A kind of multi-functional environment-protection infant wet tissue and preparation method thereof
Technical field
The present invention relates to a kind of wet tissue, particularly to a kind of multi-functional environment-protection infant wet tissue and preparation method thereof.
Background technology
Now infant wet tissue development prospect in the market is become better and better, and infant autologous skin is tender and lovely, and antibacterial ability is poor,
And defecation is more frequent, processing with great difficulty does not make hip rubescent, so inventing the multifunctional safety that a kind of infant is easy to use
Wet tissue just seem important.In the wet tissue for baby that existing market is sold, most of use is all spun-laced nonwoven fabric, this material
Expect it is more difficult to degrade for medicated napkin, and the single function of most of wet tissue, emphasis is substantially all in sterilization and peace
Quan Shang, so present invention aim at carrying out soaking mixing in joined wet tissue liquid using senior moisture-proof medicated napkin, produce one
Plant collection cleaning-sterilizing, mosquito-repellent antipruritic, preserving moisture and protecting skin, the multi-functional ring moist-retaining tissues of fresh scent.
Content of the invention
1st technical problem to be solved by this invention be provide a kind of new multi-functional containing natural component extract
Environmental protection infant wet tissue.
2nd technical problem to be solved by this invention is the preparation method of above-mentioned multi-functional environment-protection infant wet tissue.
The problem that the present invention solves is a kind of multi-functional environment-protection infant wet tissue, including senior moisture-proof medicated napkin and wet tissue
Liquid, described wet tissue liquid comprises the following raw materials by weight percent:
Deionized water 80-85%, preservative 0.05-0.1%, chamomile essential oil 1-3%, Folium Perillae extracting solution 1-2%, poly- six
Methylene guanidine 0.9-1.2%, Folium Artemisiae Argyi extract 1-3%, dehydrated alcohol 0.5-1%, xylitol 1-2%, lavandula angustifolia extracting solution
1.5-3%, Flos Pelargonii extracting solution 1-2%, Mentholum 0.05-0.1%, Oleum Eucalypti 0.5-1%, olive extract 1-4%, vitamin
E 0.5-1%, Aloe extract 1-4%, glycerol 1-1.5%.
Described Folium Perillae extracting solution is prepared by the following method:
Weigh Folium Perillae appropriate, put in round-bottomed flask, and add 15-20 times amount 80% ethanol solution, soak 0.5-
1.0h, then be positioned in electric jacket, reflux, extract, 1.5-2.5h, the 2nd time plus 10-15 times amount 80% ethanol solution, extract 1.0-
2.0h, the 3rd time plus 5-10 times amount 80% ethanol solution, extract 0.5-1.5h, filter every time, merging filtrate, finally by filtrate
Volume concentration, to 3-5 times of Folium Artemisiae Argyi weight, filters, obtains Folium Perillae extracting solution, standby.
Described Folium Artemisiae Argyi extract is prepared by the following method:
Weigh dry Folium Artemisiae Argyi appropriate, put in round-bottomed flask, and add 20-25 times amount 80% ethanol solution, soak
0.5-1.0h, then be positioned in electric jacket, reflux, extract, 2.0-3.0h, the 2nd time plus 15-20 times amount 80% ethanol solution, extract
1.5-2.5h, the 3rd time plus 10-15 times amount 80% ethanol solution, extract 1.0-2.0h, filter every time, merging filtrate, finally will filter
To 2-4 times of Folium Artemisiae Argyi weight, concentrated solution is dried under vacuum to solid constant weight through 80-100 DEG C to the volume concentration of liquid, obtains Folium Artemisiae Argyi and extracts
Thing.
Described Flos Pelargonii extracting solution is prepared by the following method:
Weigh Flos Pelargonii appropriate, put in round-bottomed flask, and add 18-23 times amount water, soak 0.5-1.0h, then place
In electric jacket, reflux, extract, 2.0-3.0h, the 2nd time plus 13-18 times amount water, extract 1.5-2.0h, the 3rd time plus 8-13 times amount
Water, extracts 0.5-1.5h, filters every time, merging filtrate, finally by 2-5 times of the volume concentration of filtrate to Flos Pelargonii weight, mistake
Filter, stand-by.
Described lavandula angustifolia extracting solution is prepared by the following method:
Weigh lavandula angustifolia appropriate, put in round-bottomed flask, and add 17-20 times amount water, soak 0.5-1.0h, then place
In electric jacket, reflux, extract, 1.5-2.5h, the 2nd time plus 11-17 times amount water, extract 1.0-2.0h, the 3rd time plus 6-11 times amount
Water, extracts 0.5-1.5h, filters every time, merging filtrate, finally by 2-4 times of the volume concentration of filtrate to lavandula angustifolia weight, mistake
Filter, stand-by.
Described olive extract is prepared by the following method:
Weigh Fructus Canarii albi appropriate, grounds travel is broken into coarse powder, puts in round-bottomed flask, add 20-30 times amount 80% ethanol molten
Immersion steeps 0.2-0.5h, then is positioned in electric jacket, reflux, extract, 1.5-2.5h, adds 10-20 times amount 80% ethanol the 2nd time molten
Liquid, extracts 1.0-1.5h, the 3rd time plus 10-15 times amount 80% ethanol solution, extracts 0.5-1h, filters every time, merging filtrate,
Afterwards by 3-5 times of the volume concentration of filtrate to Fructus Canarii albi weight, filter, stand-by.
