CN102132955B - Preparation of ethanol extracts of monostromanitidum and application of ethanol extracts of monostromanitidum in cigarettes - Google Patents
Preparation of ethanol extracts of monostromanitidum and application of ethanol extracts of monostromanitidum in cigarettes Download PDFInfo
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- CN102132955B CN102132955B CN 201110025948 CN201110025948A CN102132955B CN 102132955 B CN102132955 B CN 102132955B CN 201110025948 CN201110025948 CN 201110025948 CN 201110025948 A CN201110025948 A CN 201110025948A CN 102132955 B CN102132955 B CN 102132955B
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Abstract
The invention provides a preparation of ethanol extracts of monostromanitidum and application of ethanol extracts of monostromanitidum to cigarettes. The preparation is characterized by comprising the following steps: acquiring monostromanitidum, killing enzyme under high temperature, carrying out cleaning and impurity removal, carrying out drying and grinding, carrying out ethanol extraction, carrying out solid-liquid separation, and carrying out concentration, thus obtaining the ethanol extracts of monostromanitidum. The ethanol extracts of monostromanitidum are dissolved with water and are prepared into feed solutions of different concentrations, and the feed solutions are uniformly sprayed on the cut tobaccos. The sensory evaluation results show that after the ethanol extracts of monostromanitidum are added, the cigarette smoke is free from extraneous odour when the cigarettes burn, the miscellaneous gases and irritation of the cigarette smoke are obviously reduced, the remaining taste is clean and comfortable, the cigarettes have sweet aftertaste, and the whole smoking quality is improved. By adopting the ethanol extracts of monostromanitidum, the original performances and processing technics of the cigarettes are not changed, the aroma quality of the cigarettes is improved and the sensory comfort levels of the cigarettes are improved, so the ethanol extracts of monostromanitidum further have actual production significance and value.
Description
Technical field
The present invention relates to extraction and the application thereof of marine alga, specifically relate to a kind of preparation of reef film ethanol extract and the application in cigarette thereof.This The Application of Technology does not change the existing processing technology of cigarette, can improve the sucking quality and the sense organ comfort level of cigarette.
Background technology
Compare with external famous brand name cigarette; Still there is certain deficiency in domestic cigarette product at aspects such as flavouring essence quality and sense organ comfort levels; Therefore the research and discovery that relates to fields such as raw tobacco material, processing technology and essence and flavoring agent launches in succession, and the exploitation of novel cigarette additive also is an important component part wherein.
Vast territory and abundant resources in China, and floristics is various, and the composition of contained active ingredient also respectively has characteristics, for the exploitation of cigarette additive provides rich in natural resources.Can extract separation to effective ingredients in plant through the different modes method, and extract is applied in the cigarette with multi-form, in the hope of improving the overall quality of cigarette to the characteristics of cigarette product.
Marine alga is grown in the particular surroundings of ocean, therefore contains with land plant and compares special composition, like iodide, polyphenolic substance, many halos terpenoid, phytosterin compound, polyunsaturated fatty acid and algal polysaccharides etc.In addition, also contain rich in protein, vitamin, mineral matter and trace element, demonstrating great potential aspect food, industry, agricultural, medicine, beauty treatment and the health care.
The reef film (
Monostromanitidum)Have another name called stone dish, moss dish, green paint, be distributed widely in global tropical and marine site, subtropical zone, mainly be distributed in Korea S, Japan, the Ryukyu Islands etc. in the Asia, mainly be distributed in the East Sea, marine site, the South Sea in China.The reef film is rich in carbohydrate, aliphatic acid, vitamin, amino acid, inorganic salts and trace element, and wherein taurine accounts for 12.67% of free aminoacid content, and polyunsaturated fatty acid accounts for 50.28% of content of fatty acid; Trace element Cu, Zn, Se content enrich; Be a kind of good food resource (justice of expressing gratitude for a favour, Ma Jiahai, Chen Yangjian. wide reef film Analysis of Nutritional and nutrition evaluation. Shanghai Aquatic Products Univ. 9CN)'s journal; 2002,11 (2): 129-133).The reef film is rich in active medicinal matters such as sulfuric acid polysaccharide in addition; Have anticoagulation (room virtue. the extraction of sea lettuce polysaccharide, separation, structure and anticoagulant active research. Chinese Marine University's Master's thesis; 2008), anti-oxidant (agarase prepares marine alga oligosaccharides and Hangzhoupro oxidation activity thereof. aquatic science, 2004,70 (6): 1164-1173), antiviral (Lee J B etc. the anti-bleb of green alga sulfated polysaccharide is active. medicinal plant; 2004; 70 (9): 813-817), radiation proof (Li Yi, Wang Haiqing. the radiation protection of sea lettuce polysaccharide and Study on Mechanism thereof. Chinese Radiation Medicine with the protection magazine, 2008; 12 (6): 615-618), the function of clearing heat and eliminating phlegm, promoting diuresis to remove toxic substance, can prevent and treat multiple diseases such as sphagitis, cough.
