that when with the agilawood essential oil containing composition described above and natural botanical extraction liquid as raw material, just can make the best results of the agilawood essential oil atomized liquid prepared, effect is the most comprehensive, and primary efficacy has: (1) agilawood essential oil atomized liquid has sleeping anti-strongly fragrant effect: stable emotion, anxiety of releiving cerebral nerve tired, make that body and mind is happy, improve sleep quality.Improve neurasthenia, pacify dormancy of relaxing, the calm effect of balance.(2) agilawood essential oil atomized liquid has effect that mediation is regulated the flow of vital energy: benefit is mended internal organs, run QI and blood.Help to eliminate brain tired, releive, recover balance of body and spirit, mild emotion.(3) have and protect effect of kidney nourishing the liver: help qi-blood circulating, help metabolism Liver and kidney toxin, strengthen immunocompetence.(4) have convergence life effect: anti-inflammation and sterilization, oiliness skin sore is had specially good effect, improve the dark and gloomy tarnish of skin, promote Hemapoiesis.(5) there is effect of flat fat anti-acne: anti-inflammation and sterilization, convergence life, repair, encourage thin breast tissue regeneration function, decompose, desalinate dermal melanin.(6) there is effect with breathless interest: decompression is loosened, help enhancing activating brain cell vigor, promote memory, attention.Health is highly profitable by the agilawood essential oil atomized liquid of the present invention, has multiple health care, has overturned and it is believed that and suck the idea that electronic cigarette liquid is bound to be hazardous to the human body.
Additionally, the electronic atomized liquid of Lignum Aquilariae Resinatum of the present invention is in addition to can using as electronics ree-oil, the most important, agilawood essential oil atomized liquid is added and on censer, may also act as champignon use, its smog distributed and fragrance, capable of purifying air, reduce pathogen transmission, fragrance breath stimulates olfactory nerves, makes people's body and mind releive, plays the health preserving effect of its uniqueness.Also can use as vehicle-mounted perfume, purposes is widely.
In order to obtain the effect of Synergistic, after the proportioning raw materials of the agilawood essential oil atomized liquid of the present invention optimizes further, agilawood essential oil is 5-10 part, and natural botanical extraction liquid is 70-80 part.Optimum consumption proportion is, agilawood essential oil 7 parts, natural botanical extraction liquid 78 parts.
The present invention, except providing the formula of a kind of agilawood essential oil atomized liquid, additionally provides the preparation method of a kind of agilawood essential oil atomized liquid, comprises the steps:
Described agilawood essential oil and described natural botanical extraction liquid are sequentially added into mixing and stirring, to obtain final product.
The preparation method of the agilawood essential oil atomized liquid of the present invention is simple, easy to operate, it is possible to the complete effective ingredient retained in raw material components is not corrupted such that two kinds of raw materials merge the most completely.And the order adding raw material when mixing requires, it is initially charged agilawood essential oil and adds natural extract liquid, after because if, addition agilawood essential oil is likely to cause quintessence oil and floats over the surface of extracting solution, both cannot be made preferably to merge, it is simultaneously introduced equally and also can have problems that existence, therefore order of addition is to have certain restriction, needs great care.
Further, the stir speed (S.S.) of mix and blend is preferably controlled in 200-300rad/min, because the too fast effective ingredient that can destroy raw material of stir speed (S.S.), so that affecting the effect of product, the time also having mix and blend is preferably controlled between 30-60min and can realize allowing two kinds of raw materials well merge, it is also possible to value is 40min, 50min and 55min etc., and whipping temp should not be the highest, in case raw material can volatilization loss fall, control between 20-30 DEG C.
Finally, described agilawood essential oil atomized liquid also includes following post-processing step: filtration, ultraviolet sterilization and the step of subpackage, filtering can be to filter out impurity in the way of taking filtered through gauze, in order to reinforced effects may be used without the filter type of other higher levels.Ultraviolet sterilization can be prevented effectively from the infection of miscellaneous bacteria, it is ensured that the healthy and safe property of product, just can pack and sell after sterilization.