Described Aloe extract is prepared by the following method:
Weigh fresh aloe appropriate, clean, remove blade two edges ratchet, cut base portion and top, with rub with the hands melon plate by its
It is twisted into filament, puts in round-bottomed flask, and add 15-20 times amount 80% ethanol solution, soak 0.5-1.0h, then be positioned over electricity
In hot jacket, reflux, extract, 3.0-4.0h, the 2nd time plus 10-15 times amount 80% ethanol solution, extract 2.0-3.0h, add 8-12 the 3rd time
Times amount 80% ethanol solution, extracts 1.0-2.0h, filters every time, merging filtrate, finally by the volume concentration of filtrate to Aloe weight
3-6 times of amount, concentrated solution is dried under vacuum to solid constant weight through 80-100 DEG C, obtains Aloe extract.
Folium Perillae extracting solution described above, Folium Artemisiae Argyi extract, Flos Pelargonii extracting solution, olive extract, Aloe extract, smoke clothing
In the preparation of careless extracting solution, each amount of water or alcohol adding amount are the multiple of each raw material material weight, 80% ethanol of the present invention
Solution is for volume ratio.
Described preservative is selected from one of potassium sorbate, sorbic acid, sodium benzoate, benzoic acid or multiple.
A kind of multi-functional environment-protection infant wet tissue, its preparation method comprises the following steps:
(1) senior moisture-proof medicated napkin is put in 100-150 DEG C of baking oven and takes out after baking 10-15min, launch tiling,
Stand-by;
(2) by deionized water, preservative, xylitol, glycerol, olive extract, polyhexamethylene guanidine is mixed in proportion all
Even, stirring heating in water bath, to 90-100 DEG C, is incubated 25-30 minute;
(3) 45-50 DEG C of Temperature fall, by lavandula angustifolia extracting solution, Flos Pelargonii extracting solution, chamomile essential oil, Folium Perillae extracting solution
Sequentially add in proportion, be uniformly mixed, be incubated 5 minutes;
(4) Aloe extract, Folium Artemisiae Argyi extract, Mentholum are sequentially added at a temperature of step (3) in proportion, stirring is all
Even;
(5) naturally cool to 10-20 DEG C, add dehydrated alcohol, Oleum Eucalypti and vitamin e, be uniformly mixed;
(6) solution of step (5) gained is filtered, obtain wet tissue liquid, senior moisture-proof medicated napkin is completely soaked configuration
In good wet tissue liquid, soak 5-10 minute, take out, prepared moisture paper tissue papers;
(7) subpackage is carried out to soaked moisture paper tissue papers using wet towel package machine, packing specification is a piece of for every bag.
Various composition in the present invention is as follows:
Deionized water is exactly that water is passed through cation exchange resin (conventional for styrene type strongly acidic cation exchange tree
Fat), then the cation in water is absorbed by resin, the cations h on resin+Be displaced in water, and and water in cation
Form corresponding mineral acid;Water containing this kind of mineral acid passes through anion exchange resin again (conventional for styrene type strong basicity
Anion) oh-Be displaced in water, and and water in h+It is combined into water, as deionized water.Due to the ion in deionized water
Number can by artificial control, thus, make its resistivity, dissolubility, corrosivity, the physics such as virus and bacteria, chemistry and pathology
All obtain good control etc. index.
Folium Perillae is also named that osmanthus is weak, common perilla, red Soviet Union etc., gas delicate fragrance, taste micro-pungent.It is nutritious, containing protein, fat, can
Dissolubility sugar, dietary fiber, carotene, vitamin e, vitamin b1, vitamin b2, vitamin c, potassium, calcium, phosphorus, ferrum, manganese and selenium
Deng composition;Additionally, Folium Perillae contains volatile oil, wherein predominantly perillaldehyde is perilla alcohol, menthone, menthol, eugenol, white
Soviet Union's ketenes, left-handed limonene and a little australene etc., have special fragrance, have antisepsises.Folium Perillae have induce sweat, cold expelling, reason
Gas and effect of battalion.Folium Perillae is planted because of its distinctive active substance and nutritional labeling, the multipurpose becoming a kind of extremely World Focusing
Thing, economic worth is very high.Ming Dynasty's Li Shizhen once recorded " have leaf when Folium Perillae is tender, and vegetable eat it, or salt and greengage bittern to make the marshland full of water weeds maximum phase of an eclipse fragrant,
Xia Yue makees ripe soup and drinks it ".
Lavandula angustifolia is just widely used in medically from ancient times, and stem and Ye Douke are used as medicine, and has the effect of stomach invigorating, diaphoresis, pain relieving, is
Treatment Common Cold, stomachache, the good medicine of eczema.There are refreshment, hypermnesis;Alleviate nerve, contribute to one's peace of mind of inner tranquility;Promote blood
Circulation, can treat comedo, nourish healthy hair;Sensitive asthma of suppression hypertension, nose etc.;Adjust physiological function;Enhancing immunity;Dimension
Hold respiratory tract function;Can preventing viral, infectious disease;Go to eliminate the unusual smell, purify air;Except ant, remove the effects such as roach, acaricide.
Glycerol is most common most popular moisturizing ingredient, has functions that moisturizing, Glycerin, and horny layer can be made to maintain water
Conjunction state.After it is combined with hyaluronic acid, more the water holding capacity of hyaluronic acid can be risen to best and perfect.Its moisturizing effect
Very good, with rear skin water profit, softness, touch up very comfortable, good to cutaneous safety, it is difficult to cause allergy.