At present, domestic reef film is main to eat.Also fewer for composition network analysis of reef membrance chemistry and application study, do not find as yet in the Application in Tobacco precedent.
Summary of the invention
The present invention just is being based on above-mentioned present Research and the reef film is being studied, and the ethanol extract of reef film is put in the cigarette in a certain way, and purpose is to improve the sucking quality and the sense organ comfort level of cigarette.
The object of the invention can be realized through following technical scheme: the preparation method of reef film ethanol extract of the present invention comprises the steps:
Go out enzyme → cleaning removal of impurities → oven dry pulverizing → alcohol extract → Separation of Solid and Liquid → concentrate → reef film ethanol extract of reef film → high temperature.
In the alcohol extract step, 95% ethanol: the reef film quality is than=3～10:1, and extracting temperature is 40～90 ℃, and extraction time is 1～4h.Also can adopt supercritical carbon dioxide to extract, entrainer is selected ethanol for use, extracting pressure 20～50MPa, 30～50 ℃ of extraction temperature.Also can adopt the microwave assisted extraction, microwave power 150～500W, extraction time 10～30min.
In concentration step, being concentrated into dry matter content is 1～10%.
Reef film ethanol extract dilution back is joined on the cigarette shreds with feed liquid as cigarette, the elimination peculiar smell is arranged, reduce assorted gas, excitant, pleasant impression is totally comfortable, increases back the effect of sweet sense.Reef film ethanol extract consumption is 0.05%～1% of a pipe tobacco weight, evenly is sprayed onto on the pipe tobacco at cigarette charging process.
Sensory evaluating smoking result shows: during cigarette burning, and the flue gas free from extraneous odour, the assorted gas and the excitant of cigarette smoke obviously reduce, and pleasant impression is totally comfortable, and sweet sense is arranged back.Mainly contain ester class, organic acid, olefines, alkanes, alcohols, ketone or the like in the reef film ethanol extract liquid, particularly ester class and acids flavor component have important function to the improvement of cigarette smoking quality.
The present invention does not change original performance of cigarette, does not change the original processing technology of cigarette, has improved the flavouring essence quality of cigarette, has improved the sense organ comfort level of cigarette, therefore has more the meaning and the value of actual production.
The specific embodiment
The present invention does below in conjunction with embodiment and further describes, but does not limit the present invention.
Embodiment 1:
The reef film is through the infrared enzyme that goes out, and washes clean is behind the rejecting impurity; Dry, oven dry is pulverized the back and is crossed 40 eye mesh screens, adds 95% ethanol of 4 times of weight; Extract 2h 80 ℃ of refluxed; After the filtration filtrating being concentrated into dry matter content is 10%, and concentrate evenly is sprayed onto on the cigarette shreds by 0.05% of pipe tobacco weight, rolls into cigarette after the baking.
Through smokeing panel test, the flue gas free from extraneous odour, with the fragrant harmony of cigarette, fragrance matter is improved, and assorted gas excitant reduces, and fresh and sweet sense is suitable, and pleasant impression is comfortable.
Embodiment 3:
The reef film is through the infrared enzyme that goes out, and washes clean is behind the rejecting impurity; Dry, oven dry is pulverized the back and is crossed 20 eye mesh screens, through the Microwave Extraction device; Under 160w power, add 95% alcohol extract 20min of 3 times of weight, after the filtration filtrating being concentrated into dry matter content is 10%; Concentrate evenly is sprayed onto on the cigarette shreds by 0.1% of pipe tobacco weight, rolls into cigarette after the baking.