Compared with prior art, the invention have the benefit that
(1) in the agilawood essential oil atomized liquid raw material of the embodiment of the present invention, abandon tradition and prepare the raw material used by electronics ree-oil, creative coordinates agilawood essential oil with natural botanical extraction liquid, make the agilawood essential oil atomized liquid obtained in addition to all advantages having conditional electronic tobacco juice, and it is more healthy, soft aroma and do not have sweet soapy feeling, also has certain health-care effect；
(2) health-care effect of the agilawood essential oil atomized liquid of the embodiment of the present invention mainly has: sleeping anti-strongly fragrant effect: stable emotion, anxiety of releiving cerebral nerve tired, make that body and mind is happy, improve sleep quality.Improve neurasthenia, pacify dormancy of relaxing, the calm effect of balance；There is effect that mediation is regulated the flow of vital energy: benefit is mended internal organs, run QI and blood.Help to eliminate brain tired, releive, recover balance of body and spirit, the effect of mild emotion；There is the effect protecting kidney nourishing the liver: help qi-blood circulating, help metabolism Liver and kidney toxin, enhancing immunocompetence；Have convergence life effect: anti-inflammation and sterilization, oiliness skin sore is had specially good effect, improve the dark and gloomy tarnish of skin, promote Hemapoiesis；There is effect of flat fat anti-acne: anti-inflammation and sterilization, convergence life, repair, encourage thin breast tissue regeneration function, decompose, desalinate dermal melanin；There is effect with breathless interest: decompression is loosened, help enhancing activating brain cell vigor, promote memory, attention；
(3) proportioning that the present invention is prepared between component and the component of each of agilawood essential oil atomized liquid raw material also has specific requirement, visible selecting on raw material so that product is better, inventor has also paid substantial amounts of creative work, compared to the most common agilawood essential oil, after the composition of agilawood essential oil is detected and tested, find that the agilawood essential oil atomized liquid that the agilawood essential oil being mainly composition using aromatic series compounds and sesquiterpenoids is made as raw material is better；
(4) preparation method of the agilawood essential oil atomized liquid of the present invention is simple and convenient to operate, the effective ingredient that can be good at retaining in raw material is not destroyed, each technological parameter is all to be drawn by substantial amounts of optimization experiment final optimization pass, to improve the leaching rate of effective ingredient in raw material, and the utilization rate improving raw material is target so that the product prepared is the most all good from mouthfeel to abnormal smells from the patient.
Detailed description of the invention
Below in conjunction with embodiment, embodiment of the present invention are described in detail, it will be appreciated by those skilled in the art that the following example is merely to illustrate the present invention, and are not construed as limiting the scope of the present invention.Unreceipted actual conditions person in embodiment, the condition advised according to normal condition or manufacturer is carried out.Agents useful for same or instrument unreceipted production firm person, being can be by the commercially available conventional products bought and obtain.
Embodiment 1
The raw material composition of agilawood essential oil atomized liquid is as follows:
Agilawood essential oil 1kg
Natural botanical extraction liquid 60kg
Wherein, the component of agilawood essential oil includes aromatic series compounds and sesquiterpenoids, and the component of natural botanical extraction liquid includes N-acetyl-glucosamine, Aloe gel and Aloe polysaccharide；
The preparation method of agilawood essential oil atomized liquid is as follows:
Above-mentioned raw materials agilawood essential oil and natural botanical extraction liquid are added in glass capsulation container successively, it is thoroughly mixed uniformly, stir speed (S.S.) controls at 200rad/min, use filtered through gauze impurity the most at ambient temperature, the process filtered is veryer long but is intended to accurate operation fully to filter, last ultraviolet sterilization, is distributed into fractional pack.