Flos Pelargonii, another name fish pelargonium, fish pelargonium flower, Geranium, day rotten red, foreign certain herbaceous plants with big flowers, Mozzie buster, foreign butterfly;Strong synthesis
The compound taste of sweet taste, Flos Rosae Rugosae and Herba Menthae.Primary efficacy has pain relieving, antibacterial, puts in and knit scar, strengthen cytophylaxises function, deodorization, stop
Blood, benefit body;It is suitable for all skins, have deep layer to purify and convergence effect, balance sebum secretion;Promote Skin Cell newborn, repair
Cicatrix, striae gravidarum etc..
Folium Artemisiae Argyi, another name Radix Artemisia ordosicae, family Chinese mugwort;Matter is soft;Gas delicate fragrance, nature and flavor are bitter, pungent, warm, enter spleen, liver and kidney channel.There is warming the meridian stop
Blood, dispersing cold for relieving pain;Effect of external removing dampness to relieve itching.Folium Artemisiae Argyi also has antibacterial and antivirus action;Relieving asthma, antitussive and eliminating the phlegm are made
With;Hemostasis and blood coagulation resisting function;Calmness and anti-allergic effects;Hepatoprotective choleretic effect etc..
Aloe is Liliaceae perennial evergreen, fleshiness herbaceous plant, and stem is shorter;Nature and flavor: bitter, tremble with fear.It is to collect edible, medicine
With, improve looks, view and admire plant nova;It is secreted thing (principle active component is the Herba Alii fistulosi quinones substance such as aloin) and extensively answers
Use in medicine and daily use chemicals.Aloe contains 75 kinds of elements, almost fits like a glove with human body cell desired substance, has obvious guarantor
Strong value, by people flourish referred to as " magical plant ", " first-aid kit for domestic use ".Aloe folks of china just by as beauty treatment, take care of hair and control
Treat the natural drug of dermatosis.Record according to " book on Chinese herbal medicine is new again " " control liver-fire, town liver-wind, clear away heart-fire heat, relaxing vexation is slaked thirst and help produce saliva, clever
Ear improving eyesight, the tooth that disappears swells, and solves fire-toxin.”
Fructus Canarii albi sweet in the mouth acid, mild-natured, people's spleen, stomach, lung meridian, have heat-clearing and toxic substances removing, sore-throat relieving resolving sputum, promoting the production of body fluid to quench thirst, relieving restlessness relieving alcoholic intoxication it
Work(is it is adaptable to laryngopharynx swelling and pain, excessive thirst, cough expectorant blood etc.." Japan hanako materia medica " says its " appetizing, the therapeutic method to keep the adverse QI flowing downwards, antidiarrheal ".Compendium of Material Medica
Say its " born fluid, only excessive thirst, control throat pain, chew pharynx juice, can solve all ichthyophagy crab poison "." the southern regions of the Yunnan Province book on Chinese herbal medicine " says that it " controls all larynxs
Scorching, epidemic infection with swollen head disease on fire, can solve damp and hot, spring-warm syndrome, promoting the production of body fluid to quench thirst, sharp expectorant, solve ichthyotoxin, wine, stagnate ".Fructus Canarii albi is nutritious, sarcocarp
The mineral such as inner protein, carbohydrate, fat, vitamin c and calcium, phosphorus, ferrum, the content of wherein vitamin c is Herba Marsileae Quadrifoliae
10 times of fruit, pears, 5 times of Fructus Persicae, calcium content is also very high, and is easily absorbed by the body, and is especially suitable to women, child eats.Winter-spring season,
Chew two or three piece of fresh olive of food daily, upper respiratory tract infection can be prevented, therefore the reputation having " Radix Ginseng matched by Winter-Spring Fructus Canarii albi " among the people.Grind both at home and abroad
Study carefully data and show also to contain escoparone in olive fruits, scopoletin, (e) -3,3- dihydroxy -4,4- dimethoxystilbene,
Gallic acid, benzoaric acid, brevifolin, hyperin and some triterpenoid compound, volatile oil, flavonoid
Thing.
Mentholum calls Mentholum, by a kind of cyclic alcohol of the saturation extracted in the leaf of Herba Menthae and stem, acrid in the mouth, and cool in nature;
For colourless needles or prism-shaped crystallization or white crystalline powder;There is the special begging gas of Herba Menthae.Mentholum can be used as toothpaste, perfume (or spice)
The odorant of water, beverage and confection etc.;Pharmaceutically it is being used as excitantss, acting on skin or mucosa, have refrigerant itching-relieving action;Interior
Clothes can be as carminative, for headache and nose;Pharynx;Laryngitis etc..
Oleum Eucalypti is that myrtle Eucalyptus globulus Labill, canella Camphor tree or above-mentioned two sections belong to other plant together and obtain through vapor distillation
The volatile oil arriving.For colourless or yellowish supernatant liquid;Have a special aroma, micro- like Camphora, acrid in the mouth, cool.Primary efficacy
For wind-expelling pain-stopping, for skin pruritus, neuralgia.
Xylitol is a kind of sweet substance with nutritive value, is also the normal intermediate of human body carbohydate metabolism.Certainly
So in boundary, xylitol is widely present in various water fruits and vegetables, but content is very low.Xylitol white crystal, appearance and sucrose phase
Seemingly, it is the sweetest sweeting agent in polyhydric alcohol, taste is cool, sugariness is equivalent to sucrose, heat is equivalent to glucose.It is following sweet taste
Agent, is sucrose and Fructus Vitis viniferae sugar substitute.Xylitol also has following functions: is used as sweeting agent, the supplementary of diabetes patient
And auxiliary therapeutical agent;Liver function can be improved;Anti-caries;Can fat-reducing;Biological stability is good etc..