Through smokeing panel test, the flue gas free from extraneous odour, with the fragrant harmony of cigarette, fragrance matter slightly improves, and assorted gas excitant reduces, and Hui Tian is arranged, and pleasant impression is comfortable.
Embodiment 3:
The reef film is through the infrared enzyme that goes out, and washes clean is behind the rejecting impurity; Dry, oven dry is pulverized the back and is crossed 40 eye mesh screens, through supercritical carbon dioxide extraction apparatus; Under the 30MPa extracting pressure, make entrainer with ethanol, behind the extraction 2h; Isolate tincture, tincture evenly is sprayed onto on the cigarette shreds by 0.2% of pipe tobacco weight, toast and process cigarette.
Through smokeing panel test, the flue gas free from extraneous odour, with the fragrant harmony of cigarette, assorted gas excitant reduces, and returns comfortable suitablely, and pleasant impression is comfortable.
Claims (5)
1. the application of a reef film ethanol extract in cigarette; It is characterized in that: reef film ethanol extract dilution back is joined on the cigarette shreds with feed liquid as cigarette, the elimination peculiar smell is arranged, reduce assorted gas, excitant; Pleasant impression is totally comfortable; Increase back the effect of sweet sense, reef film ethanol extract consumption is 0.05%～1% of a pipe tobacco weight, evenly is sprayed onto on the pipe tobacco at cigarette charging process; Said reef film ethanol extract is prepared from through following concrete steps: go out enzyme → cleaning removal of impurities → oven dry pulverizing → alcohol extract → Separation of Solid and Liquid → concentrate → reef film ethanol extract of reef film → high temperature.
2. the application of reef film ethanol extract according to claim 1 in cigarette is characterized in that: in the alcohol extract step, ethanol: the reef film quality is than=3～10:1, and extracting temperature is 40～90 ℃, and extraction time is 1～4h, and used concentration of alcohol is 95%.
3. the application of reef film ethanol extract according to claim 1 in cigarette is characterized in that: in the alcohol extract step, adopt supercritical carbon dioxide to extract, entrainer is selected ethanol for use, extracting pressure 20～50MPa, 30～50 ℃ of extraction temperature.
4. the application of reef film ethanol extract according to claim 1 in cigarette is characterized in that: in the alcohol extract step, adopt the microwave assisted extraction, in concentration step, being concentrated into dry substance concentration is 1～10%.
5. the application of reef film ethanol extract according to claim 1 in cigarette is characterized in that: in concentration step, being concentrated into dry substance concentration is 1～10%.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110025948 CN102132955B (en) | 2011-01-25 | 2011-01-25 | Preparation of ethanol extracts of monostromanitidum and application of ethanol extracts of monostromanitidum in cigarettes |
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| CN 201110025948 CN102132955B (en) | 2011-01-25 | 2011-01-25 | Preparation of ethanol extracts of monostromanitidum and application of ethanol extracts of monostromanitidum in cigarettes |
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| CN102132955B true CN102132955B (en) | 2012-12-26 |
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| CN110839954A (en) * | 2019-11-28 | 2020-02-28 | 河南农业大学 | Method for manufacturing cigarette filter rod by using tobacco stem core material |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101328227A (en) * | 2008-07-16 | 2008-12-24 | 中国海洋大学 | Sea lettuce polysaccharide, preparation and use thereof |
| CN101611693A (en) * | 2009-06-09 | 2009-12-30 | 宁波大学 | The method that a kind of seed of wild monostroma nitidum is gathered and cultivates |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101328227A (en) * | 2008-07-16 | 2008-12-24 | 中国海洋大学 | Sea lettuce polysaccharide, preparation and use thereof |
| CN101611693A (en) * | 2009-06-09 | 2009-12-30 | 宁波大学 | The method that a kind of seed of wild monostroma nitidum is gathered and cultivates |
Non-Patent Citations (1)
| Title |
|---|
| 张会娟.宽礁膜（Monostroma latissium）多糖的分离、结构和抗凝血活性研究.《中国海洋大学博士学位论文》.2007,22-23. * |
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