Embodiment 2
The raw material composition of agilawood essential oil atomized liquid is as follows:
Agilawood essential oil 20kg
Natural botanical extraction liquid 90kg
Wherein, by percentage to the quality, the key component of agilawood essential oil is: 1-benzyloxy-8-naphthols 25%, ditridecyl phthalate 13%, 1,3-benzhydryl-5-fluorouracil 3%, palustrol 1%, furanoeremophilone 7%, remaining component is mostly aromatic series compounds and sesquiterpenoids, the most specifically detects, and the component of natural botanical extraction liquid includes N-acetyl-glucosamine 20%, aloe gel 20:1 % and Aloe polysaccharide 20%, remaining component does not detects；
The preparation method of agilawood essential oil atomized liquid is as follows:
Above-mentioned raw materials agilawood essential oil and natural botanical extraction liquid are added in glass capsulation container successively, it is thoroughly mixed uniformly, stir speed (S.S.) controls at 300rad/min, the time of mix and blend is 30min, whipping temp controls at 20 DEG C, and the most at ambient temperature with four layers of filtered through gauze impurity, the process of filtration is veryer long but is intended to accurate operation fully to filter, last ultraviolet sterilization under the conditions of 20-30 DEG C, is distributed into fractional pack and can form sale.
Embodiment 3
The raw material composition of agilawood essential oil atomized liquid is as follows:
Agilawood essential oil 5kg
Natural botanical extraction liquid 70kg
Wherein, by percentage to the quality, the key component of agilawood essential oil is: 1-benzyloxy-8-naphthols 30%, ditridecyl phthalate 18%, 1,3-benzhydryl-5-fluorouracil 5%, palustrol 2%, furanoeremophilone 10%, floss Virgin's milk mushroom aldehyde 1%, remaining component is mostly aromatic series compounds and sesquiterpenoids the most specifically detects, the component of natural botanical extraction liquid includes N-acetyl-glucosamine 30%, Aloe gel 30% and Aloe polysaccharide 30%, β-1,3 dextrans 5%, remaining component does not detects；
The preparation method of agilawood essential oil atomized liquid is as follows:
Above-mentioned raw materials agilawood essential oil and natural botanical extraction liquid are added in glass capsulation container successively, it is thoroughly mixed uniformly, stir speed (S.S.) controls at 250rad/min, the time of mix and blend is 60min, whipping temp controls at 30 DEG C, and the most at ambient temperature with four layers of filtered through gauze impurity, the process of filtration is veryer long but is intended to accurate operation fully to filter, last ultraviolet sterilization under the conditions of 20-30 DEG C, is distributed into fractional pack and can form sale.
Embodiment 4
The raw material composition of agilawood essential oil atomized liquid is as follows:
Agilawood essential oil 10kg
Natural botanical extraction liquid 80kg
Wherein, by percentage to the quality, the key component of agilawood essential oil is: 1-benzyloxy-8-naphthols 25%, ditridecyl phthalate 13%, 1,3-benzhydryl-5-fluorouracil 3%, palustrol 1%, furanoeremophilone 7%, floss Virgin's milk mushroom aldehyde 3%, remaining component is mostly aromatic series compounds and sesquiterpenoids the most specifically detects, the component of natural botanical extraction liquid includes N-acetyl-glucosamine 25%, Aloe gel 25% and Aloe polysaccharide 25%, β-1,3 dextrans 10%, remaining component does not detects；
The preparation method of agilawood essential oil atomized liquid is as follows:
Above-mentioned raw materials agilawood essential oil and natural botanical extraction liquid are added in glass capsulation container successively, it is thoroughly mixed uniformly, stir speed (S.S.) controls at 300rad/min, the time of mix and blend is 30min, whipping temp controls at 20 DEG C, and the most at ambient temperature with four layers of filtered through gauze impurity, the process of filtration is veryer long but is intended to accurate operation fully to filter, last ultraviolet sterilization under the conditions of 20-30 DEG C, is distributed into fractional pack and can form sale.