Polyhexamethylene guanidine is polyguanidine family macromolecule polymer, is environment-friendly type macromolecule polymer disinfection sanitizer.Have
Broad-spectrum;Valid density is low;Work fast;Stable in properties;Premium properties soluble in water;Can use at normal temperatures;Long
Phase is antibacterial, have no side effect;Non-corrosiveness;Colourless, odorless;Nontoxic;Do not fire, not quick-fried, use safety;Moderate;Convenient transportation,
Can be described as optimal antibacterial.It is true that this product is a kind of environment-friendly multipurpose new polymerss, in industry, agricultural, doctor
With with daily life in have extremely extensive purposes.
Preservative refers to naturally occurring or synthetic chemical composition, for adding food, medicine, pigment, biological sample etc., to prolong
The corruption that late growth of microorganism or chemical change cause.Preservative Main Function is growth and the breeding of suppression microorganism, to prolong
The holding time of long food, the corrupt medicament of inhibiting substances.
Chamomile essential oil is distilled from flower, and soothing effect is excellent, can alleviate anxiety, anxiety, indignation and fear, make one to loosen
There is patience, feel happy and auspicious;Mitigate worried, helpful to having a sleepless night;Also can make calm, relax, smooth clearly respiratory system, can repair
Shield sensitivity, the skin of redness, eczema, pimples;Ant insect bite can be treated;Can releive headache, gastritis, diarrhoea, with myalgia, warp
Bitterly, toothache etc., also has good effectiveness for liver, anemia and immune system problem.
Vitamin e, also known as vitamin e (vitamin e), is a kind of fatsoluble vitamin, and its hydrolyzate is tocopherol,
It is one of topmost antioxidant.
The wet tissue liquid of the present invention chooses multiple natural component extracts and plants essential oil, and each composition complements each other, and makes product
Deep layer can pin each composition, abnormal smells from the patient is pure and fresh, quality is gentle, preserving moisture and protecting skin, cleaning-sterilizing, mosquito-repellent antipruritic and to infant skin no
Stimulate.For example, vitamin e has the antioxidant effect of brilliance, and chamomile essential oil is gentle, play the role of smooth and pacify moreover it is possible to
Gently rubescent, be dried and allergy skin problem.Oleum Eucalypti can wind-expelling pain-stopping, mosquito-repellent antipruritic.Add a small amount of dehydrated alcohol and poly- six
The cleanable sterilization of methylene guanidine.The gentle pro-skin of the extracting solution such as Folium Artemisiae Argyi, Folium Perillae, Aloe, Fructus Canarii albi, antiallergic is non-stimulated, gives baby children
The warm care of youngster's skin.
The present invention compared with prior art, made infant wet tissue cleaning-sterilizing, mosquito-repellent antipruritic, preserving moisture and protecting skin,
Abnormal smells from the patient is pure and fresh, non-stimulated and safety and environmental protection.
Specific embodiment
Hereinafter the specific embodiment of the present invention is described in detail.It should be appreciated that it is described herein concrete
Embodiment is merely to illustrate and explains the present invention, is not limited to the present invention.In embodiment, polyhexamethylene guanidine, xylose
Alcohol, Mentholum, Oleum Eucalypti, vitamin e, glycerol, chamomile essential oil, potassium sorbate, sorbic acid are that permanent science and trade are limited long for Beijing Cigna
The commercially available product of company.
Embodiment 1
A kind of environmental protective wet towel of multifunctional baby, including senior medicated napkin and wet tissue liquid, described wet tissue liquid is by following heavy
The raw material composition of amount percentage ratio:
Deionized water 85%, potassium sorbate 0.05%, chamomile essential oil 1%, Folium Perillae extracting solution 1%, polyhexamethylene guanidine
0.9%th, Folium Artemisiae Argyi extract 1%, ethanol 0.5%, xylitol 1%, lavandula angustifolia extracting solution 1.5%, Flos Pelargonii extracting solution 1%, thin
Lotus brain 0.05%, Oleum Eucalypti 0.5%, olive extract 1%, vitamin e 0.5%, Aloe extract 4%, glycerol 1%.
The preparation of 1.1 Folium Perillae extracting solution:
Weigh Folium Perillae 45g, put in round-bottomed flask, and add 20 times amount 80% ethanol solution, soak 1.0h, then put
It is placed in electric jacket, reflux, extract, 2.5h, the 2nd time plus 15 times amount 80% ethanol solution, extract 2.0h, the 3rd time plus 10 times amount
80% ethanol solution, extracts 1.5h, filters every time, merging filtrate, finally by 5 times of the volume concentration of filtrate to Folium Artemisiae Argyi weight,
Filter, obtain Folium Perillae extracting solution, standby.
The preparation of 1.2 Folium Artemisiae Argyi extracts:
Weigh dry Folium Artemisiae Argyi 50g, put in round-bottomed flask, and add 25 times amount 80% ethanol solution, soak 1.0h,
It is positioned in electric jacket, reflux, extract, 3.0h, the 2nd time plus 20 times amount 80% ethanol solution again, extracts 2.5h, add 15 times the 3rd time
Measure 80% ethanol solution, extract 2.0h, filter every time, merging filtrate, finally by the volume concentration of filtrate to the 4 of Folium Artemisiae Argyi weight
Times, concentrated solution is dried under vacuum to solid constant weight through 100 DEG C, obtains Folium Artemisiae Argyi extract.
The preparation of 1.3 Flos Pelargonii extracting solution:
Weigh Flos Pelargonii 60g, put in round-bottomed flask, and add 23 times amount water, soak 1.0h, then be positioned over electric jacket
In, reflux, extract, 3.0h, the 2nd time plus 18 times amount water, extract 2.0h, the 3rd time plus 13 times amount water, extract 1.5h, filter every time, close
And filtrate, finally by 5 times of the volume concentration of filtrate to Flos Pelargonii weight, filter, stand-by.
The preparation of 1.4 lavandula angustifolia extracting solution:
Weigh lavandula angustifolia 40g, put in round-bottomed flask, and add 20 times amount water, soak 1.0h, then be positioned over electric jacket
In, reflux, extract, 2.5h, the 2nd time plus 17 times amount water, extract 2.0h, the 3rd time plus 11 times amount water, extract 1.5h, filter every time, close
And filtrate, finally by 4 times of the volume concentration of filtrate to lavandula angustifolia weight, filter, stand-by.
The preparation of 1.5 olive extracts:
Weigh Fructus Canarii albi 60g, grounds travel is broken into coarse powder, put in round-bottomed flask, add the leaching of 30 times amount 80% ethanol solution
Bubble 0.5h, then be positioned in electric jacket, reflux, extract, 2.5h, the 2nd time plus 20 times amount 80% ethanol solution, reflux, extract, 1.5h,
3rd time plus 80% ethanol solution of 15 times amount, reflux, extract, 1h, sucking filtration obtains filtrate 3;Filter every time, merging filtrate, finally will filter
The volume concentration of liquid, to 5 times of Fructus Canarii albi weight, filters, stand-by.
The preparation of 1.6 Aloe extracts:
Weigh fresh aloe 50g, clean, remove blade two edges ratchet, cut base portion and top, rubbed with the hands with rubbing melon plate with the hands
Become filament, put in round-bottomed flask, and add 20 times amount 80% ethanol solution, soak 1.0h, then be positioned in electric jacket, return
Stream extracts 4.0h, the 2nd time plus 15 times amount 80% ethanol solution, extracts 3.0h, the 3rd time plus 12 times amount 80% ethanol solution, extracts
2.0h, filters, merging filtrate, finally by 6 times of the volume concentration of filtrate to Aloe weight, concentrated solution is through 100 DEG C of vacuum every time
It is dried to solid constant weight, obtain Aloe extract.
A kind of 1.7 multi-functional environment-protection infant wet tissue, its preparation method comprises the following steps:
(1) senior moisture-proof medicated napkin is put in 150 DEG C of baking oven and take out after baking 15min, launch tiling, stand-by;
(2) by deionized water, preservative, xylitol, glycerol, olive extract, polyhexamethylene guanidine is mixed in proportion all
Even, stirring heating in water bath, to 100 DEG C, is incubated 30 minutes;
(3) 50 DEG C of Temperature fall, by lavandula angustifolia extracting solution, Flos Pelargonii extracting solution, chamomile essential oil, Folium Perillae extracting solution press than
Example sequentially adds, and is uniformly mixed, and is incubated 5 minutes;
(4) Aloe extract, Folium Artemisiae Argyi extract, Mentholum are sequentially added at a temperature of step (3) in proportion, stirring is all
Even;
(5) naturally cool to 20 DEG C, add dehydrated alcohol, Oleum Eucalypti and vitamin e, be uniformly mixed;
(6) solution of step (5) gained is filtered, obtain wet tissue liquid, senior moisture-proof medicated napkin is completely soaked configuration
In good wet tissue liquid, soak 10 minutes, take out, prepared moisture paper tissue papers;
(7) subpackage is carried out to soaked moisture paper tissue papers using wet towel package machine, packing specification is a piece of for every bag.
Embodiment 2
A kind of environmental protective wet towel of multifunctional baby, including senior medicated napkin and wet tissue liquid, described wet tissue liquid is by following heavy
The raw material composition of amount percentage ratio:
Deionized water 85%, sorbic acid 0.05%, chamomile essential oil 1%, Folium Perillae extracting solution 1%, polyhexamethylene guanidine
0.9%th, Folium Artemisiae Argyi extract 1%, ethanol 0.5%, xylitol 1%, lavandula angustifolia extracting solution 1.5%, Flos Pelargonii extracting solution 1%, thin
Lotus brain 0.05%, Oleum Eucalypti 0.5%, olive extract 4%, vitamin e 0.5%, Aloe extract 1%, glycerol 1%.2.1 it is purple
The preparation of Soviet Union's extracting solution:
Weigh Folium Perillae 50g, put in round-bottomed flask, and add 18 times amount 80% ethanol solution, soak 1.0h, then put
It is placed in electric jacket, reflux, extract, 2.0h, the 2nd time plus 13 times amount 80% ethanol solution, extract 1.5h, the 3rd time plus 8 times amount 80%
Ethanol solution, extracts 1.0h, filters every time, merging filtrate, finally by 4 times of the volume concentration of filtrate to Folium Artemisiae Argyi weight, filters,
Obtain Folium Perillae extracting solution, standby.
The preparation of 2.2 Folium Artemisiae Argyi extracts:
Weigh dry Folium Artemisiae Argyi 55g, put in round-bottomed flask, and add 23 times amount 80% ethanol solution, soak 1.0h,
It is positioned in electric jacket, reflux, extract, 2.0h, the 2nd time plus 18 times amount 80% ethanol solution again, extracts 2.0h, add 13 times the 3rd time
Measure 80% ethanol solution, extract 1.5h, filter every time, merging filtrate, finally by the volume concentration of filtrate to the 3 of Folium Artemisiae Argyi weight
Times, concentrated solution is dried under vacuum to solid constant weight through 100 DEG C, obtains Folium Artemisiae Argyi extract.