Embodiment 5
The raw material composition of agilawood essential oil atomized liquid is as follows:
Agilawood essential oil 7kg
Natural botanical extraction liquid 78kg
Wherein, by percentage to the quality, the key component of agilawood essential oil is: 1-benzyloxy-8-naphthols 28%, ditridecyl phthalate 17%, 1,3-benzhydryl-5-fluorouracil 4%, palustrol 1.5%, furanoeremophilone 9%, floss Virgin's milk mushroom aldehyde 2%, remaining component is mostly aromatic series compounds and sesquiterpenoids the most specifically detects, the component of natural botanical extraction liquid includes N-acetyl-glucosamine 25%, Aloe gel 25% and Aloe polysaccharide 25%, β-1,3 dextrans 8%, remaining component does not detects；
The preparation method of agilawood essential oil atomized liquid is as follows:
Above-mentioned raw materials agilawood essential oil and natural botanical extraction liquid are added in glass capsulation container successively, it is thoroughly mixed uniformly, stir speed (S.S.) controls at 300rad/min, the time of mix and blend is 50min, whipping temp controls at 25 DEG C, and the most at ambient temperature with four layers of filtered through gauze impurity, the process of filtration is veryer long but is intended to accurate operation fully to filter, last ultraviolet sterilization under the conditions of 20-30 DEG C, is distributed into fractional pack and can form sale.
Experimental example 1
The electronic cigarette liquid (comparative example 1) that agilawood essential oil atomized liquid embodiment of the present invention 1-5 prepared and the embodiment 1 in Application No. 201110184068.6 patent are prepared does tests as follows:
Invite 300 people the most at random, it is equally divided into 6 groups to try out, first group everyone provides the agilawood essential oil atomized liquid that embodiment 1 is prepared, second group everyone provides the agilawood essential oil atomized liquid that embodiment 2 is prepared, 3rd group everyone provides the agilawood essential oil atomized liquid that embodiment 3 is prepared, 4th group everyone provides the agilawood essential oil atomized liquid that embodiment 4 is prepared, 5th group everyone provides the agilawood essential oil atomized liquid that embodiment 5 is prepared, 6th group everyone provides the electronic cigarette liquid that comparative example 1 is prepared, after every tester is by sucking it with electronic cigarette, and result is investigated, survey result such as following table:
The trial state application form of table 1 product
As can be seen from Table 1; the electronic cigarette liquid taste mellow that the embodiment of the present invention is prepared; without sweet soapy feeling; from abnormal smells from the patient to mouthfeel truer; it is as good as with conventional cigarette; can fully meet consumer's dependence to conventional cigarette, the requirement still further aspect on the one hand meeting consumer also protects the health of human body, kills two birds with one stone.And be tracked investigating to smoker by follow-up, after sucking the agilawood essential oil atomized liquid of the embodiment of the present invention, people generally react sensation spirit and QI cleaning, work, the most more have vigour, vigorous, sleep quality also significantly improves, just because of the agilawood essential oil atomized liquid of the present invention uses safety, without nicotine, produce without nuisance under high-temperature condition, still there is health-care effect, entirely different with the composition of conventional cigarette, overturn people's understanding in the past to medicated cigarette, can be as from the point of view of health food.
Although illustrate and describing the present invention with specific embodiment, however it will be appreciated that may be made that without departing from the spirit and scope of the present invention many other change and amendment.It is, therefore, intended that include all such changes and modifications belonging in the scope of the invention in the following claims.
Claims (9)
1. an agilawood essential oil atomized liquid, it is characterised in that be mainly made up of following raw material:
In terms of mass fraction, agilawood essential oil 1-20 part, natural botanical extraction liquid 60-90 part, wherein
The component of described agilawood essential oil includes aromatic series compounds and sesquiterpenoids, described
The component of natural botanical extraction liquid includes that N-acetyl-glucosamine, Aloe gel and Aloe are many
Sugar；
Wherein, in the component of described agilawood essential oil, aromatic series compounds mainly has following several
Any one or a few combination in component: in terms of mass fraction, 1-benzyloxy-8-naphthols
25-30 part, ditridecyl phthalate 13-18 part, 1,3-benzhydryl-5-fluorouracil 3-5
Part.