The preparation of 2.3 Flos Pelargonii extracting solution:
Weigh Flos Pelargonii 50g, put in round-bottomed flask, and add 20 times amount water, soak 1.0h, then be positioned over electric jacket
In, reflux, extract, 2.0-3.0h, the 2nd time plus 13-18 times amount water, extract 1.5-2.0h, the 3rd time plus 8-13 times amount water, extract
0.5-1.5h, filters, merging filtrate every time, finally by 2-5 times of the volume concentration of filtrate to Flos Pelargonii weight, filters, stand-by.
The preparation of 2.4 lavandula angustifolia extracting solution:
Weigh lavandula angustifolia 50g, put in round-bottomed flask, and add 20 times amount water, soak 1.0h, then be positioned over electric jacket
In, reflux, extract, 2.5h, the 2nd time plus 17 times amount water, extract 2.0h, the 3rd time plus 11 times amount water, extract 1.5h, filter every time, close
And filtrate, finally by 4 times of the volume concentration of filtrate to lavandula angustifolia weight, filter, stand-by.
The preparation of 2.5 olive extracts:
Weigh Fructus Canarii albi 50g, grounds travel is broken into coarse powder, put in round-bottomed flask, add the leaching of 28 times amount 80% ethanol solution
Bubble 0.5h, then be positioned in electric jacket, reflux, extract, 2.5h, the 2nd time plus 18 times amount 80% ethanol solution, reflux, extract, 1.2h,
3rd time plus 80% ethanol solution of 13 times amount, reflux, extract, 0.5h, sucking filtration obtains filtrate 3;Filter every time, merging filtrate, finally will
The volume concentration of filtrate, to 4 times of Fructus Canarii albi weight, filters, stand-by.
The preparation of 2.6 Aloe extracts:
Weigh fresh aloe 45g, clean, remove blade two edges ratchet, cut base portion and top, rubbed with the hands with rubbing melon plate with the hands
Become filament, put in round-bottomed flask, and add 17 times amount 80% ethanol solution, soak 1.0h, then be positioned in electric jacket, return
Stream extracts 3.5h, the 2nd time plus 13 times amount 80% ethanol solution, extracts 2.5h, the 3rd time plus 10 times amount 80% ethanol solution, extracts
1.5h, filters, merging filtrate, finally by 5 times of the volume concentration of filtrate to Aloe weight, concentrated solution is through 100 DEG C of vacuum every time
It is dried to solid constant weight, obtain Aloe extract.
A kind of 2.7 multi-functional environment-protection infant wet tissue, its preparation method comprises the following steps:
(1) senior moisture-proof medicated napkin is put in 130 DEG C of baking oven and take out after baking 13min, launch tiling, stand-by;
(2) by deionized water, preservative, xylitol, glycerol, olive extract, polyhexamethylene guanidine is mixed in proportion all
Even, stirring heating in water bath, to 95 DEG C, is incubated 28 minutes;
(3) 48 DEG C of Temperature fall, by lavandula angustifolia extracting solution, Flos Pelargonii extracting solution, chamomile essential oil, Folium Perillae extracting solution press than
Example sequentially adds, and is uniformly mixed, and is incubated 5 minutes;
(4) Aloe extract, Folium Artemisiae Argyi extract, Mentholum are sequentially added at a temperature of step (3) in proportion, stirring is all
Even;
(5) naturally cool to 18 DEG C, add dehydrated alcohol, Oleum Eucalypti and vitamin e, be uniformly mixed;
(6) solution of step (5) gained is filtered, obtain wet tissue liquid, senior moisture-proof medicated napkin is completely soaked configuration
In good wet tissue liquid, soak 8 minutes, take out, prepared moisture paper tissue papers;
(7) subpackage is carried out to soaked moisture paper tissue papers using wet towel package machine, packing specification is a piece of for every bag.
Embodiment 3
A kind of environmental protective wet towel of multifunctional baby, including senior medicated napkin and wet tissue liquid, described wet tissue liquid is by following heavy
The raw material composition of amount percentage ratio:
Deionized water 85%, potassium sorbate 0.05%, chamomile essential oil 1%, Folium Perillae extracting solution 1%, polyhexamethylene guanidine
0.9%th, Folium Artemisiae Argyi extract 1%, ethanol 0.5%, xylitol 1%, lavandula angustifolia extracting solution 3%, Flos Pelargonii extracting solution 2%, Herba Menthae
Brain 0.05%, Oleum Eucalypti 1%, olive extract 1%, vitamin e 0.5%, Aloe extract 1%, glycerol 1%.
3.1 the preparation of Folium Perillae extracting solution:
Weigh Folium Perillae 35g, put in round-bottomed flask, and add 15 times amount 80% ethanol solution, soak 0.8h, then put
It is placed in electric jacket, reflux, extract, 2.0h, the 2nd time plus 12 times amount 80% ethanol solution, extract 1.5h, the 3rd time plus 7 times amount 80%
Ethanol solution, extracts 0.8h, filters every time, merging filtrate, finally by 3 times of the volume concentration of filtrate to Folium Artemisiae Argyi weight, filters,
Obtain Folium Perillae extracting solution, standby.