A kind of agilawood essential oil atomized liquid the most according to claim 1, it is characterised in that
Described raw material includes: in terms of mass fraction, agilawood essential oil 5-10 part, natural botanical extraction liquid
70-80 part.
3. according to a kind of agilawood essential oil atomized liquid described in any one of claim 1-2, its feature
Being, described raw material includes: in terms of mass fraction, agilawood essential oil 7 parts, extracted form natural plant
Liquid 78 parts.
Agilawood essential oil atomized liquid the most according to claim 1, it is characterised in that described
In the component of agilawood essential oil, it is any one that sesquiterpenoids mainly has in following several component
Kind or several combinations: in terms of mass fraction, palustrol 1-2 part, furanoeremophilone 7-10
Part, floss Virgin's milk mushroom aldehyde 1-3 part.
Agilawood essential oil atomized liquid the most according to claim 1, it is characterised in that described
The component of natural botanical extraction liquid includes: in terms of mass fraction, N-acetyl-glucosamine 20-30
Part, aloe gel 20:1-30 parts and Aloe polysaccharide 20-30 part.
Agilawood essential oil atomized liquid the most according to claim 5, it is characterised in that described
The component of natural botanical extraction liquid also includes: β-1,3 dextran 5-10 part.
7. the preparation method of the agilawood essential oil atomized liquid described in any one of claim 1-6, it is special
Levy and be, comprise the steps:
Described agilawood essential oil and described natural botanical extraction liquid are sequentially added into mixing and stirring,
Obtain.
The preparation method of agilawood essential oil atomized liquid the most according to claim 7, its feature
Being, the stir speed (S.S.) of mix and blend controls at 200-300rad/min.
The preparation method of agilawood essential oil atomized liquid the most according to claim 7, its feature
Being, the time of mix and blend is 30-60min, and whipping temp controls between 20-30 DEG C.
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| CN106833899A (en) * | 2017-02-07 | 2017-06-13 | 珠海市玖鑫化妆品有限公司 | The preparation technology and essential oil Deacne pack of a kind of linaloe oil |
| CN107216950A (en) * | 2017-07-29 | 2017-09-29 | 郑永如璧 | Agilawood spray and agilawood tobacco tar preparation method |
| CN114404541A (en) * | 2022-01-28 | 2022-04-29 | 雾化大健康产业集团(海南)有限公司 | Herbal plant atomized essential oil helpful for guiding qi downward and smoothing and preparation method thereof |
| CN114642702A (en) * | 2022-04-19 | 2022-06-21 | 大连金石斛生物技术有限公司 | Agilawood atomized liquid and preparation method thereof |
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| ITMI20112290A1 (en) * | 2011-12-16 | 2013-06-17 | Dks Aromatic Srl | COMPOSITION FOR ELECTRONIC CIGARETTES |
| CN103271853A (en) * | 2013-05-17 | 2013-09-04 | 西藏圣香海螺民族产品开发有限公司 | Tibetan perfume with rose fragrance and preparation method thereof |
| CN103520435B (en) * | 2013-10-11 | 2015-06-17 | 中山市国林沉香科学研究所 | Agilawood health care essential oil |
| CN103519352A (en) * | 2013-11-07 | 2014-01-22 | 袁恩泽 | Electronic cigarette |
| CN104026731B (en) * | 2014-07-01 | 2016-03-02 | 安徽中烟工业有限责任公司 | A kind of mental-tranquilization functional electronic cigarette tobacco juice |
| CN104585864B (en) * | 2015-01-20 | 2016-05-25 | 川渝中烟工业有限责任公司 | A kind of tobacco juice for electronic smoke containing Fructus Hippophae polysaccharide |
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