The preparation of 3.2 Folium Artemisiae Argyi extracts:
Weigh dry Folium Artemisiae Argyi 30g, put in round-bottomed flask, and add 20 times amount 80% ethanol solution, soak 0.5h,
It is positioned in electric jacket, reflux, extract, 2.0h, the 2nd time plus 15 times amount 80% ethanol solution again, extracts 1.5h, add 10 times the 3rd time
Measure 80% ethanol solution, extract 1.0h, filter every time, merging filtrate, finally by the volume concentration of filtrate to the 2 of Folium Artemisiae Argyi weight
Times, concentrated solution is dried under vacuum to solid constant weight through 95 DEG C, obtains Folium Artemisiae Argyi extract.
3.3 the preparation of Flos Pelargonii extracting solution:
Weigh Flos Pelargonii 40g, put in round-bottomed flask, and add 18 times amount water, soak 0.5h, then be positioned over electric jacket
In, reflux, extract, 2.0h, the 2nd time plus 13 times amount water, extract 1.5h, the 3rd time plus 8 times amount water, extract 0.5h, filter every time, close
And filtrate, finally by 2 times of the volume concentration of filtrate to Flos Pelargonii weight, filter, stand-by.
The preparation of 3.4 lavandula angustifolia extracting solution:
Weigh lavandula angustifolia 30g, put in round-bottomed flask, and add 18 times amount water, soak 0.8h, then be positioned over electric jacket
In, reflux, extract, 2.0h, the 2nd time plus 14 times amount water, extract 1.5h, the 3rd time plus 9 times amount water, extract 1.0h, filter every time, close
And filtrate, finally by 3 times of the volume concentration of filtrate to lavandula angustifolia weight, filter, stand-by.
The preparation of 3.5 olive extracts:
Weigh Fructus Canarii albi 40g, grounds travel is broken into coarse powder, put in round-bottomed flask, add the leaching of 22 times amount 80% ethanol solution
Bubble 0.5h, then be positioned in electric jacket, reflux, extract, 2.0h, the 2nd time plus 13 times amount 80% ethanol solution, reflux, extract, 1.3h,
3rd time plus 80% ethanol solution of 12 times amount, reflux, extract, 0.8h, sucking filtration obtains filtrate 3;Filter every time, merging filtrate, finally will
The volume concentration of filtrate, to 4 times of Fructus Canarii albi weight, filters, stand-by.
The preparation of 3.6 Aloe extracts:
Weigh fresh aloe 35g, clean, remove blade two edges ratchet, cut base portion and top, rubbed with the hands with rubbing melon plate with the hands
Become filament, put in round-bottomed flask, and add 15 times amount 80% ethanol solution, soak 0.5h, then be positioned in electric jacket, return
Stream extracts 3.0h, the 2nd time plus 10 times amount 80% ethanol solution, extracts 2.0h, the 3rd time plus 8 times amount 80% ethanol solution, extracts
1.0h, filters, merging filtrate every time, and finally by 3 times of the volume concentration of filtrate to Aloe weight, concentrated solution is done through 95 DEG C of vacuum
Dry to solid constant weight, obtain Aloe extract.
A kind of 3.7 multi-functional environment-protection infant wet tissue, its preparation method comprises the following steps:
(1) take out after senior moisture-proof medicated napkin being put into baking 10 in 100 DEG C of baking oven, launch tiling, stand-by;
(2) by deionized water, preservative, xylitol, glycerol, olive extract, polyhexamethylene guanidine is mixed in proportion all
Even, stirring heating in water bath, to 90 DEG C, is incubated 25 minutes;
(3) 45 DEG C of Temperature fall, by lavandula angustifolia extracting solution, Flos Pelargonii extracting solution, chamomile essential oil, Folium Perillae extracting solution press than
Example sequentially adds, and is uniformly mixed, and is incubated 5 minutes;
(4) Aloe extract, Folium Artemisiae Argyi extract, Mentholum are sequentially added at a temperature of step (3) in proportion, stirring is all
Even;
(5) naturally cool to 10 DEG C, add dehydrated alcohol, Oleum Eucalypti and vitamin e, be uniformly mixed;
(6) solution of step (5) gained is filtered, obtain wet tissue liquid, senior moisture-proof medicated napkin is completely soaked configuration
In good wet tissue liquid, soak 5 minutes, take out, prepared moisture paper tissue papers;
(7) subpackage is carried out to soaked moisture paper tissue papers using wet towel package machine, packing specification is a piece of for every bag.
Embodiment 4
A kind of environmental protective wet towel of multifunctional baby, including senior medicated napkin and wet tissue liquid, described wet tissue liquid is by following heavy
The raw material composition of amount percentage ratio:
Deionized water 85%, sorbic acid 0.05%, chamomile essential oil 1%, Folium Perillae extracting solution 1%, polyhexamethylene guanidine
0.9%th, Folium Artemisiae Argyi extract 3%, ethanol 0.5%, xylitol 2%, lavandula angustifolia extracting solution 1.5%, Flos Pelargonii extracting solution 1%, thin
Lotus brain 0.05%, Oleum Eucalypti 0.5%, olive extract 1%, vitamin e 0.5%, Aloe extract 1%, glycerol 1%.4.1 it is purple
The preparation of Soviet Union's extracting solution:
Weigh Folium Perillae 30g, put in round-bottomed flask, and add 15 times amount 80% ethanol solution, soak 0.5h, then put
It is placed in electric jacket, reflux, extract, 1.5h, the 2nd time plus 10 times amount 80% ethanol solution, extract 1.0h, the 3rd time plus 5 times amount 80%
Ethanol solution, extracts 0.5h, filters every time, merging filtrate, finally by 3 times of the volume concentration of filtrate to Folium Artemisiae Argyi weight, filters,
Obtain Folium Perillae extracting solution, standby.
The preparation of 4.2 Folium Artemisiae Argyi extracts:
Weigh dry Folium Artemisiae Argyi 60g, put in round-bottomed flask, and add 25 times amount 80% ethanol solution, soak 1.0h,
It is positioned in electric jacket, reflux, extract, 3.0h, the 2nd time plus 20 times amount 80% ethanol solution again, extracts 2.5h, add 15 times the 3rd time
Measure 80% ethanol solution, extract 2.0h, filter every time, merging filtrate, finally by the volume concentration of filtrate to the 4 of Folium Artemisiae Argyi weight
Times, concentrated solution is dried under vacuum to solid constant weight through 90 DEG C, obtains Folium Artemisiae Argyi extract.
The preparation of 4.3 Flos Pelargonii extracting solution:
Weigh Flos Pelargonii 60g, put in round-bottomed flask, and add 23 times amount water, soak 1.0h, then be positioned over electric jacket
In, reflux, extract, 3.0h, the 2nd time plus 18 times amount water, extract 2.0h, the 3rd time plus 13 times amount water, extract 1.5h, filter every time, close
And filtrate, finally by 5 times of the volume concentration of filtrate to Flos Pelargonii weight, filter, stand-by.
The preparation of 4.4 lavandula angustifolia extracting solution:
Weigh lavandula angustifolia 20g, put in round-bottomed flask, and add 17 times amount water, soak 0.5h, then be positioned over electric jacket
In, reflux, extract, 1.5h, the 2nd time plus 11 times amount water, extract 1.0h, the 3rd time plus 6 times amount water, extract 0.5h, filter every time, close
And filtrate, finally by 2 times of the volume concentration of filtrate to lavandula angustifolia weight, filter, stand-by.
The preparation of 4.5 olive extracts:
Weigh Fructus Canarii albi 35g, grounds travel is broken into coarse powder, put in round-bottomed flask, add the leaching of 20 times amount 80% ethanol solution
Bubble 0.5h, then be positioned in electric jacket, reflux, extract, 1.5h, the 2nd time plus 10 times amount 80% ethanol solution, reflux, extract, 1.0h,
3rd time plus 80% ethanol solution of 10 times amount, reflux, extract, 0.5h, sucking filtration obtains filtrate 3;Filter every time, merging filtrate, finally will
The volume concentration of filtrate, to 3 times of Fructus Canarii albi weight, filters, stand-by.
The preparation of 4.6 Aloe extracts:
Weigh fresh aloe 40g, clean, remove blade two edges ratchet, cut base portion and top, rubbed with the hands with rubbing melon plate with the hands
Become filament, put in round-bottomed flask, and add 16 times amount 80% ethanol solution, soak 0.8h, then be positioned in electric jacket, return
Stream extracts 3.0h, the 2nd time plus 12 times amount 80% ethanol solution, extracts 2.0h, the 3rd time plus 9 times amount 80% ethanol solution, extracts
1.0h, filters, merging filtrate every time, and finally by 4 times of the volume concentration of filtrate to Aloe weight, concentrated solution is done through 90 DEG C of vacuum
Dry to solid constant weight, obtain Aloe extract.
A kind of 4.7 multi-functional environment-protection infant wet tissue, its preparation method comprises the following steps:
(1) senior moisture-proof medicated napkin is put in 140 DEG C of baking oven and take out after baking 14min, launch tiling, stand-by;
(2) by deionized water, preservative, xylitol, glycerol, olive extract, polyhexamethylene guanidine is mixed in proportion all
Even, stirring heating in water bath, to 95 DEG C, is incubated 27 minutes;
(3) 47 DEG C of Temperature fall, by lavandula angustifolia extracting solution, Flos Pelargonii extracting solution, chamomile essential oil, Folium Perillae extracting solution press than
Example sequentially adds, and is uniformly mixed, and is incubated 5 minutes;
(4) Aloe extract, Folium Artemisiae Argyi extract, Mentholum are sequentially added at a temperature of step (3) in proportion, stirring is all
Even;
(5) naturally cool to 15 DEG C, add dehydrated alcohol, Oleum Eucalypti and vitamin e, be uniformly mixed;
(6) solution of step (5) gained is filtered, obtain wet tissue liquid, senior moisture-proof medicated napkin is completely soaked configuration
In good wet tissue liquid, soak 7 minutes, take out, prepared moisture paper tissue papers;
(7) subpackage is carried out to soaked moisture paper tissue papers using wet towel package machine, packing specification is a piece of for every bag.
Test example
1st, irritation test, anaphylaxis experiment
Wet tissue made by Example 1,2,3,4 cut 1-5 square centimeter size spread on respectively volunteer (1-50 year, 250
People) diverse location in gesture and facial expression, observe after spending 30 minutes, rubescent, dermexanthesis, foaming phenomena all do not occur.
2nd, trial effect experiment
To evaluate the effect of the wet tissue that embodiment 1,2,3,4 is made following with trial effect.Using public-opinion poll scoring
Method, choose 100 1-5 year age bracket infant as object on probation, be arbitrarily divided into four groups, use respectively embodiment 1,2,3,
The wet tissue cleaning hip skin of 4 preparations.Daily using twice, use time two months.Every using effect total score is 5 points: five
It is divided into best result, represent very well, very satisfied;4 are divided into preferably;3 are divided into and can accept;Less than 3 points can not accept for bad.With
Lower is every average, and result see table:
Resultant effect is investigated